CN109223611A

CN109223611A - One kind regrowing young state facial mask of wake-up and preparation method thereof for active cell

Info

Publication number: CN109223611A
Application number: CN201811353299.3A
Authority: CN
Inventors: 不公告发明人
Original assignee: Changsha Hao Ran Medical Technology Co Ltd
Current assignee: Changsha Hao Ran Medical Technology Co Ltd
Priority date: 2018-11-14
Filing date: 2018-11-14
Publication date: 2019-01-18

Abstract

The invention discloses one kind to regrow the young state facial mask of wake-up for active cell, including following raw material: polyvinyl alcohol, plant hydrolyzed collagen, propylene glycol, sorbierite, Trenaxmine, reed fragrant plant oil, hydrolecithin, xanthan gum, Aloe Vera Gel, carbomer, trehalose sodium, dipotassium glycyrrhizinate, hydrolyze fibroin, arginine, platinum powder, beta glucan, resveratrol, Sodium Hyaluronate, Denatonium Benzoate, phytic acid, silver oxide, volcanic rock powder, diatomite, tetrasodium pyrophosphate, pure water, aliphatic acid polyethenoxy ether, alginate fibre, tea powder, ganoderma lucidum, 4-HBA methyl esters, vitamin E, antibacterial modified auxiliary agent, it is described that regrow the young state facial mask of wake-up for active cell be by preparing material A, prepare material B, prepare mixture, mixture sterilization and etc. obtain.Facial mask of the invention has excellent antibiotic effect.

Description

One kind regrowing young state facial mask of wake-up and preparation method thereof for active cell

[technical field]

The invention belongs to the preparation technical fields of facial mask, and in particular to one kind regrows wake-up youth for active cell State facial mask and preparation method thereof.

[background technique]

The facemask powder for making facial mask is mainly the combination of a variety of Chinese herbal medicine powders currently on the market, passes through the pharmacology of Chinese herbal medicine It acts on to adjust the blood circulation of skin, promotes the metabolism etc. of cell, achieve the effect that beauty and skin care.But often due to adopting The fineness of Chinese herbal medicine powder not enough and the traditional Chinese medicine ingredients strong containing some pharmacological properties, such as rhizoma typhonii, the flower bud of lily magnolia, pueraria lobata Chinese medicine at Point, irritation and undesirable various side effects can be brought to human skin.So that the antibacterial ability of skin reduces.It colonizes in simultaneously The acarid on application on human skin surface is also one of the factor of harmful to human skin.Superoxide dismutase is also known as SOD, is that one kind is derived from The active material of life entity can eliminate the harmful substance that organism generates in metabolic processes.Human body is constantly supplemented SOD has the special-effect of antibacterial.The function of facial mask on the market is mostly moisturizing and extra-nutrition at present, and SOD content is low, right It is little in the anti-microbial property power effect for improving skin.

Chinese patent literature " a kind of facial mask (application publication number: CN105012163A) with antibiotic effect " is specifically related to A kind of Shu Run water-setting facial mask and preparation method thereof without preservative, is made: plant hydrolyzed collagen of the raw material of following weight parts 5 grams of oil of 3 grams of protein 20 gram, 9 grams of small molecule water, 6 grams of Trenaxmine, Argireline or polypeptide, reed fragrant plant, by above-mentioned each raw material mixing preparation It is adsorbed on wet cotton paper after good.Although the facial mask has certain health-care efficacy, its anti-microbial property is bad, causes to make User's skin is vulnerable to bacterial infestation.

[summary of the invention]

The present invention provides a kind of regrow for active cell and wakes up young state facial mask and preparation method thereof, to solve to exist A kind of antibiotic property of the open facial mask of Chinese patent literature " facial mask (application publication number: CN105012163A) with antibiotic effect " The insufficient problem of energy.

In order to solve the above technical problems, the invention adopts the following technical scheme:

One kind regrowing the young state facial mask of wake-up, including following raw material for active cell: polyvinyl alcohol, plant hydrolyzed Collagen, propylene glycol, sorbierite, Trenaxmine, reed fragrant plant oil, hydrolecithin, xanthan gum, Aloe Vera Gel, carbomer, trehalose Sodium, dipotassium glycyrrhizinate, hydrolysis fibroin, arginine, platinum powder, beta glucan, resveratrol, Sodium Hyaluronate, benzene first ground that Ammonium, phytic acid, silver oxide, volcanic rock powder, diatomite, tetrasodium pyrophosphate, pure water, aliphatic acid polyethenoxy ether, seaweed Fiber, tea powder, ganoderma lucidum, 4-HBA methyl esters, vitamin E, antibacterial modified auxiliary agent；

Antibacterial modified auxiliary agent is as unit of parts by weight, including following raw material: 10-20 parts of chitin fiber, bamboo fibre 4-8 Part, 3-9 parts of polyvinylpyrrolidone, 8-16 parts of deionized water, 2-6 parts of sodium chloride, 1-4 parts of defoaming agent, 3-6 parts of aluminum nitrate, oxygen Change zinc 2-5 parts, 1-4 parts of diammonium hydrogen phosphate；

It the polyvinyl alcohol, alginate fibre, tea powder, ganoderma lucidum, 4-HBA methyl esters, vitamin E and antibacterial modified helps The weight ratio of agent is (30-40): (5-15): (4-8): (3-9): (2-6): (1-5): (1-2).

