CN113041189A

CN113041189A - Antioxidant moisturizing essence body lotion and preparation method thereof

Info

Publication number: CN113041189A
Application number: CN202110294313.2A
Authority: CN
Inventors: 李雪云
Original assignee: Individual
Current assignee: Individual
Priority date: 2021-03-19
Filing date: 2021-03-19
Publication date: 2021-06-29

Abstract

The invention discloses an antioxidant moisturizing essence body lotion and a preparation method thereof, wherein the antioxidant moisturizing essence body lotion comprises the following raw materials in parts by weight: 5-10 parts of antioxidant factors, 3-10 parts of peony essential oil, 0.5-2 parts of sodium hyaluronate, 10-30 parts of shea butter, 5-10 parts of nanoparticles, 0.5-4 parts of emulsifier, 1-10 parts of roselle extract, 1-10 parts of rosemary extract and 0.2-0.5 part of sodium carboxymethylcellulose; adding sodium carboxymethylcellulose into deionized water to obtain sodium carboxymethylcellulose solution, and adding sodium hyaluronate and antioxidant factor into the sodium carboxymethylcellulose solution to obtain component one; uniformly mixing the peony essential oil, shea butter, nano particles, an emulsifier, a roselle extract and a rosemary extract to prepare a component II; adding the component I into the component II to prepare the antioxidant moisturizing essence body lotion; the antioxidant factor can endow the body milk with excellent antioxidant performance.

Description

Antioxidant moisturizing essence body lotion and preparation method thereof

Technical Field

The invention belongs to the technical field of skin care product preparation, and particularly relates to an antioxidant moisturizing essence body lotion and a preparation method thereof.

Background

The skin is a protective layer of our body and can help us to resist the damage of harmful substances in the environment. Harmful substances in the air such as ultraviolet rays, floating dust, bacteria, fungi and the like, and grease, sweat and the like secreted by the skin influence the normal function of the skin, even cause serious skin problems such as infection and the like, cause physiological and psychological burden and influence daily life. In addition, the rhythm of the modern social life is tense, people pay more attention to the facial skin problem and neglect the skin care of other parts of the body.

The body lotion, as the name implies, is a skin care lotion for the body, and has the effects of moisturizing the whole body, whitening and moistening. Particularly in dry winter, dry air can compete for moisture in skin, nutrient structures in the skin can also change, and the skin needs deep moisturizing body lotion to adjust the moisture degree of the skin and strengthen a natural skin moisturizing layer. At the moment, the body lotion can deeply moisten the horny layer of the skin while nourishing the skin, continuously supplements water and nutrients required by the skin, thoroughly changes the state of the skin, and enables the skin to be full, watery and elastic, but the prior body lotion cannot simultaneously take the effects of oxidation resistance and skin care.

Disclosure of Invention

In order to overcome the technical problems, the invention provides an antioxidant moisturizing essence body lotion and a preparation method thereof.

The purpose of the invention can be realized by the following technical scheme:

the antioxidant moisturizing essence body lotion comprises the following raw materials in parts by weight: 5-10 parts of antioxidant factors, 3-10 parts of peony essential oil, 0.5-2 parts of sodium hyaluronate, 10-30 parts of shea butter, 5-10 parts of nanoparticles, 0.5-4 parts of emulsifier, 1-10 parts of roselle extract, 1-10 parts of rosemary extract and 0.2-0.5 part of sodium carboxymethylcellulose;

the antioxidant moisturizing essence body lotion is prepared by the following method:

firstly, adding sodium carboxymethylcellulose into deionized water according to the weight ratio of 1: 10 to prepare sodium carboxymethylcellulose solution, and adding sodium hyaluronate and antioxidant factor into the sodium carboxymethylcellulose solution to prepare a component I;

secondly, uniformly mixing the peony essential oil, the shea butter, the nano particles, the emulsifier, the roselle extract and the rosemary extract to prepare a component II;

and step three, adding the component I into the component II, and stirring at the rotating speed of 500 plus materials and 800r/min for 5-10min to prepare the antioxidant moisturizing essence body lotion.

Further, the emulsifier is one or two of hexadecyl glucoside and octadecyl glucoside which are mixed according to any proportion.

