CN108042388A - A kind of moisturizing and skin rejuvenating facial mask and preparation method thereof - Google Patents
A kind of moisturizing and skin rejuvenating facial mask and preparation method thereof Download PDFInfo
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- CN108042388A CN108042388A CN201810040273.7A CN201810040273A CN108042388A CN 108042388 A CN108042388 A CN 108042388A CN 201810040273 A CN201810040273 A CN 201810040273A CN 108042388 A CN108042388 A CN 108042388A
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/65—Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/31—Hydrocarbons
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
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- A61K8/73—Polysaccharides
- A61K8/733—Alginic acid; Salts thereof
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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Abstract
The invention discloses a kind of moisturizing and skin rejuvenating facial mask and preparation method thereof, belong to the technical field of facial mask.The present invention includes the raw material of following weight percentage：Glycerine 3 10%, butanediol 1.5 4.5%, deep-sea fish collagen peptide 1 4%, trehalose 3 8%, saualane 0.05 2%, Sodium Hyaluronate 0.15 2%, propylene glycol 1 5%, xanthans 0.02 0.35%, rilanit special 0.02 0.45%, polysorbate 0.02 2%, Phenoxyethanol 0.01 1%, methyl hydroxybenzoate 0.01 0.5%, beta glucan 0.1 2%, grape seed extract 0.01 0.5%, aloe extract 0.01 3%, dipotassium glycyrrhizinate 0.01 1%, surplus is deionized water.The facial mask of the present invention promotes absorption of the skin to moisture content, is conducive to skin long-time moisturizing, non-stimulated, plays an important role of good moisturizing.
Description
Technical field
The invention belongs to the technical fields of facial mask, particularly relate to a kind of moisturizing and skin rejuvenating facial mask and preparation method thereof.
Background technology
Due to natural aging and outside environmental elements, skin can gradually lose the protection work(to outside contamination and microorganism
Can, all the more sensitive to the harm of surrounding, skin adapts to the ability of environment worse and worse, and shining upon can lead with ionising radiation etc.
Cause the drying of skin water shortage, especially summer, long-term exposed skin is also possible to be tanned severely, cause to have dry skin, relax, allergy,
It is dim, the skin problems such as lack flexibility.The skin of people was put into natural aging state from 20 years old or so, with the increasing at age
Greatly, sebum secretion amount is reduced, and water retaining capacity reduces, and the moisture content barrier function of skin progressively fails, and starts skin occur to do
The problems such as dry, elastic variation and wrinkle increase.
Various for alleviating or solving the cosmetics species of skin problem, facial mask is due to quick result, fashion and experience
Feel stronger feature and liked be subject to consumer.In daily life, moisturizing is skin care means the most basic, if skin
Water shortage, it is easy to increase the chance of wrinkle generation, thus, majority select the moisture of moisture saver mask raising skin.Existing guarantor
Wet facial mask, moisture-keeping efficacy is undesirable, moreover, partial face mask ingredient contains chemical composition, such facial mask will not only play guarantor
Effect is supported, can also make the situation of skin poorer sometimes.
The content of the invention
The object of the present invention is to provide a kind of moisturizing and skin rejuvenating facial masks and preparation method thereof, solve moisturizing face in the prior art
Film moistening effect is undesirable and easy the problem of jeopardizing skin present situation.
A kind of moisturizing and skin rejuvenating facial mask of the present invention, is mainly realized by the following technical programs：Including following
The raw material of weight percentage：Glycerine 3-10%, butanediol 1.5-4.5%, deep-sea fish collagen peptide 1-4%, trehalose 3-
8%, saualane 0.05-2%, Sodium Hyaluronate 0.15-2%, propylene glycol 1-5%, xanthans 0.02-0.35%, hydrogenated castor
Oily 0.02-0.45%, polysorbate 0.02-2%, Phenoxyethanol 0.01-1%, methyl hydroxybenzoate 0.01-0.5%, β-Portugal gathers
Sugared 0.1-2%, grape seed extract 0.01-0.5%, aloe extract 0.01-3%, dipotassium glycyrrhizinate 0.01-1%, surplus are
Deionized water.
The present invention is used obtained by abyssal fishes collagen peptide cooperation grape seed extract, beta glucan and rilanit special
Facial mask has many advantages, such as low irritability, pollution-free, non-stimulated and without zoonosis cause of disease, not only improves the warp of corresponding fish
Ji is worth and can reduce environmental pollution；Under the booster action of trehalose, aloe extract and Sodium Hyaluronate, promote
Absorption of the skin to moisture content is conducive to skin long-time moisturizing, improves the work(of the moisturizing of facial mask liquid, moisturizing and anti-aging
Effect；The present invention reduces irritation of the facial mask liquid to skin, is easily absorbed by mask carriers without using ethyl alcohol, easy to use, face
Film applies is playing the role of moisturizing on the face.