Further, the polyvinyl alcohol, alginate fibre, tea powder, ganoderma lucidum, 4-HBA methyl esters, vitamin E and anti- The weight ratio of bacterium modified additive is 36.9:11.4:5.4:6.3:4.7:3.8:1.6.

Further, as unit of parts by weight, including following raw material: 30-40 parts of polyvinyl alcohol, plant hydrolyzed collagen 5-15 parts, 2-5 parts of propylene glycol, 1-5 parts of sorbierite, 3-6 parts of Trenaxmine, 2-5 parts of reed fragrant plant oil, 1-4 parts of hydrolecithin, xanthan gum 3-6 parts, 2-5 parts of Aloe Vera Gel, 1-5 parts of carbomer, 4-6 parts of trehalose sodium, 3-5 parts of dipotassium glycyrrhizinate, hydrolysis fibroin 1-5 Part, -6 parts of arginase 12,1-4 parts of platinum powder, 1-3 parts of beta glucan, 2-6 parts of resveratrol, 1-4 parts of Sodium Hyaluronate, benzene first ground that 3-5 parts of ammonium, 2-5 parts of phytic acid, 1-3 parts of silver oxide, 2-4 parts of volcanic rock powder, 3-6 parts of diatomite, tetrasodium pyrophosphate 1-4 Part, 15-35 parts of pure water, 2-5 parts of aliphatic acid polyethenoxy ether, 5-15 parts of alginate fibre, 4-8 parts of tea powder, 3-9 parts of ganoderma lucidum, 4- hydroxyl It is 2-6 parts of yl benzoic acid methyl esters, 1-5 parts of vitamin E, auxiliary agent 1-2 parts antibacterial modified.

Further, antibacterial modified auxiliary agent is prepared by following technique: by chitin fiber, bamboo fibre, polyethylene pyrrole Pyrrolidone and deionized water are uniformly mixed, and after grinding 20-40min, are warming up to 80-90 DEG C, are kept the temperature 20-30min, chlorine is then added Change sodium and defoaming agent stirring, continue 80-90 DEG C of heating, keep the temperature 5-15min, aluminum nitrate is then added and zinc oxide is uniformly mixed, Heating water bath 1-2h is added diammonium hydrogen phosphate and is uniformly mixed, is then aged, filtration washing after being cooled to room temperature, dry, after calcining It is cooled to room temperature to obtain antibacterial modified auxiliary agent.

A kind of preparation method regrowing the young state facial mask of wake-up for active cell proposed by the present invention, including it is following Step:

S1, polyvinyl alcohol, sorbierite, hydrolecithin, xanthan gum, Aloe Vera Gel, carbomer and Sodium Hyaluronate are mixed Uniformly, it is warming up to 70-80 DEG C, keeps the temperature 5-15min, 20-49min is stirred in 350-650r/min revolving speed, is cooled to room temperature to obtain Material A；

S2, that volcanic rock powder and diatomite be ground to 110-130 mesh or more is spare, by plant hydrolyzed collagen, third Glycol, Trenaxmine, reed fragrant plant oil, trehalose sodium, dipotassium glycyrrhizinate, hydrolysis fibroin, arginine, platinum powder, beta glucan, white Chenopodiaceae Reed alcohol, Denatonium Benzoate, phytic acid, silver oxide, tetrasodium pyrophosphate, pure water, aliphatic acid polyethenoxy ether are uniformly mixed, and are risen Temperature keeps the temperature 10-30min to 40-60 DEG C, is subsequently added into volcanic rock powder and diatomite is uniformly mixed, be continuously heating to 80-90 DEG C, 30-50min is kept the temperature, 1-2h is stirred in 850-1050r/min revolving speed, is cooled to room temperature to obtain material B；

S3, by alginate fibre, tea powder, ganoderma lucidum, 4-HBA methyl esters, vitamin E, antibacterial modified auxiliary agent, material A and Material B is uniformly mixed, and is warming up to 40-60 DEG C, keeps the temperature 10-20min, stirs 20-40min in 1500-2500r/min revolving speed, cold But mixture is obtained to room temperature；

S4, S3 is obtained to the sterilizing of mixture 0.10-0.12MPa pressure above, disinfection 2-3h obtains being used to activate carefully Born of the same parents regrow the young state facial mask of wake-up.

The invention has the following advantages:

(1) it is called out by the data of embodiment 1-3 and comparative example 9 as it can be seen that applying embodiment 1-3 and being regrowed for active cell The anti-microbial property of youth of waking up state facial mask significantly improves；Simultaneously by the data of embodiment 1-3 as it can be seen that embodiment 1 is optimum embodiment.