Further, the antioxidant factor is prepared by the following method:

step S1, adding chitosan into a three-neck flask filled with isopropanol, uniformly stirring at the rotation speed of 200r/min at 100-, the dosage ratio of the isopropanol, the mixed liquor A and the sodium hydroxide aqueous solution is 10 g: 120 mL: 50 mL: 100mL, and the volume ratio of the two times of adding of the sodium hydroxide aqueous solution is 2: 3;

step S2, crushing dried pearl mussel meat, degreasing by petroleum ether, drying at 45-50 ℃ after degreasing to obtain pearl mussel meat protein, adding the pearl mussel meat protein into deionized water according to the weight ratio of 1: 10, heating to 50-60 ℃, uniformly stirring at the temperature for 30min, dropwise adding 10% by mass of dilute hydrochloric acid to adjust the pH until the pH is 6.5, adding papain, uniformly stirring and keeping the pH at 6.5, magnetically stirring for 2h, heating to 100 ℃, heating at the temperature for 5min, centrifuging at the rotating speed of 4000r/min to obtain a mixed solution B, adding glucose into a beaker, adding the mixed solution B, uniformly mixing, adjusting the pH to 5, heating in a water bath at 90-100 ℃ for 30min, cooling to room temperature after reaction, obtaining a reaction coating material, controlling the weight ratio of the pearl mussel meat protein to the papain to 1: 2, the dosage ratio of the glucose to the mixed solution B is 2g to 10 mL;

step S3, adding the product a and sodium alginate into deionized water, stirring uniformly to obtain a mixed solution C, adding a coating material and nano calcium carbonate into the mixed solution C, performing ultrasonic and magnetic stirring for 30min, controlling the ultrasonic power to be 50-80W, then washing with n-hexane, and performing vacuum drying to obtain the antioxidant factor, wherein the weight ratio of the product a, the sodium alginate and the deionized water is controlled to be 2: 1: 10, and the weight ratio of the coating material, the nano calcium carbonate and the mixed solution C is controlled to be 1: 0.5: 10.

Step S1, adding sodium hydroxide solution into the isopropanol of the chitosan twice, adding the mixed solution A, grafting carboxymethyl derivatives on primary hydroxyl and amino sites of the chitosan during the reaction process to prepare a product a, and further improving the water solubility of the chitosan, wherein the product a does not contain toxicity and has excellent solubility and biocompatibility in water; in the step S2, pearl mussel meat is degreased to prepare pearl mussel meat protein, then the pearl mussel meat protein is subjected to enzymolysis to prepare a mixed solution B, the mixed solution B is an enzymolysis solution and then is mixed with glucose to prepare a coating material, the coating material is polypeptide and has excellent oxidation resistance, in the step S3, a product a and sodium alginate are added into deionized water to prepare a mixed solution C, and the coating material and nano calcium carbonate are added to prepare an oxidation resistance factor, wherein the oxidation resistance factor is a sodium alginate and product a encapsulation coating material microsphere structure, so that the oxidation resistance factor can be endowed with excellent oxidation resistance, a slow release effect can be achieved, and the coating material can be protected.

The nano-particles are prepared by the following method:

step S11, sequentially adding deionized water and milk into a water phase pot, sequentially adding hyaluronic acid, amino acid and carotene under stirring at a rotating speed of 20-50r/min, increasing the rotating speed to 50-100r/min, and stirring at a constant speed for 30-45min to prepare a mixture, wherein the weight ratio of the deionized water to the milk to the hyaluronic acid to the amino acid to the carotene is controlled to be 50: 15: 5: 3;

step S12, adding high-purity bamboo leaf carbon glycoside flavone into deionized water, adding yuankanin anion polysaccharide into deionized water, mixing to obtain high-purity bamboo leaf carbon glycoside flavone-yuankanin polysaccharide solution, adding epsilon-polylysine into deionized water, stirring until epsilon-polylysine is completely dissolved to obtain epsilon-polylysine solution, dropwise adding the epsilon-polylysine solution into the high-purity bamboo leaf carbon glycoside flavone-yuankanin polysaccharide solution under the condition of uniform stirring, continuing low-speed magnetic stirring for 20-30min, performing ultrasonic oscillation to obtain high-purity bamboo leaf carbon glycoside flavone nano emulsion, adding the mixture, freezing at ultralow temperature of-70 to-90 ℃ for 20h, performing vacuum freeze drying until the water content is less than or equal to 5%, preparing nano particles, and controlling the weight ratio of the high-purity bamboo leaf carbon glycoside flavone, the yuankanin anion polysaccharide and the epsilon-polylysine to be 1: 8: 1, the weight ratio of the high-purity bamboo leaf carbon glycoside flavone nano emulsion to the mixture is 5: 1.

