CN111870541A - Herbal whitening compound composition, mask and preparation method thereof - Google Patents

Herbal whitening compound composition, mask and preparation method thereof Download PDF

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Publication number
CN111870541A
CN111870541A CN202010903839.1A CN202010903839A CN111870541A CN 111870541 A CN111870541 A CN 111870541A CN 202010903839 A CN202010903839 A CN 202010903839A CN 111870541 A CN111870541 A CN 111870541A
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China
Prior art keywords
weight
extract
mask
herbal
whitening compound
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CN202010903839.1A
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Chinese (zh)
Inventor
易斌
郝姗姗
陈素梅
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Jianchang Jiangxi Gang Pharmaceutical Co ltd
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Jianchang Jiangxi Gang Pharmaceutical Co ltd
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Priority to CN202010903839.1A priority Critical patent/CN111870541A/en
Publication of CN111870541A publication Critical patent/CN111870541A/en
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/02Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/0212Face masks
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/67Vitamins
    • A61K8/673Vitamin B group
    • A61K8/675Vitamin B3 or vitamin B3 active, e.g. nicotinamide, nicotinic acid, nicotinyl aldehyde
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/67Vitamins
    • A61K8/676Ascorbic acid, i.e. vitamin C
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9728Fungi, e.g. yeasts
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/02Preparations for care of the skin for chemically bleaching or whitening the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions
    • A61K2800/5922At least two compounds being classified in the same subclass of A61K8/18

Abstract

The invention provides a herbal whitening compound composition, a mask and a preparation method thereof; the herbal whitening compound composition comprises the following components: 0.02-1 part by weight of cistanche extract; 0.02-1 part by weight of a coastal angelica extract; 0.02-1 part by weight of ganoderma lucidum extract; 0.02-1 part by weight of a sea buckthorn extract; 0.02-1 part by weight of licorice extract. Compared with the prior art, the five traditional Chinese medicine components of the cistanche deserticola extract, the coastal angelica extract, the ganoderma lucidum extract, the sea buckthorn extract and the liquorice extract are compounded according to a certain proportion, are mutually supplemented and synergized, and the obtained herbal whitening compound composition has excellent whitening effect, high safety and no toxicity or stimulation to human bodies; meanwhile, the essence added with the herbal whitening compound composition is matched with a specific mask base cloth, so that the use feeling and the efficacy are better.

Description

Herbal whitening compound composition, mask and preparation method thereof
Technical Field
The invention relates to the technical field of daily chemical products, in particular to a herbal whitening compound composition, a mask and a preparation method thereof.
Background
The raw materials with whitening effect are mainly divided into chemical whitening agents, biological whitening agents and natural plant whitening agents. The chemical whitening agent has obvious effect, mainly takes direct damage to melanocytes as an action way (such as hydroquinone), has certain cytotoxicity and certain injury to human bodies; the biological whitening agent has relatively safe sources and considerable effects, is one of the hot spots (such as 3-o-ethyl ascorbic acid) of recent research, but most of the biological whitening agents have longer production period, low yield and high cost; the whitening agent derived from natural plants has better safety compared with chemical whitening agents, is easier to obtain compared with biological whitening agents and has low cost.
With the consumer's advocation of herbal products, the research reports of using herbal extracts to prepare whitening agents have increased in recent years. At present, the requirements of consumers for the herbal whitening ingredients are mainly reflected in that: (1) the required effect is obvious; (2) has high safety, and is non-toxic and non-irritant to human skin. The active ingredients from multiple herbal plants are compounded together, so that the composition can play a role in multiple ways from multiple target points, the most scientific cost performance is found through various tests, the composition has an excellent effect, and the whitening effect is really achieved. Meanwhile, safety tests are passed to ensure the safety of the composition.
With the improvement of national economic level, cosmetics become necessities of daily life of people, and the proportion of the cost spent on the cosmetics by people is gradually increased. The number of the facial masks added with the plant whitening components is also large, but most of the research objects are facial mask essence, and the interaction between the facial mask essence and a carrier facial mask base cloth is not considered. In fact, factors such as adsorption capacity, air permeability and affinity of the mask base cloth have an important influence on the use feeling and the efficacy of the mask essence.
Disclosure of Invention
In view of the above, the invention aims to provide a herbal whitening compound composition, a mask and a preparation method thereof, and the herbal whitening compound composition provided by the invention has excellent whitening effect, high safety and no toxicity or irritation to a human body; meanwhile, the essence added with the herbal whitening compound composition is matched with a specific mask base cloth, so that the use feeling and the efficacy are better.
The invention provides a herbal whitening compound composition which comprises the following components:
0.02-1 part by weight of cistanche extract;
0.02-1 part by weight of a coastal angelica extract;
0.02-1 part by weight of ganoderma lucidum extract;
0.02-1 part by weight of a sea buckthorn extract;
0.02-1 part by weight of licorice extract.
Preferably, the method further comprises the following steps:
0.3-5 parts by weight of nicotinamide;
0.01 to 2 parts by weight of ascorbyl glucoside.
The invention also provides a herbal whitening compound mask which consists of essence and mask base cloth;
the essence is prepared from the following raw materials:
76.412-88.005 parts by weight of a solvent;
0-11.75 parts by weight of a humectant;
0-1 part by weight of a solubilizer;
0.41-12 parts by weight of the compound composition;
0.22-8.578 parts by weight of a skin conditioner;
0.1-0.8 parts of thickening agent;
0.02-0.1 part by weight of a chelating agent;
0-0.05 parts by weight of an aromatic;
0.1-0.6 parts by weight of a preservative;
0-0.3 part of pH regulator;
the compound composition is the herbal whitening compound composition in the technical scheme;
the facial mask base cloth is made of cuprammonium fibers, hydrogel, pure cotton fibers, biological fibers, viscose, wormwood fibers, bamboo charcoal fibers or gel tencel.
Preferably, the humectant is selected from one or more of glycerin, sodium hyaluronate, trehalose, hydrolyzed sodium hyaluronate, hydroxyethyl urea, and glyceryl polyether-26.
Preferably, the solubilizer is selected from one or more of PEG-40 hydrogenated castor oil, PEG-60 hydrogenated castor oil, PPG-26-butanol polyether and Tween-20.