(2) by embodiment 1 and the data of comparative example 1-8 as it can be seen that polyvinyl alcohol, alginate fibre, tea powder, ganoderma lucidum, 4- hydroxyl Methyl benzoate, vitamin E and antibacterial modified auxiliary agent are regrowed in the young state facial mask of wake-up for active cell in preparation and are risen Synergistic effect is arrived, collaboration improves the anti-microbial property for regrowing for active cell and waking up young state facial mask, this is: poly- second Enol, alginate fibre, tea powder, ganoderma lucidum, 4-HBA methyl esters, vitamin E and antibacterial modified auxiliary agent as reinforcement system, with Polyvinyl alcohol is as film forming supplementary material, wherein the chief value of the alginate fibre added is algae component, in limit with The contact of skin will not allow people to have the reaction of allergy, and can actively discharge the vitamin and mineral of seaweed, this minerals packet Calcic and magnesium etc., vitamin includes vitamin A, C, E etc., in the research of cosmetics, shows the mineral that algae component has Matter and vitamin A, C, E have the properties such as natural benefit, degradable absorbability, biocompatibility to skin and hair.Spirit Sesame is able to maintain that immunity of organism balances as Chinese medicine, and skin is made to obtain required amino acid and minerals and polysaccharide activity Ingredient alleviates the damage of keratinocyte oxidative stress, anti-epidermal cell aging.Made by alginate fibre and ganoderma lucidum collaboration With the porosity of alginate fibre can provide load site for the polypeptide in ganoderma lucidum, effectively increase the anti-oxidant of alginate fibre Performance, moreover it is possible to be able to suppress the aging of Skin Cell, the grease of dirt and secretion for skin adsorbs, and substantially increases The cleaning capacity of facial mask contains the tea polyphenols of a large amount of antioxidant effect in tea powder, cell ageing can be effectively relieved, and further mends The strong antioxygenic property of reinforcement system.4-HBA methyl esters not only meets safety and biocompatibility as preservative Requirement, and antiseptic property is good, delays the shelf-life of facial mask.Vitamin E can effectively improve the anti-of facial mask as antioxidant Oxidation susceptibility.Antibacterial modified auxiliary agent is equal by mixing chitin fiber, bamboo fibre, polyvinylpyrrolidone and deionized water It is even, after grinding, heat up, heat preservation, then be added sodium chloride and defoaming agent stirring, continue to heat up, keep the temperature, then be added aluminum nitrate and Zinc oxide is uniformly mixed, heating water bath, and diammonium hydrogen phosphate is added after being cooled to room temperature and is uniformly mixed, is then aged, filtration washing, It is dry, it is cooled to room temperature to obtain after calcining, the hydroxyl of chitin fiber and bamboo fibre surface, and the ammonia after hydrolysis in solution Base, amino is by inhibiting the activity of bacterium surface respiratory enzyme in conjunction with negative electron, to cause inactivation of bacteria, and in polyethylene pyrrole It is obtained under the cohesion of pyrrolidone, in reinforcement system, under the graft modification effect of silane coupling agent KH-560, surface Hydroxyl in conjunction with the unsaturated bond on polyacrylonitrile surface, finally impart the excellent anti-microbial property of the reinforcement system.The present invention Pass through control polyvinyl alcohol, alginate fibre, tea powder, ganoderma lucidum, 4-HBA methyl esters, vitamin E and antibacterial modified auxiliary agent Weight ratio is (30-40): (5-15): (4-8): (3-9): (2-6): (1-5): (1-2).It is with polyvinyl alcohol for main film forming matter Matter, by the way that using polyvinyl alcohol as main component, polyvinyl alcohol is film forming matter as major ingredient, and the porosity of alginate fibre is ganoderma lucidum Polypeptide and tea powder in tea polyphenols provide sufficient load space, while being 4-HBA methyl esters and vitamin E The gap of load is provided, and by utilizing alginate fibre, tea powder and the performance reinforcement of the anti-aging of the ganoderma lucidum anti-aging of facial mask Performance utilizes the anti-of the antiseptic property of 4-HBA methyl esters and the antioxygenic property of vitamin E and antibacterial modified auxiliary agent Bacterium effect, so that the facial mask shelf-life of the invention is longer, and anti-microbial property is more preferable.

[specific embodiment]

To facilitate a better understanding of the present invention, it is illustrated by the following examples, these examples belong to protection of the invention Range, but do not limit the scope of the invention.

In embodiment, the active cell that is used for regrows the young state facial mask of wake-up, as unit of parts by weight, packet Include following raw material: 30-40 parts of polyvinyl alcohol, 1-5 parts of sorbierite, passes collagen 5-15 parts plant hydrolyzed, 2-5 parts of propylene glycol Bright 3-6 parts of acid, 2-5 parts of reed fragrant plant oil, 1-4 parts of hydrolecithin, 3-6 parts of xanthan gum, 2-5 parts of Aloe Vera Gel, 1-5 parts of carbomer, sea 4-6 parts of algae sugar sodium, 3-5 parts of dipotassium glycyrrhizinate, hydrolysis fibroin 1-5 parts, -6 parts of arginase 12,1-4 parts of platinum powder, beta glucan 1-3 parts, 2-6 parts of resveratrol, 1-4 parts of Sodium Hyaluronate, 3-5 parts of Denatonium Benzoate, 2-5 parts of phytic acid, silver oxide 1-3 Part, 2-4 parts of volcanic rock powder, 3-6 parts of diatomite, 1-4 parts of tetrasodium pyrophosphate, 15-35 parts of pure water, aliphatic acid polyethenoxy ether 2- 5 parts, it is 5-15 parts of alginate fibre, 4-8 parts of tea powder, 3-9 parts of ganoderma lucidum, 2-6 parts of 4-HBA methyl esters, 1-5 parts of vitamin E, anti- 1-2 parts of bacterium modified additive.