The preparation method of the antioxidant moisturizing essence body lotion comprises the following steps:

The invention has the beneficial effects that:

the antioxidant moisturizing essence body milk is prepared from raw materials such as antioxidant factors and nano particles, the antioxidant factors can endow the body milk with excellent antioxidant performance, in the preparation process, in the step S1, the chitosan is added into the isopropanol twice, the sodium hydroxide solution is added, the mixed solution A is added, the carboxymethyl derivatives are grafted on primary hydroxyl groups and amino sites of the chitosan in the reaction process, a product a is prepared, the water solubility of the chitosan is further improved, and the product a does not contain toxicity and has excellent solubility and biocompatibility in water; in the step S2, firstly, pearl mussel meat is degreased to prepare pearl mussel meat protein, then, the pearl mussel meat protein is subjected to enzymolysis to prepare a mixed solution B, the mixed solution B is an enzymolysis solution and then is mixed with glucose to prepare a coating material, the coating material is polypeptide and has excellent oxidation resistance, then, in the step S3, a product a and sodium alginate are added into deionized water to prepare a mixed solution C, and the coating material and nano calcium carbonate are added to prepare an oxidation resistance factor, wherein the oxidation resistance factor is a sodium alginate and product a encapsulating coating material microsphere structure, so that the oxidation resistance factor can be endowed with excellent oxidation resistance, a slow release effect can be achieved, and the coating material can be protected; the nano particles prepared by the invention contain a large amount of polysaccharide, the polysaccharide can be combined with hydrogen bonds of water to play a role in retaining water, and when the nano particles are used on the surface of skin, the nano particles can reduce the loss of water from the skin due to the film forming effect of the polysaccharide, so that the effects of moisturizing and protecting the skin are achieved.

Detailed Description

The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.

Example 1

The antioxidant moisturizing essence body lotion comprises the following raw materials in parts by weight: 5 parts of antioxidant factors, 3 parts of peony essential oil, 0.5 part of sodium hyaluronate, 10 parts of shea butter, 5 parts of nano particles, 0.5 part of hexadecyl glucoside, 1 part of roselle extract, 1 part of rosemary extract and 0.2 part of sodium carboxymethylcellulose;

secondly, uniformly mixing the peony essential oil, the shea butter, the nano particles, the hexadecyl glucoside, the roselle extract and the rosemary extract to prepare a component II;

and thirdly, adding the component I into the component II, and stirring at the rotating speed of 500r/min for 5min to prepare the antioxidant moisturizing essence body lotion.

The antioxidant factor is prepared by the following method:

step S1, adding chitosan into a three-neck flask filled with isopropanol, uniformly stirring at a rotating speed of 100r/min, heating in a water bath at 40 ℃ and uniformly stirring for 30min, then adding a 35% by mass sodium hydroxide aqueous solution, continuously stirring for 30min, after stirring, dropwise adding a mixed solution A while stirring, controlling the dropwise adding time to be 15min, reacting for 3h at the temperature after dropwise adding, then adding a 35% by mass sodium hydroxide aqueous solution again, uniformly stirring and reacting for 1h, filtering a reaction product, dissolving filter residue with deionized water, adjusting the pH to be 5, performing suction filtration and vacuum drying to obtain a product a, and controlling the using amount ratio of the chitosan, the isopropanol, the mixed solution A and the sodium hydroxide aqueous solution to be 10 g: 120 mL: 50 mL: 100mL, and the volume ratio of the adding amount of the two sodium hydroxide aqueous solutions to be 2: 3;