As a kind of preferred embodiment, include the raw material of following weight percentage：Glycerine 4-8%, butanediol 2-
4%, deep-sea fish collagen peptide 2-3.8%, trehalose 5-7%, saualane 0.5-1.5%, Sodium Hyaluronate 0.2-1.5%,
Propylene glycol 1.5-3%, xanthans 0.05-0.25%, rilanit special 0.05-0.25%, polysorbate 0.05-0.15%,
Phenoxyethanol 0.05-0.9%, methyl hydroxybenzoate 0.03-0.3%, beta glucan 0.1-2%, grape seed extract 0.015-
0.15%, aloe extract 0.05-2%, dipotassium glycyrrhizinate 0.01-0.5%, surplus are deionized water.Deep-sea fish collagen
Peptide is pollution-free, sensitization is low, and moisturizing can be played the role of, moisten, repair skin, the depth that the present invention selects by making an addition in cosmetics
Ocean fish collagen peptide molecular weight section is low, balanced proportion, transdermal rate are high, can pass through skin surface enhancing skin collagen again
It is raw, recover elasticity of skin, and high water solubility contains largely exposed hydrogen bond group promotion and other compatibilities, keeps system steady
It is fixed；For trehalose on the basis of moistening effect is good, moisture preserving time is lasting, has the work(for stablizing biomembrane and protein structure
Effect, is formed by two glucose molecules by hemiacetal hydroxyl condensation, has stronger hydrogen bonding capability, on the basis of dissolution
On play thickening power, enhance system stability；Saualane, the hydrocarbons being made of six isoprene double bonds, belongs to class
Terpene structure strengthens maintenance epidermis, is effectively formed natural protective film, helps the balance between skin and sebum, passes through hydrogen bonding base
Group forms the stabilising system with concertedness, validity, compatibility with other components, and in body under the action of blended emulsifier
It is stabilized in system；Trehalose has certain film forming, and can form protective film in skin surface prevents water loss；Spiny dogfish
Alkane can inhibit the peroxidating of skin lipid, can effectively infiltrate through skin, and promote the multiplication of skin base cell, to delaying skin
Aging has certain effect；Deep-sea fish collagen peptide can pass through surface layer skin, reach deeply preserving moisture, and battalion is provided for skin reparation
Support substance.The present invention also with the use of beta glucan, grape seed extract, aloe extract and other functional ingredient, reaches from inside to outside
To the effect of the tender skin of moisturizing.
As a kind of preferred embodiment, include the raw material of following weight percentage：Glycerine 5%, butanediol
3.5%, deep-sea fish collagen peptide 3.5%, trehalose 6%, saualane 0.75%, Sodium Hyaluronate 0.45%, propylene glycol
2.5%, xanthans 0.13%, rilanit special 0.15%, polysorbate 0.1%, Phenoxyethanol 0.8%, methyl hydroxybenzoate
0.2%, beta glucan 0.1-2%, grape seed extract 0.015-0.15%, aloe extract 0.1-1%, dipotassium glycyrrhizinate
0.01-0.2%, surplus are deionized water.The facial mask deep-sea fish collagen peptide of this formula, trehalose, saualane and other effects
Ingredient can play maximum performance, be optimal facial mask liquid effect, interact between each ingredient, and system is in most stable shape
State.
As a kind of preferred embodiment, the aloe extract is that butt aloe polysaccharide content is more than 800ppm, institute
Proanthocyanidin from Grape-seed Extracts is stated more than 90%.Aloe polysaccharide content is more than 800ppm in dry powder aloe extract,
Containing substantial amounts of procyanidine in grape pip, vine polyphenol is known as potent free radical scavenger, is the efficient of plant origin
One of antioxidant；Grape seed extract is a variety of with removing free radical, the collagen for repairing injury and elastomer, improvement
Allergy also makes skin moist with astriction, and addition grape seed extract can improve the anti-aging, tender of facial mask liquid
The effect of skin；Aloe extract has antiphlogistic antibacterial, enhancing skin elasticity, protects mucocutaneous, clean skin seborrhea, profit
Damp skin prevents the effects that aging that addition use makes facial mask liquid equally be used in sensitive skin, increases the applicable model of facial mask liquid
It encloses.
As a kind of preferred embodiment, the molecular weight of the deep-sea fish collagen peptide is 200-1500Da, β-Portugal
Yeast purity is 70-80% in glycan.The index of rilanit special meets ECOCERT certifications in the present invention；Beta glucan is day
Right high glycan, macromolecular structure can fully lock moisture, prevent water loss, have efficient moisture-retention, so as to keep skin
Skin is silky moist smooth, and beta glucan can promote the multiplication of fibroblast (chrotoplast) and skin histology matrix (such as collagen egg
In vain, elastin laminin, proteoglycans and other components) synthesis, increase skin elasticity, it is soft delicate, so as to improve facial mask liquid
Performance.
