CN110787100A - Anti-allergy skin-soothing essence and preparation method thereof - Google Patents
Anti-allergy skin-soothing essence and preparation method thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/13—Coniferophyta (gymnosperms)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/28—Asteraceae or Compositae (Aster or Sunflower family), e.g. chamomile, feverfew, yarrow or echinacea
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/28—Asteraceae or Compositae (Aster or Sunflower family), e.g. chamomile, feverfew, yarrow or echinacea
- A61K36/282—Artemisia, e.g. wormwood or sagebrush
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/645—Proteins of vegetable origin; Derivatives or degradation products thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9755—Gymnosperms [Coniferophyta]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P29/00—Non-central analgesic, antipyretic or antiinflammatory agents, e.g. antirheumatic agents; Non-steroidal antiinflammatory drugs [NSAID]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P37/00—Drugs for immunological or allergic disorders
- A61P37/08—Antiallergic agents
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/005—Preparations for sensitive skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/85—Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/88—Liliopsida (monocotyledons)
- A61K36/886—Aloeaceae (Aloe family), e.g. aloe vera
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/88—Liliopsida (monocotyledons)
- A61K36/896—Liliaceae (Lily family), e.g. daylily, plantain lily, Hyacinth or narcissus
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
Abstract
The invention belongs to the field of skin care products, and discloses an anti-allergy skin-soothing essence and a preparation method thereof. The essence is prepared from deionized water, herba Sidae Rhombifoliae extractive solution, Aloe extractive solution, herba Sidae Rhombifoliae/folium Artemisiae Argyi fermented extractive solution, corn gluten, hydroxyethyl cellulose, hyaluronic acid, glycerol, butanediol and Cera flava. The anti-allergy skin-soothing essence disclosed by the invention is scientific and reasonable in raw material proportion, fully utilizes the soothing and anti-allergy effects of the calendula extract, the aloe extract and the calendula/wormwood fermented extract and the effect of corn gluten on increasing the skin elasticity, and all the components supplement each other, so that the essence can effectively improve the problem of allergic skin, eliminate turbid substances accumulated in the skin and harmful substances generated due to pollution, achieve the effects of moistening the skin, resisting allergy, diminishing inflammation, tightening the skin and whitening and moisturizing, and not only can clean, nourish and protect the skin, but also can effectively relieve and resist allergy and prevent skin chapping.
Description
Technical Field
The invention belongs to the field of cosmetics, and particularly relates to an anti-allergy skin-soothing essence and a preparation method thereof.
Background
The essence can temporarily isolate outside air and pollution, improve the skin temperature, dilate pores of the skin, promote secretion and metabolism of sweat glands, and is beneficial to the skin to remove products of epidermal cell metabolism and accumulated grease substances, the components in the essence permeate into the horny layer of the epidermis, the skin can be greatly improved, and the essence becomes an important link in modern skin care. With the development of society, the current environment is worse and worse, the influence on the skin is very large, the skin becomes very sensitive by pollutants, the skin cannot be improved by only using a mask, the essence is convenient to use and effective, but most of the existing essence supplements moisture and nutrition for the skin, and the problem of sensitivity to the skin is rarely solved.
At present, products used by people with sensitive skin are launched by all major brands in the market, but few products capable of effectively relieving and treating the sensitive skin are available. Therefore, the product is developed, the calendula extracting solution and the calendula/wormwood fermentation extracting solution are mainly used as anti-allergy components, and the product can clean, nourish and protect the skin, can effectively relieve and resist allergy and solves the problem of people with sensitive skin.
Disclosure of Invention
The first technical problem to be solved by the invention is to provide the calendula extract as the main anti-allergy skin-soothing essence which has the effects of moistening skin, resisting allergy, diminishing inflammation, tightening skin, whitening and moisturizing.