The antibacterial modified auxiliary agent is prepared by following technique: by weight by 10-20 parts of chitin fibers, 4-8 Part bamboo fibre, 3-9 parts of polyvinylpyrrolidones and 8-16 parts of deionized waters are uniformly mixed, and after grinding 20-40min, are warming up to 80- 90 DEG C, 20-30min is kept the temperature, 2-6 parts of sodium chloride and 1-4 parts of defoaming agent stirrings are then added, continues 80-90 DEG C of heating, keeps the temperature 5- 15min, is then added 3-6 parts of aluminum nitrates and 2-5 parts of zinc oxide are uniformly mixed, and heating water bath 1-2h is added after being cooled to room temperature 1-4 parts of diammonium hydrogen phosphates are uniformly mixed, and are then aged, filtration washing, dry, are cooled to room temperature to obtain antibacterial modified help after calcining Agent.

Described regrows the preparation method for waking up young state facial mask for active cell, comprising the following steps:

Below by more specifically examples illustrate the present invention.

Embodiment 1

One kind regrowing the young state facial mask of wake-up for active cell, as unit of parts by weight, including following raw material: it is poly- 34.6 parts of vinyl alcohol, 9.8 parts of plant hydrolyzed collagen, 3.5 parts of propylene glycol, 3.2 parts of sorbierite, 4.6 parts of Trenaxmine, reed fragrant plant oil 3.2 parts, 2.6 parts of hydrolecithin, 4.7 parts of xanthan gum, 3.4 parts of Aloe Vera Gel, 2.7 parts of carbomer, 5.1 parts of trehalose sodium, Radix Glycyrrhizae 4.2 parts of sour dipotassium, hydrolysis 3.1 parts of fibroin, 4.2 parts of arginine, 2.4 parts of platinum powder, 2.2 parts of beta glucan, resveratrol 4.1 Part, 2.3 parts of Sodium Hyaluronate, 4.2 parts of Denatonium Benzoate, 3.6 parts of phytic acid, 2.2 parts of silver oxide, volcanic rock powder 3.1 Part, 4.7 parts of diatomite, 2.7 parts of tetrasodium pyrophosphate, 24.6 parts of pure water, 3.7 parts of aliphatic acid polyethenoxy ether, alginate fibre 9.8 Part, 5.7 parts of tea powder, 5.7 parts of ganoderma lucidum, 4.6 parts of 4-HBA methyl esters, 3.4 parts of vitamin E, 1.6 parts of antibacterial modified auxiliary agent.

The antibacterial modified auxiliary agent is prepared by following technique: by weight by 16 parts of chitin fibers, 6 parts of bamboo fibres Dimension, 5.8 parts of polyvinylpyrrolidones and 11.4 parts of deionized waters are uniformly mixed, and after grinding 32min, are warming up to 86 DEG C, heat preservation Then 27min is added 3.7 parts of sodium chloride and 2.6 parts of defoaming agent stirrings, continues 84 DEG C of heating, keep the temperature 9min, be then added 4.6 Part aluminum nitrate and 3.4 parts of zinc oxide are uniformly mixed, and it is mixed that 2.6 parts of diammonium hydrogen phosphates are added in heating water bath 1.6h after being cooled to room temperature It closes uniformly, is then aged, filtration washing, it is dry, it is cooled to room temperature to obtain antibacterial modified auxiliary agent after calcining.

S1, polyvinyl alcohol, sorbierite, hydrolecithin, xanthan gum, Aloe Vera Gel, carbomer and Sodium Hyaluronate are mixed Uniformly, 74 DEG C are warming up to, 12min is kept the temperature, 32min is stirred in 496r/min revolving speed, is cooled to room temperature to obtain material A；

S2, that volcanic rock powder and diatomite be ground to 120 mesh or more is spare, by plant hydrolyzed collagen, propylene glycol, Trenaxmine, reed fragrant plant oil, trehalose sodium, dipotassium glycyrrhizinate, hydrolysis fibroin, arginine, platinum powder, beta glucan, resveratrol, Denatonium Benzoate, phytic acid, silver oxide, tetrasodium pyrophosphate, pure water, aliphatic acid polyethenoxy ether are uniformly mixed, and are warming up to 50 DEG C, 20min is kept the temperature, volcanic rock powder is subsequently added into and diatomite is uniformly mixed, be continuously heating to 86 DEG C, keep the temperature 40min, in 950r/min revolving speed stirs 1.6h, is cooled to room temperature to obtain material B；

S3, by alginate fibre, tea powder, ganoderma lucidum, 4-HBA methyl esters, vitamin E, antibacterial modified auxiliary agent, material A and Material B is uniformly mixed, and is warming up to 5 DEG C, keeps the temperature 14min, is stirred 30min in 2000r/min revolving speed, is cooled to room temperature and is mixed Material；

S4, S3 is obtained mixture 0.11MPa pressure above sterilizing, disinfection 2-3h obtain being used for active cell again Growth wakes up young state facial mask.

Embodiment 2

One kind regrowing the young state facial mask of wake-up for active cell, as unit of parts by weight, including following raw material: it is poly- 30 parts of vinyl alcohol, 15 parts of plant hydrolyzed collagen, 2 parts of propylene glycol, 5 parts of sorbierite, 3 parts of Trenaxmine, 5 parts of reed fragrant plant oil, hydrogenation 1 part of lecithin, 6 parts of xanthan gum, 2 parts of Aloe Vera Gel, 5 parts of carbomer, 4 parts of trehalose sodium, 5 parts of dipotassium glycyrrhizinate, hydrolysis silk egg White 1 part, 6 parts of arginine, 1 part of platinum powder, 3 parts of beta glucan, 2 parts of resveratrol, 4 parts of Sodium Hyaluronate, 3 parts of Denatonium Benzoate, 5 parts of phytic acid, 1 part of silver oxide, 4 parts of volcanic rock powder, 3 parts of diatomite, 4 parts of tetrasodium pyrophosphate, 15 parts of pure water, fatty acid 5 parts of polyoxyethylene ether, 8 parts of tea powder, 3 parts of ganoderma lucidum, 6 parts of 4-HBA methyl esters, 1 part of vitamin E, resists 5 parts of alginate fibre 2 parts of bacterium modified additive.

