CN109431935A - A kind of skin whitening, moisturizing face mask of traditional Chinese medicine and preparation method thereof - Google Patents

A kind of skin whitening, moisturizing face mask of traditional Chinese medicine and preparation method thereof Download PDF

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CN109431935A
CN109431935A CN201811437292.XA CN201811437292A CN109431935A CN 109431935 A CN109431935 A CN 109431935A CN 201811437292 A CN201811437292 A CN 201811437292A CN 109431935 A CN109431935 A CN 109431935A
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chinese medicine
effective component
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whitening
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陈西成
陈欣
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9794Liliopsida [monocotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/64Proteins; Peptides; Derivatives or degradation products thereof
    • A61K8/645Proteins of vegetable origin; Derivatives or degradation products thereof
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    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/64Proteins; Peptides; Derivatives or degradation products thereof
    • A61K8/65Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
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    • A61K8/67Vitamins
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    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
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    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
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    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
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    • A61K8/98Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
    • A61K8/987Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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    • A61K8/987Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
    • A61K8/988Honey; Royal jelly, Propolis
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
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    • A61K2800/84Products or compounds obtained by lyophilisation, freeze-drying
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
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    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
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Abstract

The invention discloses a kind of skin whitening, moisturizing face mask of traditional Chinese medicine and preparation method, which is made of effective component of chinese medicine, moisturizing effective component, whitening effective component and auxiliary material according to the mass ratio of 8:5:3:1;The effective component of chinese medicine includes: radix scutellariae, honeysuckle, root of kirilow rhodiola, safflower, Herb Gynostemmae Pentaphylli extract, licorice and white pond lily flower extract;The moisturizing effective component includes: aloe protein hydrolysate, licoflavone, algal polysaccharides, deep-sea fish skin collagen;The whitening effective component includes: Rhizoma Atractylodis Macrocephalae zymophyte powder, hydrolyzed pearl powder, arbutin, vitamin;The auxiliary material includes: propylene glycol, carragheen, hydroxyethyl cellulose, hyaluronic acid.The present invention is by carrying out reasonable compatibility for four kinds of effective component of chinese medicine, moisturizing effective component, whitening effective component and auxiliary ingredients, synergistic function is played, to improve the whitening of facial mask of the present invention, moistening effect, and facial mask produced by the present invention is without side-effects, quick, effect is good.

Description

A kind of skin whitening, moisturizing face mask of traditional Chinese medicine and preparation method thereof
Technical field
The present invention relates to cosmetic technical fields, and in particular to a kind of skin whitening, moisturizing face mask of traditional Chinese medicine and its preparation process.
Background technique
Facial mask is a kind of carrier of face beautifying health keeping product.The principle of facial mask, exactly using the of short duration time for being covered on face, temporarily When the extraneous air of isolation and pollution, to promote the secretion and metabolism of sweat gland, thus to skin by improving skin temperature Skin generates maintenance effect.
A kind of germ juice skin whitening, moisturizing essence facial mask liquid is disclosed in Chinese patent application CN201710072919., is Be made of the raw material of following parts by weight: 42-50 parts of germ juice, 8-15 parts of fragrant citrus fruit extracting solution, 9-12 parts of gadol extract, 6-8 parts of polyvinyl alcohol, 9-11 parts of 1,3-BDO, 10-15 parts of glycerol, 8-10 parts of honeysuckle, 5-9 parts of lemon, lavender 4-7 Part, 3-8 parts of Hydrolyzed Collagen, 10-12 parts of hyaluronic acid, 5-10 parts of methylcellulose, 4-6 parts of dispersing agent, preservative 3-7 Part.Though the patent has effects that whitening and moisturizing, its application has limitation, it is difficult in shriveling water shortage, gloomy unglazed skin Preferable therapeutic effect is played on skin.
And Chinese patent application CN201310667039.4 disclose a kind of mask liquid for whitening hydrating mask paste and its Preparation method and application, the facial mask liquid contain following whitening and moisturizing component, other components, triethanolamine and preservative and perfume (or spice) Essence, whitening and moisturizing component include oxidoreducing enzyme, niacinamide, dipotassium glycyrrhizinate, Sodium Hyaluronate, white pond lily flower extract, PEG/PPG-70/30 gives birth to phenolic ether, Flos Mume extract.The present invention can provide facial antiallergic moist for a long time, absorb fastly, after being finished Half h can obviously see it is white, and for 24 hours continue whitening.The patent has preferable whitening effect, but it is short of in terms of moisturizing effect Point, it is difficult to play the effect that whitening is mutually cooperateed with moisturizing.
Both the above facial mask mostly uses chemical synthesis agent, and not only therapeutic effect is unsatisfactory, but also there is malicious secondary works With the various disadvantages such as big, palliative.Therefore favor of the Pure natural mask just by more and more people, and face mask of traditional Chinese medicine is exactly Not only without side-effects and quick by the cooperation of various Chinese medicine materials and the combination of different content, effect is good.
Based on this, it is necessary to a kind of skin whitening, moisturizing face mask of traditional Chinese medicine and its preparation process are provided, to solve to deposit in the prior art The problem of.
Summary of the invention
In order to solve the problems in the existing technology, the present invention provides a kind of skin whitening, moisturizing face mask of traditional Chinese medicine and its preparations Method, by the way that four kinds of effective component of chinese medicine, moisturizing effective component, whitening effective component and auxiliary ingredients are carried out reasonable compatibility, Synergistic function is played, to improve the whitening of facial mask of the present invention, moistening effect, and facial mask produced by the present invention is made without pair With quick, effect is good.
It is of the existing technology in order to solve the problems, such as, it adopts the following technical scheme that
A kind of skin whitening, moisturizing face mask of traditional Chinese medicine, the facial mask by effective component of chinese medicine, moisturizing effective component, whitening effective component and Auxiliary material is made according to the mass ratio of 8:5:3:1;
Wherein, the effective component of chinese medicine is made of the raw material of following parts by weight: 10-15 parts of radix scutellariae, 5-10 parts of honeysuckle, 3-7 parts of root of kirilow rhodiola, 2-5 parts of safflower, 1-3 parts of Herb Gynostemmae Pentaphylli extract, 0.5-1.5 parts of licorice, white pond lily flower extract 2-4 parts;
The moisturizing effective component is made of the raw material of following parts by weight: aloe hydrolyzes -30 parts of protein 20, licoflavone 5- 10 parts, 1-5 parts of algal polysaccharides, 0.5-1.5 parts of deep-sea fish skin collagen;
The whitening effective component is made of the raw material of following parts by weight: 30-40 parts of Rhizoma Atractylodis Macrocephalae zymophyte powder, hydrolyzed pearl powder 15-25 parts, 5-10 parts of arbutin, 1-4 parts of vitamin;
The auxiliary material is made of the raw material of following parts by weight: 5-10 parts of propylene glycol, 0.5-1.5 parts of carragheen, ethoxy are fine Tie up 0.4-0.8 parts of element, 1-3 parts of hyaluronic acid.
Preferably, it the preparation method of the Herb Gynostemmae Pentaphylli extract: will be ground into after gynostemma pentaphylla drinking water cleaning, drying 8 times of purified waters of gynostemma pentaphylla are added in coarse grain, decoct 2 times, decoct 2h every time, merge decoction liquor, and being concentrated into relative density is 1.15 leachings Cream is let cool, and 95%v/v ethyl alcohol is added and carries out alcohol precipitation, and final alcohol precipitation degree is 70, stands more than for 24 hours, extracts supernatant, carries out Concentration, being concentrated into relative density is 1.30, and medicinal extract is put into rail mounted film drier, is dried, and after dry, is ground into thin Powder, and sieve with 100 mesh sieve to get gynostemma pentaphylla root extract;
The preparation method of the licorice: extracting liquorice is extracted using 80%v/v alcohol reflux, and extracting solution recycles second It after alcohol, then with AB-8 macroreticular resin carries out absorption passivation, and is eluted using 90%v/v ethyl alcohol, collect ethanol eluate, return Ethyl alcohol is received, concentration is dry to get licorice;
The preparation method of the white pond lily flower extract: white pond lily flower is cleaned up with drinking water, crushed after being dried at Coarse grain is added white pond lily and 5 times 70% of ethyl alcohol is spent to carry out alcohol extracting, alcohol extracting 2 times, each 2h, merges alcohol extract, be concentrated into relatively close Degree is 1.25 medicinal extract, lets cool, medicinal extract is put into rail mounted film drier, is dried, and after dry, is ground into fine powder, and It sieves with 100 mesh sieve to get white pond lily flower extract.