A kind of preparation method of moisturizing and skin rejuvenating facial mask of the present invention, is mainly realized by the following technical programs
's：Comprise the following steps：1) glycerine, butanediol, propylene glycol and methyl hydroxybenzoate are taken, is added to the water, is heated to 80-85 DEG C, is stirred
It mixes to being completely dissolved, and keeps 5-10min, obtain mixture 1；2) by mixture 1 obtained by step 1), under vacuum, stirring
10-15min in whipping process, adds in xanthans and trehalose, it is made to be uniformly dispersed, obtains mixture 2；3) take rilanit special,
Polysorbate and saualane, mixing, are preheated to 80-85 DEG C, under vacuum, are added in mixture 2 obtained by step 2),
25-35min is stirred under vacuum, 80-85 DEG C of whipping temp obtains mixture 3；4) mixture 3 obtained by step 3) is cooled to 40-45
DEG C, add in abyssal fishes collagen peptide, Sodium Hyaluronate, Phenoxyethanol, beta glucan, grape seed extract, aloe extraction
Object and dipotassium glycyrrhizinate are stirred under vacuum, and make its dissolving complete, filtering obtains product.
The facial mask preparation method of the present invention is simple, and technological process is short, and operation temperature is low, mild condition, to equipment without spy
Different requirement, production efficiency are high, it is easy to accomplish industrialization；In the preparation process, the active ingredient in raw material is thoroughly swashed
It lives and has obtained sufficient reservation, gained facial mask promotes absorption of the skin to moisture content, is conducive to skin long-time moisturizing, improves
The moisturizing of facial mask liquid, moisturizing and the effect of slow down aging.
As a kind of preferred embodiment, in the step 2), the mixing speed in whipping process is 140-150r/
min.Raw material is kept stirring in emulsion process, and mixing speed is generally 140-150r/min, this that raw material is stirred mildly, stirs
It mixes uniformly, raw material local deposits will not be made, cause to mix non-uniform phenomenon, the active ingredient of raw material itself will not be destroyed,
Fully ensure that raw material is uniformly mixed according to itself original ingredient.
As a kind of preferred embodiment, the step 2) carries out in pot is emulsified, the vacuum under vacuum condition
It spends for 0.12-0.15MPa.Vacuum stirring can make mixing, scattered, homogeneous and emulsifying effectiveness more preferably, meanwhile, in whipping process
Prevent the generation of bubble, the high bubble-free of particles rank of high speed shear can obtain the facial mask liquid product of skin sense exquisiteness, more
Easily it is absorbed by the skin；In addition, material can be carried out to vacuumize bubble by being stirred under vacuum, it is possible to prevente effectively from the later stage is due to bubble
The problem of influence product quality and stability.
As a kind of preferred embodiment, in the step 3) and the step 4), the vacuum degree of vacuum stirring is
0.09-0.12MPa.The present invention can select different vacuum degrees according to product demand, and it is to ensure that the present invention, which is stirred under vacuum,
Functional component is not destroyed, also, vacuum stirring makes the bubble-free that is uniformly dispersed.
As a kind of preferred embodiment, in the step 4), the mesh number of strainer is 400-600 mesh during filtering.Filtering
Operation is carried out compared under low temperature, and is discharged using 400 mesh screens, and index of correlation detection is carried out to the material after discharging.
Compared with prior art, the beneficial effects of the invention are as follows：The present invention coordinates Portugal using abyssal fishes collagen peptide
Facial mask obtained by grape seed extract, beta glucan and rilanit special has low irritability, pollution-free, non-stimulated and without infecting both domestic animals and human
The advantages that disease pathogen, not only improves the economic value of corresponding fish but also can reduce environmental pollution；It is carried in trehalose, aloe
Under the booster action for taking object and Sodium Hyaluronate, absorption of the skin to moisture content is promoted, is conducive to skin long-time moisturizing, is improved
The moisturizing of facial mask liquid, moisturizing and the effect of slow down aging；The present invention reduces stimulation of the facial mask liquid to skin without using ethyl alcohol
Property, it is easily absorbed by mask carriers, easy to use, facial mask applies is playing the role of moisturizing on the face；The preparation side of the present invention
Method is simple, and technological process is short, and operation temperature is low, mild condition, does not have special requirement to equipment, the active ingredient quilt in raw material
It thoroughly activates and has obtained sufficient reservation, production efficiency is high, it is easy to accomplish industrialization.
Specific embodiment
Technical scheme is clearly and completely described below in conjunction with specific embodiments of the present invention, is shown
So, described embodiment is only the part of the embodiment of the present invention, instead of all the embodiments.Based in the present invention
Embodiment, those of ordinary skill in the art's all other embodiments obtained without creative efforts, all
Belong to the scope of protection of the invention.
