CN107714631B - Collagen peptide mask liquid and preparation method thereof - Google Patents
Collagen peptide mask liquid and preparation method thereof Download PDFInfo
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- 238000002360 preparation method Methods 0.000 title claims abstract description 15
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Classifications
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/99—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from microorganisms other than algae or fungi, e.g. protozoa or bacteria
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- A—HUMAN NECESSITIES
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
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- A—HUMAN NECESSITIES
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/65—Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
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- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/74—Biological properties of particular ingredients
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- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/85—Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine
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- Chemical & Material Sciences (AREA)
- Botany (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Gerontology & Geriatric Medicine (AREA)
- Tropical Medicine & Parasitology (AREA)
- Cosmetics (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The invention relates to a collagen peptide mask liquid and a preparation method thereof, wherein the mask liquid is prepared from the following raw materials in parts by weight: 5-15 parts of black tea fungus fermentation liquor, 2.5-5 parts of collagen peptide, 1-2 parts of water-soluble camellia seed oil, 0.8-1.2 parts of micrococcus glue, 3-5 parts of gardenia hydrolat, 5-8 parts of glycerol, 0.5-1 part of hexanediol, 0.5-1 part of sodium hyaluronate, 0.2-1 part of black tea fungus fermentation membrane modifier and 60-80 parts of deionized water. The collagen peptide facial mask liquid is prepared from natural plants, is convenient to carry and use, can effectively clean, moisturize and repair damaged cells, and is a facial mask liquid product which can be used for a long time.
Description
Technical Field
The invention relates to a collagen peptide mask liquid and a preparation method thereof, belonging to the technical field of skin care products.
Background
With the improvement of living standard, people pay more and more attention to skin care, but a series of problems of dry skin, dark skin color and the like are caused by outdoor ultraviolet rays and dust, computer radiation in a workshop, mobile phone radiation and the like, and meanwhile, skin care products are layered endlessly. To be effective, some products go to great lengths to use up various solutions, however many are harmful to the skin, such as fluorescers, heavy metal ions, excess preservatives, etc. With the safety problem of skin care products which are frequently exploded in recent years, people gradually prefer natural skin care ingredients. The first step of skin care is from the face, and the fastest to take effect is the mask, which can inject the nutrients needed by the skin in a short time.
Collagen is one of the major components of human tissue structure, and is distributed throughout various tissues and organs of the whole body, such as: skin, bone, cartilage, ligament, cornea, various intima, fascia, etc., are main components for maintaining the morphology and structure of skin and tissue organs, and are important raw materials for repairing various damaged tissues. The collagen directly supplemented in the skin care product can rapidly supplement the collagen lost from the skin, so that the skin is more permeable and elastic. The collagen peptide consists of two or more than two amino acids, can be actively absorbed by a human body without barrier, does not need digestion, is fully utilized by body tissues, and becomes a traditional Chinese medicine raw material for repairing various damaged tissues.
In the prior art, researchers have studied the application of natural component extract and the like as raw materials in the field of facial masks, but the preparation cost is high due to the complex formula, more components and complex preparation process.
Disclosure of Invention
In order to solve the problems in the prior art, the invention has the advantages that: the collagen peptide facial mask liquid is prepared by extracting and dividing natural plants, is safe and reliable, can effectively clean and moisturize skin, can deeply nourish skin and repair damaged cells, is a usable facial mask liquid product, and has the advantages of easily available raw materials, easiness in operation, mild reaction conditions, obvious effect, low cost and the like.
The technical scheme of the invention is as follows:
the collagen peptide mask liquid is prepared from the following raw materials in parts by weight: 5-15 parts of black tea fungus fermentation liquor, 2.5-5 parts of collagen peptide, 1-2 parts of water-soluble camellia seed oil, 0.8-1.2 parts of sclerotium rolfsii gum, 3-5 parts of gardenia hydrolat, 5-8 parts of glycerol, 0.5-1 part of hexanediol, 0.5-1 part of sodium hyaluronate, 0.2-1 part of black tea fungus fermentation membrane modifier and 60-80 parts of deionized water.
Further, the health-care food is prepared from the following raw materials in parts by weight: 5-12 parts of black tea fungus fermentation liquor, 3.5-5 parts of collagen peptide, 1.5-2 parts of water-soluble camellia seed oil, 0.8-1.0 part of sclerotium rolfsii gum, 4-5 parts of gardenia hydrolat, 5-6 parts of glycerol, 0.8-1 part of hexanediol, 0.5-0.8 part of sodium hyaluronate, 0.2-0.5 part of black tea fungus fermentation membrane modifier and 70-80 parts of deionized water.
Further, the black tea fungus fermentation liquor is prepared from the following raw materials in parts by weight: 2-8 parts of black tea, 8-12 parts of seaweed, 2-6 parts of kelp, 45-55 parts of white granulated sugar, 900 parts of deionized water and 1200 parts of black tea fungus mother liquor and 45-60 parts of black tea fungus mother liquor.
Further, the black tea fungus fermentation membrane modifier is prepared from the following raw materials in parts by weight: 100 parts of black tea fungus fermentation membrane solution with the mass concentration of 1.5-3%, 20-35 parts of chloroethanol and 2-10 parts of acetic acid; the black tea fungus fermentation membrane solution is prepared from the following raw materials in parts by weight: 90-110 parts of mixed aqueous solution of NaOH with the mass concentration of 5% and hydroxyethyl urea with the mass concentration of 6% and 1-3 parts of black tea fungus fermentation membrane.