The antibacterial modified auxiliary agent is prepared by following technique: by weight by 10 parts of chitin fibers, 8 parts of bamboo fibres Dimension, 3 parts of polyvinylpyrrolidones and 16 parts of deionized waters are uniformly mixed, and after grinding 20min, are warming up to 90 DEG C, are kept the temperature 20min, Then 6 parts of sodium chloride and 1 part of defoaming agent stirring are added, continues 90 DEG C of heating, keeps the temperature 5min, 6 parts of aluminum nitrates and 2 parts are then added Zinc oxide is uniformly mixed, heating water bath 2h, and 1 part of diammonium hydrogen phosphate is added after being cooled to room temperature and is uniformly mixed, is then aged, filters Washing, it is dry, it is cooled to room temperature to obtain antibacterial modified auxiliary agent after calcining.

S1, polyvinyl alcohol, sorbierite, hydrolecithin, xanthan gum, Aloe Vera Gel, carbomer and Sodium Hyaluronate are mixed Uniformly, 70 DEG C are warming up to, 15min is kept the temperature, 49min is stirred in 350r/min revolving speed, is cooled to room temperature to obtain material A；

S2, that volcanic rock powder and diatomite be ground to 110 mesh or more is spare, by plant hydrolyzed collagen, propylene glycol, Trenaxmine, reed fragrant plant oil, trehalose sodium, dipotassium glycyrrhizinate, hydrolysis fibroin, arginine, platinum powder, beta glucan, resveratrol, Denatonium Benzoate, phytic acid, silver oxide, tetrasodium pyrophosphate, pure water, aliphatic acid polyethenoxy ether are uniformly mixed, and are warming up to 60 DEG C, 10min is kept the temperature, volcanic rock powder is subsequently added into and diatomite is uniformly mixed, be continuously heating to 90 DEG C, keep the temperature 30min, in 1050r/min revolving speed stirs 1h, is cooled to room temperature to obtain material B；

S3, by alginate fibre, tea powder, ganoderma lucidum, 4-HBA methyl esters, vitamin E, antibacterial modified auxiliary agent, material A and Material B is uniformly mixed, and is warming up to 60 DEG C, keeps the temperature 10min, is stirred 20min in 2500r/min revolving speed, is cooled to room temperature and is mixed Close material；

S4, S3 is obtained to the sterilizing of mixture 0.10MPa pressure above, disinfection 3h obtain being used for active cell it is secondary again It is long to wake up young state facial mask.

Embodiment 3

One kind regrowing the young state facial mask of wake-up for active cell, as unit of parts by weight, including following raw material: it is poly- 40 parts of vinyl alcohol, 5 parts of plant hydrolyzed collagen, 5 parts of propylene glycol, 1 part of sorbierite, 6 parts of Trenaxmine, 2 parts of reed fragrant plant oil, hydrogenation ovum Phosphatidase 4 part, 3 parts of xanthan gum, 5 parts of Aloe Vera Gel, 1 part of carbomer, 6 parts of trehalose sodium, 3 parts of dipotassium glycyrrhizinate, hydrolysis fibroin 5 Part, arginase 12 part, 4 parts of platinum powder, 1 part of beta glucan, 6 parts of resveratrol, 1 part of Sodium Hyaluronate, 5 parts of Denatonium Benzoate, inositol Six 2 parts of phosphoric acid, 3 parts of silver oxide, 2 parts of volcanic rock powder, 6 parts of diatomite, 1 part of tetrasodium pyrophosphate, 35 parts of pure water, fatty acid polyoxy 2 parts of vinethene, 5 parts of alginate fibre, 8 parts of tea powder, 3 parts of ganoderma lucidum, 6 parts of 4-HBA methyl esters, 1 part of vitamin E, antibacterial change 2 parts of auxiliary agent of property.

The antibacterial modified auxiliary agent is prepared by following technique: by weight by 20 parts of chitin fibers, 4 parts of bamboo fibres Dimension, 9 parts of polyvinylpyrrolidones and 8 parts of deionized waters are uniformly mixed, and after grinding 40min, are warming up to 80 DEG C, are kept the temperature 30min, so 2 parts of sodium chloride and 4 parts of defoaming agent stirrings are added afterwards, continues 80 DEG C of heating, keeps the temperature 15min, 3 parts of aluminum nitrates and 5 parts are then added Zinc oxide is uniformly mixed, heating water bath 1h, and 4 parts of diammonium hydrogen phosphates are added after being cooled to room temperature and are uniformly mixed, are then aged, filter Washing, it is dry, it is cooled to room temperature to obtain antibacterial modified auxiliary agent after calcining.