Preferably, the Rhizoma Atractylodis Macrocephalae zymophyte powder is made of the substance of following parts by weight: 60-80 parts of Rhizoma Atractylodis Macrocephalae, hydrolysis royal jelly 5-10 parts, 3-6 parts of peptone, 0.3-0.7 parts of phosphoric acid hydrogen dimethylamino potassium, 0.5-1.5 parts of epsom salt.
Preferably, the Rhizoma Atractylodis Macrocephalae zymophyte powder fills the preparation method comprises the following steps: extra dry white wine art is mixed with water 1:10-15 in mass ratio Point mashing, as basic liquid, be added into basal liquid the hydrolysis royal jelly of above-mentioned parts by weight, peptone, phosphoric acid hydrogen dimethylamino potassium and Epsom salt sterilizes after mixing well, and microbe inoculation leavening, is kept for 25-35 DEG C of temperature, after the 48-54h that ferments, high temperature Sterilizing is freeze-dried to get aloe zymophyte powder.
Preferably, the microbe leaven is by Bacillus acidi lactici, bacillus licheniformis, Corynebacterium glutamicum in mass ratio 3: 2:1 mixing gained.
Preferably, the vitamin is vitamin B, vitamin C and vitamin E, and weight ratio is 1:2:3.
Preferably, the hyaluronic acid is macromolecular Sodium Hyaluronate, middle numerator sodium hyaluronate and small molecule hyalomitome The mixture of sour sodium, and its weight ratio is 1:1:2.
Preferably, the present invention also provides the preparation methods of above-mentioned skin whitening, moisturizing face mask of traditional Chinese medicine, comprising the following steps:
(1) radix scutellariae, honeysuckle, root of kirilow rhodiola and safflower are weighed in proportion, is added water to cook twice, are added for the first time into raw material Enter the 8-10 times of water measured, heating decocts 1-2h;After separation of solid and liquid, the 4-6 times of water measured is added, heating decocts 1-2h, merges two The filtrate of secondary decoction, and filtrate low-temperature evaporation is concentrated into relative density as 1.10-1.20, under stirring condition, it is slowly added into 2 times The 95%v/v ethanol solution of amount stirs, and stands, filtering, and it is 1.20-1.30 that filtrate low-temperature evaporation, which is concentrated into relative density, and is returned Ethyl alcohol is received, Chinese medicine extract is obtained;
(2) Herb Gynostemmae Pentaphylli extract, licorice and white pond lily flower are added in the Chinese medicine extract in step (1) to extract Object, warming while stirring keep 10-20min to 40-50 DEG C at such a temperature, obtain effective component of chinese medicine, for use;
(3) by the propylene glycol of formula ratio and carragheen, after weighing in proportion, the stainless steel kettle for having agitating device is added It is interior, it dissolves by heating completely under the stirring of revolving speed 30-50rpm, and constant temperature disinfection 20min at a temperature of 80 DEG C, then adds The hydroxyethyl cellulose and hyaluronic acid of formula ratio, stir evenly, and obtain mixture A;
(4) it by Rhizoma Atractylodis Macrocephalae zymophyte powder, hydrolyzed pearl powder, arbutin and the vitamin of formula ratio, after weighing in proportion, is added Into emulsion pot, it is heated with stirring to 50-60 DEG C, is extracted into stainless steel homogeneous kettle by strainer later, in the stirring of 30-40rpm Under, continue to be heated to 70-80 DEG C, and constant temperature disinfection 10-20min, obtains mixture B;
(5) by aloe protein hydrolysate, licoflavone, algal polysaccharides and the deep-sea fish skin collagen of formula ratio, in proportion It after weighing, is added in emulsion pot, and keeps the temperature 10-15min after stirring 3-5min under the conditions of 45-55 DEG C, obtain mixture C;
(6) effective component of chinese medicine, mixture A and mixture B are slowly added into mixture C, and scrape wall stirring, turned After stirring 5min under fast 50-60rpm, high speed homogenization device is opened, the homogeneous 4-6min under the high speed of 800-900rpm will turn later Prompt drop speed is cooled to interior to 130-160rpm, and under this revolving speed, obtains skin whitening, moisturizing face mask of traditional Chinese medicine.
Compared with prior art, the present invention it has the advantages that
1, the present invention is carried out by four kinds of effective component of chinese medicine, moisturizing effective component, whitening effective component and auxiliary material ingredients Reasonable compatibility plays synergistic function, to improve the whitening of facial mask of the present invention, moistening effect, and produced by the present invention Facial mask is without side-effects, quick, and effect is good, and skin whitening, moisturizing face mask of traditional Chinese medicine obtained is in paste, more convenient using saving;
2, effective component of chinese medicine of the invention have preferable moisturizing water lock function, and with moisturizing effective component phase interworking It closes, skin bottom can be goed deep into and kept the skin wet, can be quickly absorbed by the skin, the performance of keeping humidity of facial mask is effectively improved, meanwhile, Chinese medicine has It is effective to imitate the whitenings such as Rhizoma Atractylodis Macrocephalae zymophyte powder, the hydrolyzed pearl powder contained in whitening conditioning ingredients, with whitening effective component in ingredient Ingredient is organically combined, and functionally carries out balanced collocation, to guarantee to reach efficient beauty under the premise of being perfectly safe White soothing effect further enhances the whitening of facial mask of the present invention in addition, auxiliary material of the invention can be such that each component is effectively dispersed Moisture-keeping functions;
3, Herb Gynostemmae Pentaphylli extract, licorice and the white pond lily flower extract being added in effective component of chinese medicine of the present invention, Trans epidermal water loss can be effectively reduced, keyed moisture plays the function of moisturizing water lock, and skin can be made tender pale, improves glue The synthesis of former albumen and elastic fibers element supplies various kinds of cell growth factor, to have the function that skin whitening;
4, skin whitening, moisturizing face mask of traditional Chinese medicine each component collaboration of the present invention, moistening effect is good, and safe and non-stimulating, while the present invention The preparation method of skin whitening, moisturizing face mask of traditional Chinese medicine is simple, can promote the use of.
Specific embodiment
To make the object, technical solutions and advantages of the present invention clearer, technical solution of the present invention will be carried out below Clear, complete description.Obviously, the described embodiment is only a part of the embodiment of the present invention, instead of all the embodiments. Based on the embodiments of the present invention, those of ordinary skill in the art obtained institute without making creative work There are other embodiments, belongs to the range that the present invention is protected.
Embodiment 1
The skin whitening, moisturizing face mask of traditional Chinese medicine of the present embodiment, the facial mask are effective by effective component of chinese medicine, moisturizing effective component, whitening Ingredient and auxiliary material are made according to the mass ratio of 8:5:3:1;
Wherein, the effective component of chinese medicine is made of the raw material of following parts by weight: 10 parts of radix scutellariae, 5 parts of honeysuckle, root of kirilow rhodiola 3 parts, 2 parts of safflower, 1 part of Herb Gynostemmae Pentaphylli extract, 0.5 part of licorice, 2 parts of white pond lily flower extract;
The moisturizing effective component is made of the raw material of following parts by weight: aloe hydrolyze protein 20 part, 5 parts of licoflavone, 1 part of algal polysaccharides, 0.5 part of deep-sea fish skin collagen;
The whitening effective component is made of the raw material of following parts by weight: 30 parts of Rhizoma Atractylodis Macrocephalae zymophyte powder, hydrolyzed pearl powder 15 Part, 5 parts of arbutin, 1 part of vitamin;
The auxiliary material is made of the raw material of following parts by weight: 5 parts of propylene glycol, 0.5 part of carragheen, hydroxyethyl cellulose 0.4 Part, 1 part of hyaluronic acid.