Further, the water-soluble camellia oleosa seed oil is prepared from the following raw materials in parts by weight:
the invention also comprises a preparation method of the collagen peptide facial mask liquid, which comprises the following steps: (1) dissolving 0.2-1 part by weight of black tea fungus fermentation membrane modifier with 60-80 parts by weight of deionized water at normal temperature; (2) adding 2.5-5 parts by weight of collagen peptide and 0.5-1 part by weight of sodium hyaluronate, heating to 60 ℃, stirring to dissolve and uniformly mixing; (3) keeping the temperature at 60 ℃, adding 5-8 parts by weight of glycerol and 0.8-1.2 parts by weight of sclerotium rolfsii gum, stirring to dissolve and uniformly mixing; (4) cooling to room temperature, sequentially adding 1-2 parts by weight of water-soluble camellia oleosa seed oil and 5-15 parts by weight of black tea fungus fermentation liquor, and uniformly mixing; (5) adding 3-5 parts by weight of gardenia hydrolat and 0.5-1 part by weight of hexanediol, uniformly mixing, and obtaining the mask liquid.
Further, the black tea fungus fermentation liquor is prepared by the following steps: mixing and boiling black tea of 2-8 parts by weight, seaweed of 8-12 parts by weight, kelp of 2-6 parts by weight, white granulated sugar of 45-55 parts by weight and deionized water of 900-1200 parts by weight for 120min, standing, cooling, filtering, adding deionized water into the filtrate to keep the filtrate at 900-1200 parts by weight, uniformly mixing, adding into a container, placing into a high-temperature sterilization and re-sterilization for 20min, cooling to room temperature after the sterilization is finished, adding black tea fungus mother liquor of 45-60 parts by weight, sealing with gauze, fermenting at normal temperature and normal pressure for 6-9 days, and filtering with a screen to obtain black tea fungus fermentation liquor.
Further, the black tea fungus fermentation membrane modifier is prepared by the following steps: (1) pre-cooling 90-110 parts by weight of mixed aqueous solution of 5 mass percent NaOH and 6 mass percent hydroxyethyl urea to-7 ℃; (2) rapidly adding 1-3 weight parts of black tea fungus fermentation membrane before the solution is not frozen, rapidly stirring at room temperature for 5min, and standing at-7 deg.C for 20min to obtain 1.5-3% black tea fungus fermentation membrane solution; (3) adding 20-35 parts by weight of chloroethanol into 100 parts by weight of black tea fungus fermentation membrane solution with the mass concentration of 1.5-3%, reacting for 2 hours at room temperature, heating to 50 ℃ for reaction for 2 hours, adding acetic acid for neutralization to neutrality, and stopping reaction; (4) after the solution after reaction is dialyzed, centrifuging for 10min at 400r/min for separation; (5) collecting supernatant, and vacuum drying to obtain black tea fungus fermentation membrane modified substance.
Further, the water-soluble camellia oleosa seed oil is prepared by the following steps: (1) adding 100 parts by weight of polyglycerol-10 and 1-2 parts by weight of saturated disodium hydrogen phosphate solution into a three-neck flask provided with a spherical reflux condenser pipe; (2) stirring in water bath at 60 ℃ for 1 h; (3) then, dropwise adding 12-20 parts by weight of camellia oleosa seed oil, adding 2 parts by weight of p-toluenesulfonic acid, and continuing to react for 1h at 60 ℃; (4) dropwise adding saturated sodium bicarbonate solution until the pH value of the solution is 6.5-7.5; (5) and (3) cooling the liquid, transferring the liquid into a separating funnel, and directly separating to obtain a lower-layer solution, namely the water-soluble camellia seed oil.
The invention has the following beneficial effects:
the black tea fungus fermentation liquor is added into the product, the black tea fungus fermentation liquor contains rich tea polyphenol, small molecular peptide, acetic acid, heat-resistant protein, polysaccharide and other antibacterial substances, has a good inhibition effect on common pathogenic bacteria such as escherichia coli, salmonella enteritidis, shigella dysenteriae, listeria monocytogenes, pseudomonas fluorescens, staphylococcus aureus and the like, has no drug resistance on the bacteria, is not added with artificial preservatives, has a good anticorrosion effect, has good biocompatibility of components and human skin, and has no uncomfortable effects such as allergy, stimulation and the like. Meanwhile, the black tea fungus fermentation liquor contains rich tea polyphenol, amino acid and other components, and has strong oxidation resistance. The product has the effects of repairing cells and protecting mucosa.
The product is added with a black tea fungus fermentation membrane modifier, the black tea fungus fermentation membrane is natural cellulose generated by black tea fungus fermentation, has the same chemical composition with plant cellulose, belongs to typical biological nano-cellulose, and has the characteristics of high water retention, high tensile strength and the like. The black tea fungus fermentation membrane modifier is modified on the basis of the black tea fungus fermentation membrane, cellulose polysaccharide and protein in the black tea fungus fermentation membrane are modified into active substances such as small molecular peptides, oligosaccharides and the like, so that the water retention property of the black tea fungus fermentation membrane modifier is maintained, the modified small molecular bioactive substances can be well combined with skin, and the black tea fungus fermentation membrane modifier has good effects of resisting bacteria, resisting wrinkles, whitening and the like.
The water-soluble oil tea seed oil is modified on the basis of the oil tea seed oil, and the water-insoluble oil tea seed oil is modified to be soluble in water, so that the oil tea seed oil can be matched with other components in the facial mask liquid, and the anti-aging and anti-oxidation effects of the facial mask liquid are improved.
The product is added with the fibroin hydrolysate, the active ingredients in the natural fibroin hydrolysate are released in layers, and can permeate into the dermis layer of the skin in 10 seconds, thereby promoting the synthesis of collagen, activating cells, improving the immunity of the cells, promoting the metabolism rate of the skin, helping to repair damaged skin tissues and adding the machine to the dull and tired skin, and further restoring the white and glossy skin in a very short time. Meanwhile, the fibroin can inhibit the generation of melanin more effectively, and the serine can also inhibit the activity of tyrosinase in the skin, so that the tyrosinase can be inhibited from generating melanin, and the effects of whitening and brightening the skin can be achieved
The black tea fungus fermentation facial mask liquid is prepared by extracting and dividing natural plants, is safe and reliable, can effectively clean and preserve moisture, can deeply nourish skin and repair damaged cells, and is a facial mask liquid product which can be used for a long time.