Preferably, the skin conditioning agent is selected from one or more of allantoin, Althaea officinalis root extract, Portulaca oleracea extract, BPN-desoro 1600solution, carnosine, dipeptide diaminobutyrylbenzylamide diacetate, Prolevis, dipotassium glycyrrhizinate, sodium metabisulfite, arginine, ethylhexyl glycerol, and p-hydroxyacetophenone.
Preferably, the thickening agent is selected from one or more of carbomer, polyacrylic acid, xanthan gum, acrylate/C10-30 alkanol acrylate cross-linked polymer and hydroxyethyl cellulose.
Preferably, the chelating agent is selected from disodium EDTA, trisodium EDTA or tetrasodium EDTA.
Preferably, the pH adjusting agent is selected from citric acid and/or sodium citrate.
The invention also provides a preparation method of the herbal whitening compound mask, which comprises the following steps:
a) uniformly mixing a solvent, a humectant, a solubilizer, a skin conditioner, a thickening agent, a chelating agent, an aromatic and a pH regulator in a vacuum emulsification tank; then adding the compound composition and the preservative to be uniformly dispersed; then cooling to 32-35 ℃, defoaming, filtering and discharging to obtain essence;
b) filling the essence obtained in the step a) and mask base cloth together to obtain the herbal whitening compound mask.
The invention provides a herbal whitening compound composition, a mask and a preparation method thereof; the herbal whitening compound composition comprises the following components: 0.02-1 part by weight of cistanche extract; 0.02-1 part by weight of a coastal angelica extract; 0.02-1 part by weight of ganoderma lucidum extract; 0.02-1 part by weight of a sea buckthorn extract; 0.02-1 part by weight of licorice extract. Compared with the prior art, the five traditional Chinese medicine components of the cistanche deserticola extract, the coastal angelica extract, the ganoderma lucidum extract, the sea buckthorn extract and the liquorice extract are compounded according to a certain proportion, are mutually supplemented and synergized, and the obtained herbal whitening compound composition has excellent whitening effect, high safety and no toxicity or stimulation to human bodies; meanwhile, the essence added with the herbal whitening compound composition is matched with a specific mask base cloth, so that the use feeling and the efficacy are better.
In addition, the preparation method provided by the invention has the advantages of simple process, mild conditions, easiness in operation control, suitability for large-scale production and wide application prospect.
Detailed Description
The technical solutions of the present invention will be described clearly and completely with reference to the following embodiments of the present invention, and it should be understood that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
The invention provides a herbal whitening compound composition which comprises the following components:
0.02-1 part by weight of cistanche extract;
0.02-1 part by weight of a coastal angelica extract;
0.02-1 part by weight of ganoderma lucidum extract;
0.02-1 part by weight of a sea buckthorn extract;
0.02-1 part by weight of licorice extract.
In the present invention, the herbal whitening compound composition comprises a cistanche extract, a angelica sinensis extract, a ganoderma lucidum extract, a hippophae rhamnoides extract and a licorice extract, and preferably further comprises:
0.3-5 parts by weight of nicotinamide;
0.01 to 2 parts by weight of ascorbyl glucoside. In the invention, the five traditional Chinese medicine components in the herbal whitening compound composition are used in combination with nicotinamide and ascorbyl glucoside, so that a synergistic effect can be further generated, and the whitening effect is enhanced. On the basis, the herbal whitening compound composition preferably comprises a cistanche extract, a angelica sinensis extract, a ganoderma lucidum extract, a sea buckthorn extract, a licorice extract, nicotinamide and ascorbyl glucoside.
The sources of the cistanche deserticola extract, the angelica sinensis extract, the ganoderma lucidum extract, the sea buckthorn extract, the licorice extract, the nicotinamide and the ascorbyl glucoside are not particularly limited in the present invention, and commercially available products well known to those skilled in the art can be used.
In the invention, the cistanche salsa extract is extracted by a conventional method and is available on the market. Cistanche salsa is a rare and old traditional Chinese medicine, and is preferably fleshy, thick and long, brown and moist; because the meat quality is oily, the medicinal value is high, the nourishing curative effect is strong, and the meat is generated near desert, the ginseng is called desert ginseng; the cosmetic is prepared from dried meat stem. The cistanche deserticola extract has the inhibition effect on tyrosinase, has the effect of whitening the skin and can be used in whitening cosmetics; has excellent water holding capacity, can be used in moisture-retaining cosmetics for preventing and treating dry skin and preventing wrinkles and fine lines.
In the invention, the herbal whitening compound composition comprises 0.02-1 part by weight of cistanche deserticola extract, preferably 0.02 part by weight, 0.06 part by weight, 0.1 part by weight, 0.3 part by weight, 0.5 part by weight, 0.8 part by weight, 1 part by weight, more preferably 0.5 part by weight.
In the invention, the angelica maritima extract is extracted by a conventional method and is available on the market. Angelica maritima is known under the Japanese name "アシタバ (Angelica keiskei)" and is a cold-resistant perennial plant belonging to this country; probably because of the unique chalcone component in the angelica sinensis, local residents have habits and customs to regard the chalcone component as a main assistant and minister which can make people more healthy and prolong life; coastal angelica is a large herbaceous plant mainly growing in the middle area of japan, and the roots, leaves, and stems thereof are used for pharmaceutical preparations; in vitro studies have shown that Angelica maritima has antioxidant, anti-inflammatory and antimicrobial properties.
In the invention, the herbal whitening compound composition comprises 0.02-1 part by weight of the angelica maritima extract, preferably 0.02 part by weight, 0.08 part by weight, 0.2 part by weight, 0.3 part by weight, 0.4 part by weight, 0.5 part by weight, 0.7 part by weight, 1 part by weight, and more preferably 0.2 part by weight.
In the invention, the ganoderma lucidum extract is extracted by a conventional method and is available on the market. Ganoderma lucidum (Ganodermalucidum) also known as Danzhi, which is called Ganoderma lucidum folk, is one of the best types of traditional Chinese medicines. Ganoderma has six kinds of purple, red, green, yellow, white and black, but the cosmetics can only adopt Ganoderma sinensis and Ganoderma lucidum, which are the whole plant of Ganoderma sinensis or Ganoderma lucidum of the family Polyporaceae. The compendium of materia medica records ganoderma lucidum: cure all kinds of diseases, the function should be tested, the effective of Ling Tong Shen, so named Shen Zhi, also named Shen Lu Chi Zhi. At present, ganoderma lucidum is officially collected and carried by national formulary as a medicine, is a new resource food approved by the country, has no toxic or side effect, and can be used as both medicine and food. The Ganoderma lucidum extract has good activation effect on aromatase, and can be used for anti-aging products by combining the anti-oxygen property; the Ganoderma lucidum extract has an activating effect on luciferase, shows that the Ganoderma lucidum extract has anti-inflammatory effect, and can be used for treating skin inflammation; the inhibition of tyrosinase by Ganoderma lucidum extract is indicated to be useful in skin whitening cosmetics.