Wherein, it the preparation method of the Herb Gynostemmae Pentaphylli extract: will be ground into after gynostemma pentaphylla drinking water cleaning, drying thick 8 times of purified waters of gynostemma pentaphylla are added in grain, decoct 2 times, decoct 2h every time, merge decoction liquor, and being concentrated into relative density is 1.15 leachings Cream is let cool, and 95%v/v ethyl alcohol is added and carries out alcohol precipitation, and final alcohol precipitation degree is 70, stands more than for 24 hours, extracts supernatant, carries out Concentration, being concentrated into relative density is 1.30, and medicinal extract is put into rail mounted film drier, is dried, and after dry, is ground into thin Powder, and sieve with 100 mesh sieve to get gynostemma pentaphylla root extract;
The preparation method of the licorice: extracting liquorice is extracted using 80%v/v alcohol reflux, and extracting solution recycles second It after alcohol, then with AB-8 macroreticular resin carries out absorption passivation, and is eluted using 90%v/v ethyl alcohol, collect ethanol eluate, return Ethyl alcohol is received, concentration is dry to get licorice;
The preparation method of the white pond lily flower extract: white pond lily flower is cleaned up with drinking water, crushed after being dried at Coarse grain is added white pond lily and 5 times 70% of ethyl alcohol is spent to carry out alcohol extracting, alcohol extracting 2 times, each 2h, merges alcohol extract, be concentrated into relatively close Degree is 1.25 medicinal extract, lets cool, medicinal extract is put into rail mounted film drier, is dried, and after dry, is ground into fine powder, and It sieves with 100 mesh sieve to get white pond lily flower extract.
Wherein, the Rhizoma Atractylodis Macrocephalae zymophyte powder is made of the substance of following parts by weight: 60 parts of Rhizoma Atractylodis Macrocephalae, hydrolysis 5 parts of royal jelly, egg 3 parts of white peptone, 0.3 part of phosphoric acid hydrogen dimethylamino potassium, 0.5 part of epsom salt.
Wherein, the Rhizoma Atractylodis Macrocephalae zymophyte powder is sufficiently beaten the preparation method comprises the following steps: extra dry white wine art is mixed with water 1:10 in mass ratio Slurry, as basic liquid, hydrolysis royal jelly, peptone, phosphoric acid hydrogen dimethylamino potassium and seven water of above-mentioned parts by weight are added into basal liquid Magnesium sulfate sterilizes after mixing well, and microbe inoculation leavening, is kept for 25 DEG C of temperature, after the 48h that ferments, high-temperature sterilization, and freezing Drying is to get aloe zymophyte powder.
Wherein, the microbe leaven is by Bacillus acidi lactici, bacillus licheniformis, Corynebacterium glutamicum 3:2 in mass ratio: 1 mixing gained.
Wherein, the vitamin is vitamin B, vitamin C and vitamin E, and weight ratio is 1:2:3.
Wherein, the hyaluronic acid is macromolecular Sodium Hyaluronate, middle numerator sodium hyaluronate and micromolecule hyaluronic acid The mixture of sodium, and its weight ratio is 1:1:2.
Wherein, the present invention also provides the preparation methods of above-mentioned skin whitening, moisturizing face mask of traditional Chinese medicine, comprising the following steps:
(1) radix scutellariae, honeysuckle, root of kirilow rhodiola and safflower are weighed in proportion, is added water to cook twice, are added for the first time into raw material Enter the water of 8 times of amounts, heating decocts 1h;After separation of solid and liquid, the water of 4 times of amounts is added, heating decocts 1h, merges the filter decocted twice Liquid, and it is 1.10 that filtrate low-temperature evaporation, which is concentrated into relative density, under stirring condition, is slowly added into the 95%v/v ethyl alcohol of 2 times of amounts Solution stirs, and stands, filtering, and it is 1.20 that filtrate low-temperature evaporation, which is concentrated into relative density, and recycles ethyl alcohol, obtains traditional Chinese medicine extraction Liquid;
(2) Herb Gynostemmae Pentaphylli extract, licorice and white pond lily flower are added in the Chinese medicine extract in step (1) to extract Object, warming while stirring keep 10min to 40 DEG C at such a temperature, obtain effective component of chinese medicine, for use;
(3) by the propylene glycol of formula ratio and carragheen, after weighing in proportion, the stainless steel kettle for having agitating device is added It is interior, it is dissolved by heating completely under the stirring of revolving speed 30rpm, and constant temperature disinfection 20min at a temperature of 80 DEG C, then adds formula The hydroxyethyl cellulose and hyaluronic acid of amount, stir evenly, and obtain mixture A;
(4) it by Rhizoma Atractylodis Macrocephalae zymophyte powder, hydrolyzed pearl powder, arbutin and the vitamin of formula ratio, after weighing in proportion, is added Into emulsion pot, 50 DEG C are heated with stirring to, is extracted into stainless steel homogeneous kettle by strainer later, under the stirring of 30rpm, is continued It is heated to 70 DEG C, and constant temperature disinfection 10min, obtains mixture B;
(5) by aloe protein hydrolysate, licoflavone, algal polysaccharides and the deep-sea fish skin collagen of formula ratio, in proportion It after weighing, is added in emulsion pot, and keeps the temperature 10min after stirring 3min under the conditions of 45 DEG C, obtain mixture C;
(6) effective component of chinese medicine, mixture A and mixture B are slowly added into mixture C, and scrape wall stirring, turned After stirring 5min under fast 50rpm, high speed homogenization device is opened, the homogeneous 4min under the high speed of 800rpm later arrives revolving speed reduction of speed 130rpm, and it is cooled to interior under this revolving speed, obtain skin whitening, moisturizing face mask of traditional Chinese medicine.
Embodiment 2
The skin whitening, moisturizing face mask of traditional Chinese medicine of the present embodiment, the facial mask are effective by effective component of chinese medicine, moisturizing effective component, whitening Ingredient and auxiliary material are made according to the mass ratio of 8:5:3:1;
Wherein, the effective component of chinese medicine is made of the raw material of following parts by weight: 15 parts of radix scutellariae, 10 parts of honeysuckle, red scape It 7 parts, 5 parts of safflower, 3 parts of Herb Gynostemmae Pentaphylli extract, 1.5 parts of licorice, 4 parts of white pond lily flower extract;
The moisturizing effective component is made of the raw material of following parts by weight: 30 parts of aloe protein hydrolysate, 10 parts of licoflavone, 5 parts of algal polysaccharides, 1.5 parts of deep-sea fish skin collagen;
The whitening effective component is made of the raw material of following parts by weight: 40 parts of Rhizoma Atractylodis Macrocephalae zymophyte powder, hydrolyzed pearl powder 25 Part, 10 parts of arbutin, 4 parts of vitamin;
The auxiliary material is made of the raw material of following parts by weight: 10 parts of propylene glycol, 1.5 parts of carragheen, hydroxyethyl cellulose 0.8 Part, 3 parts of hyaluronic acid.
Wherein, it the preparation method of the Herb Gynostemmae Pentaphylli extract: will be ground into after gynostemma pentaphylla drinking water cleaning, drying thick 8 times of purified waters of gynostemma pentaphylla are added in grain, decoct 2 times, decoct 2h every time, merge decoction liquor, and being concentrated into relative density is 1.15 leachings Cream is let cool, and 95%v/v ethyl alcohol is added and carries out alcohol precipitation, and final alcohol precipitation degree is 70, stands more than for 24 hours, extracts supernatant, carries out Concentration, being concentrated into relative density is 1.30, and medicinal extract is put into rail mounted film drier, is dried, and after dry, is ground into thin Powder, and sieve with 100 mesh sieve to get gynostemma pentaphylla root extract;
The preparation method of the licorice: extracting liquorice is extracted using 80%v/v alcohol reflux, and extracting solution recycles second It after alcohol, then with AB-8 macroreticular resin carries out absorption passivation, and is eluted using 90%v/v ethyl alcohol, collect ethanol eluate, return Ethyl alcohol is received, concentration is dry to get licorice;
The preparation method of the white pond lily flower extract: white pond lily flower is cleaned up with drinking water, crushed after being dried at Coarse grain is added white pond lily and 5 times 70% of ethyl alcohol is spent to carry out alcohol extracting, alcohol extracting 2 times, each 2h, merges alcohol extract, be concentrated into relatively close Degree is 1.25 medicinal extract, lets cool, medicinal extract is put into rail mounted film drier, is dried, and after dry, is ground into fine powder, and It sieves with 100 mesh sieve to get white pond lily flower extract.