In addition, the invention has the advantages of easily obtained raw materials, easy operation, mild reaction conditions, obvious effect, low cost and the like.
Detailed Description
The present invention will be described in detail with reference to specific examples.
Example 1
The collagen peptide mask liquid is prepared from the following raw materials in parts by weight: 5 parts of black tea fungus fermentation liquor, 4 parts of collagen peptide, 1.5 parts of water-soluble camellia seed oil, 0.8 part of sclerotium rolfsii gum, 4 parts of gardenia hydrolat, 5 parts of glycerol, 1 part of hexanediol, 0.6 part of sodium hyaluronate, 0.5 part of black tea fungus fermentation membrane modifier and 78.1 parts of deionized water.
A preparation method of collagen peptide facial mask liquid comprises the following steps: (1) dissolving 0.5 weight part of black tea fungus fermentation membrane modifier with 78.1 weight parts of deionized water at normal temperature; (2) adding 4 parts by weight of collagen peptide and 0.6 part by weight of sodium hyaluronate, heating to 60 ℃, stirring to dissolve and uniformly mixing; (3) keeping the temperature at 60 ℃, adding 5 parts by weight of glycerol and 0.8 part by weight of sclerotium rolfsii gum, stirring to dissolve and uniformly mixing; (4) cooling to room temperature, sequentially adding 1.5 parts by weight of water-soluble camellia oleosa seed oil and 5 parts by weight of black tea fungus fermentation liquor, and uniformly mixing; (5) adding 4 parts by weight of gardenia hydrolat and 1 part by weight of hexanediol, uniformly mixing, and obtaining the mask liquid.
Further, the black tea fungus fermentation liquor is prepared by the following steps: mixing and boiling 2 parts by weight of black tea, 8 parts by weight of seaweed, 2 parts by weight of kelp, 45 parts by weight of white granulated sugar and 900 parts by weight of deionized water for 100min, standing, cooling, filtering, adding the deionized water into the filtrate to keep the filtrate at 900 parts by weight, uniformly mixing, adding the filtrate into a container, placing the container into a high-temperature sterilization and over-sterilization container for 20min, cooling to room temperature after sterilization, adding 45 parts by weight of black tea fungus mother liquor, sealing the container with gauze, fermenting for 7 days at normal temperature and normal pressure, and filtering with a screen to obtain black tea fungus fermentation liquor.
Further, the black tea fungus fermentation membrane modifier is prepared by the following steps: (1) pre-cooling 95 parts by weight of mixed aqueous solution of 5 mass percent NaOH and 6 mass percent hydroxyethyl urea to-7 ℃; (2) rapidly adding 2 parts by weight of black tea fungus fermentation membrane before the solution is not frozen, rapidly stirring at room temperature for 5min, and standing at-7 deg.C for 20min to obtain black tea fungus fermentation membrane solution with mass concentration of 2%; (3) adding 25 parts by weight of chloroethanol into 100 parts by weight of black tea fungus fermentation membrane solution with the mass concentration of 2%, reacting for 2 hours at room temperature, heating to 50 ℃ for reaction for 2 hours, adding acetic acid for neutralization to neutrality, and stopping reaction; (4) after the solution after reaction is dialyzed, centrifuging for 10min at 400r/min for separation; (5) collecting supernatant, and vacuum drying to obtain black tea fungus fermentation membrane modified substance.
Further, the water-soluble camellia oleosa seed oil is prepared by the following steps: (1) 100 parts by weight of polyglycerol-10 and 2 parts by weight of saturated disodium hydrogen phosphate solution are added into a three-neck flask provided with a spherical reflux condenser pipe; (2) stirring in water bath at 60 ℃ for 1 h; (3) then, 14 parts by weight of camellia seed oil is firstly dripped, and then 2 parts by weight of p-toluenesulfonic acid is added to continue to react for 1 hour at 60 ℃; (4) dropwise adding saturated sodium bicarbonate solution until the pH value of the solution is 6.5-7.5; (5) and (3) cooling the liquid, transferring the liquid into a separating funnel, and directly separating to obtain a lower-layer solution, namely the water-soluble camellia seed oil.
Example 2
The collagen peptide mask liquid is prepared from the following raw materials in parts by weight: 5 parts of black tea fungus fermentation liquor, 4.5 parts of collagen peptide, 1.8 parts of water-soluble camellia seed oil, 0.9 part of sclerotium rolfsii gum, 4 parts of gardenia hydrolat, 5 parts of glycerol, 0.9 part of hexanediol, 0.7 part of sodium hyaluronate, 0.3 part of black tea fungus fermentation membrane modifier and 76.9 parts of deionized water.
A preparation method of collagen peptide facial mask liquid comprises the following steps: (1) dissolving 0.3 weight part of black tea fungus fermentation membrane modifier with 76.9 weight parts of deionized water at normal temperature; (2) adding 4.5 parts by weight of collagen peptide and 0.7 part by weight of sodium hyaluronate, heating to 60 ℃, stirring to dissolve and uniformly mixing; (3) keeping the temperature at 60 ℃, adding 5 parts by weight of glycerol and 0.9 part by weight of sclerotium rolfsii gum, stirring to dissolve and uniformly mixing; (4) cooling to room temperature, sequentially adding 1.8 parts by weight of water-soluble camellia oleosa seed oil and 5 parts by weight of black tea fungus fermentation liquor, and uniformly mixing; (5) adding 4 parts by weight of gardenia hydrolat and 0.9 part by weight of hexanediol, uniformly mixing, and obtaining the mask liquid.