A kind of moisturizing and skin rejuvenating facial mask includes the raw material of following weight percentage：Glycerine 3-10%, butanediol 1.5-
4.5%, deep-sea fish collagen peptide 1-4%, trehalose 3-8%, saualane 0.05-2%, Sodium Hyaluronate 0.15-2%, third
Glycol 1-5%, xanthans 0.02-0.35%, rilanit special 0.02-0.45%, polysorbate 0.02-2%, Phenoxyethanol
0.01-1%, methyl hydroxybenzoate 0.01-0.5%, beta glucan 0.1-2%, grape seed extract 0.01-0.5%, aloe extraction
Object 0.01-3%, dipotassium glycyrrhizinate 0.01-1%, surplus are deionized water.
Preferably, the raw material of following weight percentage is included：Glycerine 4-8%, butanediol 2-4%, deep-sea fish collagen egg
White peptide 2-3.8%, trehalose 5-7%, saualane 0.5-1.5%, Sodium Hyaluronate 0.2-1.5%, propylene glycol 1.5-3%, it is yellow
Virgin rubber 0.05-0.25%, rilanit special 0.05-0.25%, polysorbate 0.05-0.15%, Phenoxyethanol 0.05-
0.9%, methyl hydroxybenzoate 0.03-0.3%, beta glucan 0.1-2%, grape seed extract 0.015-0.15%, aloe extraction
Object 0.05-2%, dipotassium glycyrrhizinate 0.01-0.5%, surplus are deionized water.
It is further preferred that include the raw material of following weight percentage：Glycerine 5%, butanediol 3.5%, deep-sea fish glue
Former protein peptides 3.5%, trehalose 6%, saualane 0.75%, Sodium Hyaluronate 0.45%, propylene glycol 2.5%, xanthans
0.13%, rilanit special 0.15%, polysorbate 0.1%, Phenoxyethanol 0.8%, methyl hydroxybenzoate 0.2%, β-Portugal gathers
Sugared 0.1-2%, grape seed extract 0.015-0.15%, aloe extract 0.1-1%, dipotassium glycyrrhizinate 0.01-0.2% are remaining
It measures as deionized water.
Specifically, the aloe extract is that butt aloe polysaccharide content is more than 800ppm, in the grape seed extract
Procyanidin content is more than 90%.
Further, the molecular weight of the deep-sea fish collagen peptide is 200-1500Da, yeast purity in beta glucan
For 70-80%.
A kind of preparation method of moisturizing and skin rejuvenating facial mask, comprises the following steps：1) glycerine, butanediol, propylene glycol and Ni Bo are taken
Tortoise beetle ester, is added to the water, and is heated to 80-85 DEG C, and stirring keeps 5-10min to being completely dissolved, and obtains mixture 1；2) by step
1) gained mixture 1 under vacuum, stirs 10-15min, in whipping process, adds in xanthans and trehalose, makes its point
It dissipates uniformly, obtains mixture 2；3) rilanit special, polysorbate and saualane are taken, mixes, 80-85 DEG C is preheated to, in vacuum
Under the conditions of, it is added in mixture 2 obtained by step 2), is stirred under vacuum 25-35min, 80-85 DEG C of whipping temp obtains mixture 3；
4) mixture 3 obtained by step 3) is cooled to 40-45 DEG C, adds in abyssal fishes collagen peptide, Sodium Hyaluronate, benzene oxygen second
Alcohol, beta glucan, grape seed extract, aloe extract and dipotassium glycyrrhizinate are stirred under vacuum, and make its dissolving complete, filtering obtains
Product.
Preferably, in the step 2), the mixing speed in whipping process is 140-150r/min.
It is further preferred that the step 2) carries out in pot is emulsified, the vacuum degree under vacuum condition is 0.12-
0.15MPa。
Specifically, in the step 3) and the step 4), the vacuum degree of vacuum stirring is 0.09-0.12MPa.
Further, in the step 4), the mesh number of strainer is 400-600 mesh during filtering.
Embodiment one
A kind of preparation method of moisturizing and skin rejuvenating facial mask, comprises the following steps：
1) following raw material is weighed according to the proportioning shown in the 3rd column data in table 1：
Glycerine, butanediol, deep-sea fish collagen peptide, trehalose, saualane, Sodium Hyaluronate, propylene glycol, xanthans,
It is rilanit special, polysorbate, Phenoxyethanol, methyl hydroxybenzoate, beta glucan, grape seed extract, aloe extract, sweet
Oxalic acid dipotassium and deionized water；
2) glycerine, butanediol, propylene glycol and methyl hydroxybenzoate are taken, is added to the water, is heated to 80 DEG C, is stirred to completely molten
Solution, and 10min is kept, obtain mixture 1；
3) by mixture 1 obtained by step 2), under vacuum, stir 10min, in whipping process, add in xanthans and
Trehalose makes it be uniformly dispersed, and obtains mixture 2；
4) rilanit special, polysorbate and saualane are taken, is mixed, is preheated to 80 DEG C, under vacuum, is added to
In mixture 2 obtained by step 3), 25min is stirred under vacuum, 80 DEG C of whipping temp obtains mixture 3；
5) mixture 3 obtained by step 4) is cooled to 40 DEG C, adds in abyssal fishes collagen peptide, Sodium Hyaluronate, benzene
Oxyethanol, beta glucan, grape seed extract, aloe extract and dipotassium glycyrrhizinate are stirred under vacuum, and make its dissolving complete, mistake
Filter, obtains product.