Wherein, the Rhizoma Atractylodis Macrocephalae zymophyte powder is made of the substance of following parts by weight: 80 parts of Rhizoma Atractylodis Macrocephalae, hydrolysis 10 parts of royal jelly, 6 parts of peptone, 0.7 part of phosphoric acid hydrogen dimethylamino potassium, 1.5 parts of epsom salt.
Wherein, the Rhizoma Atractylodis Macrocephalae zymophyte powder is sufficiently beaten the preparation method comprises the following steps: extra dry white wine art is mixed with water 1:15 in mass ratio Slurry, as basic liquid, hydrolysis royal jelly, peptone, phosphoric acid hydrogen dimethylamino potassium and seven water of above-mentioned parts by weight are added into basal liquid Magnesium sulfate sterilizes after mixing well, and microbe inoculation leavening, is kept for 35 DEG C of temperature, after the 54h that ferments, high-temperature sterilization, and freezing Drying is to get aloe zymophyte powder.
Wherein, the microbe leaven is by Bacillus acidi lactici, bacillus licheniformis, Corynebacterium glutamicum 3:2 in mass ratio: 1 mixing gained.
Wherein, the vitamin is vitamin B, vitamin C and vitamin E, and weight ratio is 1:2:3.
Wherein, the hyaluronic acid is macromolecular Sodium Hyaluronate, middle numerator sodium hyaluronate and micromolecule hyaluronic acid The mixture of sodium, and its weight ratio is 1:1:2.
Wherein, the present invention also provides the preparation methods of above-mentioned skin whitening, moisturizing face mask of traditional Chinese medicine, comprising the following steps:
(1) radix scutellariae, honeysuckle, root of kirilow rhodiola and safflower are weighed in proportion, is added water to cook twice, are added for the first time into raw material Enter the water of 10 times of amounts, heating decocts 2h;After separation of solid and liquid, the water of 6 times of amounts is added, heating decocts 2h, what merging decocted twice Filtrate, and it is 1.20 that filtrate low-temperature evaporation, which is concentrated into relative density, under stirring condition, is slowly added into the 95%v/v second of 2 times of amounts Alcoholic solution stirs, and stands, filtering, and it is 1.30 that filtrate low-temperature evaporation, which is concentrated into relative density, and recycles ethyl alcohol, obtains Chinese medicine and mentions Take liquid;
(2) Herb Gynostemmae Pentaphylli extract, licorice and white pond lily flower are added in the Chinese medicine extract in step (1) to extract Object, warming while stirring keep 20min to 50 DEG C at such a temperature, obtain effective component of chinese medicine, for use;
(3) by the propylene glycol of formula ratio and carragheen, after weighing in proportion, the stainless steel kettle for having agitating device is added It is interior, it is dissolved by heating completely under the stirring of revolving speed 50rpm, and constant temperature disinfection 20min at a temperature of 80 DEG C, then adds formula The hydroxyethyl cellulose and hyaluronic acid of amount, stir evenly, and obtain mixture A;
(4) it by Rhizoma Atractylodis Macrocephalae zymophyte powder, hydrolyzed pearl powder, arbutin and the vitamin of formula ratio, after weighing in proportion, is added Into emulsion pot, 60 DEG C are heated with stirring to, is extracted into stainless steel homogeneous kettle by strainer later, under the stirring of 40rpm, is continued It is heated to 80 DEG C, and constant temperature disinfection 20min, obtains mixture B;
(5) by aloe protein hydrolysate, licoflavone, algal polysaccharides and the deep-sea fish skin collagen of formula ratio, in proportion It after weighing, is added in emulsion pot, and keeps the temperature 15min after stirring 5min under the conditions of 55 DEG C, obtain mixture C;
(6) effective component of chinese medicine, mixture A and mixture B are slowly added into mixture C, and scrape wall stirring, turned After stirring 5min under fast 60rpm, high speed homogenization device is opened, the homogeneous 6min under the high speed of 900rpm later arrives revolving speed reduction of speed 160rpm, and it is cooled to interior under this revolving speed, obtain skin whitening, moisturizing face mask of traditional Chinese medicine.
Embodiment 3
The skin whitening, moisturizing face mask of traditional Chinese medicine of the present embodiment, the facial mask are effective by effective component of chinese medicine, moisturizing effective component, whitening Ingredient and auxiliary material are made according to the mass ratio of 8:5:3:1;
Wherein, the effective component of chinese medicine is made of the raw material of following parts by weight: 12 parts of radix scutellariae, 7.5 parts of honeysuckle, red scape It 5 parts, 3.5 parts of safflower, 2 parts of Herb Gynostemmae Pentaphylli extract, 1 part of licorice, 3 parts of white pond lily flower extract;
The moisturizing effective component is made of the raw material of following parts by weight: aloe hydrolyzes protein 25 part, licoflavone 7.5 Part, 3 parts of algal polysaccharides, 1 part of deep-sea fish skin collagen;
The whitening effective component is made of the raw material of following parts by weight: 35 parts of Rhizoma Atractylodis Macrocephalae zymophyte powder, hydrolyzed pearl powder 20 Part, 7.5 parts of arbutin, 2.5 parts of vitamin;
The auxiliary material is made of the raw material of following parts by weight: 7.5 parts of propylene glycol, 1 part of carragheen, hydroxyethyl cellulose 0.6 Part, 2 parts of hyaluronic acid.
Wherein, it the preparation method of the Herb Gynostemmae Pentaphylli extract: will be ground into after gynostemma pentaphylla drinking water cleaning, drying thick 8 times of purified waters of gynostemma pentaphylla are added in grain, decoct 2 times, decoct 2h every time, merge decoction liquor, and being concentrated into relative density is 1.15 leachings Cream is let cool, and 95%v/v ethyl alcohol is added and carries out alcohol precipitation, and final alcohol precipitation degree is 70, stands more than for 24 hours, extracts supernatant, carries out Concentration, being concentrated into relative density is 1.30, and medicinal extract is put into rail mounted film drier, is dried, and after dry, is ground into thin Powder, and sieve with 100 mesh sieve to get gynostemma pentaphylla root extract;
The preparation method of the licorice: extracting liquorice is extracted using 80%v/v alcohol reflux, and extracting solution recycles second It after alcohol, then with AB-8 macroreticular resin carries out absorption passivation, and is eluted using 90%v/v ethyl alcohol, collect ethanol eluate, return Ethyl alcohol is received, concentration is dry to get licorice;
The preparation method of the white pond lily flower extract: white pond lily flower is cleaned up with drinking water, crushed after being dried at Coarse grain is added white pond lily and 5 times 70% of ethyl alcohol is spent to carry out alcohol extracting, alcohol extracting 2 times, each 2h, merges alcohol extract, be concentrated into relatively close Degree is 1.25 medicinal extract, lets cool, medicinal extract is put into rail mounted film drier, is dried, and after dry, is ground into fine powder, and It sieves with 100 mesh sieve to get white pond lily flower extract.
Wherein, the Rhizoma Atractylodis Macrocephalae zymophyte powder is made of the substance of following parts by weight: 70 parts of Rhizoma Atractylodis Macrocephalae, hydrolysis 7.5 parts of royal jelly, 4.5 parts of peptone, 0.5 part of phosphoric acid hydrogen dimethylamino potassium, 1 part of epsom salt.
Wherein, the Rhizoma Atractylodis Macrocephalae zymophyte powder is sufficiently beaten the preparation method comprises the following steps: extra dry white wine art is mixed with water 1:12 in mass ratio Slurry, as basic liquid, hydrolysis royal jelly, peptone, phosphoric acid hydrogen dimethylamino potassium and seven water of above-mentioned parts by weight are added into basal liquid Magnesium sulfate sterilizes after mixing well, and microbe inoculation leavening, is kept for 30 DEG C of temperature, after the 51h that ferments, high-temperature sterilization, and freezing Drying is to get aloe zymophyte powder.