In order to solve the technical problems, the invention adopts the technical scheme that:
the anti-allergy skin-soothing essence is prepared from the following raw materials in parts by weight: 15-30 parts of calendula extract, 10-20 parts of aloe extract, 5-10 parts of calendula/wormwood fermentation extract, 300-500 parts of deionized water, 3-8 parts of corn gluten, 1-3 parts of hydroxyethyl cellulose, 1-3 parts of hyaluronic acid, 10-20 parts of glycerol, 5-10 parts of butanediol and 3-5 parts of beeswax.
The anti-allergy skin-soothing essence is prepared from the following raw materials in parts by weight: 20-30 parts of a calendula extract, 15-20 parts of an aloe extract, 6-8 parts of a calendula/wormwood fermentation extract, 350-450 parts of deionized water, 5-8 parts of corn gluten, 1-2 parts of hydroxyethyl cellulose, 2-3 parts of hyaluronic acid, 15-20 parts of glycerol, 6-8 parts of butanediol and 3-5 parts of beeswax.
The anti-allergy skin-soothing essence is prepared from the following raw materials in parts by weight: 20 parts of calendula extract, 15 parts of aloe extract, 8 parts of calendula/wormwood fermented extract, 400 parts of deionized water, 6 parts of corn gluten, 2 parts of hydroxyethyl cellulose, 3 parts of hyaluronic acid, 15 parts of glycerol, 7 parts of butanediol and 4 parts of beeswax.
In the anti-allergy skin-soothing essence, the calendula extract is prepared by the following steps:
(1) and (3) drying: drying the calendula at 30-50 ℃ for 3-5 h;
(2) and (3) cooking: steaming dried herba Sidae Rhombifoliae at high temperature under high pressure;
(3) crushing: pulverizing the cooked calendula to particle size of more than 60 meshes to obtain calendula powder;
(4) and (3) extraction: adding organic solvent and carbon powder into the calendula officinalis powder for extraction;
(5) and (3) distillation: distilling under reduced pressure to obtain herba Sidae Rhombifoliae extract.
In the anti-allergy skin-soothing essence, the aloe extract is prepared by the following steps:
(1) and (3) drying: drying aloe at 30-50 ℃ for 3-5 h;
(2) and (3) cooking: steaming the dried aloe at high temperature and high pressure;
(3) crushing: pulverizing the steamed aloe to particle size of more than 60 meshes to obtain calendula officinalis powder;
(4) and (3) extraction: adding organic solvent and carbon powder into the aloe powder for extraction;
(5) and (3) distillation: distilling under reduced pressure to obtain Aloe extract.
Wherein, in the anti-allergy skin-soothing essence, the calendula/wormwood fermented extract is prepared by the following steps:
(1) and (3) drying: drying the calendula and the wormwood at the temperature of 30-50 ℃ for 3-5 h;
(2) and (3) cooking: steaming dried herba Sidae Rhombifoliae and folium Artemisiae Argyi at high temperature and high pressure;
(3) crushing: respectively crushing the cooked calendula and wormwood to obtain powder with the granularity of over 60 meshes;
(4) fermentation: taking 10 parts by weight of the calendula officinalis powder and 3-20 parts by weight of wormwood powder, uniformly mixing, and fermenting in a fermentation tank for 12-36 hours;
(5) and (3) extraction: adding an organic solvent and carbon powder into the fermentation liquor for extraction;
(6) and (3) distillation: distilling under reduced pressure after extraction to obtain herba Sidae Rhombifoliae/folium Artemisiae Argyi fermented extract.
Wherein, in the anti-allergy skin-soothing essence, the specific conditions of high-temperature and high-pressure cooking are as follows: the temperature is 70-120 ℃, the pressure is 0.5-1.5 Mpa, and the cooking time is 0.5-5 h.
Wherein, in the anti-allergy skin-soothing essence, the organic solvent is at least one of acetone, ethanol, isopropanol and methanol.