Embodiment two
A kind of preparation method of moisturizing and skin rejuvenating facial mask, comprises the following steps：
1) following raw material is weighed according to the proportioning shown in the 4th column data in table 1：
Glycerine, butanediol, deep-sea fish collagen peptide, trehalose, saualane, Sodium Hyaluronate, propylene glycol, xanthans,
It is rilanit special, polysorbate, Phenoxyethanol, methyl hydroxybenzoate, beta glucan, grape seed extract, aloe extract, sweet
Oxalic acid dipotassium and deionized water；
2) glycerine, butanediol, propylene glycol and methyl hydroxybenzoate are taken, is added to the water, is heated to 85 DEG C, is stirred to completely molten
Solution, and 5min is kept, obtain mixture 1；
3) by mixture 1 obtained by step 2), under vacuum, stir 15min, in whipping process, add in xanthans and
Trehalose makes it be uniformly dispersed, and obtains mixture 2；
4) rilanit special, polysorbate and saualane are taken, is mixed, is preheated to 85 DEG C, under vacuum, is added to
In mixture 2 obtained by step 3), 35min is stirred under vacuum, 85 DEG C of whipping temp obtains mixture 3；
5) mixture 3 obtained by step 4) is cooled to 45 DEG C, adds in abyssal fishes collagen peptide, Sodium Hyaluronate, benzene
Oxyethanol, beta glucan, grape seed extract, aloe extract and dipotassium glycyrrhizinate are stirred under vacuum, and make its dissolving complete, mistake
Filter, obtains product.
Embodiment three
A kind of preparation method of moisturizing and skin rejuvenating facial mask, comprises the following steps：
1) following raw material is weighed according to the proportioning shown in the 5th column data in table 1：
Glycerine, butanediol, deep-sea fish collagen peptide, trehalose, saualane, Sodium Hyaluronate, propylene glycol, xanthans,
It is rilanit special, polysorbate, Phenoxyethanol, methyl hydroxybenzoate, beta glucan, grape seed extract, aloe extract, sweet
Oxalic acid dipotassium and deionized water；
2) glycerine, butanediol, propylene glycol and methyl hydroxybenzoate are taken, is added to the water, is heated to 82 DEG C, is stirred to completely molten
Solution, and 7min is kept, obtain mixture 1；
3) by mixture 1 obtained by step 2), under vacuum, stir 12min, in whipping process, add in xanthans and
Trehalose makes it be uniformly dispersed, and obtains mixture 2；
4) rilanit special, polysorbate and saualane are taken, is mixed, is preheated to 82 DEG C, under vacuum, is added to
In mixture 2 obtained by step 3), 30min is stirred under vacuum, 83 DEG C of whipping temp obtains mixture 3；
5) mixture 3 obtained by step 4) is cooled to 42 DEG C, adds in abyssal fishes collagen peptide, Sodium Hyaluronate, benzene
Oxyethanol, beta glucan, grape seed extract, aloe extract and dipotassium glycyrrhizinate are stirred under vacuum, and make its dissolving complete, mistake
Filter, obtains product.
Example IV
A kind of preparation method of moisturizing and skin rejuvenating facial mask, comprises the following steps：
1) following raw material is weighed according to the proportioning shown in the 6th column data in table 1：
Glycerine, butanediol, deep-sea fish collagen peptide, trehalose, saualane, Sodium Hyaluronate, propylene glycol, xanthans,
It is rilanit special, polysorbate, Phenoxyethanol, methyl hydroxybenzoate, beta glucan, grape seed extract, aloe extract, sweet
Oxalic acid dipotassium and deionized water；
2) glycerine, butanediol, propylene glycol and methyl hydroxybenzoate are taken, is added to the water, is heated to 81 DEG C, is stirred to completely molten
Solution, and 9min is kept, obtain mixture 1；
3) by mixture 1 obtained by step 2), under vacuum, stir 14min, in whipping process, add in xanthans and
Trehalose makes it be uniformly dispersed, and obtains mixture 2；
4) rilanit special, polysorbate and saualane are taken, is mixed, is preheated to 84 DEG C, under vacuum, is added to
In mixture 2 obtained by step 3), 32min is stirred under vacuum, 83 DEG C of whipping temp obtains mixture 3；
5) mixture 3 obtained by step 4) is cooled to 41 DEG C, adds in abyssal fishes collagen peptide, Sodium Hyaluronate, benzene
Oxyethanol, beta glucan, grape seed extract, aloe extract and dipotassium glycyrrhizinate are stirred under vacuum, and make its dissolving complete, mistake
Filter, obtains product.
