CN110237004A - A kind of body lotion formula and preparation method thereof - Google Patents
A kind of body lotion formula and preparation method thereof Download PDFInfo
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Abstract
The invention discloses a kind of body lotion formulas and preparation method thereof, are related to body lotion technical field, the component including following parts by weight: 0.1-1 parts of Geranium Essentials；0.1-1 parts of safflower essential oils；0.1-1 parts of deodar essential oils；0.1-1 parts of Radix et Caulis Opuntiae Dillenii extracts；0.1-1 portions of trehaloses；0.1-1 parts of moisturizer；0.5-1 portions of preservatives；0.1-2 parts of emulsifiers；30-45 parts of oil phase substrates；Surplus is aqueous phase substrate.The present invention can make skin surface transparent, beautiful, skin is enabled to form water conservation barrier, water lock ability is preferable, while also having both blood circulation, removing blood stasis and acesodyne effect, it can be relieved arthritis, relieve stress, and the compact skin of subcutaneous fat can be eliminated, adjust human secretory function and adjust the activity of lipase, superabundant fats are promoted to decompose rapidly, incremental loses weight, and smoothly lifts skin, and skin recovery is made to elastically keep youth.
Description
Technical field
The present invention relates to body lotion technical fields more particularly to a kind of body lotion formula and preparation method thereof.
Background technique
With the progress of society and economic development and the continuous improvement of living standards of the people, people are to body lotion
It is required that it is also higher and higher, increasingly develop to the direction of " naturalization, nutrient laden, curative effect ".But currently on the market each
It is most of all containing the chemical substance being harmful to the human body, such as leaded, mercury poisonous and harmful substance, these bodies in kind body lotion
Cream easily causes people's skin allergy, causes to damage to human organ and function, and traditional body lotion is only for skin surface
Improved, no activating microcirculation and removing stasis medicinal relieves pain and other effects.Various natural originals are thus added in body lotion, especially body lotion
Material, has good nourishing effect to skin, and have no toxic side effect, effective component is especially extracted from plants and is added to body
Remarkable effect is had more in cream.
Summary of the invention
The purpose of the present invention is to solve above-mentioned problem, and a kind of body lotion formula disclosed in function, including it is as follows
The component of parts by weight:
0.1-1 parts of Geranium Essentials；
0.1-1 parts of safflower essential oils；
0.1-1 parts of deodar essential oils；
1-3 parts of Radix et Caulis Opuntiae Dillenii extracts；
0.1-1 portions of trehaloses；
0.1-1 parts of moisturizer；
0.5-1 portions of preservatives；
0.1-2 parts of emulsifiers；
30-45 parts of oil phase substrates；
Surplus is aqueous phase substrate.
Optionally, the oil phase substrate is hydrogenated olive oil, hydrogenated jojoba oil, hydrogenated glucose seed oil, the poly- diformazan of ring five
One of radical siloxane or ethylhexyl palmitate are a variety of.
Optionally, the aqueous phase substrate is one of carbomer, allantoin or water or a variety of.
Optionally, the emulsifier is cetyl alcohol, cetyl glucoside, stearyl alcohol or octadecyl Portugal
One of glucosides is a variety of.
Optionally, the preservative is that Phenoxyethanol/ethylhexyl compounds at least one of glycerol or Kathon CG.
Optionally, the moisturizer is using in glycerine, Sodium Hyaluronate, Ovshinsky marine algae extract or oligofructose
It is one or more.
Optionally, the effective component of the Radix et Caulis Opuntiae Dillenii extract is hydroxymalonic acid, triterpenoid saponin and flavones.