In the invention, the herbal whitening compound composition comprises 0.02-1 part by weight of ganoderma lucidum extract, preferably 0.02 part by weight, 0.08 part by weight, 0.1 part by weight, 0.2 part by weight, 0.4 part by weight, 0.5 part by weight, 0.6 part by weight, 1 part by weight, more preferably 0.2 part by weight.
In the invention, the sea buckthorn extract is extracted by a conventional method and is available on the market. Seabuckthorn (Hippophaerhamnoides) is shrub or small arbor of the genus hippophae of the family elaeagnus, named as hippophae rhamnoides, black thorn, sour thorn and the like, is mainly distributed in more than ten provinces such as northwest China, northeast China, southwest China and the like, is a main distribution area of seabuckthorn in Sichuan China, Tibet, Yunnan China and the like, and is the country with the most abundant seabuckthorn resources; the fruits, leaves, roots, seeds and stems of the sea buckthorn are all medicinal; the cosmetic is mainly prepared from fructus Hippophae. The sea buckthorn extract contains abundant vitamins, polysaccharides, amino acids, organic acids, various trace elements and other nutrient components required by human bodies, and bioactive substances such as flavonoids, triterpenes, steroids, 5-hydroxytryptamine, procyanidine and the like; the Chinese medicinal preparation can promote blood circulation to remove blood stasis, is a precious economic forest species containing most natural microorganisms in the world at present, has the content of vitamin C far higher than that of fresh jujube and kiwi fruit, is praised as a treasure house of natural vitamins and has rich nutrition; has good inhibitory effect on metalloprotease, and the activation of metalloprotease is an index of skin aging, and has anti-aging effect by combining with the elimination of superoxide radical. The flavonoids in fructus Hippophae can enhance the stability of vitamin C, inhibit tyrosinase activity, protect skin, and promote whitening.
In the invention, the herbal whitening compound composition comprises 0.02-1 part by weight of sea buckthorn extract, preferably 0.02 part by weight, 0.06 part by weight, 0.1 part by weight, 0.3 part by weight, 0.5 part by weight, 0.6 part by weight, 0.8 part by weight, 1 part by weight, and more preferably 0.3 part by weight.
In the invention, the licorice extract is extracted by a conventional method and is available on the market. The Glycyrrhrizae radix extract can improve skin activity, promote proliferation of muscle cells and generation of collagen-4, inhibit melanin, and whiten skin; has certain inhibiting effect on bacteria and anti-inflammatory effect.
In the invention, the herbal whitening compound composition comprises 0.02-1 part by weight of licorice extract, preferably 0.02 part by weight, 0.06 part by weight, 0.1 part by weight, 0.3 part by weight, 0.5 part by weight, 0.6 part by weight, 0.8 part by weight, 1 part by weight, and more preferably 0.3 part by weight.
The five traditional Chinese medicine components of the cistanche deserticola extract, the coastal angelica extract, the ganoderma lucidum extract, the sea buckthorn extract and the liquorice extract are compounded according to a certain proportion, are mutually supplemented and synergized, are used for whitening, can inhibit the activity of tyrosinase, can remove redundant free radicals, and reduce the release of inflammatory factors, thereby reducing the generation of melanin; meanwhile, the skin whitening cream can increase skin blood microcirculation and accelerate skin metabolism, thereby promoting melanin metabolism, improving the dark and yellow state of skin and achieving the whitening effect; meanwhile, the safety is high, and the product is non-toxic and non-irritant to human bodies.
In the invention, the nicotinamide is also called vitamin B3, has high safety as a medical ingredient, is also a basic vitamin supplement in clinical dermatology treatment, and is widely used for treating photosensitive dermatitis, acne and the like. The research in recent years proves that the medicine also has good curative effect on the aspects of inhibiting melanin pigmentation, resisting inflammation and the like; based on the characteristics, the application of the nicotinamide in the field of cosmetics is further extended, and besides the traditional whitening effect, the nicotinamide is also used for reducing the generated and precipitated melanin, blocking the transfer of the melanin to surface layer cells, accelerating cell metabolism, accelerating the shedding of melanin keratinocytes and the like; moreover, the nicotinamide can also maintain the moisture content of the skin, promote microcirculation of the dermis, greatly reduce or eliminate skin aging phenomena such as wrinkles, peeling, large pores and the like, reduce damage of free radicals to the skin, and play roles in preventing aging, repairing the skin and reducing facial darkness.
In the invention, the herbal whitening compound composition comprises 0.3-5 parts by weight of nicotinamide, preferably 0.3 part by weight, 0.6 part by weight, 1 part by weight, 2 parts by weight, 3 parts by weight, 4 parts by weight and 5 parts by weight, and more preferably 1 part by weight.
In the present invention, the ascorbyl glucoside, commonly known as vitamin C glucoside, is a derivative of vitamin C, has an inhibitory effect on melanin, and inhibits the formation of melanin by releasing vitamin C by α -glucosidase; meanwhile, the pigment has a reduction effect on the existing melanin, thereby playing a role in fading the color spots.
In the invention, the herbal whitening compound composition comprises 0.01-2 parts by weight of ascorbyl glucoside, preferably 0.01 part by weight, 0.2 part by weight, 0.5 part by weight, 1 part by weight, 1.5 parts by weight and 2 parts by weight, and more preferably 0.5 part by weight.
The invention is based on the composition consisting of five traditional Chinese medicine components of cistanche deserticola extract, angelica coastal extract, ganoderma lucidum extract, sea buckthorn extract and liquorice extract, and nicotinamide and ascorbyl glucoside are added, so that the synergistic effect can be further generated, and the whitening effect is enhanced.