Embodiment five
A kind of preparation method of moisturizing and skin rejuvenating facial mask, comprises the following steps：
1) following raw material is weighed according to the proportioning shown in the 7th column data in table 1：
Glycerine, butanediol, deep-sea fish collagen peptide, trehalose, saualane, Sodium Hyaluronate, propylene glycol, xanthans,
It is rilanit special, polysorbate, Phenoxyethanol, methyl hydroxybenzoate, beta glucan, grape seed extract, aloe extract, sweet
Oxalic acid dipotassium and deionized water；
2) glycerine, butanediol, propylene glycol and methyl hydroxybenzoate are taken, is added to the water, is heated to 84 DEG C, is stirred to completely molten
Solution, and 6min is kept, obtain mixture 1；
3) by mixture 1 obtained by step 2), under vacuum, stir 11min, in whipping process, add in xanthans and
Trehalose makes it be uniformly dispersed, and obtains mixture 2；
4) rilanit special, polysorbate and saualane are taken, is mixed, is preheated to 81 DEG C, under vacuum, is added to
In mixture 2 obtained by step 3), 28min is stirred under vacuum, 82 DEG C of whipping temp obtains mixture 3；
5) mixture 3 obtained by step 4) is cooled to 44 DEG C, adds in abyssal fishes collagen peptide, Sodium Hyaluronate, benzene
Oxyethanol, beta glucan, grape seed extract, aloe extract and dipotassium glycyrrhizinate are stirred under vacuum, and make its dissolving complete, mistake
Filter, obtains product.
Embodiment six
Raw material is weighed according to the proportioning shown in the 8th column data in table 1, and it is tender according to the method preparation moisturizing of embodiment one
Skin facial mask.
Embodiment seven
Raw material is weighed according to the proportioning shown in the 9th column data in table 1, and it is tender according to the method preparation moisturizing of embodiment two
Skin facial mask.
Embodiment eight
Raw material is weighed according to the proportioning shown in the tenth column data in table 1, and it is tender according to the method preparation moisturizing of embodiment three
Skin facial mask.
Embodiment nine
Raw material is weighed according to the proportioning shown in the 11st column data in table 1, and moisturizing is prepared according to the method for example IV
Skin rejuvenating facial mask.
Facial mask and existing commercially available both of which prepared by the method for the embodiment of the present invention one to embodiment nine contains
The facial mask of polypeptide carries out performance test experiments respectively, including replenishing water and preserving moisture performance measurement experiment, removes DPPH effects in fact
The effect experiment of superoxide anion is tested and removes, related experiment rolls out version with reference to daily chemical industry the 3rd phase the 41st in 2011
Write by Yan Mingyan etc. wall pollack fishskin collagen polypeptide composition washing facial mask development (i.e. daily chemical industry, 2011,41
(3):Test method in 194-199) carries out, and experimental result is as shown in table 2 and table 3.
As can be seen from Table 2, facial mask of the invention shows apparent advantage when testing 12h, and moisturizing rate is apparent
More than existing commercially available facial mask, that is, control sample one and control sample two containing polypeptide, experimental period gradually extends to 72h by 12h
When, the moisturizing rate of facial mask of the invention is continuously decreasing, meanwhile, existing commercially available facial mask, that is, control sample one containing polypeptide and right
Two moisturizing rate is also continuously decreasing in the same old way；But under the identical experiment time, the moisturizing rate of facial mask of the invention is above existing
Commercially available facial mask, that is, control sample one containing polypeptide and control sample two moisturizing rate.Therefore, facial mask of the invention has apparent
Replenishing water and preserving moisture advantage.
The different facial mask water conservation performance of keeping humidity test result contrast tables of table 2
3 different faces membrane removal DPPH the performance test results contrast tables of table
As can be seen from Table 3, facial mask of the invention, can to the clearance rate of DPPH when removing DPPH effect experiments
Up to 83.23%, all facial masks of the present invention are all higher than the clearance rate of DPPH the existing commercially available facial mask containing polypeptide i.e. pair
In the same old way one and control sample two to the clearance rate of DPPH；Therefore, compared with control sample one and control sample two, facial mask table of the invention
Reveal preferable DPPH elimination effects.Facial mask liquid of the present invention contains small-molecular-weight collagen peptide, grape seed extract, aloe extraction
The ingredients such as object, DPPH are also explained from principle and superoxide anion clearance rate is higher the effect of being respectively provided with high-efficiency antioxidant
Experimental result.In addition, the present invention facial mask remove superoxide anion effect experiment when, to the clearance rate of superoxide anion
Between 15.03-16.90%, this is far longer than 9.90% and 6.30%, i.e. all facial masks of the present invention are to superoxide anion
Clearance rate is apparently higher than the existing commercially available removing of facial mask, that is, control sample one and control sample two to superoxide anion containing polypeptide
Rate；Therefore, compared with control sample one and control sample two, facial mask of the invention shows preferable superoxide anion elimination effect.