The invention also discloses a kind of production method of body lotion formula, which includes the following steps:
S1: the effective component in cactus is extracted, spare；
S2: being added water in emulsion pot, then is separately added into antioxidant weighed in parts by weight, emulsifier, thickening
Agent, preservative, trehalose, stirring carry out homogeneous, 85-90 DEG C are heated to, until all components are completely dispersed uniformly；
S3: being added oil phase substrate in emulsion pot, is being separately added into deodar essential oil weighed in parts by weight, safflower essence
Respectively oily phase pot is added by weight in object by oil and Geranium Essential, is stirred homogeneous and is heated to 80-85 DEG C；
S4: importing emulsion pot for component interior in oily phase pot, carries out emulsifying 15-20 minutes, then protects at 65-75 DEG C
Temperature 30 minutes；
S5: being cooled to 43-48 DEG C, in parts by weight addition Radix et Caulis Opuntiae Dillenii extract and moisturizer, stirs 10-15 minutes extremely
It is uniformly dispersed.
Effective component extraction step is as follows in cactus in above-mentioned S1:
It is 210~250 targeted fine powders that cactus powder is broken to fineness by S1.1, obtains cactus powder；
S1.2 adds water into cactus powder, and the pH value for adjusting solution is 7, enzymolysis agent is added, in 65-70 DEG C of temperature
Degree is lower to hydrolyze 1h, obtains enzymolysis liquid；
Enzymolysis liquid is sent into ultrasonic device by S1.3, in the item that ultrasonic frequency is 40-50KHz, temperature is 55-65 DEG C
40-50min is handled under part, and filtrate is collected by filtration；
Filtrate is concentrated into soluble solid under conditions of vacuum degree is -0.05MPa, temperature is 55-60 DEG C by S1.4
>=18 parts, obtain concentrate；
85 parts of ethyl alcohol is added into concentrate by S1.5, after standing 1h, is centrifugated under the revolving speed of 2500r/min
20min obtains Radix et Caulis Opuntiae Dillenii extract.
Compared with prior art, the present invention has following advantages:
The present invention can make skin surface transparent, beautiful, enable skin form water conservation barrier, water lock ability is preferable, while also simultaneous
Has blood circulation, removing blood stasis and acesodyne effect can be relieved arthritis, relieve stress, and can eliminate the compact skin of subcutaneous fat, adjust
It saves human secretory function and adjusts the activity of lipase, superabundant fats is promoted to decompose rapidly, incremental loses weight, and puts down
Sliding lifting skin, makes skin recovery elastically keep youth.
Specific embodiment
The technical scheme in the embodiments of the invention will be clearly and completely described below, it is clear that described reality
Applying example is only a part of the embodiment of the present invention, instead of all the embodiments.
Embodiment one
Formula
Component including following parts by weight:
0.3 part of Geranium Essential；
0.3 part of safflower essential oil；
0.2 part of deodar essential oil；
1 part of Radix et Caulis Opuntiae Dillenii extract；
0.2 portion of trehalose；
0.3 part of moisturizer；
Moisturizer uses glycerine；
0.5 portion of preservative；
Preservative Phenoxyethanol/ethylhexyl compounds glycerol；
0.1 part of emulsifier；
Emulsifier uses cetyl alcohol；
30 parts of oil phase substrates；
Oil phase substrate uses hydrogenated olive oil；
67.3 part aqueous phase substrate；
Aqueous phase substrate adds water using carbomer.
Experimental procedure:
S1: the effective component in cactus is extracted, spare；
S2: being added water in emulsion pot, then is separately added into antioxidant weighed in parts by weight, emulsifier, thickening
Agent, preservative, trehalose, stirring carry out homogeneous, 85 DEG C are heated to, until all components are completely dispersed uniformly；
S3: being added oil phase substrate in emulsion pot, is being separately added into deodar essential oil weighed in parts by weight, safflower essence
Respectively oily phase pot is added by weight in object by oil and Geranium Essential, is stirred homogeneous and is heated to 80 DEG C；
S4: importing emulsion pot for component interior in oily phase pot, carries out emulsifying 15 minutes, then keeps the temperature 30 points at 65 DEG C
Clock；
S5: being cooled to 43 DEG C, in parts by weight addition Radix et Caulis Opuntiae Dillenii extract and moisturizer, and stirring 10 minutes equal to dispersing
It is even.