Further, the black tea fungus fermentation liquor is prepared by the following steps: mixing 3 parts by weight of black tea, 10 parts by weight of seaweed, 4 parts by weight of kelp, 50 parts by weight of white granulated sugar and 1000 parts by weight of deionized water, boiling for 110min, standing, cooling, filtering, adding deionized water into the filtrate to keep the filtrate at 1000 parts by weight, uniformly mixing, adding into a container, placing into a high-temperature sterilization and over-sterilization container for 20min, cooling to room temperature after sterilization, adding 50 parts by weight of black tea fungus mother liquor, sealing with gauze, fermenting at normal temperature and normal pressure for 8 days, and filtering with a screen to obtain black tea fungus fermentation liquor.
Further, the black tea fungus fermentation membrane modifier is prepared by the following steps: (1) pre-cooling 95 parts by weight of mixed aqueous solution of 5 mass percent NaOH and 6 mass percent hydroxyethyl urea to-7 ℃; (2) quickly adding 1.5 weight parts of black tea fungus fermentation membrane before the solution is not frozen, quickly stirring at room temperature for 5min, and standing at-7 deg.C for 20min to obtain 1.5-3% black tea fungus fermentation membrane solution; (3) adding 20 parts by weight of chloroethanol into 100 parts by weight of black tea fungus fermentation membrane solution with the mass concentration of 1.5%, reacting for 2 hours at room temperature, heating to 50 ℃ for reaction for 2 hours, adding acetic acid for neutralization to neutrality, and stopping reaction; (4) after the solution after reaction is dialyzed, centrifuging for 10min at 400r/min for separation; (5) collecting supernatant, and vacuum drying to obtain black tea fungus fermentation membrane modified substance.
Further, the water-soluble camellia oleosa seed oil is prepared by the following steps: (1) 100 parts by weight of polyglycerol-10 and 1.5 parts by weight of saturated disodium hydrogen phosphate solution are added into a three-necked flask provided with a spherical reflux condenser pipe; (2) stirring in water bath at 60 ℃ for 1 h; (3) then, dropwise adding 15 parts by weight of camellia oleosa seed oil, adding 2 parts by weight of p-toluenesulfonic acid, and continuing to react for 1 hour at 60 ℃; (4) dropwise adding saturated sodium bicarbonate solution until the pH value of the solution is 6.5; (5) and (3) cooling the liquid, transferring the liquid into a separating funnel, and directly separating to obtain a lower-layer solution, namely the water-soluble camellia seed oil.
Example 3
The collagen peptide mask liquid is prepared from the following raw materials in parts by weight: 7 parts of black tea fungus fermentation liquor, 3.5 parts of collagen peptide, 1.5 parts of water-soluble camellia seed oil, 0.8 part of sclerotium rolfsii gum, 4.5 parts of gardenia hydrolat, 6 parts of glycerol, 0.8 part of hexanediol, 0.6 part of sodium hyaluronate, 0.3 part of black tea fungus fermentation membrane modifier and 75 parts of deionized water.
A preparation method of collagen peptide facial mask liquid comprises the following steps: (1) dissolving 0.3 weight part of black tea fungus fermentation membrane modifier with 75 weight parts of deionized water at normal temperature; (2) adding 3.5 parts by weight of collagen peptide and 0.6 part by weight of sodium hyaluronate, heating to 60 ℃, stirring to dissolve and uniformly mixing; (3) keeping the temperature at 60 ℃, adding 6 parts by weight of glycerol and 0.8 part by weight of sclerotium rolfsii gum, stirring to dissolve and uniformly mixing; (4) cooling to room temperature, sequentially adding 1.5 parts by weight of water-soluble camellia oleosa seed oil and 7 parts by weight of black tea fungus fermentation liquor, and uniformly mixing; (5) adding 4.5 parts by weight of gardenia hydrolat and 0.8 part by weight of hexanediol, uniformly mixing, and obtaining the mask liquid.
Further, the black tea fungus fermentation liquor is prepared by the following steps: mixing 5 parts by weight of black tea, 10 parts by weight of seaweed, 5 parts by weight of kelp, 48 parts by weight of white granulated sugar and 1000 parts by weight of deionized water, boiling for 110min, standing, cooling, filtering, adding deionized water into the filtrate to keep the filtrate at 1000 parts by weight, uniformly mixing, adding into a container, placing into a high-temperature sterilization and over-sterilization container for 20min, cooling to room temperature after sterilization, adding 50 parts by weight of black tea fungus mother liquor, sealing with gauze, fermenting at normal temperature and normal pressure for 8 days, and filtering with a screen mesh to obtain black tea fungus fermentation liquor.
Further, the black tea fungus fermentation membrane modifier is prepared by the following steps: (1) precooling 100 parts by weight of mixed aqueous solution of NaOH with the mass concentration of 5% and hydroxyethyl urea with the mass concentration of 6% to-7 ℃; (2) rapidly adding 1-3 weight parts of black tea fungus fermentation membrane before the solution is not frozen, rapidly stirring at room temperature for 5min, and standing at-7 deg.C for 20min to obtain 3% black tea fungus fermentation membrane solution; (3) adding 30 parts by weight of chloroethanol into 100 parts by weight of black tea fungus fermentation membrane solution with the mass concentration of 3%, reacting for 2 hours at room temperature, heating to 50 ℃ for reaction for 2 hours, adding acetic acid for neutralization to neutrality, and stopping reaction; (4) after the solution after reaction is dialyzed, centrifuging for 10min at 400r/min for separation; (5) collecting supernatant, and vacuum drying to obtain black tea fungus fermentation membrane modified substance.