Wherein, the microbe leaven is by Bacillus acidi lactici, bacillus licheniformis, Corynebacterium glutamicum 3:2 in mass ratio: 1 mixing gained.
Wherein, the vitamin is vitamin B, vitamin C and vitamin E, and weight ratio is 1:2:3.
Wherein, the hyaluronic acid is macromolecular Sodium Hyaluronate, middle numerator sodium hyaluronate and micromolecule hyaluronic acid The mixture of sodium, and its weight ratio is 1:1:2.
Wherein, the present invention also provides the preparation methods of above-mentioned skin whitening, moisturizing face mask of traditional Chinese medicine, comprising the following steps:
(1) radix scutellariae, honeysuckle, root of kirilow rhodiola and safflower are weighed in proportion, is added water to cook twice, are added for the first time into raw material Enter the water of 9 times of amounts, heating decocts 1.5h;After separation of solid and liquid, the water of 5 times of amounts is added, heating decocts 1.5h, and merging decocts twice Filtrate, and it is 1.15, under stirring condition that filtrate low-temperature evaporation, which is concentrated into relative density, is slowly added into the 95%v/v of 2 times of amounts Ethanol solution stirs, and stands, filtering, and it is 1.25 that filtrate low-temperature evaporation, which is concentrated into relative density, and recycles ethyl alcohol, obtains Chinese medicine Extracting solution;
(2) Herb Gynostemmae Pentaphylli extract, licorice and white pond lily flower are added in the Chinese medicine extract in step (1) to extract Object, warming while stirring keep 15in to 45 DEG C at such a temperature, obtain effective component of chinese medicine, for use;
(3) by the propylene glycol of formula ratio and carragheen, after weighing in proportion, the stainless steel kettle for having agitating device is added It is interior, it is dissolved by heating completely under the stirring of revolving speed 40rpm, and constant temperature disinfection 20min at a temperature of 80 DEG C, then adds formula The hydroxyethyl cellulose and hyaluronic acid of amount, stir evenly, and obtain mixture A;
(4) it by Rhizoma Atractylodis Macrocephalae zymophyte powder, hydrolyzed pearl powder, arbutin and the vitamin of formula ratio, after weighing in proportion, is added Into emulsion pot, 55 DEG C are heated with stirring to, is extracted into stainless steel homogeneous kettle by strainer later, under the stirring of 35rpm, is continued It is heated to 75 DEG C, and constant temperature disinfection 15min, obtains mixture B;
(5) by aloe protein hydrolysate, licoflavone, algal polysaccharides and the deep-sea fish skin collagen of formula ratio, in proportion It after weighing, is added in emulsion pot, and keeps the temperature 12min after stirring 4min under the conditions of 50 DEG C, obtain mixture C;
(6) effective component of chinese medicine, mixture A and mixture B are slowly added into mixture C, and scrape wall stirring, turned After stirring 5min under fast 55rpm, high speed homogenization device is opened, the homogeneous 5min under the high speed of 850rpm later arrives revolving speed reduction of speed 145rpm, and it is cooled to interior under this revolving speed, obtain skin whitening, moisturizing face mask of traditional Chinese medicine.
Embodiment 4
The skin whitening, moisturizing face mask of traditional Chinese medicine of the present embodiment, the facial mask are effective by effective component of chinese medicine, moisturizing effective component, whitening Ingredient and auxiliary material are made according to the mass ratio of 8:5:3:1;
Wherein, the effective component of chinese medicine is made of the raw material of following parts by weight: 11 parts of radix scutellariae, 6 parts of honeysuckle, root of kirilow rhodiola 4 parts, 3 parts of safflower, 1.5 parts of Herb Gynostemmae Pentaphylli extract, 0.8 part of licorice, 2.5 parts of white pond lily flower extract;
The moisturizing effective component is made of the raw material of following parts by weight: aloe hydrolyze protein 23 part, 6 parts of licoflavone, 2 parts of algal polysaccharides, 0.8 part of deep-sea fish skin collagen;
The whitening effective component is made of the raw material of following parts by weight: 33 parts of Rhizoma Atractylodis Macrocephalae zymophyte powder, hydrolyzed pearl powder 18 Part, 6 parts of arbutin, 2 parts of vitamin;
The auxiliary material is made of the raw material of following parts by weight: 6 parts of propylene glycol, 0.8 part of carragheen, hydroxyethyl cellulose 0.5 Part, 1.5 parts of hyaluronic acid.
Wherein, it the preparation method of the Herb Gynostemmae Pentaphylli extract: will be ground into after gynostemma pentaphylla drinking water cleaning, drying thick 8 times of purified waters of gynostemma pentaphylla are added in grain, decoct 2 times, decoct 2h every time, merge decoction liquor, and being concentrated into relative density is 1.15 leachings Cream is let cool, and 95%v/v ethyl alcohol is added and carries out alcohol precipitation, and final alcohol precipitation degree is 70, stands more than for 24 hours, extracts supernatant, carries out Concentration, being concentrated into relative density is 1.30, and medicinal extract is put into rail mounted film drier, is dried, and after dry, is ground into thin Powder, and sieve with 100 mesh sieve to get gynostemma pentaphylla root extract;
The preparation method of the licorice: extracting liquorice is extracted using 80%v/v alcohol reflux, and extracting solution recycles second It after alcohol, then with AB-8 macroreticular resin carries out absorption passivation, and is eluted using 90%v/v ethyl alcohol, collect ethanol eluate, return Ethyl alcohol is received, concentration is dry to get licorice;
The preparation method of the white pond lily flower extract: white pond lily flower is cleaned up with drinking water, crushed after being dried at Coarse grain is added white pond lily and 5 times 70% of ethyl alcohol is spent to carry out alcohol extracting, alcohol extracting 2 times, each 2h, merges alcohol extract, be concentrated into relatively close Degree is 1.25 medicinal extract, lets cool, medicinal extract is put into rail mounted film drier, is dried, and after dry, is ground into fine powder, and It sieves with 100 mesh sieve to get white pond lily flower extract.
Wherein, the Rhizoma Atractylodis Macrocephalae zymophyte powder is made of the substance of following parts by weight: 65 parts of Rhizoma Atractylodis Macrocephalae, hydrolysis 6 parts of royal jelly, egg 4 parts of white peptone, 0.4 part of phosphoric acid hydrogen dimethylamino potassium, 0.8 part of epsom salt.
Wherein, the Rhizoma Atractylodis Macrocephalae zymophyte powder is sufficiently beaten the preparation method comprises the following steps: extra dry white wine art is mixed with water 1:11 in mass ratio Slurry, as basic liquid, hydrolysis royal jelly, peptone, phosphoric acid hydrogen dimethylamino potassium and seven water of above-mentioned parts by weight are added into basal liquid Magnesium sulfate sterilizes after mixing well, and microbe inoculation leavening, is kept for 28 DEG C of temperature, after the 50h that ferments, high-temperature sterilization, and freezing Drying is to get aloe zymophyte powder.
Wherein, the microbe leaven is by Bacillus acidi lactici, bacillus licheniformis, Corynebacterium glutamicum 3:2 in mass ratio: 1 mixing gained.
Wherein, the vitamin is vitamin B, vitamin C and vitamin E, and weight ratio is 1:2:3.
Wherein, the hyaluronic acid is macromolecular Sodium Hyaluronate, middle numerator sodium hyaluronate and micromolecule hyaluronic acid The mixture of sodium, and its weight ratio is 1:1:2.