The second technical problem to be solved by the invention is to provide a preparation method of the anti-allergy skin-soothing essence, which specifically comprises the following steps:
(1) sequentially adding deionized water, a calendula extract, an aloe extract, a calendula/wormwood fermented extract, corn gluten and hyaluronic acid into a stirring kettle, mixing and stirring until the mixture is completely dissolved, and heating to 60-80 ℃ to form a water phase;
(2) sequentially adding glycerol, butanediol and beeswax into a stirring kettle, mixing and stirring, heating to 60-80 ℃, and stirring for 10-20 min to form an oil phase;
(3) and adding the oil phase into the water phase at the temperature of 60-80 ℃, mixing and stirring for 10-30 min at the stirring speed of 2000-10000 r/min, adding hydroxyethyl cellulose, stirring for 10-20 min, and cooling to room temperature to obtain the anti-allergy skin-soothing essence.
According to the preparation method of the anti-allergy skin-soothing essence, the stirring speed in the steps (1) and (2) is 500-3000 r/min; and (3) when the oil phase is added into the water phase, the stirring speed is 2000-10000 r/min, and the stirring speed after the hydroxyethyl cellulose is added is 500-3000 r/min.
In the preparation method of the anti-allergy skin-soothing essence, the cooling mode in the step (3) is preferably a water cooling mode.
Aloe is one of sago cycas, the variety of aloe is various, wherein the fresh aloe extract is the best product, and the aloe vera is a magic natural food, medicine and cosmetic additive, contains rich skin nutrients, such as vitamins, amino acids, glycoside, choline sugar and aloe vera gel, and has the effects of activating cell activity, delaying skin aging, astringing, regulating skin, nourishing skin and protecting skin. The aloe has the medical value which is confirmed and accepted by world medical scientists, contains abundant vitamins, amino acids, fatty acids and polysaccharide substances, has natural anti-inflammatory and antibacterial effects, can quickly permeate into the skin and directly reach the deep layer of the skin, and has certain curative effect on pox caused by acne bacilli. Aloe has effects of promoting wound healing, diminishing inflammation, killing bacteria, absorbing heat, relieving swelling, softening skin, and maintaining cell activity, and has effects of moistening skin, accelerating skin metabolism, improving skin elasticity, and eliminating acne, freckle, and rhagadia.
The calendula is also called calendula, calendula officinalis, chrysanthemum changchini, sobering-up flower, evergreen flower, calendula and the like, and the calendula mainly has the effects of diminishing inflammation and resisting bacteria of flowers and leaves, promoting qi and blood circulation of roots, and cooling blood and stopping bleeding of flowers. The beauty treatment effect is as follows: 1. the calendula is rich in flavonoid active ingredients, has the effects of resisting oxidation, resisting vascular proliferation, diminishing inflammation, resisting allergy and viruses, can sterilize and astringe wounds, treat inflammation, acne and large pores, and prevents scars; 2. the calendula extract can promote skin metabolism, and has high moistening effect especially on dry skin.
Sodium hyaluronate is a physiological active substance widely existing in animals and human bodies, is distributed in human skin, synovial fluid of joints, umbilical cord, aqueous humor and vitreous humor, has high viscoelasticity and profile modeling property, and has good moisturizing and anti-aging effects.
Compared with the prior art, the invention has the beneficial effects that: the anti-allergy skin-soothing essence disclosed by the invention is scientific and reasonable in raw material proportion, fully utilizes the soothing and anti-allergy effects of the calendula extract, the aloe extract and the calendula/wormwood fermented extract and the effect of corn gluten on increasing the skin elasticity, and all the components supplement each other, so that the essence can effectively improve the problem of allergic skin, eliminate turbid substances accumulated in the skin and harmful substances generated due to pollution, achieve the effects of moistening the skin, resisting allergy, diminishing inflammation, tightening the skin and whitening and moisturizing, and not only can clean, nourish and protect the skin, but also can effectively relieve and resist allergy and prevent skin chapping.
Detailed Description
The following detailed description of the preferred embodiments of the present invention is provided to enable those skilled in the art to more readily understand the advantages and features of the present invention, and to clearly and unequivocally define the scope of the present invention.
The calendula extract, aloe extract and calendula/wormwood fermented extract used in the following examples were obtained by a self-made method, and the remaining raw materials were all commercially available products.