step S2, pulverizing dried pearl mussel meat, degreasing with petroleum ether, drying at 45 deg.C after degreasing to obtain pearl mussel meat protein, adding the pearl mussel meat protein into deionized water at a weight ratio of 1: 10, heating to 50 deg.C, stirring at constant speed for 30min, adding 10 wt% dilute hydrochloric acid to adjust pH to 6.5, adding papain, stirring at constant speed while maintaining pH at 6.5, magnetically stirring for 2 hr, heating to 100 deg.C, heating at the temperature for 5min, centrifuging at 4000r/min to obtain mixed solution B, adding glucose into a beaker, adding the mixed solution B, uniformly mixing, adjusting the pH value to 5, heating in a water bath at 90 ℃ for 30min, cooling to room temperature after the reaction is finished to obtain a coating material, wherein the weight ratio of the pearl mussel meat protein to the papain is controlled to be 1: 2, and the dosage ratio of the glucose to the mixed solution B is 2 g: 10 mL;

step S3, adding the product a and sodium alginate into deionized water, stirring uniformly to obtain a mixed solution C, adding a coating material and nano calcium carbonate into the mixed solution C, performing ultrasonic and magnetic stirring for 30min, controlling the ultrasonic power to be 50W, then washing with n-hexane, and drying in vacuum to obtain the antioxidant factor, wherein the weight ratio of the product a, the sodium alginate and the deionized water is controlled to be 2: 1: 10, and the weight ratio of the coating material, the nano calcium carbonate and the mixed solution C is controlled to be 1: 0.5: 10.

The nano particles are prepared by the following method:

step S11, sequentially adding deionized water and milk into a water phase pot, sequentially adding hyaluronic acid, amino acid and carotene while stirring at a rotating speed of 20r/min, increasing the rotating speed to 50r/min, stirring at a constant speed for 30min to obtain a mixture, and controlling the weight ratio of the deionized water to the milk to the hyaluronic acid to the amino acid to the carotene to be 50: 15: 5: 3;

step S12, adding high-purity bamboo leaf carbon glycoside flavone into deionized water, adding lilac daphne root anionic polysaccharide into deionized water, mixing to obtain high-purity bamboo leaf carbon glycoside flavone-lilac daphne root polysaccharide solution, adding epsilon-polylysine into deionized water, stirring until epsilon-polylysine is completely dissolved to obtain epsilon-polylysine solution, dropwise adding the epsilon-polylysine solution into the high-purity bamboo leaf carbon glycoside flavone-lilac daphne root polysaccharide solution under the condition of uniform stirring, continuing low-speed magnetic stirring for 20min, performing ultrasonic oscillation to obtain high-purity bamboo leaf carbon glycoside flavone nano emulsion, adding the mixture, freezing at-70 ℃ and ultralow temperature for 20h, performing vacuum freeze drying until the water content is less than or equal to 5%, preparing nano particles, and controlling the weight ratio of the high-purity bamboo leaf carbon glycoside flavone, the lilac daphne root anionic polysaccharide and the epsilon-polylysin, the weight ratio of the high-purity bamboo leaf carbon glycoside flavone nano emulsion to the mixture is 5: 1.

Example 2

The antioxidant moisturizing essence body lotion comprises the following raw materials in parts by weight: 6 parts of antioxidant factors, 4 parts of peony essential oil, 0.6 part of sodium hyaluronate, 11 parts of shea butter, 6 parts of nano particles, 0.6 part of hexadecyl glucoside, 2 parts of roselle extract, 2 parts of rosemary extract and 0.3 part of sodium carboxymethylcellulose;

The antioxidant factor is prepared by the following method:

The nano particles are prepared by the following method:

Example 3

The antioxidant moisturizing essence body lotion comprises the following raw materials in parts by weight: 8 parts of antioxidant factors, 6 parts of peony essential oil, 1.2 parts of sodium hyaluronate, 20 parts of shea butter, 8 parts of nanoparticles, 1.2 parts of hexadecyl glucoside, 6 parts of roselle extract, 6 parts of rosemary extract and 0.4 part of sodium carboxymethylcellulose;

The antioxidant factor is prepared by the following method:

The nano particles are prepared by the following method:

Example 4

The antioxidant moisturizing essence body lotion comprises the following raw materials in parts by weight: 10 parts of antioxidant factors, 10 parts of peony essential oil, 2 parts of sodium hyaluronate, 30 parts of shea butter, 10 parts of nanoparticles, 4 parts of hexadecyl glucoside, 10 parts of roselle extract, 10 parts of rosemary extract and 0.5 part of sodium carboxymethylcellulose;

The antioxidant factor is prepared by the following method:

The nano particles are prepared by the following method:

Comparative example 1

In comparison with example 1, no antioxidant factor was added in this comparative example.