Wherein, the present invention also provides the preparation methods of above-mentioned skin whitening, moisturizing face mask of traditional Chinese medicine, comprising the following steps:
(1) radix scutellariae, honeysuckle, root of kirilow rhodiola and safflower are weighed in proportion, is added water to cook twice, are added for the first time into raw material Enter the water of 8.5 times of amounts, heating decocts 1.2h;After separation of solid and liquid, the water of 4.5 times of amounts is added, heating decocts 1.2h, merges twice The filtrate of decoction, and it is 1.12 that filtrate low-temperature evaporation, which is concentrated into relative density, under stirring condition, is slowly added into 2 times of amounts 95%v/v ethanol solution stirs, and stands, filtering, and it is 1.23 that filtrate low-temperature evaporation, which is concentrated into relative density, and recycles ethyl alcohol, obtains To Chinese medicine extract;
(2) Herb Gynostemmae Pentaphylli extract, licorice and white pond lily flower are added in the Chinese medicine extract in step (1) to extract Object, warming while stirring keep 13min to 42 DEG C at such a temperature, obtain effective component of chinese medicine, for use;
(3) by the propylene glycol of formula ratio and carragheen, after weighing in proportion, the stainless steel kettle for having agitating device is added It is interior, it is dissolved by heating completely under the stirring of revolving speed 35rpm, and constant temperature disinfection 20min at a temperature of 80 DEG C, then adds formula The hydroxyethyl cellulose and hyaluronic acid of amount, stir evenly, and obtain mixture A;
(4) it by Rhizoma Atractylodis Macrocephalae zymophyte powder, hydrolyzed pearl powder, arbutin and the vitamin of formula ratio, after weighing in proportion, is added Into emulsion pot, 53 DEG C are heated with stirring to, is extracted into stainless steel homogeneous kettle by strainer later, under the stirring of 33rpm, is continued It is heated to 72 DEG C, and constant temperature disinfection 13min, obtains mixture B;
(5) by aloe protein hydrolysate, licoflavone, algal polysaccharides and the deep-sea fish skin collagen of formula ratio, in proportion It after weighing, is added in emulsion pot, and keeps the temperature 11min after stirring 3.5min under the conditions of 48 DEG C, obtain mixture C;
(6) effective component of chinese medicine, mixture A and mixture B are slowly added into mixture C, and scrape wall stirring, turned After stirring 5min under fast 53rpm, high speed homogenization device, the homogeneous 4.5min under the high speed of 830rpm, later by revolving speed reduction of speed are opened It is cooled to interior to 140rpm, and under this revolving speed, obtains skin whitening, moisturizing face mask of traditional Chinese medicine.
Embodiment 5
The skin whitening, moisturizing face mask of traditional Chinese medicine of the present embodiment, the facial mask are effective by effective component of chinese medicine, moisturizing effective component, whitening Ingredient and auxiliary material are made according to the mass ratio of 8:5:3:1;
Wherein, the effective component of chinese medicine is made of the raw material of following parts by weight: 14 parts of radix scutellariae, 9 parts of honeysuckle, root of kirilow rhodiola 6 parts, 4 parts of safflower, 2.5 parts of Herb Gynostemmae Pentaphylli extract, 1.2 parts of licorice, 3.5 parts of white pond lily flower extract;
The moisturizing effective component is made of the raw material of following parts by weight: aloe hydrolyze protein 28 part, 9 parts of licoflavone, 4 parts of algal polysaccharides, 1.2 parts of deep-sea fish skin collagen;
The whitening effective component is made of the raw material of following parts by weight: 38 parts of Rhizoma Atractylodis Macrocephalae zymophyte powder, hydrolyzed pearl powder 22 Part, 9 parts of arbutin, 3 parts of vitamin;
The auxiliary material is made of the raw material of following parts by weight: 9 parts of propylene glycol, 1.3 parts of carragheen, hydroxyethyl cellulose 0.7 Part, 2.5 parts of hyaluronic acid.
Wherein, it the preparation method of the Herb Gynostemmae Pentaphylli extract: will be ground into after gynostemma pentaphylla drinking water cleaning, drying thick 8 times of purified waters of gynostemma pentaphylla are added in grain, decoct 2 times, decoct 2h every time, merge decoction liquor, and being concentrated into relative density is 1.15 leachings Cream is let cool, and 95%v/v ethyl alcohol is added and carries out alcohol precipitation, and final alcohol precipitation degree is 70, stands more than for 24 hours, extracts supernatant, carries out Concentration, being concentrated into relative density is 1.30, and medicinal extract is put into rail mounted film drier, is dried, and after dry, is ground into thin Powder, and sieve with 100 mesh sieve to get gynostemma pentaphylla root extract;
The preparation method of the licorice: extracting liquorice is extracted using 80%v/v alcohol reflux, and extracting solution recycles second It after alcohol, then with AB-8 macroreticular resin carries out absorption passivation, and is eluted using 90%v/v ethyl alcohol, collect ethanol eluate, return Ethyl alcohol is received, concentration is dry to get licorice;
The preparation method of the white pond lily flower extract: white pond lily flower is cleaned up with drinking water, crushed after being dried at Coarse grain is added white pond lily and 5 times 70% of ethyl alcohol is spent to carry out alcohol extracting, alcohol extracting 2 times, each 2h, merges alcohol extract, be concentrated into relatively close Degree is 1.25 medicinal extract, lets cool, medicinal extract is put into rail mounted film drier, is dried, and after dry, is ground into fine powder, and It sieves with 100 mesh sieve to get white pond lily flower extract.
Wherein, the Rhizoma Atractylodis Macrocephalae zymophyte powder is made of the substance of following parts by weight: 75 parts of Rhizoma Atractylodis Macrocephalae, hydrolysis 9 parts of royal jelly, egg 5 parts of white peptone, 0.6 part of phosphoric acid hydrogen dimethylamino potassium, 1.2 parts of epsom salt.
Wherein, the Rhizoma Atractylodis Macrocephalae zymophyte powder is sufficiently beaten the preparation method comprises the following steps: extra dry white wine art is mixed with water 1:14 in mass ratio Slurry, as basic liquid, hydrolysis royal jelly, peptone, phosphoric acid hydrogen dimethylamino potassium and seven water of above-mentioned parts by weight are added into basal liquid Magnesium sulfate sterilizes after mixing well, and microbe inoculation leavening, is kept for 32 DEG C of temperature, after the 52h that ferments, high-temperature sterilization, and freezing Drying is to get aloe zymophyte powder.
Wherein, the microbe leaven is by Bacillus acidi lactici, bacillus licheniformis, Corynebacterium glutamicum 3:2 in mass ratio: 1 mixing gained.
Wherein, the vitamin is vitamin B, vitamin C and vitamin E, and weight ratio is 1:2:3.
Wherein, the hyaluronic acid is macromolecular Sodium Hyaluronate, middle numerator sodium hyaluronate and micromolecule hyaluronic acid The mixture of sodium, and its weight ratio is 1:1:2.
Wherein, the present invention also provides the preparation methods of above-mentioned skin whitening, moisturizing face mask of traditional Chinese medicine, comprising the following steps:
(1) radix scutellariae, honeysuckle, root of kirilow rhodiola and safflower are weighed in proportion, is added water to cook twice, are added for the first time into raw material Enter the water of 9 times of amounts, heating decocts 1.8h;After separation of solid and liquid, the water of 5.5 times of amounts is added, heating decocts 1.8h, and merging is decocted twice The filtrate boiled, and it is 1.18 that filtrate low-temperature evaporation, which is concentrated into relative density, under stirring condition, is slowly added into the 95% of 2 times of amounts V/v ethanol solution stirs, and stands, filtering, it is 1.28 that filtrate low-temperature evaporation, which is concentrated into relative density, and recycles ethyl alcohol, obtains Medicament extracting solution;
(2) Herb Gynostemmae Pentaphylli extract, licorice and white pond lily flower are added in the Chinese medicine extract in step (1) to extract Object, warming while stirring keep 18min to 48 DEG C at such a temperature, obtain effective component of chinese medicine, for use;
(3) by the propylene glycol of formula ratio and carragheen, after weighing in proportion, the stainless steel kettle for having agitating device is added It is interior, it is dissolved by heating completely under the stirring of revolving speed 45rpm, and constant temperature disinfection 20min at a temperature of 80 DEG C, then adds formula The hydroxyethyl cellulose and hyaluronic acid of amount, stir evenly, and obtain mixture A;
(4) it by Rhizoma Atractylodis Macrocephalae zymophyte powder, hydrolyzed pearl powder, arbutin and the vitamin of formula ratio, after weighing in proportion, is added Into emulsion pot, 58 DEG C are heated with stirring to, is extracted into stainless steel homogeneous kettle by strainer later, under the stirring of 38rpm, is continued It is heated to 78 DEG C, and constant temperature disinfection 18min, obtains mixture B;
(5) by aloe protein hydrolysate, licoflavone, algal polysaccharides and the deep-sea fish skin collagen of formula ratio, in proportion It after weighing, is added in emulsion pot, and keeps the temperature 14min after stirring 4.5min under the conditions of 52 DEG C, obtain mixture C;
(6) effective component of chinese medicine, mixture A and mixture B are slowly added into mixture C, and scrape wall stirring, turned After stirring 5min under fast 58rpm, high speed homogenization device, the homogeneous 5.5min under the high speed of 880rpm, later by revolving speed reduction of speed are opened It is cooled to interior to 150rpm, and under this revolving speed, obtains skin whitening, moisturizing face mask of traditional Chinese medicine.