The calendula extract is prepared by the following steps:
(1) and (3) drying: drying calendula officinalis at 40 deg.C for 4 hr;
(2) and (3) cooking: steaming dried herba Sidae Rhombifoliae at 95 deg.C under 1.1Mpa for 1 hr;
(3) crushing: crushing the cooked calendula to obtain calendula powder with the granularity of 60-100 meshes;
(4) and (3) extraction: adding calendula officinalis powder into an ethanol solvent and carbon powder for extraction;
(5) and (3) distillation: distilling under reduced pressure to obtain herba Sidae Rhombifoliae extract.
The aloe extract is prepared by the following steps:
(1) and (3) drying: drying Aloe at 30 deg.C for 5 hr;
(2) and (3) cooking: steaming dried Aloe at 80 deg.C under 1.3Mpa for 1.5 hr;
(3) crushing: crushing the steamed aloe to 60-100 meshes to obtain aloe powder;
(4) and (3) extraction: extracting Aloe powder with mixed solvent of ethanol and acetone and carbon powder;
(5) and (3) distillation: distilling under reduced pressure to obtain Aloe extract.
The calendula/wormwood fermented extract is prepared by the following steps:
(1) and (3) drying: drying calendula and folium Artemisiae Argyi at 50 deg.C for 3 hr;
(2) and (3) cooking: steaming dried herba Sidae Rhombifoliae and folium Artemisiae Argyi at 90 deg.C under 1.2Mpa for 1 hr;
(3) crushing: respectively crushing the cooked calendula and wormwood to obtain powder with the granularity of over 60 meshes;
(4) fermentation: taking 10 parts of calendula officinalis powder and 12 parts of wormwood powder according to parts by weight, uniformly mixing, and fermenting in a fermentation tank for 36 hours;
(5) and (3) extraction: adding a mixed solvent of ethanol and acetone into the fermentation liquor, and extracting with carbon powder;
(6) and (3) distillation: distilling under reduced pressure after extraction to obtain herba Sidae Rhombifoliae/folium Artemisiae Argyi fermented extract.
Example 1
The anti-allergy skin-soothing essence is prepared by the following method:
(1) sequentially adding 300g of deionized water, 15g of calendula extract, 10g of aloe extract, 10g of calendula/wormwood fermented extract, 3g of corn gluten and 3g of hyaluronic acid into a stirring kettle, mixing and stirring until the mixture is completely dissolved at the stirring speed of 1000 revolutions per minute, and heating to 60 ℃ to form a water phase;
(2) sequentially adding 10g of glycerol, 10g of butanediol and 3g of beeswax into a stirring kettle, mixing and stirring, heating to 60 ℃, stirring for 15min at the stirring speed of 1000 revolutions per minute to form an oil phase;
(3) adding the oil phase into the water phase at 60 ℃, mixing and stirring for 20min at the stirring speed of 3000 r/min, adding 3g of hydroxyethyl cellulose, stirring for 10min at the stirring speed of 800 r/min, and cooling to room temperature by water cooling to obtain the anti-allergy skin-soothing essence.
Example 2
The anti-allergy skin-soothing essence is prepared by the following method:
(1) sequentially adding 350g of deionized water, 20g of calendula extract, 20g of aloe extract, 6g of calendula/wormwood fermented extract, 8g of corn gluten and 1g of hyaluronic acid into a stirring kettle, mixing and stirring until the mixture is completely dissolved at the stirring speed of 800 revolutions per minute, and heating to 70 ℃ to form a water phase;
(2) sequentially adding 20g of glycerol, 5g of butanediol and 3g of beeswax into a stirring kettle, mixing and stirring, heating to 70 ℃, stirring for 15min at the stirring speed of 2000 rpm to form an oil phase;
(3) adding the oil phase into the water phase at 70 ℃, mixing and stirring for 15min at the stirring speed of 4000 revolutions per minute, adding 1g of hydroxyethyl cellulose, stirring for 10min at the stirring speed of 800 revolutions per minute, and cooling to room temperature by water cooling to obtain the anti-allergy skin-soothing essence.