Further, the water-soluble camellia oleosa seed oil is prepared by the following steps: (1) 100 parts by weight of polyglycerol-10 and 1.5 parts by weight of saturated disodium hydrogen phosphate solution are added into a three-necked flask provided with a spherical reflux condenser pipe; (2) stirring in water bath at 60 ℃ for 1 h; (3) then, 18 parts by weight of camellia oleosa seed oil is firstly dripped, and then 2 parts by weight of p-toluenesulfonic acid is added to continue to react for 1 hour at 60 ℃; (4) dropwise adding saturated sodium bicarbonate solution until the pH value of the solution is 6.5-7.5; (5) and (3) cooling the liquid, transferring the liquid into a separating funnel, and directly separating to obtain a lower-layer solution, namely the water-soluble camellia seed oil.
Example 4
The collagen peptide mask liquid is prepared from the following raw materials in parts by weight: 7 parts of black tea fungus fermentation liquor, 4 parts of collagen peptide, 1.8 parts of water-soluble camellia seed oil, 0.8 part of sclerotium rolfsii gum, 4 parts of gardenia hydrolat, 5 parts of glycerol, 0.8 part of hexanediol, 0.5 part of sodium hyaluronate, 0.4 part of black tea fungus fermentation membrane modifier and 75.7 parts of deionized water.
A preparation method of collagen peptide facial mask liquid comprises the following steps: (1) dissolving 0.4 weight part of black tea fungus fermentation membrane modifier with 75.7 weight parts of deionized water at normal temperature; (2) adding 4 parts by weight of collagen peptide and 0.5 part by weight of sodium hyaluronate, heating to 60 ℃, stirring to dissolve and uniformly mixing; (3) keeping the temperature at 60 ℃, adding 5 parts by weight of glycerol and 0.8 part by weight of sclerotium rolfsii gum, stirring to dissolve and uniformly mixing; (4) cooling to room temperature, sequentially adding 1.8 parts by weight of water-soluble camellia oleosa seed oil and 7 parts by weight of black tea fungus fermentation liquor, and uniformly mixing; (5) adding 3 parts by weight of gardenia hydrolat and 0.3 part by weight of hexanediol, uniformly mixing, and obtaining the mask liquid.
Further, the black tea fungus fermentation liquor is prepared by the following steps: mixing 6 parts by weight of black tea, 11 parts by weight of seaweed, 4 parts by weight of kelp, 50 parts by weight of white granulated sugar and 1100 parts by weight of deionized water, boiling for 110min, standing, cooling, filtering, adding deionized water into the filtrate to keep the weight of the filtrate at 1100 parts, uniformly mixing, adding into a container, placing into a high-temperature sterilization and over-sterilization container for 20min, cooling to room temperature after sterilization, adding 55 parts by weight of black tea fungus mother liquor, sealing with gauze, fermenting at normal temperature and normal pressure for 8 days, and filtering with a screen to obtain black tea fungus fermentation liquor.
Further, the black tea fungus fermentation membrane modifier is prepared by the following steps: (1) precooling 100 parts by weight of mixed aqueous solution of NaOH with the mass concentration of 5% and hydroxyethyl urea with the mass concentration of 6% to-7 ℃; (2) rapidly adding 2 parts by weight of black tea fungus fermentation membrane before the solution is not frozen, rapidly stirring at room temperature for 5min, and standing at-7 deg.C for 20min to obtain black tea fungus fermentation membrane solution with mass concentration of 2%; (3) adding 30 parts by weight of chloroethanol into 100 parts by weight of black tea fungus fermentation membrane solution with the mass concentration of 2%, reacting for 2 hours at room temperature, heating to 50 ℃ for reaction for 2 hours, adding acetic acid for neutralization to neutrality, and stopping reaction; (4) after the solution after reaction is dialyzed, centrifuging for 10min at 400r/min for separation; (5) collecting supernatant, and vacuum drying to obtain black tea fungus fermentation membrane modified substance.
Further, the water-soluble camellia oleosa seed oil is prepared by the following steps: (1) 100 parts by weight of polyglycerol-10 and 2 parts by weight of saturated disodium hydrogen phosphate solution are added into a three-neck flask provided with a spherical reflux condenser pipe; (2) stirring in water bath at 60 ℃ for 1 h; (3) then, 19 parts by weight of camellia oleosa seed oil is firstly dripped, and then 2 parts by weight of p-toluenesulfonic acid is added to continue to react for 1 hour at 60 ℃; (4) dropwise adding saturated sodium bicarbonate solution until the pH value of the solution is 6.5-7.5; (5) and (3) cooling the liquid, transferring the liquid into a separating funnel, and directly separating to obtain a lower-layer solution, namely the water-soluble camellia seed oil.
Example 5
The collagen peptide mask liquid is prepared from the following raw materials in parts by weight: 10 parts of black tea fungus fermentation liquor, 3.5 parts of collagen peptide, 1.5 parts of water-soluble camellia seed oil, 0.8 part of sclerotium rolfsii gum, 4.5 parts of gardenia hydrolat, 5 parts of glycerol, 0.9 part of hexanediol, 0.5 part of sodium hyaluronate, 0.2 part of black tea fungus fermentation membrane modifier and 73.1 parts of deionized water.
A preparation method of collagen peptide facial mask liquid comprises the following steps: (1) dissolving 0.2 weight part of black tea fungus fermentation membrane modifier with 73.1 weight parts of deionized water at normal temperature; (2) adding 3.5 parts by weight of collagen peptide and 0.5 part by weight of sodium hyaluronate, heating to 60 ℃, stirring to dissolve and uniformly mixing; (3) keeping the temperature at 60 ℃, adding 5 parts by weight of glycerol and 0.8 part by weight of sclerotium rolfsii gum, stirring to dissolve and uniformly mixing; (4) cooling to room temperature, sequentially adding 1.5 parts by weight of water-soluble camellia oleosa seed oil and 10 parts by weight of black tea fungus fermentation liquor, and uniformly mixing; (5) adding 4.5 parts by weight of gardenia hydrolat and 0.9 part by weight of hexanediol, uniformly mixing, and obtaining the mask liquid.