Comparative example 1
In addition to Herb Gynostemmae Pentaphylli extract, licorice and the white pond lily flower extract in effective component of chinese medicine are saved, Its material content and preparation step are consistent with embodiment 1.
Comparative example 2
In addition to saving moisturizing effective component, other material contents and preparation step are consistent with embodiment 1.
Comparative example 3
In addition to the aloe protein hydrolysate in moisturizing effective component is saved, other material contents and the same embodiment of preparation step 1 is consistent.
Comparative example 4
In addition to saving whitening effective component, other material contents and preparation step are consistent with embodiment 1.
Comparative example 5
In addition to saving the Rhizoma Atractylodis Macrocephalae zymophyte powder in whitening effective component, material content and preparation step are the same as embodiment 1 Unanimously.
Experimental example 1
Product Safety evaluates (experiment of human skin patch)
1, trial target: skin whitening, moisturizing face mask of traditional Chinese medicine prepared by embodiment 1-5, comparative example 1-5
Tested crowd's number: 50 people
Age: between 20-50 years old
Gender: 35 people of female, male 15 people
Health status: subjects skin's health, no skin disease allergies meet subject and volunteer inclusion criteria.
2, patch method: qualified spot tester is selected, with closed patch experiment method, by tested material about 0.020ml- For 0.025ml drop in spot tester, external application special adhesive tape is covered on subject back, and tested material is removed after 24 hours, is removed respectively Observation dermoreaction in 0.5,6,12,24,48 hour afterwards, records it according to dermoreaction grade scale in " cosmetics health specification " As a result.
3, experimental result: human skin patch test result is shown: 50 subjects pass through embodiment 1-5, comparative example 1-5 Skin whitening, moisturizing face mask of traditional Chinese medicine patch test, in observation dermoreaction in 0.5,6,12,24,48 hour, wherein 0 there is skin It is safe to illustrate that skin whitening, moisturizing face mask of traditional Chinese medicine of the invention uses for adverse reaction.
Experimental example 2
Product moisturizing effect measuring
1,100 female volunteers are invited, are randomly divided into 10 groups, are tried out made from embodiment 1-5, comparative example 1-5 respectively Skin whitening, moisturizing face mask of traditional Chinese medicine.Volunteer is distinguished using after clear water cleaning face using Fiss Kai Er SK-III skin moisture detector The moisture content of forehead, left face, right face and chin skin is tested, and takes arithmetic mean of instantaneous value, volunteer reuses above-mentioned whitening and protects Wet face mask of traditional Chinese medicine is uniformly applied to face, gently pats, and tests forehead, left face, right face with skin moisture tester after 10min With the skin moisture content of chin same location, and arithmetic mean of instantaneous value is taken, skin moisture tester test one is reused after 12h Time.The result tested is taken arithmetic mean of instantaneous value by every group of 10 volunteers, test result is as follows table 1.
Wherein, skin moisture content gradient after moisture retention water 10min=use skin average water after moisture retention water 10min is used Point-use skin average moisture before moisture retention water.
Use skin moisture content gradient after moisture retention water 12h=use skin average moisture after moisture retention water 12h-use guarantor Skin average moisture before wet water.
1 skin moisture content test result table of table
As shown in Table 1, the moisturizing of skin whitening, moisturizing face mask of traditional Chinese medicine of the invention, moistening effect are good, can not only be significant after use Skin moisture content is improved, moisture can be also lockked, reduces water loss, skin is made to keep long-acting water profit.Wherein with embodiment 3 The moisturizing of skin whitening, moisturizing face mask of traditional Chinese medicine, water lock effect are best, are highly preferred embodiment of the present invention.And by comparative example 1-5 it is found that It is effective by the way that Herb Gynostemmae Pentaphylli extract, licorice and white pond lily flower extract and moisturizing are added in whitening and moisturizing facial mask Ingredient, whitening effective component can effectively improve moisturizing, the water lock effect of whitening and moisturizing facial mask.
2, (one month) the feedback conclusive table on probation of skin whitening, moisturizing face mask of traditional Chinese medicine
Gender number: female, 200 people
Age: between 20-40 years old
Health status: subjects skin's health, no skin disease allergies meet subject and volunteer inclusion criteria.
Grouping: being randomly divided into 10 groups, and every group of 20 people average age 28 ± 2 years old, try out embodiment 1-5, comparative example 1- respectively Using effect is observed and experienced to skin whitening, moisturizing face mask of traditional Chinese medicine made from 5
Test method: after volunteer cleans face, film cloth is unfolded inwardly to be lightly spread in face, flicking is bonded to complete, gently It pats to beat to skin and all absorb, it is each using primary daily morning and evening, adhere to using one month, at least checks weekly once to understand Whether there is or not whole body and local adverse reactions, and record result in detail.Test assessment result such as the following table 2:
2 skin whitening, moisturizing face mask of traditional Chinese medicine of table tries out (one month) feedback conclusive table
The skin whitening, moisturizing face mask of traditional Chinese medicine of 1-5 of the embodiment of the present invention liking and approving by volunteer on probation as shown in Table 2, Volunteer on probation indicates the mild pro-skin of moisture retention water, easily absorbs, and using the salubrious non-greasy of rear face, moistening effect is good, tries out one Feel after month dry skin, it is coarse, low and deep etc. be improved significantly, skin water profit is smooth, flexible.In embodiment 1-5, implement The degree of recognition highest of 3 skin whitening, moisturizing face mask of traditional Chinese medicine of example, therefore embodiment 3 is highly preferred embodiment of the present invention.And comparative example 1-5 Using effect is not so good as embodiment 1-5, it can be seen that, by the way that Herb Gynostemmae Pentaphylli extract is added in whitening and moisturizing facial mask, Radix Glycyrrhizae mentions Object and white pond lily flower extract and moisturizing effective component, whitening effective component are taken, can effectively improve whitening and moisturizing facial mask Moisturizing, water lock effect.
Experimental example 3
The skin whitening, moisturizing face mask of traditional Chinese medicine of embodiment 1-5 and comparative example 1-5 are verified, trier uses 2-3 times weekly, Continuous use one month, each embodiment are chosen 10 volunteers and are tried out, and whitening effect is divided into three grades:
Whitening effect is obvious: skin obviously bleaches, and is moistened with rear skin water, and white effect protects special a whole day;
Whitening effect is general: skin has that darkening is bright, is moistened with rear skin water, and white effect protects special half a day;
Whitening effect is unchanged: skin does not bleach, but the sign also deepened without black.
Application product result on trial of the present invention is as shown in table 3.
Table 3
As shown in Table 3, the whitening function that skin whitening, moisturizing face mask of traditional Chinese medicine of the invention has had, and by comparative example 1-5 it is found that It is effective by the way that Herb Gynostemmae Pentaphylli extract, licorice and white pond lily flower extract and moisturizing are added in whitening and moisturizing facial mask Ingredient, whitening effective component powder, can be improved the whitening effect of skin whitening, moisturizing face mask of traditional Chinese medicine.
In conclusion the present invention provides a kind of skin whitening, moisturizing face mask of traditional Chinese medicine and preparation method thereof, by the way that Chinese medicine is effective Four kinds of ingredient, moisturizing effective component, whitening effective component and auxiliary ingredients carry out reasonable compatibility, play synergistic function, from And the whitening of facial mask of the present invention, moistening effect are improved, and facial mask produced by the present invention is without side-effects, quick, effect is good.
Specific embodiments of the present invention are described above.It is to be appreciated that the invention is not limited to above-mentioned Particular implementation, those skilled in the art can make various deformations or amendments within the scope of the claims, this not shadow Ring substantive content of the invention.