S1, polyvinyl alcohol, sorbierite, hydrolecithin, xanthan gum, Aloe Vera Gel, carbomer and Sodium Hyaluronate are mixed Uniformly, 80 DEG C are warming up to, 5min is kept the temperature, 20min is stirred in 650r/min revolving speed, is cooled to room temperature to obtain material A；

S2, that volcanic rock powder and diatomite be ground to 130 mesh or more is spare, by plant hydrolyzed collagen, propylene glycol, Trenaxmine, reed fragrant plant oil, trehalose sodium, dipotassium glycyrrhizinate, hydrolysis fibroin, arginine, platinum powder, beta glucan, resveratrol, Denatonium Benzoate, phytic acid, silver oxide, tetrasodium pyrophosphate, pure water, aliphatic acid polyethenoxy ether are uniformly mixed, and are warming up to 40 DEG C, 30min is kept the temperature, volcanic rock powder is subsequently added into and diatomite is uniformly mixed, be continuously heating to 80 DEG C, keep the temperature 50min, in 850r/min revolving speed stirs 2h, is cooled to room temperature to obtain material B；

S3, by alginate fibre, tea powder, ganoderma lucidum, 4-HBA methyl esters, vitamin E, antibacterial modified auxiliary agent, material A and Material B is uniformly mixed, and is warming up to 40 DEG C, keeps the temperature 20min, is stirred 40min in 1500r/min revolving speed, is cooled to room temperature and is mixed Close material；

Comparative example 1

It is essentially identical with the preparation process of embodiment 1, it has only the difference is that preparation regrows wake-up for active cell Lack in the raw material of young state facial mask polyvinyl alcohol, alginate fibre, tea powder, ganoderma lucidum, 4-HBA methyl esters, vitamin E and Antibacterial modified auxiliary agent.

Comparative example 2

It is essentially identical with the preparation process of embodiment 1, it has only the difference is that preparation regrows wake-up for active cell Lack polyvinyl alcohol in the raw material of young state facial mask.

Comparative example 3

It is essentially identical with the preparation process of embodiment 1, it has only the difference is that preparation regrows wake-up for active cell Lack alginate fibre in the raw material of young state facial mask.

Comparative example 4

It is essentially identical with the preparation process of embodiment 1, it has only the difference is that preparation regrows wake-up for active cell Lack tea powder in the raw material of young state facial mask.

Comparative example 5

It is essentially identical with the preparation process of embodiment 1, it has only the difference is that preparation regrows wake-up for active cell Lack ganoderma lucidum in the raw material of young state facial mask.

Comparative example 6

It is essentially identical with the preparation process of embodiment 1, it has only the difference is that preparation regrows wake-up for active cell Lack 4-HBA methyl esters in the raw material of young state facial mask.

Comparative example 7

It is essentially identical with the preparation process of embodiment 1, it has only the difference is that preparation regrows wake-up for active cell Lack vitamin E in the raw material of young state facial mask.

Comparative example 8

It is essentially identical with the preparation process of embodiment 1, it has only the difference is that preparation regrows wake-up for active cell Lack antibacterial modified auxiliary agent in the raw material of young state facial mask.

Comparative example 9

Using Chinese patent literature " a kind of facial mask and preparation method thereof (Authorization Notice No.: CN105250203B) " embodiment The facial mask of the technique preparation of 1-3.

Comparative example 10

It is essentially identical with the preparation process of embodiment 1, it has only the difference is that preparation regrows wake-up for active cell Polyvinyl alcohol is 22 parts, 17 parts of alginate fibre, 3 parts of tea powder, 11 parts of ganoderma lucidum, 4-HBA first in the raw material of young state facial mask 1 part of ester, 7 parts of vitamin E and 3 parts of antibacterial modified auxiliary agent.

Comparative example 11

It is essentially identical with the preparation process of embodiment 1, it has only the difference is that preparation regrows wake-up for active cell Polyvinyl alcohol is 44 parts, 18 parts of alginate fibre, 2 parts of tea powder, 12 parts of ganoderma lucidum, 4-HBA first in the raw material of young state facial mask 8 parts of ester, 7 parts of vitamin E and 0.6 part of antibacterial modified auxiliary agent.

Embodiment 12

It is essentially identical with the preparation process of embodiment 1, it has only the difference is that preparation regrows wake-up for active cell Polyvinyl alcohol is 41 parts, 17 parts of alginate fibre, 2 parts of tea powder, 11 parts of ganoderma lucidum, 4-HBA first in the raw material of young state facial mask 1 part of ester, 8 parts of vitamin E and 0.2 part of antibacterial modified auxiliary agent.

It for active cell the young state facial mask of wake-up is regrowed to embodiment 1-3 and comparative example 1-12 carries out items and refer to Mark detection, obtained testing result are as follows:

Wherein anti-microbial property carries out antibacterial test to the facial mask using national standard GBT21510-2008, to detect to large intestine The killing rate of bacillus or golden yellow grape ball, national standard GBT21510-2008's is defined as 90%.

Test group	Sterilizing rate (%)	SOD content (u/100ml)
			Embodiment 1	99.86	16698.9
Embodiment 2	99.64	16435.7
			Embodiment 3	98.78	16653.4
Comparative example 1	43.45	10163.2
			Comparative example 2	97.64	16336.2
Comparative example 3	98.13	16416.9
			Comparative example 4	99.02	16598.4
Comparative example 5	98.43	16794.6
			Comparative example 6	97.36	16468.5
Comparative example 7	96.78	16359.3
			Comparative example 8	98.64	16516.4
Comparative example 9	8.32-9.31	8068.4-8693.5

As seen from the above table: (1) by the data of embodiment 1-3 and comparative example 9 as it can be seen that application embodiment 1-3 is thin for activating The anti-microbial property that born of the same parents regrow the young state facial mask of wake-up significantly improves；Simultaneously by the data of embodiment 1-3 as it can be seen that embodiment 1 For optimum embodiment.