Example 3
The anti-allergy skin-soothing essence is prepared by the following method:
(1) sequentially adding 450g of deionized water, 30g of calendula extract, 15g of aloe extract, 5g of calendula/wormwood fermented extract, 5g of corn gluten and 2g of hyaluronic acid into a stirring kettle, mixing and stirring until the mixture is completely dissolved at the stirring speed of 1000 revolutions per minute, and heating to 80 ℃ to form a water phase;
(2) sequentially adding 20g of glycerol, 8g of butanediol and 5g of beeswax into a stirring kettle, mixing and stirring, heating to 80 ℃, stirring for 10min at the stirring speed of 800 revolutions per minute to form an oil phase;
(3) adding the oil phase into the water phase at 80 deg.C, mixing and stirring for 20min at 8000 rpm, adding hydroxyethyl cellulose 2g, stirring for 10min at 1000 rpm, and cooling to room temperature with water to obtain the anti-allergy skin-smoothing essence.
Example 4
The anti-allergy skin-soothing essence is prepared by the following method:
(1) sequentially adding 400g of deionized water, 20g of calendula extract, 15g of aloe extract, 8g of calendula/wormwood fermented extract, 6g of corn gluten and 3g of hyaluronic acid into a stirring kettle, mixing and stirring until the components are completely dissolved at the stirring speed of 800 revolutions per minute, and heating to 70 ℃ to form a water phase;
(2) sequentially adding 15g of glycerol, 7g of butanediol and 4g of beeswax into a stirring kettle, mixing and stirring, heating to 70 ℃, stirring for 20min at the stirring speed of 800 revolutions per minute to form an oil phase;
(3) adding the oil phase into the water phase at 70 deg.C, mixing and stirring for 30min at 3000 r/min, adding hydroxyethyl cellulose 2g, stirring for 15min at 800 r/min, and cooling to room temperature to obtain the anti-allergy skin-soothing essence.
Effects of the embodiment
The invention performs the following tests:
case-related data: 60 test subjects with loose and rough skin, much wrinkles and easy allergy are selected, and the age is between 30 and 55 years old.
The using method comprises the following steps: after thoroughly cleaning the skin, the essence prepared in example 1 is uniformly applied to the skin, gently patted, and is used once in the morning and evening, wherein each 28 days is a treatment course, and the treatment course is 1-4.
And (4) judging the standard:
the effect is shown: the user feels very satisfactory, the skin has elasticity which is more compact and smooth, the skin is fine and smooth, the skin is permanently moist, soft and smooth and glossy, wrinkles are obviously reduced, and the number of times of easy allergy is obviously reduced; the texture density of the skin is obviously reduced under a microscope, and the color of the skin is obviously lightened. The subjects had no allergic or other toxic side effects.
The method has the following advantages: the user feels generally satisfactory by self, and the elastic, glossy and smooth degree of the skin is increased; wrinkles are reduced; the density of the skin texture is reduced under a microscope, and the skin color becomes lighter; the number of allergic reaction is reduced.
And (4) invalidation: the user feels dissatisfied, the rough and dry feeling of the skin is not obviously improved, the wrinkles are not reduced, and the elastic, glossy and smooth degree of the skin is not increased; the skin texture density is not obviously improved under a microscope, and the epidermal pigmentation is not obviously improved; the allergic condition is not improved.
Effects of use
The 60 cases were recorded and reviewed, with the specific results shown in table 1:
TABLE 1
The total effective rate of the invention reaches 96.67%, and the same effect is achieved in the embodiments 2-4.
Claims (10)
1. The anti-allergy skin-soothing essence is characterized by being prepared from the following raw materials in parts by weight: 15-30 parts of calendula extract, 10-20 parts of aloe extract, 5-10 parts of calendula/wormwood fermentation extract, 300-500 parts of deionized water, 3-8 parts of corn gluten, 1-3 parts of hydroxyethyl cellulose, 1-3 parts of hyaluronic acid, 10-20 parts of glycerol, 5-10 parts of butanediol and 3-5 parts of beeswax.