Further, the black tea fungus fermentation liquor is prepared by the following steps: mixing 8 parts by weight of black tea, 12 parts by weight of seaweed, 6 parts by weight of kelp, 55 parts by weight of white granulated sugar and 1200 parts by weight of deionized water, boiling for 120min, standing, cooling, filtering, adding the deionized water into the filtrate to keep the filtrate at 1200 parts by weight, uniformly mixing, adding into a container, placing into a high-temperature sterilization and over-sterilization container for 20min, cooling to room temperature after sterilization, adding 60 parts by weight of black tea fungus mother liquor, sealing with gauze, fermenting at normal temperature and normal pressure for 9 days, and filtering with a screen to obtain black tea fungus fermentation liquor.
Further, the black tea fungus fermentation membrane modifier is prepared by the following steps: (1) pre-cooling 110 parts by weight of mixed aqueous solution of 5 mass percent NaOH and 6 mass percent hydroxyethyl urea to-7 ℃; (2) quickly adding 3 parts by weight of black tea fungus fermentation membrane before the solution is not frozen, quickly stirring at room temperature for 5min, and standing at-7 ℃ for 20min to obtain a black tea fungus fermentation membrane solution with the mass concentration of 3%; (3) adding 35 parts by weight of chloroethanol into 100 parts by weight of black tea fungus fermentation membrane solution with the mass concentration of 3%, reacting for 2 hours at room temperature, heating to 50 ℃ for reaction for 2 hours, adding acetic acid for neutralization to neutrality, and stopping reaction; (4) after the solution after reaction is dialyzed, centrifuging for 10min at 400r/min for separation; (5) collecting supernatant, and vacuum drying to obtain black tea fungus fermentation membrane modified substance.
Further, the water-soluble camellia oleosa seed oil is prepared by the following steps: (1) 100 parts by weight of polyglycerol-10 and 2 parts by weight of saturated disodium hydrogen phosphate solution are added into a three-neck flask provided with a spherical reflux condenser pipe; (2) stirring in water bath at 60 ℃ for 1 h; (3) then, dropwise adding 20 parts by weight of camellia oleosa seed oil, adding 2 parts by weight of p-toluenesulfonic acid, and continuing to react for 1 hour at 60 ℃; (4) dropwise adding saturated sodium bicarbonate solution until the pH value of the solution is 6.5-7.5; (5) and (3) cooling the liquid, transferring the liquid into a separating funnel, and directly separating to obtain a lower-layer solution, namely the water-soluble camellia seed oil.
Example 6:
the collagen peptide mask liquid is prepared from the following raw materials in parts by weight: 10 parts of black tea fungus fermentation liquor, 4 parts of collagen peptide, 1.8 parts of water-soluble camellia seed oil, 0.9 part of sclerotium rolfsii gum, 4.5 parts of gardenia hydrolat, 5 parts of glycerol, 0.8 part of hexanediol, 0.7 part of sodium hyaluronate, 0.2 part of black tea fungus fermentation membrane modifier and 72.1 parts of deionized water.
A preparation method of collagen peptide facial mask liquid comprises the following steps: (1) dissolving 0.2 weight part of black tea fungus fermentation membrane modifier with 72.1 weight parts of deionized water at normal temperature; (2) adding 4 parts by weight of collagen peptide and 0.7 part by weight of sodium hyaluronate, heating to 60 ℃, stirring to dissolve and uniformly mixing; (3) keeping the temperature at 60 ℃, adding 5 parts by weight of glycerol and 0.9 part by weight of sclerotium rolfsii gum, stirring to dissolve and uniformly mixing; (4) cooling to room temperature, sequentially adding 1.8 parts by weight of water-soluble camellia oleosa seed oil and 10 parts by weight of black tea fungus fermentation liquor, and uniformly mixing; (5) adding 4.5 parts by weight of gardenia hydrolat and 0.8 part by weight of hexanediol, uniformly mixing, and obtaining the mask liquid.
Further, the black tea fungus fermentation liquor is prepared by the following steps: mixing 6 parts by weight of black tea, 11 parts by weight of seaweed, 4 parts by weight of kelp, 50 parts by weight of white granulated sugar and 1100 parts by weight of deionized water, boiling for 110min, standing, cooling, filtering, adding deionized water into the filtrate to keep the weight of the filtrate at 1100 parts, uniformly mixing, adding into a container, placing into a high-temperature sterilization and over-sterilization container for 20min, cooling to room temperature after sterilization, adding 55 parts by weight of black tea fungus mother liquor, sealing with gauze, fermenting at normal temperature and normal pressure for 8 days, and filtering with a screen to obtain black tea fungus fermentation liquor.
Further, the black tea fungus fermentation membrane modifier is prepared by the following steps: (1) precooling 100 parts by weight of mixed aqueous solution of NaOH with the mass concentration of 5% and hydroxyethyl urea with the mass concentration of 6% to-7 ℃; (2) rapidly adding 2 parts by weight of black tea fungus fermentation membrane before the solution is not frozen, rapidly stirring at room temperature for 5min, and standing at-7 deg.C for 20min to obtain black tea fungus fermentation membrane solution with mass concentration of 2%; (3) adding 30 parts by weight of chloroethanol into 100 parts by weight of black tea fungus fermentation membrane solution with the mass concentration of 2%, reacting for 2 hours at room temperature, heating to 50 ℃ for reaction for 2 hours, adding acetic acid for neutralization to neutrality, and stopping reaction; (4) after the solution after reaction is dialyzed, centrifuging for 10min at 400r/min for separation; (5) collecting supernatant, and vacuum drying to obtain black tea fungus fermentation membrane modified substance.