(2) by embodiment 1 and the data of comparative example 1-8 as it can be seen that polyvinyl alcohol, alginate fibre, tea powder, ganoderma lucidum, 4- hydroxyl Methyl benzoate, vitamin E and antibacterial modified auxiliary agent are regrowed in the young state facial mask of wake-up for active cell in preparation and are risen Synergistic effect is arrived, collaboration improves the anti-microbial property for regrowing for active cell and waking up young state facial mask, this is: poly- second Enol, alginate fibre, tea powder, ganoderma lucidum, 4-HBA methyl esters, vitamin E and antibacterial modified auxiliary agent as reinforcement system, with Polyvinyl alcohol is as film forming supplementary material, wherein the chief value of the alginate fibre added is algae component, in limit with The contact of skin will not allow people to have the reaction of allergy, and can actively discharge the vitamin and mineral of seaweed, this minerals packet Calcic and magnesium etc., vitamin includes vitamin A, C, E etc., in the research of cosmetics, shows the mineral that algae component has Matter and vitamin A, C, E have the properties such as natural benefit, degradable absorbability, biocompatibility to skin and hair.Spirit Sesame is able to maintain that immunity of organism balances as Chinese medicine, and skin is made to obtain required amino acid and minerals and polysaccharide activity Ingredient alleviates the damage of keratinocyte oxidative stress, anti-epidermal cell aging.Made by alginate fibre and ganoderma lucidum collaboration With due to the porosity of alginate fibre, load site can be provided for the polypeptide in ganoderma lucidum, effectively increases the anti-of alginate fibre Oxidation susceptibility, moreover it is possible to be able to suppress the aging of Skin Cell, the grease of dirt and secretion for skin adsorbs, and mentions significantly The high cleaning capacity of facial mask contains the tea polyphenols of a large amount of antioxidant effect in tea powder, cell ageing can be effectively relieved, into one Walk the reinforcement antioxygenic property of reinforcement system.4-HBA methyl esters not only meets safety and biofacies as preservative The requirement of capacitive, and antiseptic property is good, delays the shelf-life of facial mask.Vitamin E can effectively improve facial mask as antioxidant Antioxygenic property.Antibacterial modified auxiliary agent is by mixing chitin fiber, bamboo fibre, polyvinylpyrrolidone and deionized water Uniformly, it after grinding, heats up, then heat preservation is added sodium chloride and defoaming agent stirring, continues to heat up, keeps the temperature, aluminum nitrate is then added It is uniformly mixed with zinc oxide, heating water bath, diammonium hydrogen phosphate is added after being cooled to room temperature and is uniformly mixed, is then aged, crosses diafiltration It washs, it is dry, it is cooled to room temperature to obtain after calcining, the hydroxyl of chitin fiber and bamboo fibre surface, and after hydrolysis in solution Amino, amino is by inhibiting the activity of bacterium surface respiratory enzyme in conjunction with negative electron, to cause inactivation of bacteria, and in polyethylene It is obtained under the cohesion of pyrrolidones, in reinforcement system, under the graft modification effect of silane coupling agent KH-560, table The hydroxyl in face finally imparts the excellent anti-microbial property of the reinforcement system in conjunction with the unsaturated bond on polyacrylonitrile surface.This hair It is bright to pass through control polyvinyl alcohol, alginate fibre, tea powder, ganoderma lucidum, 4-HBA methyl esters, vitamin E and antibacterial modified auxiliary agent Weight ratio be (30-40): (5-15): (4-8): (3-9): (2-6): (1-5): (1-2).It is main film forming with polyvinyl alcohol Substance, by the way that using polyvinyl alcohol as main component, polyvinyl alcohol is film forming matter as major ingredient, and the porosity of alginate fibre is spirit Tea polyphenols in the polypeptide and tea powder of sesame provide sufficient load space, while being 4-HBA methyl esters and vitamin E The gap of load is also provided, and by utilizing the anti-ageing of alginate fibre, tea powder and the performance reinforcement of the anti-aging of ganoderma lucidum facial mask Old performance utilizes the antiseptic property of 4-HBA methyl esters and the antioxygenic property of vitamin E and antibacterial modified auxiliary agent Antibacterial action, so that the facial mask shelf-life of the invention is longer, and anti-microbial property is more preferable.

The above content is it cannot be assumed that present invention specific implementation is only limited to these instructions, for the technical field of the invention Those of ordinary skill for, under the premise of not departing from present inventive concept, a number of simple deductions or replacements can also be made, all answers When being considered as belonging to present invention scope of patent protection determined by the appended claims.