The invention also provides a herbal whitening compound mask which consists of essence and mask base cloth;
the essence is prepared from the following raw materials:
76.412-88.005 parts by weight of a solvent;
0-11.75 parts by weight of a humectant;
0-1 part by weight of a solubilizer;
0.41-12 parts by weight of the compound composition;
0.22-8.578 parts by weight of a skin conditioner;
0.1-0.8 parts of thickening agent;
0.02-0.1 part by weight of a chelating agent;
0-0.05 parts by weight of an aromatic;
0.1-0.6 parts by weight of a preservative;
0-0.3 part of pH regulator;
the compound composition is the herbal whitening compound composition in the technical scheme;
the facial mask base cloth is made of cuprammonium fibers, hydrogel, pure cotton fibers, biological fibers, viscose, wormwood fibers, bamboo charcoal fibers or gel tencel.
In the present invention, the essence includes a solvent, a humectant, a solubilizer, a complex composition, a skin conditioner, a thickener, a chelating agent, a fragrance, a preservative, and a pH adjuster, and preferably consists of a solvent, a humectant, a solubilizer, a complex composition, a skin conditioner, a thickener, a chelating agent, a fragrance, a preservative, and a pH adjuster.
In the present invention, the solvent includes one or more of water, butanediol, 1, 2-hexanediol, 1, 2-pentanediol, 1, 3-propanediol, and 1, 2-propanediol, and more preferably one or more of water, butanediol, 1, 2-pentanediol, and 1, 2-propanediol. The source of the solvent is not particularly limited in the present invention, and commercially available products of the above-mentioned butanediol, 1, 2-hexanediol, 1, 2-pentanediol, 1, 3-propanediol, and 1, 2-propanediol, which are well known to those skilled in the art, may be used; the water may be deionized water as is well known to those skilled in the art. In the invention, the solvent is used to ensure that other components can be dissolved, dispersed and uniformly mixed.
In the present invention, the humectant is preferably selected from one or more of glycerin, sodium hyaluronate, trehalose, hydrolyzed sodium hyaluronate, hydroxyethyl urea, and glyceryl polyether-26. The source of the moisturizer is not particularly limited in the present invention, and commercially available products of the above glycerin, sodium hyaluronate, trehalose, hydrolyzed sodium hyaluronate, hydroxyethyl urea and glyceryl polyether-26, which are well known to those skilled in the art, may be used.
In the present invention, the solubilizer is preferably selected from one or more of PEG-40 hydrogenated castor oil, PEG-60 hydrogenated castor oil, PPG-26-butanol polyether and Tween-20, and more preferably PEG-40 hydrogenated castor oil.
In the invention, the compound composition is the herbal whitening compound composition in the technical scheme. In the invention, the essence comprises 0.41-12 parts by weight of the compound composition, preferably 0.41 part by weight, 3 parts by weight, 8 parts by weight, 10 parts by weight, 12 parts by weight, and more preferably 3 parts by weight.
In the present invention, the skin conditioning agent is preferably selected from the group consisting of allantoin, marshmallow root extract, purslane extract, BPN-tesoro 1600solution (palmitoyl tetrapeptide-7/palmitoyl pentapeptide-4/acetyl hexapeptide-8/water/polysorbate-20/1, 2-hexanediol/glycerin/carbomer), carnosine, dipeptide diaminobutyrylbenzylamide diacetate, Prolevis (water/hydrolyzed vegetable protein/phenoxyethanol/sodium benzoate/potassium sorbate/ethylhexyl glycerin), dipotassium glycyrrhizinate, sodium metabisulfite, arginine, ethylhexyl glycerin and p-hydroxyacetophenone, more preferably one or more of allantoin, marshmallow root extract, purslane extract, BPN-tesoro 1600solution (palmitoyl tetrapeptide-7/palmitoyl pentapeptide-4/acetyl hexapeptide-8- Water/polysorbate-20/1, 2-hexanediol/glycerin/carbomer), carnosine, dipeptide diaminobutyrylbenzylamide diacetate, Prolevis (water/hydrolyzed vegetable protein/phenoxyethanol/sodium benzoate/potassium sorbate/ethylhexylglycerin), dipotassium glycyrrhizinate, sodium metabisulfite, arginine, and p-hydroxyacetophenone. The source of the skin conditioner of the present invention is not particularly limited, and commercially available products of the above-mentioned allantoin, marshmallow root extract, purslane extract, BPN-tetro 1600solution (palmitoyl tetrapeptide-7/palmitoyl pentapeptide-4/acetyl hexapeptide-8/water/polysorbate-20/1, 2-hexanediol/glycerin/carbomer), carnosine, dipeptide diaminobutyrylbenzylamide diacetate, prolivis (water/hydrolyzed vegetable protein/phenoxyethanol/sodium benzoate/potassium sorbate/ethylhexylglycerin), dipotassium glycyrrhizinate, sodium metabisulfite, arginine, ethylhexylglycerin and p-hydroxyacetophenone, which are well known to those skilled in the art, may be used.
In the present invention, the thickener is preferably selected from one or more of carbomer, polyacrylic acid, xanthan gum, acrylate/C10-30 alkanol acrylate crosspolymer and hydroxyethyl cellulose, and more preferably from one or more of polyacrylic acid, xanthan gum, acrylate/C10-30 alkanol acrylate crosspolymer and hydroxyethyl cellulose. The source of the thickener in the present invention is not particularly limited, and commercially available carbomers, polyacrylic acid, xanthan gum, acrylates/C10-30 alkanol acrylate crosspolymer, hydroxyethyl cellulose, as described above, which are well known to those skilled in the art, may be used.
In the present invention, the chelating agent is preferably selected from disodium EDTA, trisodium EDTA or tetrasodium EDTA, more preferably disodium EDTA. The source of the chelating agent is not particularly limited in the present invention, and commercially available products of disodium EDTA, trisodium EDTA, and tetrasodium EDTA, which are well known to those skilled in the art, may be used.
In the present invention, the fragrance is preferably a perfume; the present invention is not particularly limited in its kind and origin.
In the present invention, the preservative is preferably selected from one or more of phenoxyethanol, potassium sorbate and sodium benzoate, more preferably phenoxyethanol. The source of the preservative is not particularly limited in the present invention, and commercially available products of phenoxyethanol, potassium sorbate and sodium benzoate as described above, which are well known to those skilled in the art, may be used.
In the present invention, the pH adjusting agent is preferably selected from citric acid and/or sodium citrate, more preferably citric acid and sodium citrate. The source of the pH adjuster is not particularly limited in the present invention, and commercially available products of the above citric acid and sodium citrate, which are well known to those skilled in the art, may be used.
In the invention, the facial mask base fabric is copper ammonia fiber, hydrogel, pure cotton fiber, biological fiber, viscose fiber, wormwood fiber, bamboo charcoal fiber or gel tencel, and preferably gel tencel (membrane fabric). The source of the mask base cloth is not particularly limited, and the mask base cloth can be obtained from the commercial products of the copper ammonia fiber, hydrogel, pure cotton fiber, biological fiber, viscose fiber, wormwood fiber, bamboo charcoal fiber and gel tencel, which are well known to those skilled in the art.
The copper ammonia fiber is a regenerated cellulose fiber, which is prepared by dissolving natural cellulose raw materials such as cotton linters and the like in a concentrated ammonia solution of copper hydroxide or alkaline copper salt to prepare spinning solution, decomposing copper ammonia cellulose molecular chemicals in a coagulating bath to regenerate cellulose, and post-processing the generated hydrated cellulose to obtain the copper ammonia fiber, wherein the dry strength of the copper ammonia fiber is close to that of viscose fiber, but the wet strength is higher than that of the viscose fiber, the wear resistance is also better than that of the viscose fiber, and the copper ammonia fiber has the characteristics of fine and soft fiber, proper gloss, good hygroscopicity and performance similar to silk.
In the invention, the hydrogel takes hydrophilic gel as a mask matrix, and is rich in a large amount of nutrients and moisture required by the skin; when the hydrogel facial mask is attached to the skin, the nutritional ingredients contained in the facial mask gradually permeate into the skin, and the facial mask has no stimulation to the skin.
In the invention, the pure cotton fiber is made of 100 percent pure natural cellulose, and the spunlace nonwoven fabric structure is prepared by a cross lapping method, so that the spunlace nonwoven fabric structure has the characteristics of difficult deformation after water absorption, strong longitudinal and transverse tension, white and soft property, good skin-attaching property and the like; the pure cotton cloth film is thickened and encrypted, has strong water absorption capacity, can absorb high-concentration nutrient substances and can effectively prevent the evaporation and the loss of nutrient components.
In the invention, the biological fiber is microbial cellulose generated by natural fermentation of acetobacter xylinum, has excellent water retention capacity, good biocompatibility and no stimulation; the biological fiber has the function similar to that of skin, has the fiber diameter of 50-80 nm, can penetrate into skin gully repair cells and tightly hold the skin cells to generate an upward pulling effect.
In the invention, the viscose fiber is cellulose fiber produced by using cotton or other natural fibers as raw materials, has the moisture content meeting the physiological requirement of human skin, and has the characteristics of smoothness, coolness, ventilation, static resistance and the like.
In the invention, the bamboo charcoal fiber is prepared by taking moso bamboo as a raw material, adopting a new calcining process and a new technology of pure oxygen high temperature and nitrogen blocking delay to enable micropores of the natural bamboo charcoal to be more refined and honeycombed, and then carrying out melt spinning with a polyester modified slice with a honeycomb micropore structure trend; the unique fiber structure enables the bamboo charcoal fiber mask to have good moisture absorption, air permeability and bacteriostatic effects.
In the invention, the wormwood fiber takes tencel fiber as a carrier, and is complexed with natural wormwood extraction factors, so that the wormwood fiber has strong moisture absorption performance and good skin adhesion.
According to the invention, the gel tencel is a crystal transparent gel tencel mask which is developed by taking natural plant fibers as raw materials and matching with a strong tencel mask processing technology, has the excellent properties of environmental protection, and has the characteristics of light and transparent lamination, full storage, fine touch and smooth touch and strong adsorption force; the light and transparent gel tencel can effectively moisturize and whiten skin and can also enable skin to breathe freely; the skin care product has more excellent heavy metal adsorption capacity, brings deep moisturizing and repairing force to skin by soft touch, and brings light and thorough 'no-feel' skin care enjoyment to users.
The facial mask provided by the invention adopts the essence added with the herbal whitening compound composition, and the whitening effect is good through skin tests; the use feeling and the efficacy are better by matching with the specific mask base cloth.
The invention also provides a preparation method of the herbal whitening compound mask, which comprises the following steps:
a) uniformly mixing a solvent, a humectant, a solubilizer, a skin conditioner, a thickening agent, a chelating agent, an aromatic and a pH regulator in a vacuum emulsification tank; then adding the compound composition and the preservative to be uniformly dispersed; then cooling to 32-35 ℃, defoaming, filtering and discharging to obtain essence;
b) filling the essence obtained in the step a) and mask base cloth together to obtain the herbal whitening compound mask.
The invention firstly mixes solvent, humectant, solubilizer, skin conditioner, thickener, chelating agent, aromatic and pH regulator evenly in a vacuum emulsification tank. In the present invention, the solvent, the humectant, the solubilizer, the skin conditioner, the thickener, the chelating agent, the fragrance, and the pH adjuster are the same as those described in the above technical solution, and are not described herein again.
The invention carries out the mixing process according to the solubility between the specific components of the humectant, the solubilizer, the skin conditioner, the thickener, the chelating agent, the aromatic and the pH regulator and different solvents; preferably specifically
a1) Putting water, glycerol, sodium hyaluronate, hydrolyzed sodium hyaluronate, hydroxyethyl urea, trehalose, glyceryl polyether-26, allantoin, p-hydroxyacetophenone, carbomer, acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, xanthan gum, polyacrylic acid, hydroxyethyl cellulose, EDTA disodium, EDTA trisodium and EDTA tetrasodium into a vacuum emulsification tank, dissolving at 80-85 ℃, uniformly stirring, and cooling to 43-47 ℃ to obtain phase A;
a2) completely dissolving arginine, citric acid and sodium citrate with a part of water in a separate dissolving tank to obtain a phase B;
a3) completely dissolving butanediol, 1, 2-hexanediol, 1, 2-pentanediol, 1, 3-propanediol, 1, 2-propanediol, essence, PEG-40 hydrogenated castor oil, PEG-60 hydrogenated castor oil, PPG-26-butanol polyether and Tween-20 in a single dissolving tank to obtain a phase C;
a4) adding the phase B and the phase C into a vacuum emulsification tank (phase A) in sequence, and uniformly dispersing.
Then, adding the compound composition and the preservative to disperse uniformly; then cooling to 32-35 ℃, defoaming, filtering and discharging to obtain the essence. In the present invention, the compound composition and the preservative are the same as those described in the above technical scheme, and are not described herein again.