Further, the water-soluble camellia oleosa seed oil is prepared by the following steps: (1) 100 parts by weight of polyglycerol-10 and 2 parts by weight of saturated disodium hydrogen phosphate solution are added into a three-neck flask provided with a spherical reflux condenser pipe; (2) stirring in water bath at 60 ℃ for 1 h; (3) then, 19 parts by weight of camellia oleosa seed oil is firstly dripped, and then 2 parts by weight of p-toluenesulfonic acid is added to continue to react for 1 hour at 60 ℃; (4) dropwise adding saturated sodium bicarbonate solution until the pH value of the solution is 6.5-7.5; (5) and (3) cooling the liquid, transferring the liquid into a separating funnel, and directly separating to obtain a lower-layer solution, namely the water-soluble camellia seed oil.
Example 7:
the collagen peptide mask liquid is prepared from the following raw materials in parts by weight: 11 parts of black tea fungus fermentation liquor, 4 parts of collagen peptide, 1.5 parts of water-soluble camellia seed oil, 0.8 part of sclerotium rolfsii gum, 4 parts of gardenia hydrolat, 5 parts of glycerol, 0.8 part of hexanediol, 0.5 part of sodium hyaluronate, 0.3 part of black tea fungus fermentation membrane modifier and 72.1 parts of deionized water.
A preparation method of collagen peptide facial mask liquid comprises the following steps: (1) dissolving 0.3 weight part of black tea fungus fermentation membrane modifier with 72.1 weight parts of deionized water at normal temperature; (2) adding 4 parts by weight of collagen peptide and 0.5 part by weight of sodium hyaluronate, heating to 60 ℃, stirring to dissolve and uniformly mixing; (3) keeping the temperature at 60 ℃, adding 5 parts by weight of glycerol and 0.8 part by weight of sclerotium rolfsii gum, stirring to dissolve and uniformly mixing; (4) cooling to room temperature, sequentially adding 1.5 parts by weight of water-soluble camellia oleosa seed oil and 11 parts by weight of black tea fungus fermentation liquor, and uniformly mixing; (5) adding 4 parts by weight of gardenia hydrolat and 0.8 part by weight of hexanediol, uniformly mixing, and obtaining the mask liquid.
Further, the black tea fungus fermentation liquor is prepared by the following steps: mixing 8 parts by weight of black tea, 12 parts by weight of seaweed, 6 parts by weight of kelp, 55 parts by weight of white granulated sugar and 1200 parts by weight of deionized water, boiling for 120min, standing, cooling, filtering, adding the deionized water into the filtrate to keep the filtrate at 1200 parts by weight, uniformly mixing, adding into a container, placing into a high-temperature sterilization and over-sterilization container for 20min, cooling to room temperature after sterilization, adding 60 parts by weight of black tea fungus mother liquor, sealing with gauze, fermenting at normal temperature and normal pressure for 9 days, and filtering with a screen to obtain black tea fungus fermentation liquor.
Further, the black tea fungus fermentation membrane modifier is prepared by the following steps: (1) pre-cooling 110 parts by weight of mixed aqueous solution of 5 mass percent NaOH and 6 mass percent hydroxyethyl urea to-7 ℃; (2) quickly adding 3 parts by weight of black tea fungus fermentation membrane before the solution is not frozen, quickly stirring at room temperature for 5min, and standing at-7 ℃ for 20min to obtain a black tea fungus fermentation membrane solution with the mass concentration of 3%; (3) adding 35 parts by weight of chloroethanol into 100 parts by weight of black tea fungus fermentation membrane solution with the mass concentration of 3%, reacting for 2 hours at room temperature, heating to 50 ℃ for reaction for 2 hours, adding acetic acid for neutralization to neutrality, and stopping reaction; (4) after the solution after reaction is dialyzed, centrifuging for 10min at 400r/min for separation; (5) collecting supernatant, and vacuum drying to obtain black tea fungus fermentation membrane modified substance.
Further, the water-soluble camellia oleosa seed oil is prepared by the following steps: (1) 100 parts by weight of polyglycerol-10 and 2 parts by weight of saturated disodium hydrogen phosphate solution are added into a three-neck flask provided with a spherical reflux condenser pipe; (2) stirring in water bath at 60 ℃ for 1 h; (3) then, dropwise adding 20 parts by weight of camellia oleosa seed oil, adding 2 parts by weight of p-toluenesulfonic acid, and continuing to react for 1 hour at 60 ℃; (4) dropwise adding saturated sodium bicarbonate solution until the pH value of the solution is 6.5-7.5; (5) and (3) cooling the liquid, transferring the liquid into a separating funnel, and directly separating to obtain a lower-layer solution, namely the water-soluble camellia seed oil.
The facial mask liquid prepared in the example 1 is used for testing to show that the facial mask liquid has the effects of effectively moisturizing, deeply nourishing skin, relieving allergy, repairing damaged cells, improving dull complexion and improving wrinkles.
The facial mask liquid has an obvious moisturizing effect, after 20 female volunteers use the facial mask liquid for 3 weeks, the facial mask liquid is detected by using a VISIA full-face analyzer to find that the facial mask liquid has obvious improvement on skin color, and the results are shown in Table 1 by taking common glycerin moisturizing liquid as a control.
TABLE 1 skin hydration Change
The facial mask liquid has obvious effects of resisting wrinkles and the like, 20 female volunteers use the facial mask liquid for 8 weeks, and find that the facial mask liquid has obvious improvement on the number of wrinkles by using a VISIA full-face analyzer, and the results are shown in Table 2 by using common glycerin moisturizing liquid as a control.
TABLE 2 variation in the number of skin wrinkles
The facial mask liquid has obvious anti-allergy and relieving effects, 20 female volunteers use the facial mask liquid for 8 weeks, and the improvement of the lactic acid stimulation pain degree after using the facial mask liquid is examined by taking common glycerin moisturizing liquid as a control, and the results are shown in table 3.