Effective component extraction step is as follows in cactus in above-mentioned S1:
It is 210 targeted fine powders that cactus powder is broken to fineness by S1.1, obtains cactus powder；
S1.2 is into cactus powder plus water, and the pH value for adjusting solution is 7, adds enzymolysis agent, 65 DEG C at a temperature of
1h is hydrolyzed, enzymolysis liquid is obtained；
S1.3 by enzymolysis liquid be sent into ultrasonic device in, under conditions of ultrasonic frequency is 40KHz, temperature is 55 DEG C at
40min is managed, and filtrate is collected by filtration；
S1.4 filtrate is concentrated under conditions of vacuum degree is -0.05MPa, temperature is 55 DEG C soluble solid >=
18 parts, obtain concentrate；
85 parts of ethyl alcohol is added into concentrate by S1.5, after standing 1h, is centrifugated under the revolving speed of 2500r/min
20min obtains Radix et Caulis Opuntiae Dillenii extract.
Embodiment two
Formula
Component including following parts by weight:
0.5 part of Geranium Essential；
0.6 part of safflower essential oil；
0.5 part of deodar essential oil；
2 parts of Radix et Caulis Opuntiae Dillenii extracts；
0.6 portion of trehalose；
0.4 part of moisturizer；
Moisturizer uses Sodium Hyaluronate；
0.6 portion of preservative；
Preservative uses Kathon CG；
0.3 part of emulsifier；
Emulsifier uses cetyl alcohol；
35 parts of oil phase substrates；
Oil phase substrate uses hydrogenated jojoba oil and hydrogenated glucose seed oil mixture；
59.5 part aqueous phase substrate；
Aqueous phase substrate adds water using allantoin.
Experimental procedure:
S1: the effective component in cactus is extracted, spare；
S2: being added water in emulsion pot, then is separately added into antioxidant weighed in parts by weight, emulsifier, thickening
Agent, preservative, trehalose, stirring carry out homogeneous, 86 DEG C are heated to, until all components are completely dispersed uniformly；
S3: being added oil phase substrate in emulsion pot, is being separately added into deodar essential oil weighed in parts by weight, safflower essence
Respectively oily phase pot is added by weight in object by oil and Geranium Essential, is stirred homogeneous and is heated to 82 DEG C；
S4: importing emulsion pot for component interior in oily phase pot, carries out emulsifying 17 minutes, then keeps the temperature 30 points at 70 DEG C
Clock；
S5: being cooled to 45 DEG C, in parts by weight addition Radix et Caulis Opuntiae Dillenii extract and moisturizer, and stirring 10 minutes equal to dispersing
It is even.
Effective component extraction step is as follows in cactus in above-mentioned S1:
It is 210 targeted fine powders that cactus powder is broken to fineness by S1.1, obtains cactus powder；
S1.2 is into cactus powder plus water, and the pH value for adjusting solution is 7, adds enzymolysis agent, 65 DEG C at a temperature of
1h is hydrolyzed, enzymolysis liquid is obtained；
S1.3 by enzymolysis liquid be sent into ultrasonic device in, under conditions of ultrasonic frequency is 45KHz, temperature is 60 DEG C at
40min is managed, and filtrate is collected by filtration；
S1.4 filtrate is concentrated under conditions of vacuum degree is -0.05MPa, temperature is 55 DEG C soluble solid >=
18 parts, obtain concentrate；
85 parts of ethyl alcohol is added into concentrate by S1.5, after standing 1h, is centrifugated under the revolving speed of 2500r/min
20min obtains Radix et Caulis Opuntiae Dillenii extract.
Embodiment three
Formula
Component including following parts by weight:
1 part of Geranium Essential；
0.8 part of safflower essential oil；
0.7 part of deodar essential oil；
3 parts of Radix et Caulis Opuntiae Dillenii extracts；
0.8 portion of trehalose；
0.8 part of moisturizer；
Moisturizer uses Ovshinsky marine algae extract and oligofructose；
0.9 portion of preservative；
Preservative compounds glycerol using Phenoxyethanol/ethylhexyl；
1 part of emulsifier；
Emulsifier uses stearyl alcohol or octadecyl glucoside mixture；
45 parts of oil phase substrates；
Oil phase substrate uses ring five dimethyl silicone polymer or ethylhexyl palmitate mixture；
45.9 part aqueous phase substrate；
Aqueous phase substrate adds water using carbomer and allantoin.
Experimental procedure:
S1: the effective component in cactus is extracted, spare；
S2: being added water in emulsion pot, then is separately added into antioxidant weighed in parts by weight, emulsifier, thickening
Agent, preservative, trehalose, stirring carry out homogeneous, 90 DEG C are heated to, until all components are completely dispersed uniformly；
S3: being added oil phase substrate in emulsion pot, is being separately added into deodar essential oil weighed in parts by weight, safflower essence
Respectively oily phase pot is added by weight in object by oil and Geranium Essential, is stirred homogeneous and is heated to 85 DEG C；
S4: importing emulsion pot for component interior in oily phase pot, carries out emulsifying 17 minutes, then keeps the temperature 30 points at 75 DEG C
Clock；
S5: being cooled to 48 DEG C, in parts by weight addition Radix et Caulis Opuntiae Dillenii extract and moisturizer, and stirring 15 minutes equal to dispersing
It is even.
Effective component extraction step is as follows in cactus in above-mentioned S1:
It is 250 targeted fine powders that cactus powder is broken to fineness by S1.1, obtains cactus powder；
S1.2 is into cactus powder plus water, and the pH value for adjusting solution is 7, adds enzymolysis agent, 70 DEG C at a temperature of
1h is hydrolyzed, enzymolysis liquid is obtained；
S1.3 by enzymolysis liquid be sent into ultrasonic device in, under conditions of ultrasonic frequency is 50KHz, temperature is 65 DEG C at
50min is managed, and filtrate is collected by filtration；
S1.4 filtrate is concentrated under conditions of vacuum degree is -0.05MPa, temperature is 60 DEG C soluble solid >=
18 parts, obtain concentrate；
85 parts of ethyl alcohol is added into concentrate by S1.5, after standing 1h, is centrifugated under the revolving speed of 2500r/min
20min obtains Radix et Caulis Opuntiae Dillenii extract.
Experiment 1
Based on the above embodiments 1 to embodiment 3, moisturizing experiment is as follows:
Experimental group: the body lotion in embodiment 1,2,3；
Control group: body lotion is not used；
Experimental basis: QB/T4256-2011 " cosmetics moisture-keeping efficacy evaluation guide "；
Test method: each body lotion respectively looks for 30 subjects；
Subject characteristics: women, average age 30 ± 5 years old；
Recipient site: double inner forearms mark recipient site at symmetrical two, are randomly assigned as the area Tu Yang and check plot.
Product smears dosage: application area: 4cm × 3cm, smears dosage: 10mg/cm2.
Test index: keratoderma water content.
Test procedure: subject sits quietly after 10min, and (T0) keratoderma is aqueous before test recipient site sample is smeared
Then amount smears tested material by prescribed dose, the area Tu Yang is smeared after tested material 1 hour, and 8 hours, 12 hours, 24 hours were tested
Recipient site keratoderma water content.
Table 1: keratoderma water content test comparison
Test result shows that the body lotion prepared in embodiment 3 after smearing 1 hour, 8 hours, 12 hours, all has
Excellent moistening effect, and as the increase water lock ability of oil phase substance and Radix et Caulis Opuntiae Dillenii extract are more preferable, enable skin form water conservation
Barrier, the increase of moisture make skin recovery elastically keep youth, keep skin health, inject vigour into.
Experiment 2
Based on the above embodiments 1 to embodiment 3, the rouge that disappears experiment is as follows:
Experimental group: the body lotion in embodiment 1,2,3；
Control group: body lotion is not used；
Test method: each body lotion respectively looks for 30 subjects, without metabolic problems and BMI (body-mass index, (body
Weight (kilogram)/height (rice)) 2) it is 20-25；
Subject characteristics: women, average age 30 ± 5 years old；
Recipient site: femoribus internus marks recipient site at symmetrical two, is randomly assigned as the area Tu Yang and check plot.
Product smears dosage: application area: 4cm × 4cm, smears dosage: 15mg/cm2.
Test index: the thickness of subcutaneous fat.
Test procedure: and then the body lotion prepared in embodiment 1-3 is administered to by femoribus internus, morning and evening each 1 by massage
It is secondary, continuous administration 6 weeks, subcutaneous rouge was measured using using the Ultrasound-EuB 415US scanner with ultrasonic wave every 2 weeks
The thickness of fat verifies effect.
Table 2: the thickness change of subcutaneous fat
Test result shows that the body lotion prepared in embodiment 3 has after smearing 6 weeks and preferably disappears rouge function, and with
The increase of Radix et Caulis Opuntiae Dillenii extract eliminate that fatty ability is more preferable, and the hydroxymalonic acid in cactus can have suppression to the growth of fat
Production is used；Triterpenoid saponin in cactus is substance necessary to human body, they can directly adjust human secretory function and tune
The activity of lipase is saved, superabundant fats is promoted to decompose rapidly, and can effectively prevent fat in intestinal absorption, fat is inhibited to exist
Synthesis in liver, to the deposition of anti-cholesterol wall in the blood vessels, incremental loses weight.
Experiment 3
Based on the above embodiments 1 to embodiment 3, blood circulation, removing blood stasis and acesodyne Efficacy experiments are as follows:
Experimental group: the body lotion in embodiment 1,2,3；
Control group: common commercially available moisturizing body dairy products；
Test method: every kind of physical problems look for 40 sensitive aging subjects respectively, mean allocation experimental and control group,
The effect of smearing of progress 30 days, front and back is smeared in observation, inquiry.
Subject characteristics: women, average age 30 ± 10 years old；
Recipient site: dissipating bind lump, hand anesthesia, foot numbness, cervical pain, arthralgia, pruitus.
Product smears dosage: application area: 6cm × 6cm, smears dosage: 20mg/cm2.
Table 3: physical problems improvement rate
By table 3 it is found that embodiment 1 to embodiment 3 to dissipating bind lump, hand anesthesia, foot numbness, cervical pain, pass
Section pain, pruitus have different degrees of improvement, and with the increasing of Geranium Essential, safflower essential oil, deodar essential oil content
Add, can effective blood circulation, removing blood stasis and acesodyne, wherein Geranium Essential can achieve the purpose of promoting blood circulation channels and collaterals, safflower essential oil
Blood circulation, removing blood stasis and acesodyne, deodar essential oil can be relieved arthritis, relieve stress, and control group considers patient's self-healing, needle
The problems such as to dissipating bind lump, hand anesthesia, foot numbness, cervical pain, arthralgia, pruitus, is without improvement.
Although disclosed above show illustrative embodiment of the invention, it is noted that can make wherein each
The scope of the present invention that kind replacement and change are defined without departing from such as appended claims.According to described herein
Function, step and/or the movement of the claim to a method of inventive embodiments need not be executed by any certain order.In addition, to the greatest extent
Pipe element of the invention may be described or claimed with odd number, but plural number be also it is contemplated, unless aobvious
It states to be defined in odd number likes.