Compared with prior art, the beneficial effects of the invention are as follows：The present invention coordinates Portugal using abyssal fishes collagen peptide
Facial mask obtained by grape seed extract, beta glucan and rilanit special has low irritability, pollution-free, non-stimulated and without infecting both domestic animals and human
The advantages that disease pathogen, not only improves the economic value of corresponding fish but also can reduce environmental pollution；It is carried in trehalose, aloe
Under the booster action for taking object and Sodium Hyaluronate, absorption of the skin to moisture content is promoted, is conducive to skin long-time moisturizing, is improved
The moisturizing of facial mask liquid, moisturizing and the effect of slow down aging；The present invention reduces stimulation of the facial mask liquid to skin without using ethyl alcohol
Property, it is easily absorbed by mask carriers, easy to use, facial mask applies is playing the role of moisturizing on the face；The preparation side of the present invention
Method is simple, and technological process is short, and operation temperature is low, mild condition, does not have special requirement to equipment, the active ingredient quilt in raw material
It thoroughly activates and has obtained sufficient reservation, production efficiency is high, it is easy to accomplish industrialization.
The foregoing is merely illustrative of the preferred embodiments of the present invention, is not intended to limit the invention, all essences in the present invention
With within principle, any modifications, equivalent replacements and improvements are made should all be included in the protection scope of the present invention god.
Claims (10)
1. a kind of moisturizing and skin rejuvenating facial mask, it is characterised in that：Include the raw material of following weight percentage：
Glycerine 3-10%, butanediol 1.5-4.5%, deep-sea fish collagen peptide 1-4%, trehalose 3-8%, saualane 0.05-
2%, Sodium Hyaluronate 0.15-2%, propylene glycol 1-5%, xanthans 0.02-0.35%, rilanit special 0.02-0.45% gather
Sorbitol ester 0.02-2%, Phenoxyethanol 0.01-1%, methyl hydroxybenzoate 0.01-0.5%, beta glucan 0.1-2%, grape pip
Extract 0.01-0.5%, aloe extract 0.01-3%, dipotassium glycyrrhizinate 0.01-1%, surplus are deionized water.
2. moisturizing and skin rejuvenating facial mask according to claim 1, it is characterised in that：Include the raw material of following weight percentage：
Glycerine 4-8%, butanediol 2-4%, deep-sea fish collagen peptide 2-3.8%, trehalose 5-7%, saualane 0.5-
1.5%, Sodium Hyaluronate 0.2-1.5%, propylene glycol 1.5-3%, xanthans 0.05-0.25%, rilanit special 0.05-
0.25%, polysorbate 0.05-0.15%, Phenoxyethanol 0.05-0.9%, methyl hydroxybenzoate 0.03-0.3%, beta glucan
0.1-2%, grape seed extract 0.015-0.15%, aloe extract 0.05-2%, dipotassium glycyrrhizinate 0.01-0.5%, surplus
For deionized water.
3. moisturizing and skin rejuvenating facial mask according to claim 2, it is characterised in that：Include the raw material of following weight percentage：
Glycerine 5%, butanediol 3.5%, deep-sea fish collagen peptide 3.5%, trehalose 6%, saualane 0.75%, hyaluronic acid
Sodium 0.45%, propylene glycol 2.5%, xanthans 0.13%, rilanit special 0.15%, polysorbate 0.1%, Phenoxyethanol
0.8%, methyl hydroxybenzoate 0.2%, beta glucan 0.1-2%, grape seed extract 0.015-0.15%, aloe extract 0.1-
1%, dipotassium glycyrrhizinate 0.01-0.2%, surplus is deionized water.
4. moisturizing and skin rejuvenating facial mask according to claim 1, it is characterised in that：
The butt aloe polysaccharide content of the aloe extract is more than 800ppm, the Proanthocyanidin from Grape-seed Extracts
More than 90%.
5. moisturizing and skin rejuvenating facial mask according to claim 1, it is characterised in that：
The molecular weight of the deep-sea fish collagen peptide is 200-1500Da, and the purity of yeast is 70-80% in beta glucan.
6. the preparation method of the moisturizing and skin rejuvenating facial mask according to any one in claim 1-5, it is characterised in that：Including with
Lower step：
1) glycerine, butanediol, propylene glycol and methyl hydroxybenzoate are taken, is added to the water, is heated to 80-85 DEG C, stirring to being completely dissolved,
And 5-10min is kept, obtain mixture 1；
2) by mixture 1 obtained by step 1), under vacuum, stir 10-15min, in whipping process, add in xanthans and sea
Algae sugar, makes it be uniformly dispersed, obtains mixture 2；
3) rilanit special, polysorbate and saualane are taken, is mixed, is preheated to 80-85 DEG C, under vacuum, is added to
In mixture 2 obtained by step 2), 25-35min is stirred under vacuum, 80-85 DEG C of whipping temp obtains mixture 3；
4) mixture 3 obtained by step 3) is cooled to 40-45 DEG C, adds in abyssal fishes collagen peptide, Sodium Hyaluronate, benzene oxygen
Ethyl alcohol, beta glucan, grape seed extract, aloe extract and dipotassium glycyrrhizinate are stirred under vacuum, and make its dissolving complete, filtering,
Obtain product.