Comparative example 2

This comparative example compares to example 1 without the addition of nanoparticles.

Comparative example 3

The comparative example is a senior urea body lotion in the market.

Sensory tests were conducted for examples 1 to 4 and comparative examples 1 to 3, and the results are shown in the following table;

before using the sample, a user uses the same mild shower gel product to clean the body, the body milk provided in examples 1-4 and comparative examples 1-3 is smeared, the using frequency is once at night, the body milk is continuously used every day, the trial period is 2 weeks, and sensory evaluation is carried out, the main evaluation indexes are antioxidant and skin care effects and are divided into 1-5 grades, wherein, the 1 grade is no improvement, the 2 grade is unobvious improvement, the 3 grade is general improvement, the 4 grade is good improvement, and the 5 grade is obvious improvement.

	Example 1	Example 2	Example 3	Example 4	Comparative example 1	Comparative example 2	Comparative example 3
								Results	5	5	5	5	2	3	3

It can be seen from the above table that the sensory evaluations of examples 1 to 4 were of grade 5, and the sensory evaluations of comparative examples 1 to 3 were of grade 2 to 3.

In the description herein, references to the description of "one embodiment," "an example," "a specific example" or the like are intended to mean that a particular feature, structure, material, or characteristic described in connection with the embodiment or example is included in at least one embodiment or example of the invention. In this specification, the schematic representations of the terms used above do not necessarily refer to the same embodiment or example. Furthermore, the particular features, structures, materials, or characteristics described may be combined in any suitable manner in any one or more embodiments or examples.

The foregoing is illustrative and explanatory only and is not intended to be exhaustive or to limit the invention to the precise embodiments described, and various modifications, additions, and substitutions may be made by those skilled in the art without departing from the scope of the invention or exceeding the scope of the claims.

Claims

1. The antioxidant moisturizing essence body lotion is characterized by comprising the following raw materials in parts by weight: 5-10 parts of antioxidant factors, 3-10 parts of peony essential oil, 0.5-2 parts of sodium hyaluronate, 10-30 parts of shea butter, 5-10 parts of nanoparticles, 0.5-4 parts of emulsifier, 1-10 parts of roselle extract, 1-10 parts of rosemary extract and 0.2-0.5 part of sodium carboxymethylcellulose;

2. The antioxidant moisture-retention essence body lotion as claimed in claim 1, wherein the emulsifier is one or two of cetyl glucoside and stearyl glucoside mixed in any proportion.

3. The antioxidant moisturizing essence body lotion as claimed in claim 1, wherein the antioxidant factor is prepared by the following method:

step S1, adding chitosan into a three-neck flask filled with isopropanol, stirring at a constant speed, heating in a water bath at 40-50 ℃, stirring at a constant speed for 30min, then adding a 35% sodium hydroxide aqueous solution by mass fraction, continuing to stir for 30min, after stirring, dropwise adding a mixed solution A, stirring while dropwise adding, controlling the dropwise adding time to be 15min, reacting for 3h at the temperature after dropwise adding, then adding a 35% sodium hydroxide aqueous solution by mass fraction again, stirring at a constant speed, reacting for 1h, filtering a reaction product, dissolving filter residue with deionized water, adjusting the pH to 5-7, performing suction filtration and vacuum drying to obtain a product a, controlling the use ratio of the chitosan, the isopropanol, the mixed solution A and the sodium hydroxide aqueous solution to be 10 g: 120 mL: 50 mL: 100mL, and controlling the volume ratio of the two-time sodium hydroxide aqueous solution addition to be 2: 3;

4. The preparation method of the antioxidant moisturizing essence body lotion as claimed in claim 1, which is characterized by comprising the following steps: