CN107233275A - A kind of light spot is dispelled yellow fermentation Chinese wolfberry fruit liquid level film and preparation method thereof - Google Patents

A kind of light spot is dispelled yellow fermentation Chinese wolfberry fruit liquid level film and preparation method thereof Download PDF

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Publication number
CN107233275A
CN107233275A CN201710547066.6A CN201710547066A CN107233275A CN 107233275 A CN107233275 A CN 107233275A CN 201710547066 A CN201710547066 A CN 201710547066A CN 107233275 A CN107233275 A CN 107233275A
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China
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parts
chinese wolfberry
wolfberry fruit
fermentation chinese
extract
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Inventor
刘建军
乔长晟
严婷婷
张飞扬
牛思思
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Tianjin Qi Yuan Tang Biological Engineering Co Ltd
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Tianjin Qi Yuan Tang Biological Engineering Co Ltd
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Priority to CN201710547066.6A priority Critical patent/CN107233275A/en
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL, OR TOILET PURPOSES
    • A61K8/00Cosmetics or similar toilet preparations
    • A61K8/18Cosmetics or similar toilet preparations characterised by the composition
    • A61K8/96Cosmetics or similar toilet preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toilet preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL, OR TOILET PURPOSES
    • A61K8/00Cosmetics or similar toilet preparations
    • A61K8/18Cosmetics or similar toilet preparations characterised by the composition
    • A61K8/72Cosmetics or similar toilet preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL, OR TOILET PURPOSES
    • A61K8/00Cosmetics or similar toilet preparations
    • A61K8/18Cosmetics or similar toilet preparations characterised by the composition
    • A61K8/72Cosmetics or similar toilet preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • A61K8/736Chitin; Chitosan; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL, OR TOILET PURPOSES
    • A61K8/00Cosmetics or similar toilet preparations
    • A61K8/18Cosmetics or similar toilet preparations characterised by the composition
    • A61K8/72Cosmetics or similar toilet preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84Cosmetics or similar toilet preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/88Polyamides
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL, OR TOILET PURPOSES
    • A61K8/00Cosmetics or similar toilet preparations
    • A61K8/18Cosmetics or similar toilet preparations characterised by the composition
    • A61K8/96Cosmetics or similar toilet preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/98Cosmetics or similar toilet preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
    • A61K8/987Cosmetics or similar toilet preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILET PREPARATIONS
    • A61Q17/00Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
    • A61Q17/04Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILET PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILET PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/02Preparations for care of the skin for chemically bleaching or whitening the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILET PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/08Anti-ageing preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL, OR TOILET PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions
    • A61K2800/5922At least two compounds being classified in the same subclass of A61K8/18
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL, OR TOILET PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/74Biological properties of particular ingredients
    • A61K2800/78Enzyme modulators, e.g. Enzyme agonists
    • A61K2800/782Enzyme inhibitors; Enzyme antagonists

Abstract

The invention belongs to cosmetic skin field, it is related to a kind of light spot and dispels yellow fermentation Chinese wolfberry fruit liquid level film and preparation method thereof.The facial mask of the present invention includes spunlace non-woven cloth Face film towel and infiltration in facial mask stoste thereon;Facial mask stoste includes following components:Pure water, fermentation Chinese wolfberry fruit liquid, polyglutamic acid, vitamin C, asparagus juice, pearl powder, propane diols, chitosan oligomer, bletilla striata zymotic fluid, Flos Pelargonii Hortori, angelica extract, dandelion extract, Millettia extract and pulullan polysaccharide.The reparation facial mask of the present invention is when laying, chitosan oligomer and angelica extract, which can take the lead in entering in Skin Cell, carries out bactericidal antiphlogistic, then polyglutamic acid can control the slow reparation and cytothesis for being extracted into skin, carrying out cell of bletilla striata zymotic fluid, fish pelargonium and the nutritional ingredient in fermentation Chinese wolfberry fruit liquid.The sun-proof reparation facial mask of the present invention effectively controls each nutritional ingredient into the order of Skin Cell, by mutually being cooperateed between each component, collective effect, quick repair cell.

Description

A kind of light spot is dispelled yellow fermentation Chinese wolfberry fruit liquid level film and preparation method thereof
Technical field
The invention belongs to cosmetic skin field, and in particular to a kind of light spot is dispelled yellow fermentation Chinese wolfberry fruit liquid level film and its preparation side Method.
Background technology
Skin is made up of epidermis, basilar memebrane and skin corium from outside to inside.Epidermis is divided into cuticula, stratum granulosum, had again Spinous layer and basalis.It is 5~20 layers of dead pinacocyte positioned at the cuticula of body surface, when cuticula is blocked up or water content is low When, the ability of skin reflex light reduces and the dull colour of skin is presented;In addition, originating from the melanin in basal layer of epidermis to light The absorbability of line is most strong, and the colour of skin that melanin content is more at most presented is deeper;Further, in corium angioplerosis degree not enough or Poor blood circulation, then hemochrome cohesion or content, which decline, causes the colour of skin dark red or pale;Finally, the collagenous fibres in corium Skin tension and toughness are assigned, its skewness or structure change will cause light uniformly to be reflected and cause the colour of skin It is uneven and lackluster.
Although present social pressures are increased, the pressure stayed up late of working overtime is rested bad, sleep is not into the daily of modern Foot, is the most active moment of skin cell renewal during the length of one's sleep in evening, sleeps or have not enough sleep too late, metabolic function No longer smoothly, cause aging cutin layer to thicken, skin loses transparent feel, the dark color of graying is presented.When we bear pressure, fatigue When excessive, body can be in tension, causes vessel retraction, poor circulation, and face is also obscure to get off.And tired mistake Degree, the sluggish metabolism of skin, face becomes more obscure because cutin is gathered.If scaly dry skin, cuticula moisture is not Foot, the colour of skin seems dark yellow.And microgroove occurs in the skin dried, do not see to be difficult to observe carefully sometimes, but more than microgroove Skin is just as having covered one layer of ash, it appears dark yellow.Some and skin senescence have after certain relation, skin senescence above, new old generation Thank and slow down, skin is oxidized.The colour of skin is intense darkness without light coloured silk.
Whitening is the dream of each woman, is at this moment just badly in need of a light spot and dispels yellow fermentation Chinese wolfberry fruit liquid level film to repair skin, And the complex manufacturing technology of the most cosmetics of in the market and contain artificial synthesized chemicals mostly, easily stimulate and arrive skin, especially It is some skin sensitivities crowd and the crowd of particular time, causes allergy, people is produced query to the composition of cosmetics.
The content of the invention
The purpose of the present invention is to be dispelled yellow fermentation Chinese wolfberry fruit liquid level film and its system there is provided a kind of light spot in view of the shortcomings of the prior art Preparation Method.The light spot of the present invention is dispelled in yellow fermentation Chinese wolfberry fruit liquid level film, compound in bletilla striata zymotic fluid and fermentation Chinese wolfberry fruit liquid mixed liquor Polysaccharide, with synergy, can effectively remove free radical and suppress the activity of tyrosinase, deep layer repair cell gives skin With nutrition, impaired cell, tissue can be made to obtain timely high-quality repairing, make skin gloss high resilience, delaying senility.My god The active component that Zhu Kui extracts contain can effectively nti-freckle, the tender pale skin of beauty treatment.The angelica extract promoting flow of qi and blood circulation, increases blood stream Speed, blood circulation provides the oxygen and nutriment of abundance for fibroblast, collagen of skin etc.;Be conducive to cell Metabolite and various harmful substances remove in time, it is ensured that the metabolism of skin.Dandelion extract, which has to clear liver, to be dredged It is strongly fragrant, effect of toxin expelling sore;Millettia extract, with promoting the circulation of qi, Fufeng, the effectiveness invigorated blood circulation.The polyglutamic acid that the present invention is used This composition, due to its larger strand and large number of ultrahydrophilic group (- COOH), can make the bletilla striata ferment Effectively absorption is around its strand in liquid, fish pelargonium, fermentation Chinese wolfberry fruit liquid, chitosan oligomer and Radix Angelicae Sinensis.In addition, chitosan oligomer Substantial amounts of-NH in molecule3Make it have positive charge, enable chitosan oligomer effectively with the quick knot such as the collagen in skin Close, pro-skin performance is very good;Therefore, when laying facial mask, chitosan oligomer can take the lead in entering progress sterilization in Skin Cell and disappear Inflammation, then polyglutamic acid can control bletilla striata zymotic fluid, fish pelargonium, dandelion extract, Millettia extract and fermentation Chinese wolfberry fruit liquid In nutritional ingredient the reparation and cytothesis that are slowly extracted into skin successively again, carry out cell.The sun-proof of the present invention is repaiied Coverlay film effectively controls each nutritional ingredient into the order of Skin Cell, by mutually being cooperateed between each component, collective effect, soon Fast repair cell.
To achieve the above object, the present invention is adopted the following technical scheme that:
A kind of light spot is dispelled yellow fermentation Chinese wolfberry fruit liquid level film, and the light spot yellow fermentation Chinese wolfberry fruit liquid level film of dispelling includes spunlace non-woven cloth face The facial mask stoste of film towel and infiltration on spunlace non-woven cloth;The facial mask stoste includes the component of following parts by weight:
The molecular weight of the polyglutamic acid is 91-101 ten thousand.
It is used as preferred technical scheme:
It is preferred that, the molecular weight of the chitosan oligomer is 1300-1600;Fermentation Chinese wolfberry fruit liquid is red fermentation Chinese wolfberry fruit liquid.
It is preferred that, the lactic acid bacteria used during fermentation Chinese wolfberry fruit liquid and the bletilla striata zymotic fluid fermentation is CGMCC NO.1.1 breasts Sour bacterium.
After lactic fermentation, pH declines, and oxidation-reduction potential rises, and environment is in reduction-state.Therefore, the lactobacillus-fermented bletilla striata is used And matrimony vine, the polysaccharide in the bletilla striata and matrimony vine can be made fully to preserve, enable nutritional ingredient in matrimony vine and the bletilla striata more fully Using and release.
It is preferred that, the particle diameter of the pearl powder is 100-200nm;The molecular weight of the pulullan polysaccharide is 20-40 ten thousand.
It is preferred that, the facial mask stoste includes the component of following parts by weight:30 parts of pure water, 28 parts of fermentation Chinese wolfberry fruit liquid, It is 3 parts of polyglutamic acid, 0.4 part of vitamin C, 16 parts of asparagus juice, 12 parts of pearl powder, 0.5 part of propane diols, 3 parts of chitosan oligomer, white 5 parts of 8 parts of splendid achnatherum zymotic fluid, 5 parts of Flos Pelargonii Hortori, 2 parts of angelica extract and pulullan polysaccharide, 3 parts of dandelion extract and chicken 5 parts of blood boisiana extract;The molecular weight of the polyglutamic acid is 950,000.
Dispelled present invention also offers a kind of light spot the preparation method of yellow fermentation Chinese wolfberry fruit liquid level film, it is characterized in that, including it is following Step:
(1) polyglutamic acid and pearl powder are dissolved in pure water, and stirred, become thick liquid;
(2) asparagus juice is added in aforesaid liquid, sequentially adds vitamin C, propane diols, pulullan polysaccharide and matrimony vine Zymotic fluid, chitosan oligomer, bletilla striata zymotic fluid, Flos Pelargonii Hortori and angelica extract, dandelion extract and reticulate millettia carry Take thing to stir and evenly mix, obtain facial mask stoste;
(3) after facial mask stoste is sterilized, then spunlace non-woven cloth Face film towel soaked in facial mask stoste, then vacuum seal Dress, is made matrimony vine facial mask.
It is preferred that, the preparation method of the fermentation Chinese wolfberry fruit liquid is:By dry wolfberry and water in mass ratio 1:8-15 mixing is abundant Mashing, based on liquid, following percentage by weight material is added into basal liquid:Yeast extract 0.1-0.4%, phosphoric acid hydrogen two Potassium 0.03-0.2%, magnesium sulfate 0.01-0.2%, Triammonium citrate 0.1-0.2%, manganese sulfate 0.001-0.005%, it is fully mixed Sterilized after even, inoculating lactic acid bacterium is placed in 180rpm on shaking table, 30 DEG C, cultivates 48h, obtain fermentation Chinese wolfberry fruit stoste;By the proferment Liquid filtration sterilization, retains supernatant and the pH value of supernatant is adjusted into neutrality, obtain fermentation Chinese wolfberry fruit liquid.
It is preferred that, the stir speed (S.S.) used when being stirred in step (1) or step (2) is 80-100r/min;In step (3) The time of immersion is 30-40min.
It is preferred that, bletilla striata zymotic fluid is identical with the preparation method of fermentation Chinese wolfberry fruit liquid.
It is preferred that, angelica extract, Flos Pelargonii Hortori, the extracting method of dandelion extract and Millettia extract For:After the extract that will be prepared is crushed, add volume fraction and filtered for 30%-95% ethanol solution;Then by filtered fluid It is placed in after concentration on large pore resin absorption column, after the ethanol solution elution of same volume fraction, dries and obtain the extract.
Inventive principle:
Chitosan oligomer and angelica extract in the present invention have good inhibiting bacteria and diminishing inflammation and moisturizing effects.Oligopolymerization chitosan Substantial amounts of-NH in glycan molecule3Presence it is carried positive charge, can effectively with the collagen in skin etc. is quick combines, Pro-skin performance is very good;Therefore, when laying facial mask, chitosan oligomer, which can take the lead in entering in Skin Cell, carries out moisturizing, makes thin Born of the same parents fill, and then polyglutamic acid can control the slow of bletilla striata zymotic fluid, fish pelargonium, Radix Angelicae Sinensis and the nutritional ingredient in fermentation Chinese wolfberry fruit liquid Skin is extracted into, the reparation and cytothesis of cell is carried out.
Due to, containing the ultrahydrophilic group (- COOH) of more than 1000, can fully keep water in polyglutamic acid molecule Point, for improving voidage in matrimony vine facial mask between nutritional ingredient, being carried beneficial to bletilla striata zymotic fluid, fish pelargonium, Radix Angelicae Sinensis, dandelion The effectively nutritional ingredient such as thing, Millettia extract and fermentation Chinese wolfberry fruit liquid is taken to absorb, can be in skin surface formation thin film protection Skin absorbs, and is the optimal transport platform of nutrient, moisture and Touch skin familiarity in sun-proof facial mask, effectively increases sun-proof facial mask Dissolving, storage, conveying in active ingredient is with absorbing.In addition, polyglutamic acid has hydrophilic radical, carboxyl is ionizable negatively charged Lotus, the adsorbable nutritional ingredient of negative electrical charge;When laying facial mask, adsorb in polyglutamic acid group surrounding nutrient composition, due to concentration difference Under effect and the intermolecular force seen with skin, polyglutamic acid can slowly release above-mentioned nutritional ingredient, in the phase of face mask film Between, moisture and the uniform dissolution of nutrition can be made so that skin slow-absorbing.Also need to propose, due to bletilla striata zymotic fluid, day Nutritional ingredient in Zhu Kui, Radix Angelicae Sinensis, fermentation Chinese wolfberry fruit liquid, dandelion extract, Millettia extract includes Flavonoid substances, β-Hu The materials such as radish element, forulic acid, black alcohol compound, Ligustilide, Quercetin, polysaccharose substance, due to them and polyglutamic acid Active force it is different, during sustained release, usually the alkaloids substance with bactericidal action take the lead in entering it is intracellular again Anti-inflammation and sterilization is carried out, followed by Flavonoid substances, forulic acid, black alcohol compound and polysaccharose substance are repaired into cell And cytothesis, it is finally that the materials such as beta carotene and Ligustilide enter cell enhancing cell viability, shines skin.This hair Bright sun-proof reparation facial mask effectively controls each nutritional ingredient into the order of Skin Cell, by mutually being cooperateed between each component, Collective effect, quick repair cell.
Therefore, using pure natural polyglutamic acid, this is not merely that instead of collagen, hyaluronic acid, glycerine to the present invention Etc. this moisturizing ingredient, moreover it is possible to fermentation Chinese wolfberry fruit liquid, bletilla striata zymotic fluid and fish pelargonium and chitosan oligomer and angelica extract Deng synergy, make the using effect of matrimony vine facial mask more preferable.
Beneficial effect:
Polyglutamic acid has extremely strong moisture retention, can form layer protecting film on skin to prevent the steaming of skin moisture Hair, it can penetrate into skin deep layer, self moisture-keeping system of recovery skin.With advancing age with the aggravation of physical fatigue, The function of profit certainly of skin can gradually weaken, or even disappear, and the facial mask that with the addition of polyglutamic acid can repair the profit work(certainly of skin Energy.Therefore polyglutamic acid has good beauty protecting effect for the skin of the mankind.
Polyglutamic acid be it is a kind of water-soluble, it is biodegradable, be a kind of to the high-end of the nutritious effect of skin without toxicity Product, is completely suitable for all skins, and provide the lasting moistening effect better than hyaluronic acid and collagen, it is only necessary to Very low concentration, it is possible to reach good effect, therefore cost is very low.Available for skin care item, shampoo, hair-cream, shaving cream In lipstick.Therefore, matrimony vine preparation method of the invention is easy, and feasibility is high, it is easy to promote production, and cost is not high.
The present invention polyglutamic acid this be not merely instead of this moisturizing of collagen, hyaluronic acid, glycerine etc. into Point, polyglutamic acid of the invention not only has extremely strong moisture retention, moreover it is possible to fermentation Chinese wolfberry fruit liquid, bletilla striata zymotic fluid and fish pelargonium, Synergy, makes the using effect of sun-proof facial mask more preferable.
The present invention uses the fermentation Chinese wolfberry fruit liquid of lactobacillus-fermented, and some skins of farthest degrading are not easy to absorb and easy The material of sensitization, retains the active ingredient in fermentation Chinese wolfberry fruit liquid, and the facial mask of preparation has moisturizing, a whitening, effect of anti-aging, There is certain effect to different crowd.
The bletilla striata hair polysaccharide and LBP-X that the present invention is used mutually are cooperateed with, and can effectively be removed free radical and be suppressed tyrosine The activity of enzyme, deep layer repair cell gives skin with nutrition, and impaired cell, tissue can be made to obtain timely high-quality repairing, Make skin gloss high resilience, delaying senility.
The light spot of the present invention is dispelled in yellow fermentation Chinese wolfberry fruit liquid level film, and the active component that fish pelargonium contains can effectively suppress tyrosine The activity of enzyme, blocks the synthesis of DOPA and DOPA quinone, so that contain the growth of melanin, therefore with skin brightening effect.
The light spot of the present invention is dispelled in yellow fermentation Chinese wolfberry fruit liquid level film, the angelica extract promoting flow of qi and blood circulation, increases velocity of blood flow, blood Circulate oxygen and nutriment that fibroblast, collagen for skin etc. provide abundance;Be conducive to the metabolism of cell Product and various harmful substances are removed in time, it is ensured that the metabolism of skin.
The light spot of the present invention is dispelled in yellow fermentation Chinese wolfberry fruit liquid level film, and dandelion extract, which has to clear liver, dredges strongly fragrant, toxin expelling sore Effect;Millettia extract, with promoting the circulation of qi, Fufeng, the effectiveness invigorated blood circulation.
The present invention is using substantial amounts of-NH in oligopolymerization chitosan glycan molecule3With the presence of the highly polar groups of-OH, make itself not Only make chitosan oligomer that there is good moisture-absorbing moisture-keeping function, transepidermal water can be hydrated again, protected so as to play humidification Wet effect.Moreover, the good gas permeability of chitosan oligomer does not disturb excretion of the epidermis to waste and toxin again, skin is not resulted in Acne.The skin-protection product of chitosan oligomer also plays the role of easily to be absorbed by the skin, stimulated circulation.
Black fruit fructus lycii whitening and moisturizing smoothing toner and preparation method of smoothing toner provided by the present invention, active matter is used as using the extract of pure natural product Matter, without ethanol, is not stimulated without any toxicity and side effects, gently, its active ingredient is excellent to be absorbed by the skin by aquation, is prevented Only the moisture evaporation in cuticula is reduced, with good replenishing water and preserving moisture, skin care, supplement skin-nourishing, cutin-softening, whitening Nti-freckle, prevent skin aging, isolating and protecting, improve skin quality, keep skin vigor effect;Both it can overcome the disadvantages that generalization adornment water could not The weak point of effective wetting, can overcome again common skin care item can not moisturizing whitening rapidly shortcoming, it is adaptable to various skin quality Consumer.
Embodiment
The invention will be further elucidated with reference to specific embodiments.It should be understood that these embodiments are merely to illustrate this hair Bright rather than limitation the scope of the present invention.In addition, it is to be understood that after the content of the invention lectured has been read, art technology Personnel can make various changes or modifications to the present invention, and these equivalent form of values equally fall within the application appended claims and limited Fixed scope.
Embodiment 1
The light spot of the present invention is dispelled yellow fermentation Chinese wolfberry fruit liquid level film, by weight, including composition it is as follows:
25 parts of pure water;
20 parts of fermentation Chinese wolfberry fruit liquid;
2 parts of polyglutamic acid;Molecular weight is 950,000
0.3 part of vitamin C;
15 parts of asparagus juice;
10 parts of pearl powder;The particle diameter of pearl powder is 100 nanometers;
0.3 part of propane diols;
2 parts of chitosan oligomer;Molecular weight is 1300;
10 parts of bletilla striata zymotic fluid;
6 parts of Flos Pelargonii Hortori;
1 part of angelica extract;
2 parts of dandelion extract;
5 parts of Millettia extract;
2 parts of pulullan polysaccharide;Molecular weight is 200,000;
The light spot of the present invention is dispelled the preparation method of yellow fermentation Chinese wolfberry fruit liquid level film, is comprised the following steps:In prepared by matrimony vine facial mask The addition of each component is identical with the parts by weight of each component in above-mentioned matrimony vine facial mask;
(1) polyglutamic acid and pearl powder are dissolved in pure water, and stirred, stir speed (S.S.) is 80r/min, make its into For thick liquid;
(2) asparagus juice is added in aforesaid liquid, sequentially adds vitamin C, propane diols, pulullan polysaccharide and matrimony vine Zymotic fluid, chitosan oligomer, bletilla striata zymotic fluid, Flos Pelargonii Hortori and angelica extract, dandelion extract and reticulate millettia carry Take thing to stir and evenly mix, stir speed (S.S.) is 80r/min, obtain facial mask stoste;The preparation method of bletilla striata zymotic fluid and fermentation Chinese wolfberry fruit liquid It is identical.
(3) after facial mask stoste is sterilized, then spunlace non-woven cloth Face film towel soaked into 30min, Ran Houzhen in facial mask stoste Sky encapsulation, is made matrimony vine facial mask.
Wherein fermentation Chinese wolfberry fruit liquid and preparation method thereof is as follows:By dry wolfberry and water in mass ratio 1:8 mixing fully mashing, is used as base Plinth liquid, following percentage by weight material is added into basal liquid:Yeast extract 0.1%, dipotassium hydrogen phosphate 0.03%, magnesium sulfate 0.01%, Triammonium citrate 0.1%, manganese sulfate 0.001% sterilizes, inoculating lactic acid bacterium is placed on shaking table after fully mixing 180rpm, cultivates 48h, obtains fermentation Chinese wolfberry fruit stoste by 30 DEG C;By the fermenation raw liquid filtration sterilization, retain supernatant and by supernatant The pH value of liquid is adjusted to neutrality, obtains fermentation Chinese wolfberry fruit liquid.
Angelica extract, Flos Pelargonii Hortori, the extracting method of dandelion extract and Millettia extract are:It will make After standby extract is crushed, add volume fraction and filtered for 45% ethanol solution;Then macropore is placed in after filtered fluid is concentrated On adsorption resin column, after the ethanol solution elution of same volume fraction, dry and obtain the extract.
Embodiment 2
The light spot of the present invention is dispelled yellow fermentation Chinese wolfberry fruit liquid level film, by weight, including composition it is as follows:
40 parts of pure water;
22 parts of fermentation Chinese wolfberry fruit liquid;
4 parts of polyglutamic acid;Molecular weight is 910,000
0.4 part of vitamin C;
16 parts of asparagus juice;
12 parts of pearl powder;The particle diameter of pearl powder is 200 nanometers;
0.4 part of propane diols;
5 parts of chitosan oligomer;Molecular weight is 1600;
5 parts of bletilla striata zymotic fluid;
3 parts of Flos Pelargonii Hortori;
3 parts of angelica extract;
4 parts of dandelion extract;
3 parts of Millettia extract;
4 parts of pulullan polysaccharide;Molecular weight is 250,000;
The light spot of the present invention is dispelled the preparation method of yellow fermentation Chinese wolfberry fruit liquid level film, is comprised the following steps:In prepared by matrimony vine facial mask The addition of each component is identical with the parts by weight of each component in above-mentioned matrimony vine facial mask;
(1) polyglutamic acid and pearl powder are dissolved in pure water, and stirred, stir speed (S.S.) is 90r/min, make its into For thick liquid;
(2) asparagus juice is added in aforesaid liquid, sequentially adds vitamin C, propane diols, pulullan polysaccharide and matrimony vine Zymotic fluid, chitosan oligomer, bletilla striata zymotic fluid, Flos Pelargonii Hortori and angelica extract, dandelion extract and reticulate millettia carry Take thing to stir and evenly mix, stir speed (S.S.) is 90r/min, obtain facial mask stoste;The preparation method of bletilla striata zymotic fluid and fermentation Chinese wolfberry fruit liquid It is identical.
(3) after facial mask stoste is sterilized, then spunlace non-woven cloth Face film towel soaked into 35min, Ran Houzhen in facial mask stoste Sky encapsulation, is made matrimony vine facial mask.
Wherein fermentation Chinese wolfberry fruit liquid and preparation method thereof is as follows:By dry wolfberry and water in mass ratio 1:8 mixing fully mashing, is used as base Plinth liquid, following percentage by weight material is added into basal liquid:Yeast extract 0.1%, dipotassium hydrogen phosphate 0.03%, magnesium sulfate 0.01%, Triammonium citrate 0.1%, manganese sulfate 0.001% sterilizes, inoculating lactic acid bacterium is placed on shaking table after fully mixing 180rpm, cultivates 48h, obtains fermentation Chinese wolfberry fruit stoste by 30 DEG C;By the fermenation raw liquid filtration sterilization, retain supernatant and by supernatant The pH value of liquid is adjusted to neutrality, obtains fermentation Chinese wolfberry fruit liquid.Lactic acid bacteria is CGMCC NO.1.1 lactic acid bacterias.
Angelica extract, Flos Pelargonii Hortori, the extracting method of dandelion extract and Millettia extract are:It will make After standby extract is crushed, add volume fraction and filtered for 75% ethanol solution;Then macropore is placed in after filtered fluid is concentrated On adsorption resin column, after the ethanol solution elution of same volume fraction, dry and obtain the extract.
Embodiment 3
The light spot of the present invention is dispelled yellow fermentation Chinese wolfberry fruit liquid level film, by weight, including composition it is as follows:It is prepared by matrimony vine facial mask The addition of middle each component is identical with the parts by weight of each component in above-mentioned matrimony vine facial mask;
30 parts of pure water;
25 parts of fermentation Chinese wolfberry fruit liquid;
3 parts of polyglutamic acid;Molecular weight is 1,000,000
0.4 part of vitamin C;
17 parts of asparagus juice;
15 parts of pearl powder;The particle diameter of pearl powder is 100 nanometers;
0.8 part of propane diols;
4 parts of chitosan oligomer;Molecular weight is 1500;
6 parts of bletilla striata zymotic fluid;
4 parts of Flos Pelargonii Hortori;
2 parts of angelica extract;
3 parts of dandelion extract;
5 parts of Millettia extract;
5 parts of pulullan polysaccharide;Molecular weight is 300,000;
The light spot of the present invention is dispelled the preparation method of yellow fermentation Chinese wolfberry fruit liquid level film, is comprised the following steps:In prepared by matrimony vine facial mask The addition of each component is identical with the parts by weight of each component in above-mentioned matrimony vine facial mask;
(1) polyglutamic acid and pearl powder are dissolved in pure water, and stirred, stir speed (S.S.) is 100r/min, makes it As thick liquid;
(2) asparagus juice is added in aforesaid liquid, sequentially adds vitamin C, propane diols, pulullan polysaccharide and matrimony vine Zymotic fluid, chitosan oligomer, bletilla striata zymotic fluid, Flos Pelargonii Hortori and angelica extract, dandelion extract and reticulate millettia carry Take thing to stir and evenly mix, stir speed (S.S.) is 100r/min, obtain facial mask stoste;The preparation method of bletilla striata zymotic fluid and fermentation Chinese wolfberry fruit liquid It is identical.
(3) after facial mask stoste is sterilized, then spunlace non-woven cloth Face film towel soaked into 40min, Ran Houzhen in facial mask stoste Sky encapsulation, is made matrimony vine facial mask.
Wherein fermentation Chinese wolfberry fruit liquid and preparation method thereof is as follows:By dry wolfberry and water in mass ratio 1:15 mixing fully mashing, as Basal liquid, following percentage by weight material is added into basal liquid:Yeast extract 0.4%, dipotassium hydrogen phosphate 0.2%, sulfuric acid Magnesium 0.2%, Triammonium citrate 0.2%, manganese sulfate 0.005% sterilizes, inoculating lactic acid bacterium is placed on shaking table after fully mixing 180rpm, cultivates 48h, obtains fermentation Chinese wolfberry fruit stoste by 30 DEG C;By the fermenation raw liquid filtration sterilization, retain supernatant and by supernatant The pH value of liquid is adjusted to neutrality, obtains fermentation Chinese wolfberry fruit liquid.Lactic acid bacteria is CGMCC NO.1.1 lactic acid bacterias.
Angelica extract, Flos Pelargonii Hortori, the extracting method of dandelion extract and Millettia extract are:It will make After standby extract is crushed, add volume fraction and filtered for 60% ethanol solution;Then macropore is placed in after filtered fluid is concentrated On adsorption resin column, after the ethanol solution elution of same volume fraction, dry and obtain the extract.
Embodiment 4
The light spot of the present invention is dispelled yellow fermentation Chinese wolfberry fruit liquid level film, by weight, including composition it is as follows:
40 parts of pure water;
35 parts of fermentation Chinese wolfberry fruit liquid;
3 parts of polyglutamic acid;Molecular weight is 1,000,000
0.5 part of vitamin C;
20 parts of asparagus juice;
15 parts of pearl powder;The particle diameter of pearl powder is 100 nanometers;
0.8 part of propane diols;
3 parts of chitosan oligomer;Molecular weight is 1500;
7 parts of bletilla striata zymotic fluid;
5 parts of Flos Pelargonii Hortori;
2.5 parts of angelica extract;
4 parts of dandelion extract;
3 parts of Millettia extract;
3 parts of pulullan polysaccharide;Molecular weight is 200,000;
The light spot of the present invention is dispelled the preparation method of yellow fermentation Chinese wolfberry fruit liquid level film, is comprised the following steps:In prepared by matrimony vine facial mask The addition of each component is identical with the parts by weight of each component in above-mentioned matrimony vine facial mask;
(1) polyglutamic acid and pearl powder are dissolved in pure water, and stirred, stir speed (S.S.) is 85r/min, make its into For thick liquid;
(2) asparagus juice is added in aforesaid liquid, sequentially adds vitamin C, propane diols, pulullan polysaccharide and matrimony vine Zymotic fluid, chitosan oligomer, bletilla striata zymotic fluid, Flos Pelargonii Hortori and angelica extract, dandelion extract and reticulate millettia carry Take thing to stir and evenly mix, stir speed (S.S.) is 85r/min, obtain facial mask stoste;The preparation method of bletilla striata zymotic fluid and fermentation Chinese wolfberry fruit liquid It is identical.
(3) after facial mask stoste is sterilized, then spunlace non-woven cloth Face film towel soaked into 33min, Ran Houzhen in facial mask stoste Sky encapsulation, is made matrimony vine facial mask.
Wherein fermentation Chinese wolfberry fruit liquid and preparation method thereof is as follows:By dry wolfberry and water in mass ratio 1:15 mixing fully mashing, as Basal liquid, following percentage by weight material is added into basal liquid:Yeast extract 0.4%, dipotassium hydrogen phosphate 0.2%, sulfuric acid Magnesium 0.2%, Triammonium citrate 0.2%, manganese sulfate 0.005% sterilizes, inoculating lactic acid bacterium is placed on shaking table after fully mixing 180rpm, cultivates 48h, obtains fermentation Chinese wolfberry fruit stoste by 30 DEG C;By the fermenation raw liquid filtration sterilization, retain supernatant and by supernatant The pH value of liquid is adjusted to neutrality, obtains fermentation Chinese wolfberry fruit liquid.Lactic acid bacteria is CGMCC NO.1.1 lactic acid bacterias.
Angelica extract, Flos Pelargonii Hortori, the extracting method of dandelion extract and Millettia extract are:It will make After standby extract is crushed, add volume fraction and filtered for 30% ethanol solution;Then macropore is placed in after filtered fluid is concentrated On adsorption resin column, after the ethanol solution elution of same volume fraction, dry and obtain the extract.
Embodiment 5
The light spot of the present invention is dispelled yellow fermentation Chinese wolfberry fruit liquid level film, by weight, including composition it is as follows:
35 parts of pure water;
30 parts of fermentation Chinese wolfberry fruit liquid;
4 parts of polyglutamic acid;Molecular weight is 1,010,000
0.4 part of vitamin C;
18 parts of asparagus juice;
13 parts of pearl powder;The particle diameter of pearl powder is 100nm;
0.6 part of propane diols;
2 parts of chitosan oligomer;Molecular weight is 1400;
0 part of bletilla striata zymotic fluid;
4 parts of Flos Pelargonii Hortori;
2 parts of angelica extract;
2 parts of dandelion extract;
4 parts of Millettia extract;
5 parts of pulullan polysaccharide;Molecular weight is 300,000;
The light spot of the present invention is dispelled the preparation method of yellow fermentation Chinese wolfberry fruit liquid level film, is comprised the following steps:In prepared by matrimony vine facial mask The addition of each component is identical with the parts by weight of each component in above-mentioned matrimony vine facial mask;
(1) polyglutamic acid and pearl powder are dissolved in pure water, and stirred, stir speed (S.S.) is 95r/min, make its into For thick liquid;
(2) asparagus juice is added in aforesaid liquid, sequentially adds vitamin C, propane diols, pulullan polysaccharide and matrimony vine Zymotic fluid, chitosan oligomer, bletilla striata zymotic fluid, Flos Pelargonii Hortori and angelica extract, dandelion extract and reticulate millettia carry Take thing to stir and evenly mix, stir speed (S.S.) is 95r/min, obtain facial mask stoste;The preparation method of bletilla striata zymotic fluid and fermentation Chinese wolfberry fruit liquid It is identical.
(3) after facial mask stoste is sterilized, then spunlace non-woven cloth Face film towel soaked into 38min, Ran Houzhen in facial mask stoste Sky encapsulation, is made matrimony vine facial mask.
Wherein fermentation Chinese wolfberry fruit liquid and preparation method thereof is as follows:By dry wolfberry and water in mass ratio 1:12 mixing fully mashing, as Basal liquid, following percentage by weight material is added into basal liquid:Yeast extract 0.3%, dipotassium hydrogen phosphate 0.1%, sulfuric acid Magnesium 0.05%, Triammonium citrate 0.12%, manganese sulfate 0.004% sterilizes, inoculating lactic acid bacterium is placed on shaking table after fully mixing 180rpm, cultivates 48h, obtains fermentation Chinese wolfberry fruit stoste by 30 DEG C;By the fermenation raw liquid filtration sterilization, retain supernatant and by supernatant The pH value of liquid is adjusted to neutrality, obtains fermentation Chinese wolfberry fruit liquid.Lactic acid bacteria is CGMCC NO.1.1 lactic acid bacterias.
Angelica extract, Flos Pelargonii Hortori, the extracting method of dandelion extract and Millettia extract are:It will make After standby extract is crushed, add volume fraction and filtered for 95% ethanol solution;Then macropore is placed in after filtered fluid is concentrated On adsorption resin column, after the ethanol solution elution of same volume fraction, dry and obtain the extract.
Embodiment 6
The light spot of the present invention is dispelled yellow fermentation Chinese wolfberry fruit liquid level film, by weight, including composition it is as follows:
30 parts of pure water;
28 parts of fermentation Chinese wolfberry fruit liquid;
3 parts of polyglutamic acid;The molecular weight of polyglutamic acid is 950,000
0.4 part of vitamin C;
16 parts of asparagus juice;
12 parts of pearl powder;
0.5 part of propane diols;
3 parts of chitosan oligomer;Molecular weight is 1500;
8 parts of bletilla striata zymotic fluid;
5 parts of Flos Pelargonii Hortori;
2 parts of angelica extract;
3 parts of dandelion extract;
5 parts of Millettia extract;
5 parts of pulullan polysaccharide;The molecular weight of pulullan polysaccharide is 300,000;
The light spot of the present invention is dispelled the preparation method of yellow fermentation Chinese wolfberry fruit liquid level film, is comprised the following steps:In prepared by matrimony vine facial mask The addition of each component is identical with the parts by weight of each component in above-mentioned matrimony vine facial mask;
(1) polyglutamic acid and pearl powder are dissolved in pure water, and stirred, stir speed (S.S.) is 95r/min, make its into For thick liquid;
(2) asparagus juice is added in aforesaid liquid, sequentially adds vitamin C, propane diols, pulullan polysaccharide and matrimony vine Zymotic fluid, chitosan oligomer, bletilla striata zymotic fluid, Flos Pelargonii Hortori and angelica extract, dandelion extract and reticulate millettia carry Take thing to stir and evenly mix, stir speed (S.S.) is 95r/min, obtain facial mask stoste;The preparation method of bletilla striata zymotic fluid and fermentation Chinese wolfberry fruit liquid It is identical.
(3) after facial mask stoste is sterilized, then spunlace non-woven cloth Face film towel soaked into 38min, Ran Houzhen in facial mask stoste Sky encapsulation, is made matrimony vine facial mask.
Wherein fermentation Chinese wolfberry fruit liquid and preparation method thereof is as follows:By dry wolfberry and water in mass ratio 1:12 mixing fully mashing, as Basal liquid, following percentage by weight material is added into basal liquid:Yeast extract 0.3%, dipotassium hydrogen phosphate 0.1%, sulfuric acid Magnesium 0.05%, Triammonium citrate 0.12%, manganese sulfate 0.004% sterilizes, inoculating lactic acid bacterium is placed on shaking table after fully mixing 180rpm, cultivates 48h, obtains fermentation Chinese wolfberry fruit stoste by 30 DEG C;By the fermenation raw liquid filtration sterilization, retain supernatant and by supernatant The pH value of liquid is adjusted to neutrality, obtains fermentation Chinese wolfberry fruit liquid.Lactic acid bacteria is CGMCC NO.1.1 lactic acid bacterias.
Angelica extract, Flos Pelargonii Hortori, the extracting method of dandelion extract and Millettia extract are:It will make After standby extract is crushed, add volume fraction and filtered for 40% ethanol solution;Then macropore is placed in after filtered fluid is concentrated On adsorption resin column, after the ethanol solution elution of same volume fraction, dry and obtain the extract.
Comparative example 1
A kind of light spot is dispelled yellow fermentation Chinese wolfberry fruit liquid level film, and light spot prepared by itself and embodiment 6 is dispelled yellow fermentation Chinese wolfberry fruit liquid level film Difference, which is only that, does not contain bletilla striata zymotic fluid.
Comparative example 2
A kind of light spot is dispelled yellow fermentation Chinese wolfberry fruit liquid level film, and light spot prepared by itself and embodiment 6 is dispelled yellow fermentation Chinese wolfberry fruit liquid level film Difference, which is only that, does not contain fermentation Chinese wolfberry fruit liquid.
Comparative example 3
A kind of light spot is dispelled yellow fermentation Chinese wolfberry fruit liquid level film, and light spot prepared by itself and embodiment 6 is dispelled yellow fermentation Chinese wolfberry fruit liquid level film Difference, which is only that, does not contain polyglutamic acid.
Performance detection
Rationally, property is stable for the face pack prescription for the skin whitening, moisturizing function that the present invention is provided, action temperature and no skin irritatin Property, and by the synergy of various active ingredients, the effects such as with significant skin whitening, moisturizing;
First, human skin patch
With reference to the Ministry of Public Health《Cosmetics health specification》In (version in 2007) related request of " human skin patch " and Method carries out " human body skin enclosed type patch test ".
1st, given the test agent:The facial mask stoste that the embodiment of the present invention 6, comparative example 1-3 are prepared.
2nd, test method:The volunteer that selection 140 meets inclusion criteria participates in experiment, is randomly divided into 4 groups, every group 35 People.From 4 layers of 1cm2The gauze facial mask stoste of size is soaked, and gauze is pasted on into trial volunteer with non-stimulated adhesive tape cloth The bent side of forearm, gently pressed with palm and be allowed to equably be pasted on skin, tested material spot examination device is removed after 24h, respectively at Dermoreaction is observed after 30min, 2h, 4h, 24h and 48h, according to《Skin adverse reaction grade scale table》Record reaction result.
3rd, result of the test:Embodiment 6, the result of the test of all trial volunteers of comparative example 1-3 groups are negative findings, by This can determine that the facial mask of skin whitening, moisturizing function prepared by the embodiment of the present invention 6, comparative example 1-3 is without skin adverse reaction, security It is high.
2nd, the inhibition experiment of tyrosinase
2.1 treatment groups (the facial mask stoste that EXAMPLE Example 6, comparative example 1-3 are prepared).
1mL facial mask stostes, 0.9mL pH=6.8 phosphate buffer and 1mL 0.03% tyrosinase in test tube, It is placed in 37 DEG C of thermostat 10 minutes, adds 0.1mL (1070units/mL) tyrosinase aqueous solution, solution is mixed equal It is even, it is placed in constant temperature water bath and reacts 25 minutes, its 475nm absorbance A is measured with spectrophotometric.
2.2 blank group
Tyrosinase is replaced with isometric phosphate buffer, its absorbance B is surveyed.
2.3 control group
Facial mask stoste is replaced with isometric distilled water, its absorbance C is surveyed.
2.4 total blank groups
Facial mask stoste is replaced with isometric distilled water, tyrosinase is replaced with isometric phosphate buffer, its suction is surveyed Luminosity D.
Inhibiting rate (%)=[(C-D)-(A-B)]/(C-D) × 100%, the results are shown in Table 2.
The inhibition of the embodiment 6 of table 1 and comparative example 1-3 group tyrosinases
3rd, radicals scavenging experimental result
3.1 experimental principle
After skin cell is oxidized, a kind of harmful substance can be produced free radical to encroach on skin, when there is radicals scavenging In the presence of agent, absorb its due to being matched with its unimolecule and disappear, the electron amount that its fading extent receives with it is into quantitatively Relation, thus available spectrophotometer carries out quick quantitative analysis.
3.2 test method
3.2.1 treatment group
A certain amount of Chinese medicine extract and a certain amount of ethanol solution is gone to make both volume sums be 1mL, with 2mLDPPH free radicals are sufficiently mixed uniformly, stand 30 minutes, and absorbance A at 517nm is measured with spectrophotometric.
3.2.2 treatment group
Extract solution is replaced with distilled water, its absorbance B is surveyed.
Clearance rate (%)=(B-A)/B*100%, the results are shown in Table 3.
The radicals scavenging experiment effect of the embodiment 6 of table 2 and comparative example 1-3 groups
4th, sensory evaluation
1st, given the test agent:The facial mask stoste that the embodiment of the present invention 6, comparative example 1-3 are prepared.
2nd, test method:The volunteer that selection 140 meets inclusion criteria participates in experiment, is randomly divided into 4 groups, every group 35 People, each 35 people of embodiment 6, comparative example 1-3 groups.Each group trial volunteer tries out above-mentioned given the test agent respectively, continuous to use one Month, try out after terminating, the using effect such as each trial volunteer this self-assessment moisturizing, whitening, sun-proof, overall assessment is done sense organ and commented Valency, according to using effect in a 0-10/marking, 9-10 points are fine, and 7-8 points are preferable, and 5-6 points are general, and 3-4 points are Poor, 1-2 points are very poor, are averaged.
3rd, result of the test:It is shown in Table 3.
The skin whitening, moisturizing effect assessment of the embodiment 6 of table 3 and comparative example 1-3 groups
Group Embodiment 1 Comparative example 1 Comparative example 2 Comparative example 3
Light spot effect 9.0 8.5 8.4 8.0
Dispel yellow effect 8.5 8.3 8.3 8.3
Clearly without greasy feeling 9.0 8.9 8.9 9.0
Assimilation effect 8.9 8.9 8.9 8.9
Overall assessment 9.0 8.5 8.3 8.2
As can be known from the results of Table 3, the degree of recognition of the facial mask of skin whitening, moisturizing function prepared by the embodiment of the present invention 6 is high, uses Effect assessment is high.The light spot that the present invention is prepared dispels yellow fermentation Chinese wolfberry fruit liquid level film repairing effect significantly, and after use, skin is salubrious Without greasy feeling, good absorbing effect.Continuously using after one month, the phenomenon such as trial volunteer's dry skin, epidermal pigment calmness is bright It is aobvious to improve.In process of the test, trial volunteer is without allergy or other skin adverse reactions.The light spot that contrast 1-3 is prepared The reparation facial mask that the using effect of yellow fermentation Chinese wolfberry fruit liquid level film of dispelling is prepared not as embodiment 6.
Above content is to combine specific preferred embodiment further description made for the present invention, it is impossible to assert The specific implementation of the present invention is confined to these explanations.For general technical staff of the technical field of the invention, On the premise of not departing from present inventive concept, some simple deduction or replace can also be made, should all be considered as belonging to the present invention's Design.

Claims (10)

  1. The yellow fermentation Chinese wolfberry fruit liquid level film 1. a kind of light spot is dispelled, it is characterized in that:The light spot dispels yellow fermentation Chinese wolfberry fruit liquid level film including spun lacing The facial mask stoste of non-woven fabrics Face film towel and infiltration on spunlace non-woven cloth;The facial mask stoste includes the group of following parts by weight Point:
    25-40 parts of pure water;
    20-35 parts of fermentation Chinese wolfberry fruit liquid;
    2-4 parts of polyglutamic acid;
    0.3-0.5 parts of vitamin C;
    15-20 parts of asparagus juice;
    10-15 parts of pearl powder;
    0.3-0.8 parts of propane diols;
    2-5 parts of chitosan oligomer;
    5-10 parts of bletilla striata zymotic fluid;
    3-6 parts of Flos Pelargonii Hortori;
    1-3 parts of angelica extract;
    3-7 parts of pulullan polysaccharide;
    2-4 parts of dandelion extract;
    3-5 parts of Millettia extract;
    The molecular weight of the polyglutamic acid is 91-101 ten thousand.
  2. The yellow fermentation Chinese wolfberry fruit liquid level film 2. light spot according to claim 1 is dispelled, it is characterised in that point of the chitosan oligomer Son amount is 1300-1600;Fermentation Chinese wolfberry fruit liquid is red fermentation Chinese wolfberry fruit liquid.
  3. The yellow fermentation Chinese wolfberry fruit liquid level film 3. light spot according to claim 1 is dispelled, it is characterised in that the fermentation Chinese wolfberry fruit liquid and white The lactic acid bacteria that splendid achnatherum zymotic fluid is used when fermenting is CGMCC NO.1.1 lactic acid bacterias.
  4. The yellow fermentation Chinese wolfberry fruit liquid level film 4. light spot according to claim 1 is dispelled, it is characterised in that the particle diameter of the pearl powder is 100-200nm;The molecular weight of the pulullan polysaccharide is 20-40 ten thousand.
  5. 5. yellow fermentation Chinese wolfberry fruit liquid level film of being dispelled according to any described light spot of claim 1, it is characterised in that the facial mask stoste bag Include the component of following parts by weight:30 parts of pure water, 28 parts of fermentation Chinese wolfberry fruit liquid, 3 parts of polyglutamic acid, 0.4 part of vitamin C, aloe 16 parts of juice, 12 parts of pearl powder, 0.5 part of propane diols, 3 parts of chitosan oligomer, 8 parts of bletilla striata zymotic fluid, 5 parts of Flos Pelargonii Hortori, when Return 2 parts of extract and 5 parts of 5 parts of pulullan polysaccharide, 3 parts of dandelion extract and Millettia extract;Point of the polyglutamic acid Son amount is 950,000.
  6. The preparation method of yellow fermentation Chinese wolfberry fruit liquid level film 6. the light spot as described in claim 1-5 is any is dispelled, it is characterized in that, including with Lower step:
    (1)Polyglutamic acid and pearl powder are dissolved in pure water, and stirred, thick liquid is become;
    (2)Asparagus juice is added in aforesaid liquid, vitamin C, propane diols, pulullan polysaccharide and fermentation Chinese wolfberry fruit is sequentially added Liquid, chitosan oligomer, bletilla striata zymotic fluid, Flos Pelargonii Hortori and angelica extract, dandelion extract and Millettia extract Stir and evenly mix, obtain facial mask stoste;
    (3)Soaked after the sterilizing of facial mask stoste, then by spunlace non-woven cloth Face film towel in facial mask stoste, then Vacuum Package, system Obtain matrimony vine facial mask.
  7. The preparation method of yellow fermentation Chinese wolfberry fruit liquid level film 7. light spot according to claim 6 is dispelled, it is characterised in that:The matrimony vine The preparation method of zymotic fluid is:By dry wolfberry and water in mass ratio 1:The abundant mashing of 8-15 mixing, based on liquid, to basal liquid It is middle to add following percentage by weight material:Yeast extract 0.1-0.4%, dipotassium hydrogen phosphate 0.03-0.2%, magnesium sulfate 0.01- 0.2%, Triammonium citrate 0.1-0.2%, manganese sulfate 0.001-0.005%, sterilize, inoculating lactic acid bacterium is placed in shaking table after fully mixing Upper 180rpm, cultivates 48h, obtains fermentation Chinese wolfberry fruit stoste by 30 DEG C;By the fermenation raw liquid filtration sterilization, reservation supernatant simultaneously will be upper The pH value of clear liquid is adjusted to neutrality, obtains fermentation Chinese wolfberry fruit liquid.
  8. The preparation method of yellow fermentation Chinese wolfberry fruit liquid level film 8. light spot according to claim 6 is dispelled, it is characterised in that:Step(1) Or step(2)The stir speed (S.S.) used during middle stirring is 80-100r/min;Step(3)The time of middle immersion is 30-40min.
  9. The preparation method of yellow fermentation Chinese wolfberry fruit liquid level film 9. the light spot according to claim 6 or 7 is dispelled, it is characterised in that:The bletilla striata Zymotic fluid is identical with the preparation method of fermentation Chinese wolfberry fruit liquid.
  10. The preparation method of yellow fermentation Chinese wolfberry fruit liquid level film 10. light spot according to claim 6 is dispelled, it is characterised in that:Radix Angelicae Sinensis is carried The extracting method for taking thing, Flos Pelargonii Hortori, dandelion extract and Millettia extract is:The extract that will be prepared is crushed Afterwards, volume fraction is added to filter for 30%-95% ethanol solution;Then large pore resin absorption column is placed in after filtered fluid is concentrated On, after the ethanol solution elution of same volume fraction, dry and obtain the extract.
CN201710547066.6A 2017-07-06 2017-07-06 A kind of light spot is dispelled yellow fermentation Chinese wolfberry fruit liquid level film and preparation method thereof Pending CN107233275A (en)

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CN112245648A (en) * 2020-10-30 2021-01-22 广州润虹医药科技股份有限公司 Anti-inflammatory and antibacterial hydrocolloid oily yarn and preparation method thereof

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CN109077954A (en) * 2018-08-06 2018-12-25 佗鹊堂国投生物科技股份有限公司 Cordyceps sinensis facial mask
CN112245648A (en) * 2020-10-30 2021-01-22 广州润虹医药科技股份有限公司 Anti-inflammatory and antibacterial hydrocolloid oily yarn and preparation method thereof
CN112245648B (en) * 2020-10-30 2022-05-17 广州润虹医药科技股份有限公司 Anti-inflammatory and antibacterial hydrocolloid oily yarn and preparation method thereof

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Application publication date: 20171010