After the essence is obtained, the obtained essence and mask base cloth are filled together to obtain the herbal whitening compound mask. In the invention, the mask base cloth is the same as that in the technical scheme, and is not described again.
The preparation method provided by the invention has the advantages of simple process, mild conditions, easiness in operation control, suitability for large-scale production and wide application prospect.
The invention provides a herbal whitening compound composition, a mask and a preparation method thereof; the herbal whitening compound composition comprises the following components: 0.02-1 part by weight of cistanche extract; 0.02-1 part by weight of a coastal angelica extract; 0.02-1 part by weight of ganoderma lucidum extract; 0.02-1 part by weight of a sea buckthorn extract; 0.02-1 part by weight of licorice extract. Compared with the prior art, the five traditional Chinese medicine components of the cistanche deserticola extract, the coastal angelica extract, the ganoderma lucidum extract, the sea buckthorn extract and the liquorice extract are compounded according to a certain proportion, are mutually supplemented and synergized, and the obtained herbal whitening compound composition has excellent whitening effect, high safety and no toxicity or stimulation to human bodies; meanwhile, the essence added with the herbal whitening compound composition is matched with a specific mask base cloth, so that the use feeling and the efficacy are better.
In addition, the preparation method provided by the invention has the advantages of simple process, mild conditions, easiness in operation control, suitability for large-scale production and wide application prospect.
To further illustrate the present invention, the following examples are provided for illustration. The starting materials used in the following examples of the present invention are all commercially available products.
Example 1: the herbal whitening compound composition
(1) Formulations 1 to 11
Table 1 formula of herbal whitening compound composition in example 1
Figure BDA0002660691690000121
Figure BDA0002660691690000131
(2) Comparative examples 1 to 6
Comparative example 1: compared with the formula 3, only the nicotinamide and the ascorbyl glucoside are contained, and the rest is unchanged;
comparative example 2: compared with the formula 3, the traditional Chinese medicine composition does not contain cistanche salsa extract, and the rest is unchanged;
comparative example 3: compared with the formula 3, the Chinese angelica coastal areas do not contain the Chinese angelica extract, and the rest is unchanged;
comparative example 4: compared with formula 3, it does not contain Ganoderma lucidum extract, and the rest is unchanged;
comparative example 5: compared with the formula 3, the sea buckthorn fruit vinegar does not contain sea buckthorn extract, and the balance is unchanged;
comparative example 6: compared with formula 3, the composition does not contain licorice extract, and the rest is unchanged.
Test example:
(1) the safety of the herbal whitening compound composition provided by the embodiment 1 of the invention is verified, and compared with the compositions of comparative examples 1-6:
human skin patch test: 2 parts by weight of each composition was added to 98 parts by weight of water to prepare a composition solution with a mass fraction of 2%. 540 volunteers meeting the selection criteria (male and female with the age of 18-60 years, no disease, smooth back skin, no scar, birthmark and no pox, female has no lactation, pregnancy or pregnancy intention temporarily and can complete continuous 4-day uninterrupted follow-up as required) are selected to participate in the test and randomly divided into 18 groups of 30 persons. Negative control: blank control (without any material). The spot test method comprises the following steps: selecting a qualified spot tester, applying 0.025mL of a test object into the spot tester by a closed spot test method, externally applying a special adhesive tape to the back of a test object, removing the test object after 24 hours, observing skin reactions at 0.5 hour, 24 hours and 48 hours after removal, and recording the observation results (Table 3) according to skin closed spot test skin reaction grading standards (Table 2) in technical Specification for cosmetic safety (2015 edition).
Skin reaction grading Standard of skin Enclosed Patch test in Table 2 technical Specification for safety of cosmetics (2015 edition)
Figure BDA0002660691690000132
Figure BDA0002660691690000141
TABLE 3 Patch test results
Figure BDA0002660691690000142
Figure BDA0002660691690000151
(2) The ability of the herbal whitening compound composition provided in embodiment 1 of the invention to inhibit tyrosinase activity was tested and compared with the compositions of comparative examples 1-6:
the method for measuring the inhibition rate of the in vitro tyrosinase activity comprises the following steps: 2 parts by weight of each composition was added to 98 parts by weight of water to prepare a composition solution with a mass fraction of 2%. Performing sample addition experiments according to Table 4, without adding tyrosinase, placing the solution in a water bath kettle at 37 ℃ and keeping the temperature for 10 min; adding tyrosinase, placing the solution in water bath AT 37 deg.C, keeping the temperature for 10min, and measuring absorbance AT 475nm (AT1, AT2, AC1, AC2) for 3 times.
TABLE 4 tyrosinase Activity test sample addition
Figure BDA0002660691690000152
The tyrosinase activity inhibition rate is calculated by the formula: inhibition rate ═ 1- (AC 2-AC 1)/(AT 2-AT 1) × 100%; the results are shown in Table 5.
TABLE 5 ability data to inhibit tyrosinase activity
Figure BDA0002660691690000161
TABLE 5 continuation
Serial number Comparative example 1 Comparative example 2 Comparative example 3 Comparative example 4 Comparative example 5 Comparative example 6
Inhibition rate 7.03% 11.15% 12.67% 13.36% 11.95% 12.29%
(3) The herbal whitening compound composition provided in the embodiment 1 of the invention is tested for DPPH removal capability and compared with the compositions of comparative examples 1-6:
the determination method comprises the following steps: respectively putting 2.0mL of composition ethanol solutions (3, 6, 9, 12, 15, 18 mu g/mL) with different mass concentrations and 2.0mL of 0.2mmol/L DPPH solution in a test tube with a plug, shaking uniformly, reacting for 30min in a dark place, and measuring the absorbance A1 at 517nm by using absolute ethanol as a reference; the absorbance A0 of a mixture of 2.0mL of 0.2mmol/L DPPH solution and 2.0mL of absolute ethanol and the absorbance A2 of a mixture of 2.0mL of sample solution and 2.0mL of absolute ethanol were measured simultaneously. The measurement results are expressed as clearance (E) and are calculated by the formula: e ═ 1- (a 1-a 2) ]/a0 × 100%. And drawing a curve for eliminating DPPH & of the sample to be detected by taking the concentration of the sample to be detected as an abscissa and the elimination rate value as an ordinate, and calculating the concentration of the sample to be detected when the free radical elimination rate is 50% according to a linear regression equation of the curve, wherein the concentration is defined as a half inhibition concentration (IC 50). The DPPH-removing ability of the sample is measured by the IC50 value of the sample concentration with the removing rate of 50%. The results are shown in Table 6.
TABLE 6 clear DPPH & Capacity data
Figure BDA0002660691690000162
TABLE 6 continuation
Figure BDA0002660691690000163
As can be seen from tables 3, 5 and 6, the whitening effects of the formulas 8, 10 and 11 are superior to those of the comparative examples 2 to 6, which shows that the combination of the cistanche extract, the angelica sinensis extract, the ganoderma lucidum extract, the sea buckthorn extract and the licorice extract provided by the invention can obtain good whitening effects; the whitening effect of formulas 8 and 10 is superior to that of formula 11, indicating that the ratio of the cistanche extract, the angelica sinensis, the ganoderma lucidum extract, the sea buckthorn extract and the licorice extract is 5: 2: 2: 3: 3, the whitening effect is good; the whitening effect of formula 8 is superior to that of formula 10, indicating that the whitening effect is better when the total weight of the cistanche extract, the angelica sinensis extract, the ganoderma lucidum extract, the sea buckthorn extract and the licorice extract is 1.5 parts by weight. The whitening effect of formulas 1 and 6 is superior to that of formulas 8, 10 and 11, which shows that the addition of nicotinamide and ascorbyl glucoside can enhance the whitening effect; while the whitening effect of the formulas 2-3 and the formulas 7 and 9 is superior to that of the formulas 1 and 6, which shows that the whitening effect can be synergized by further adding nicotinamide and ascorbyl glucoside into the five traditional Chinese medicine components of the cistanche extract, the coastal angelica extract, the ganoderma lucidum extract, the seabuckthorn extract and the liquorice extract; meanwhile, the whitening effects of the formulas 1 to 7 and the formula 9 are superior to those of the comparative examples 1 to 6, which shows that the combination of the cistanche extract, the angelica maritima extract, the ganoderma lucidum extract, the sea buckthorn extract, the licorice extract, the nicotinamide and the ascorbyl glucoside has a synergistic effect, and a better whitening effect can be obtained. Finally, formulas 3 and 9 are superior to the other formulas, indicating that the ratio of cistanche extract, angelica sinensis extract, ganoderma lucidum extract, hippophae rhamnoides extract, licorice extract, niacinamide and ascorbyl glucoside is 5: 2: 2: 3: 3: 10: 5, the whitening effect is better; the whitening effect of formula 3 is superior to that of formula 9, indicating that the whitening effect is optimal when the total weight of the cistanche extract, the angelica sinensis extract, the ganoderma lucidum extract, the sea buckthorn extract, the licorice extract, the nicotinamide and the ascorbyl glucoside is 3 parts by weight.
Example 2: the herbal whitening compound mask
(1) 1-5 mask
Table 7 formula table of herbal whitening compound mask in example 2
Figure BDA0002660691690000171
Figure BDA0002660691690000181
Figure BDA0002660691690000191
(2) Comparative examples 7 to 14
Comparative example 7, compared with mask 3, the compound composition was replaced with the composition of comparative example 1, and the rest was unchanged;
comparative example 8, compared with mask 3, the compound composition was replaced with the composition of comparative example 2, and the rest was unchanged;
comparative example 9, compared with mask 3, the compound composition was replaced with the composition of comparative example 3, and the rest was unchanged;
comparative example 10, compared with mask 3, the compound composition was replaced with the composition of comparative example 4, and the rest was unchanged;
comparative example 11, compared with mask 3, the compound composition was replaced with the composition of comparative example 5, and the rest was unchanged;
comparative example 12, compared with mask 3, the compound composition was replaced with the composition of comparative example 6, and the rest was unchanged;
comparative example 13, compared with mask 3, the compound composition was replaced with water, the remainder was unchanged;
comparative example 14, compared with mask 3, the compound composition was replaced with formula 8 whitening compound composition, the rest was unchanged.
The preparation method of the facial mask is as follows (when a certain component is not contained in the formula, the component is not added in the preparation process):
(1) putting water, glycerol, sodium hyaluronate, hydrolyzed sodium hyaluronate, hydroxyethyl urea, trehalose, glyceryl polyether-26, allantoin, p-hydroxyacetophenone, carbomer, acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, xanthan gum, polyacrylic acid, hydroxyethyl cellulose, EDTA disodium, EDTA trisodium and EDTA tetrasodium into a vacuum emulsification tank, dissolving at 82 ℃, uniformly stirring, and cooling to 45 ℃ to obtain phase A;
(2) completely dissolving arginine, citric acid and sodium citrate with a part of water in a separate dissolving tank to obtain a phase B;
(3) completely dissolving butanediol, 1, 2-hexanediol, 1, 2-pentanediol, 1, 3-propanediol, 1, 2-propanediol, essence, PEG-40 hydrogenated castor oil, PEG-60 hydrogenated castor oil, PPG-26-butanol polyether and Tween-20 in a single dissolving tank to obtain a phase C;
(4) sequentially adding the phase B and the phase C into a vacuum emulsification tank (phase A), and uniformly dispersing;
(5) sequentially adding Cistanchis herba extract, Angelica maritima extract, Ganoderma lucidum extract, fructus Hippophae extract, Glycyrrhrizae radix extract, nicotinamide, ascorbyl glucoside, radix Althaeae Roseae extract, herba Portulacae extract, BPN-desoro 1600solution, carnosine, dipeptide diaminobutyryl benzylamide diacetate, Prolevis, dipotassium glycyrrhizinate, sodium pyrosulfite, ethylhexyl glycerol, phenoxyethanol, potassium sorbate, and sodium benzoate into a vacuum emulsification tank, and uniformly dispersing;
(6) cooling to 33 ℃, defoaming, filtering and discharging;
(7) after being inspected to be qualified, the mask base cloth and the mask base cloth are filled into finished products, and the finished products are packaged and put in storage.
And (3) efficacy verification:
performing efficacy verification on the facial masks 1-5 and the facial masks of comparative examples 7-14; the specific verification method comprises the following steps:
390 ginseng and samples of people with dark skin color caused by insufficient sleep, excessive pressure, smoking, unclean makeup removal and the like are selected to have whitening effect
Figure BDA0002660691690000203
The test of (1). Grouping according to the number of samples, wherein each group comprises 30 persons, each group of tested persons respectively use the samples of the facial masks 1-5 and the comparative examples 7-14, and ITA values before and after 4 weeks of continuous use of the samples are measured and calculated by adopting ITA individual type angles.
Evaluation of feeling of use: the volunteers evaluated the feeling of use after 7 days of continuous use. People who feel more than 80% feel that the mask is very soft, close to the skin and breathable, and are rated as plus minus 60%.
The results are shown in Table 8.
Table 8 efficacy test results of the mask
Figure BDA0002660691690000201
TABLE 8 continuation
Figure BDA0002660691690000202
Note: shoulder marks indicate significant differences in ITA values after use of the mask compared to before use, P < 0.05.
As can be seen from table 8, (1) efficacy: compared with comparative examples 7-13, the ITA values of the facial masks 1-5 and the facial masks 14 after the facial masks are used are significantly different from that before the facial masks are used, and P is less than 0.05, which shows that the whitening effects of the facial masks 1-5 and the comparative examples 14 are superior to those of the comparative examples 7-13; further, the whitening effect of the comparative example 14 is superior to that of the comparative examples 8-12, which shows that the cistanche extract, the angelica coastal extract, the ganoderma lucidum extract, the sea buckthorn extract and the licorice extract provided by the invention can obtain good whitening effect; the whitening effect of the mask 1-5 is better than that of the comparative example 14, which shows that the whitening effect of the composition is further improved by further adding nicotinamide and ascorbyl glucoside; meanwhile, the whitening effect of the mask 1-5 is superior to that of the comparative examples 7-14, which shows that the optimal whitening effect can be obtained only by combining the cistanche extract, the angelica maritima extract, the ganoderma lucidum extract, the sea buckthorn extract, the licorice extract, the nicotinamide and the ascorbyl glucoside; compared with the masks 1-2 and the masks 4-5, the mask 3 basically improves the whitening effect along with the increase of the addition amount of the whitening composition, but when the addition amount of the whitening composition in the mask is 3 parts by weight, the whitening effect is the best when the gel tencel is used as the mask base cloth, and the effect of the gel tencel on the mask base cloth provided by the invention is promoted. (2) The use feeling is as follows: compared with the facial masks 1-2 and 4-5, the facial mask 3 has the best use feeling when the material of the facial mask base cloth is gel tencel.
The previous description of the disclosed embodiments is provided to enable any person skilled in the art to make or use the present invention. Various modifications to these embodiments will be readily apparent to those skilled in the art, and the generic principles defined herein may be applied to other embodiments without departing from the spirit or scope of the invention. Thus, the present invention is not intended to be limited to the embodiments shown herein but is to be accorded the widest scope consistent with the principles and novel features disclosed herein.

Claims (10)

1. The herbal whitening compound composition comprises the following components:
0.02-1 part by weight of cistanche extract;
0.02-1 part by weight of a coastal angelica extract;
0.02-1 part by weight of ganoderma lucidum extract;
0.02-1 part by weight of a sea buckthorn extract;
0.02-1 part by weight of licorice extract.
2. The herbal whitening compound composition according to claim 1, further comprising:
0.3-5 parts by weight of nicotinamide;
0.01 to 2 parts by weight of ascorbyl glucoside.
3. A herbal whitening compound facial mask comprises essence and facial mask base cloth;
the essence is prepared from the following raw materials:
76.412-88.005 parts by weight of a solvent;
0-11.75 parts by weight of a humectant;
0-1 part by weight of a solubilizer;
0.41-12 parts by weight of the compound composition;
0.22-8.578 parts by weight of a skin conditioner;
0.1-0.8 parts of thickening agent;
0.02-0.1 part by weight of a chelating agent;
0-0.05 parts by weight of an aromatic;
0.1-0.6 parts by weight of a preservative;
0-0.3 part of pH regulator;
the compound composition is the herbal whitening compound composition as defined in any one of claims 1-2;
the facial mask base cloth is made of cuprammonium fibers, hydrogel, pure cotton fibers, biological fibers, viscose, wormwood fibers, bamboo charcoal fibers or gel tencel.
4. The herbal whitening compound mask as claimed in claim 3, wherein the moisturizer is one or more selected from glycerin, sodium hyaluronate, trehalose, hydrolyzed sodium hyaluronate, hydroxyethyl urea and glyceryl polyether-26.
5. The herbal whitening compound mask as claimed in claim 3, wherein the solubilizer is selected from one or more of PEG-40 hydrogenated castor oil, PEG-60 hydrogenated castor oil, PPG-26-butanol polyether and Tween-20.
6. The herbal whitening compound mask as claimed in claim 3, wherein the skin conditioning agent is selected from one or more of allantoin, Althea officinalis root extract, Portulaca oleracea extract, BPN-meso 1600solution, carnosine, dipeptide diaminobutyrobenzyl amide diacetate, Prolevis, dipotassium glycyrrhizinate, sodium metabisulfite, arginine, ethylhexyl glycerol and p-hydroxyacetophenone.
7. The herbal whitening compound mask as claimed in claim 3, wherein the thickener is one or more selected from carbomer, polyacrylic acid, xanthan gum, acrylate/C10-30 alkanol acrylate crosspolymer and hydroxyethyl cellulose.
8. The herbal whitening compound mask as claimed in claim 3, wherein the chelating agent is selected from disodium EDTA, trisodium EDTA or tetrasodium EDTA.
9. The herbal whitening compound mask as claimed in claim 3, wherein the pH regulator is selected from citric acid and/or sodium citrate.
10. The preparation method of the herbal whitening compound mask as claimed in any one of claims 3 to 9, comprising the following steps:
a) uniformly mixing a solvent, a humectant, a solubilizer, a skin conditioner, a thickening agent, a chelating agent, an aromatic and a pH regulator in a vacuum emulsification tank; then adding the compound composition and the preservative to be uniformly dispersed; then cooling to 32-35 ℃, defoaming, filtering and discharging to obtain essence;
b) filling the essence obtained in the step a) and mask base cloth together to obtain the herbal whitening compound mask.
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陆香珍: "明日叶查尔酮制备方法与抗衰老作用研究进展", 《食品研究与开发》 *

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112813731A (en) * 2021-01-06 2021-05-18 刘桂峥 Preparation method of wormwood fiber composite surface film substrate
CN113599336A (en) * 2021-08-13 2021-11-05 深圳市巨印科技有限公司 Metabolism conditioning herbal membrane powder

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