Claims (9)
1. a kind of body lotion formula, it is characterised in that: the component including following parts by weight:
0.1-1 parts of Geranium Essentials；
0.1-1 parts of safflower essential oils；
0.1-1 parts of deodar essential oils；
1-3 parts of Radix et Caulis Opuntiae Dillenii extracts；
0.1-1 portions of trehaloses；
0.1-1 parts of moisturizer；
0.5-1 portions of preservatives；
0.1-2 parts of emulsifiers；
30-45 parts of oil phase substrates；
Surplus is aqueous phase substrate.
2. a kind of body lotion formula according to claim 1, which is characterized in that the oil phase substrate be hydrogenated olive oil,
One of hydrogenated jojoba oil, hydrogenated glucose seed oil, ring five dimethyl silicone polymer or ethylhexyl palmitate are a variety of.
3. a kind of body lotion formula according to claim 1, which is characterized in that the aqueous phase substrate is carbomer, allantois
One of element or water are a variety of.
4. a kind of body lotion formula according to claim 1, which is characterized in that the emulsifier is cetyl alcohol, ten
One of six alkyl glucosides, stearyl alcohol or octadecyl glucoside are a variety of.
5. a kind of body lotion formula according to claim 1, which is characterized in that the preservative is Phenoxyethanol/ethyl
Hexyl compounds at least one of glycerol or Kathon CG.
6. a kind of body lotion formula according to claim 1, which is characterized in that the moisturizer is using glycerine, transparent
One of matter acid sodium, Ovshinsky marine algae extract or oligofructose are a variety of.
7. a kind of body lotion formula according to claim 1, which is characterized in that the effective component of the Radix et Caulis Opuntiae Dillenii extract
For hydroxymalonic acid, triterpenoid saponin and flavones.
8. a kind of production method of body lotion formula, which is characterized in that the production method includes the following steps:
S1: the effective component in cactus is extracted, spare；
S2: being added water in emulsion pot, then is separately added into antioxidant weighed in parts by weight, emulsifier, thickener, anti-corrosion
Agent, trehalose, stirring carry out homogeneous, 85-90 DEG C are heated to, until all components are completely dispersed uniformly；
S3: being added oil phase substrate in emulsion pot, is being separately added into deodar essential oil weighed in parts by weight, safflower essential oil and day
Respectively oily phase pot is added by weight in object by Zhu Kui essential oil, is stirred homogeneous and is heated to 80-85 DEG C；
S4: importing emulsion pot for component interior in oily phase pot, carries out emulsifying 15-20 minutes, then keeps the temperature 30 points at 65-75 DEG C
Clock；
S5: being cooled to 43-48 DEG C, in parts by weight addition Radix et Caulis Opuntiae Dillenii extract and moisturizer, and stirring 10-15 minutes equal to dispersing
It is even.
9. a kind of production method of body lotion formula according to claim 8, which is characterized in that the celestial being in above-mentioned S1
Effective component extraction step is as follows in the palm:
It is 210~250 targeted fine powders that cactus powder is broken to fineness by S1.1, obtains cactus powder；
S1.2 adds water into cactus powder, and the pH value for adjusting solution is 7, adds enzymolysis agent, is lauched in 65-70 DEG C of temperature
1h is solved, enzymolysis liquid is obtained；
S1.3 by enzymolysis liquid be sent into ultrasonic device in, under conditions of ultrasonic frequency is 40-50KHz, temperature is 55-65 DEG C at
40-50min is managed, and filtrate is collected by filtration；
Filtrate is concentrated into soluble solid >=18 under conditions of vacuum degree is -0.05MPa, temperature is 55-60 DEG C by S1.4
Part, obtain concentrate；
85 parts of ethyl alcohol is added into concentrate by S1.5, after standing 1h, is centrifugated 20min under the revolving speed of 2500r/min, obtains
Radix et Caulis Opuntiae Dillenii extract.
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