7. the preparation method of moisturizing and skin rejuvenating facial mask according to claim 6, it is characterised in that：
In the step 2), the mixing speed in whipping process is 140-150r/min.
8. the preparation method of moisturizing and skin rejuvenating facial mask according to claim 6, it is characterised in that：
The step 2) carries out in pot is emulsified, and the vacuum degree under vacuum condition is 0.12-0.15MPa.
9. the preparation method of moisturizing and skin rejuvenating facial mask according to claim 6, it is characterised in that：
In the step 3) and the step 4), the vacuum degree of vacuum stirring is 0.09-0.12MPa.
10. the preparation method of moisturizing and skin rejuvenating facial mask according to claim 6, it is characterised in that：
In the step 4), sieve mesh number during filtering is 400-600 mesh.
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| CN108420757A (en) * | 2018-06-02 | 2018-08-21 | 杭州兰茜化妆品有限公司 | A kind of moisture retention water and its preparation process |
| CN108815018A (en) * | 2018-05-28 | 2018-11-16 | 黑龙江力海鑫生物科技股份有限公司 | A kind of castor rat-tail muscle extracts the facial mask liquid and preparation method thereof of collagen peptide |
| CN109044869A (en) * | 2018-10-10 | 2018-12-21 | 广州雷诺生物科技有限公司 | A kind of tender skin moisturizing moisture lock mask |
| CN109044946A (en) * | 2018-09-27 | 2018-12-21 | 张言聚 | A kind of whitening and moisturizing facial mask liquid and its preparation process |
| CN109223611A (en) * | 2018-11-14 | 2019-01-18 | 长沙浩然医疗科技有限公司 | One kind regrowing young state facial mask of wake-up and preparation method thereof for active cell |
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| CN109568151A (en) * | 2019-01-14 | 2019-04-05 | 恒天量子（厦门）科技有限公司 | A kind of Essence skin care moisture saver mask and preparation method thereof containing small-molecular peptides |
| CN110559240A (en) * | 2018-06-05 | 2019-12-13 | 冯松平 | whitening and anti-aging mask and preparation method thereof |
| CN111773170A (en) * | 2020-08-03 | 2020-10-16 | 广州虹美生物科技有限公司 | Facial mask patch added with grease and preparation method |
| CN112336668A (en) * | 2019-08-06 | 2021-02-09 | 中国科学院烟台海岸带研究所 | Deep sea fish collagen peptide seaweed rejuvenating facial mask and preparation method thereof |
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| CN108815018A (en) * | 2018-05-28 | 2018-11-16 | 黑龙江力海鑫生物科技股份有限公司 | A kind of castor rat-tail muscle extracts the facial mask liquid and preparation method thereof of collagen peptide |
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| CN110559240A (en) * | 2018-06-05 | 2019-12-13 | 冯松平 | whitening and anti-aging mask and preparation method thereof |
| CN109044946A (en) * | 2018-09-27 | 2018-12-21 | 张言聚 | A kind of whitening and moisturizing facial mask liquid and its preparation process |
| CN109044869A (en) * | 2018-10-10 | 2018-12-21 | 广州雷诺生物科技有限公司 | A kind of tender skin moisturizing moisture lock mask |
| CN109223611A (en) * | 2018-11-14 | 2019-01-18 | 长沙浩然医疗科技有限公司 | One kind regrowing young state facial mask of wake-up and preparation method thereof for active cell |
| CN109394592A (en) * | 2018-11-22 | 2019-03-01 | 医美生物科技(上海)有限公司 | A kind of multiple-effect flesh bottom water of replenishing water and preserving moisture oil-control |
| CN109568151A (en) * | 2019-01-14 | 2019-04-05 | 恒天量子（厦门）科技有限公司 | A kind of Essence skin care moisture saver mask and preparation method thereof containing small-molecular peptides |
| CN112336668A (en) * | 2019-08-06 | 2021-02-09 | 中国科学院烟台海岸带研究所 | Deep sea fish collagen peptide seaweed rejuvenating facial mask and preparation method thereof |
| CN111773170A (en) * | 2020-08-03 | 2020-10-16 | 广州虹美生物科技有限公司 | Facial mask patch added with grease and preparation method |
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| CN114010572A (en) * | 2021-11-17 | 2022-02-08 | 广东画景医药生物科技有限公司 | Marine collagen firming sleeping mask and preparation method thereof |
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