Claims

1. one kind regrows the young state facial mask of wake-up for active cell, which is characterized in that including following raw material: polyethylene Alcohol, plant hydrolyzed collagen, propylene glycol, sorbierite, Trenaxmine, reed fragrant plant oil, hydrolecithin, xanthan gum, Aloe Vera Gel, card wave Nurse, trehalose sodium, dipotassium glycyrrhizinate, hydrolysis fibroin, arginine, platinum powder, beta glucan, resveratrol, Sodium Hyaluronate, Denatonium Benzoate, phytic acid, silver oxide, volcanic rock powder, diatomite, tetrasodium pyrophosphate, pure water, aliphatic acid polyethenoxy Ether, alginate fibre, tea powder, ganoderma lucidum, 4-HBA methyl esters, vitamin E, antibacterial modified auxiliary agent；

Antibacterial modified auxiliary agent is as unit of parts by weight, including following raw material: 10-20 parts of chitin fiber, gathers 4-8 parts of bamboo fibre 3-9 parts of vinylpyrrolidone, 8-16 parts of deionized water, 2-6 parts of sodium chloride, 1-4 parts of defoaming agent, 3-6 parts of aluminum nitrate, zinc oxide 2- 5 parts, 1-4 parts of diammonium hydrogen phosphate；

The polyvinyl alcohol, alginate fibre, tea powder, ganoderma lucidum, 4-HBA methyl esters, vitamin E and antibacterial modified auxiliary agent Weight ratio is (30-40): (5-15): (4-8): (3-9): (2-6): (1-5): (1-2).

2. according to claim 1 regrow the young state facial mask of wake-up for active cell, which is characterized in that described poly- Vinyl alcohol, alginate fibre, tea powder, ganoderma lucidum, 4-HBA methyl esters, vitamin E and antibacterial modified auxiliary agent weight ratio be 36.9:11.4:5.4:6.3:4.7:3.8:1.6。

3. according to claim 1 regrow the young state facial mask of wake-up for active cell, which is characterized in that with weight Part is unit, including following raw material: 30-40 parts of polyvinyl alcohol, collagen 5-15 parts plant hydrolyzed, 2-5 parts of propylene glycol, sorb 1-5 parts of alcohol, 3-6 parts of Trenaxmine, 2-5 parts of reed fragrant plant oil, 1-4 parts of hydrolecithin, 3-6 parts of xanthan gum, 2-5 parts of Aloe Vera Gel, card wave 1-5 parts of nurse, 4-6 parts of trehalose sodium, 3-5 parts of dipotassium glycyrrhizinate, hydrolysis fibroin 1-5 parts, -6 parts of arginase 12, platinum powder 1-4 Part, 1-3 parts of beta glucan, 2-6 parts of resveratrol, 1-4 parts of Sodium Hyaluronate, 3-5 parts of Denatonium Benzoate, phytic acid 2-5 Part, 1-3 parts of silver oxide, 2-4 parts of volcanic rock powder, 3-6 parts of diatomite, 1-4 parts of tetrasodium pyrophosphate, 15-35 parts of pure water, fatty acid 2-5 parts of polyoxyethylene ether, 5-15 parts of alginate fibre, 4-8 parts of tea powder, 3-9 parts of ganoderma lucidum, 2-6 parts of 4-HBA methyl esters, dimension life Plain E 1-5 parts, it is auxiliary agent 1-2 parts antibacterial modified.

4. according to claim 1 regrow the young state facial mask of wake-up for active cell, which is characterized in that antibacterial changes Property auxiliary agent prepared by following technique: chitin fiber, bamboo fibre, polyvinylpyrrolidone and deionized water are mixed equal It is even, after grinding 20-40min, it is warming up to 80-90 DEG C, keeps the temperature 20-30min, sodium chloride and defoaming agent stirring is then added, continues 80-90 DEG C of heating keeps the temperature 5-15min, and aluminum nitrate is then added and zinc oxide is uniformly mixed, heating water bath 1-2h is cooled to room Diammonium hydrogen phosphate is added after temperature to be uniformly mixed, is then aged, filtration washing, it is dry, it is cooled to room temperature to obtain antibacterial after calcining and changes Property auxiliary agent.

5. a kind of preparation according to claim 1-4 for regrowing the young state facial mask of wake-up for active cell Method, which comprises the following steps:

S1, polyvinyl alcohol, sorbierite, hydrolecithin, xanthan gum, Aloe Vera Gel, carbomer and Sodium Hyaluronate are uniformly mixed, It is warming up to 70-80 DEG C, keeps the temperature 5-15min, 20-49min is stirred in 350-650r/min revolving speed, is cooled to room temperature to obtain material A；

S2, that volcanic rock powder and diatomite be ground to 110-130 mesh or more is spare, by plant hydrolyzed collagen, propylene glycol, Trenaxmine, reed fragrant plant oil, trehalose sodium, dipotassium glycyrrhizinate, hydrolysis fibroin, arginine, platinum powder, beta glucan, resveratrol, Denatonium Benzoate, phytic acid, silver oxide, tetrasodium pyrophosphate, pure water, aliphatic acid polyethenoxy ether are uniformly mixed, and are warming up to 40-60 DEG C, 10-30min is kept the temperature, volcanic rock powder is subsequently added into and diatomite is uniformly mixed, be continuously heating to 80-90 DEG C, protect Warm 30-50min stirs 1-2h in 850-1050r/min revolving speed, is cooled to room temperature to obtain material B；

S3, by alginate fibre, tea powder, ganoderma lucidum, 4-HBA methyl esters, vitamin E, antibacterial modified auxiliary agent, material A and material B is uniformly mixed, and is warming up to 40-60 DEG C, keeps the temperature 10-20min, is stirred 20-40min in 1500-2500r/min revolving speed, is cooled to Room temperature obtains mixture；

S4, S3 is obtained mixture 0.10-0.12MPa pressure above sterilizing, disinfection 2-3h obtain being used for active cell again Secondary growth wakes up young state facial mask.