TABLE 3 reduction of lactic acid stimulated pain levels
The above description is only an embodiment of the present invention, and not intended to limit the scope of the present invention, and all modifications of equivalent structures and equivalent processes, which are made by the present specification, or directly or indirectly applied to other related technical fields, are included in the scope of the present invention.
Claims (4)
1. The collagen peptide mask liquid is characterized by being prepared from the following raw materials in parts by weight: 5-15 parts of black tea fungus fermentation liquor, 2.5-5 parts of collagen peptide, 1-2 parts of water-soluble camellia seed oil, 0.8-1.2 parts of sclerotium rolfsii gum, 3-5 parts of gardenia hydrolat, 5-8 parts of glycerol, 0.5-1 part of hexanediol, 0.5-1 part of sodium hyaluronate, 0.2-1 part of black tea fungus fermentation membrane modifier and 60-80 parts of deionized water; the black tea fungus fermentation membrane modifier is prepared from the following raw materials in parts by weight: 100 parts of black tea fungus fermentation membrane solution with the mass concentration of 1.5-3%, 20-35 parts of chloroethanol and 2-10 parts of acetic acid; the black tea fungus fermentation membrane solution is prepared from the following raw materials in parts by weight: 90-110 parts of mixed aqueous solution of NaOH with the mass concentration of 5% and hydroxyethyl urea with the mass concentration of 6% and 1-3 parts of black tea fungus fermentation membrane; the water-soluble camellia seed oil is prepared from the following raw materials in parts by weight: polyglycerol-10100 parts; 1-2 parts of saturated disodium hydrogen phosphate solution; 12-20 parts of camellia seed oil; 2 parts of p-toluenesulfonic acid; 1-3 parts of saturated sodium bicarbonate solution.
2. The collagen peptide mask liquid as claimed in claim 1, wherein the black tea fungus fermentation liquid is prepared from the following raw materials in parts by weight: 2-8 parts of black tea, 8-12 parts of seaweed, 2-6 parts of kelp, 45-55 parts of white granulated sugar, 900 parts of deionized water and 1200 parts of black tea fungus mother liquor and 45-60 parts of black tea fungus mother liquor.
3. The preparation method of the collagen peptide facial mask liquid is characterized by comprising the following steps: (1) dissolving 0.2-1 part by weight of black tea fungus fermentation membrane modifier with 60-80 parts by weight of deionized water at normal temperature; (2) adding 2.5-5 parts by weight of collagen peptide and 0.5-1 part by weight of sodium hyaluronate, heating to 60 ℃, stirring to dissolve and uniformly mixing; (3) keeping the temperature at 60 ℃, adding 5-8 parts by weight of glycerol and 0.8-1.2 parts by weight of sclerotium rolfsii gum, stirring to dissolve and uniformly mixing; (4) cooling to room temperature, sequentially adding 1-2 parts by weight of water-soluble camellia oleosa seed oil and 5-15 parts by weight of black tea fungus fermentation liquor, and uniformly mixing; (5) adding 3-5 parts by weight of gardenia hydrolat and 0.5-1 part by weight of hexanediol, uniformly mixing, and obtaining the mask liquid; the black tea fungus fermentation membrane modifier is prepared by the following steps: (1) pre-cooling 90-110 parts by weight of mixed aqueous solution of 5 mass percent NaOH and 6 mass percent hydroxyethyl urea to-7 ℃; (2) rapidly adding 1-3 weight parts of black tea fungus fermentation membrane before the solution is not frozen, rapidly stirring at room temperature for 5min, and standing at-7 deg.C for 20min to obtain 1.5-3% black tea fungus fermentation membrane solution; (3) adding 20-35 parts by weight of chloroethanol into 100 parts by weight of black tea fungus fermentation membrane solution with the mass concentration of 1.5-3%, reacting for 2 hours at room temperature, heating to 50 ℃ for reaction for 2 hours, adding acetic acid for neutralization to neutrality, and stopping reaction; (4) after the solution after reaction is dialyzed, centrifuging for 10min at 400r/min for separation; (5) collecting supernatant, and vacuum drying to obtain black tea fungus fermentation membrane modified substance; the water-soluble camellia oleosa seed oil is prepared by the following steps: (1) adding 100 parts by weight of polyglycerol-10 and 1-2 parts by weight of saturated disodium hydrogen phosphate solution into a three-neck flask provided with a spherical reflux condenser pipe; (2) stirring in water bath at 60 ℃ for 1 h; (3) then, dropwise adding 12-20 parts by weight of camellia oleosa seed oil, adding 2 parts by weight of p-toluenesulfonic acid, and continuing to react for 1h at 60 ℃; (4) dropwise adding saturated sodium bicarbonate solution until the pH value of the solution is 6.5-7.5; (5) and (3) cooling the liquid, transferring the liquid into a separating funnel, and directly separating to obtain a lower-layer solution, namely the water-soluble camellia seed oil.
4. The method for preparing the collagen peptide mask liquid according to claim 3, wherein the black tea fungus fermentation liquid is prepared by the following steps: mixing and boiling black tea of 2-8 parts by weight, seaweed of 8-12 parts by weight, kelp of 2-6 parts by weight, white granulated sugar of 45-55 parts by weight and deionized water of 900-1200 parts by weight for 120min, standing, cooling, filtering, adding deionized water into the filtrate to keep the filtrate at 900-1200 parts by weight, uniformly mixing, adding into a container, placing into a high-temperature sterilization and re-sterilization for 20min, cooling to room temperature after the sterilization is finished, adding black tea fungus mother liquor of 45-60 parts by weight, sealing with gauze, fermenting at normal temperature and normal pressure for 6-9 days, and filtering with a screen to obtain black tea fungus fermentation liquor.
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