Claims (8)

1. a kind of skin whitening, moisturizing face mask of traditional Chinese medicine, which is characterized in that the facial mask is by effective component of chinese medicine, moisturizing effective component, whitening Effective component and auxiliary material are made according to the mass ratio of 8:5:3:1;
Wherein, the effective component of chinese medicine is made of the raw material of following parts by weight: 10-15 parts of radix scutellariae, 5-10 parts of honeysuckle, red scape Its 3-7 parts, 2-5 parts of safflower, 1-3 parts of Herb Gynostemmae Pentaphylli extract, 0.5-1.5 parts of licorice, white pond lily flower extract 2-4 Part;
The moisturizing effective component is made of the raw material of following parts by weight: aloe hydrolyzes -30 parts of protein 20, licoflavone 5-10 Part, 1-5 parts of algal polysaccharides, 0.5-1.5 parts of deep-sea fish skin collagen;
The whitening effective component is made of the raw material of following parts by weight: 30-40 parts of Rhizoma Atractylodis Macrocephalae zymophyte powder, hydrolyzed pearl powder 15- 25 parts, 5-10 parts of arbutin, 1-4 parts of vitamin;
The auxiliary material is made of the raw material of following parts by weight: 5-10 parts of propylene glycol, 0.5-1.5 parts of carragheen, hydroxyethyl cellulose 0.4-0.8 parts, 1-3 parts of hyaluronic acid.
2. skin whitening, moisturizing face mask of traditional Chinese medicine according to claim 1, which is characterized in that the preparation of the Herb Gynostemmae Pentaphylli extract Method: will be ground into coarse grain after gynostemma pentaphylla drinking water cleaning, drying, 8 times of purified waters of gynostemma pentaphylla are added, and decoct 2 times, decoct every time 2h is boiled, decoction liquor is merged, being concentrated into relative density is 1.15 medicinal extract, is let cool, and 95%v/v ethyl alcohol is added and carries out alcohol precipitation, final alcohol precipitation Degree is 70, stands more than for 24 hours, extracts supernatant, be concentrated, and being concentrated into relative density is 1.30, and medicinal extract is put into track Formula film drier, is dried, and after dry, is ground into fine powder, and sieve with 100 mesh sieve to get gynostemma pentaphylla root extract;
The preparation method of the licorice: extracting liquorice is extracted using 80%v/v alcohol reflux, after extracting solution recycles ethyl alcohol, Absorption passivation is carried out with AB-8 macroreticular resin again, and is eluted using 90%v/v ethyl alcohol, ethanol eluate is collected, recycles second Alcohol, concentration are dry to get licorice;
The preparation method of the white pond lily flower extract: white pond lily flower is cleaned up with drinking water, crushed after being dried at coarse grain, White pond lily, which is added, spends 5 times 70% of ethyl alcohol to carry out alcohol extracting, alcohol extracting 2 times, each 2h, merges alcohol extract, being concentrated into relative density is 1.25 medicinal extract, let cool, and medicinal extract is put into rail mounted film drier, is dried, and after dry, are ground into fine powder, and cross 100 Mesh is to get white pond lily flower extract.
3. skin whitening, moisturizing face mask of traditional Chinese medicine according to claim 1, which is characterized in that the Rhizoma Atractylodis Macrocephalae zymophyte powder is by following heavy The substance of amount part is made: 60-80 parts of Rhizoma Atractylodis Macrocephalae, hydrolysis royal jelly 5-10 parts, 3-6 parts of peptone, phosphoric acid hydrogen dimethylamino potassium 0.3-0.7 Part, 0.5-1.5 parts of epsom salt.
4. skin whitening, moisturizing face mask of traditional Chinese medicine according to claim 3, which is characterized in that the preparation side of the Rhizoma Atractylodis Macrocephalae zymophyte powder Method are as follows: extra dry white wine art is mixed to sufficiently mashing with water 1:10-15 in mass ratio, as basic liquid, is added into basal liquid above-mentioned heavy The hydrolysis royal jelly, peptone, phosphoric acid hydrogen dimethylamino potassium and epsom salt of amount part sterilize after mixing well, and microbe inoculation is sent out Ferment agent is kept for 25-35 DEG C of temperature, and after the 48-54h that ferments, high-temperature sterilization is freeze-dried to get aloe zymophyte powder.
5. skin whitening, moisturizing face mask of traditional Chinese medicine according to claim 4, which is characterized in that the microbe leaven is by lactic acid bar Bacterium, bacillus licheniformis, Corynebacterium glutamicum 3:2:1 in mass ratio mixing gained.
6. skin whitening, moisturizing face mask of traditional Chinese medicine according to claim 5, which is characterized in that the vitamin is vitamin B, dimension life Plain C and vitamin E, and weight ratio is 1:2:3.
7. skin whitening, moisturizing face mask of traditional Chinese medicine according to claim 1, which is characterized in that the hyaluronic acid is that macromolecular is transparent The mixture of matter acid sodium, middle numerator sodium hyaluronate and micromolecule hyaluronic acid sodium, and its weight ratio is 1:1:2.
8. the preparation method of skin whitening, moisturizing face mask of traditional Chinese medicine according to claim 1-7, which is characterized in that including with Lower step:
(1) radix scutellariae, honeysuckle, root of kirilow rhodiola and safflower are weighed in proportion, add water to cook twice, 8- is added into raw material for the first time The water of 10 times of amounts, heating decoct 1-2h;After separation of solid and liquid, the 4-6 times of water measured is added, heating decocts 1-2h, and merging is decocted twice The filtrate boiled, and filtrate low-temperature evaporation is concentrated into relative density as 1.10-1.20, under stirring condition, it is slowly added into 2 times of amounts 95%v/v ethanol solution stirs, and stands, and filtering, it is 1.20-1.30 that filtrate low-temperature evaporation, which is concentrated into relative density, and recycles second Alcohol obtains Chinese medicine extract;
(2) Herb Gynostemmae Pentaphylli extract, licorice and white pond lily flower extract are added in the Chinese medicine extract in step (1), Warming while stirring keeps 10-20min to 40-50 DEG C at such a temperature, obtains effective component of chinese medicine, for use;
(3) it by the propylene glycol of formula ratio and carragheen, after weighing in proportion, is added in the stainless steel kettle with agitating device, It is dissolved by heating completely under the stirring of revolving speed 30-50rpm, and constant temperature disinfection 20min at a temperature of 80 DEG C, then adds formula ratio Hydroxyethyl cellulose and hyaluronic acid, stir evenly, obtain mixture A;
(4) by Rhizoma Atractylodis Macrocephalae zymophyte powder, hydrolyzed pearl powder, arbutin and the vitamin of formula ratio, after weighing in proportion, it is added to cream Change in pot, is heated with stirring to 50-60 DEG C, is extracted into stainless steel homogeneous kettle by strainer later, under the stirring of 30-40rpm, after It is continuous to be heated to 70-80 DEG C, and constant temperature disinfection 10-20min, obtain mixture B;
(5) it by aloe protein hydrolysate, licoflavone, algal polysaccharides and the deep-sea fish skin collagen of formula ratio, weighs in proportion Afterwards, it is added in emulsion pot, and keeps the temperature 10-15min after stirring 3-5min under the conditions of 45-55 DEG C, obtain mixture C;
(6) and wall stirring is scraped, after stirring 5min at revolving speed 50-60rpm, high speed homogenization device is opened, in the height of 800-900rpm The lower homogeneous 4-6min of speed, later by revolving speed reduction of speed to 130-160rpm, and is cooled to interior under this revolving speed, obtains skin whitening, moisturizing Face mask of traditional Chinese medicine.
CN201811437292.XA 2018-11-28 2018-11-28 A kind of skin whitening, moisturizing face mask of traditional Chinese medicine and preparation method thereof Pending CN109431935A (en)

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CN111249194A (en) * 2020-02-18 2020-06-09 广州清淞泉生物科技有限公司 Non-irritant composition with whitening and moisturizing functions and preparation method thereof
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CN109908068A (en) * 2019-04-16 2019-06-21 四川圣雪生物科技有限公司 A kind of preparation method of safflower facial mask
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