2. The anti-allergy skin-soothing essence according to claim 1, which is prepared from the following raw materials in parts by weight: 20-30 parts of a calendula extract, 15-20 parts of an aloe extract, 6-8 parts of a calendula/wormwood fermentation extract, 350-450 parts of deionized water, 5-8 parts of corn gluten, 1-2 parts of hydroxyethyl cellulose, 2-3 parts of hyaluronic acid, 15-20 parts of glycerol, 6-8 parts of butanediol and 3-5 parts of beeswax.
3. The anti-allergy skin-soothing essence according to claim 1 or 2, which is prepared from the following raw materials in parts by weight: 20 parts of calendula extract, 15 parts of aloe extract, 8 parts of calendula/wormwood fermented extract, 400 parts of deionized water, 6 parts of corn gluten, 2 parts of hydroxyethyl cellulose, 3 parts of hyaluronic acid, 15 parts of glycerol, 7 parts of butanediol and 4 parts of beeswax.
4. The anti-allergy skin-soothing essence according to any one of claims 1 to 3, wherein the calendula extract is prepared by the following steps:
(1) and (3) drying: drying the calendula at 30-50 ℃ for 3-5 h;
(2) and (3) cooking: steaming dried herba Sidae Rhombifoliae at high temperature under high pressure;
(3) crushing: pulverizing the cooked calendula to particle size of more than 60 meshes to obtain calendula powder;
(4) and (3) extraction: adding organic solvent and carbon powder into the calendula officinalis powder for extraction;
(5) and (3) distillation: distilling under reduced pressure to obtain herba Sidae Rhombifoliae extract.
5. The anti-allergy skin-soothing essence according to any one of claims 1 to 3, wherein the aloe extract is prepared by the following steps:
(1) and (3) drying: drying aloe at 30-50 ℃ for 3-5 h;
(2) and (3) cooking: steaming the dried aloe at high temperature and high pressure;
(3) crushing: pulverizing the steamed aloe to particle size of more than 60 meshes to obtain calendula officinalis powder;
(4) and (3) extraction: adding organic solvent and carbon powder into the aloe powder for extraction;
(5) and (3) distillation: distilling under reduced pressure to obtain Aloe extract.
6. The anti-allergy skin-soothing essence according to any one of claims 1 to 3, wherein the calendula/wormwood fermented extract is prepared by the following steps:
(1) and (3) drying: drying the calendula and the wormwood at the temperature of 30-50 ℃ for 3-5 h;
(2) and (3) cooking: steaming dried herba Sidae Rhombifoliae and folium Artemisiae Argyi at high temperature and high pressure;
(3) crushing: respectively crushing the cooked calendula and wormwood to obtain powder with the granularity of over 60 meshes;
(4) fermentation: taking 10 parts by weight of the calendula officinalis powder and 3-20 parts by weight of wormwood powder, uniformly mixing, and fermenting in a fermentation tank for 12-36 hours;
(5) and (3) extraction: adding an organic solvent and carbon powder into the fermentation liquor for extraction;
(6) and (3) distillation: distilling under reduced pressure after extraction to obtain herba Sidae Rhombifoliae/folium Artemisiae Argyi fermented extract.
7. The anti-allergy skin-soothing essence according to any one of claims 4 to 6, wherein the specific conditions of high-temperature and high-pressure cooking are as follows: the temperature is 70-120 ℃, the pressure is 0.5-1.5 Mpa, and the cooking time is 0.5-5 h.
8. The anti-allergy skin-soothing essence according to any one of claims 4 to 7, wherein the organic solvent is at least one of acetone, ethanol, isopropanol and methanol.
9. The method for preparing the anti-allergy skin-soothing essence of any one of claims 1 to 8, which is characterized by comprising the following steps:
(1) sequentially adding deionized water, a calendula extract, an aloe extract, a calendula/wormwood fermented extract, corn gluten and hyaluronic acid into a stirring kettle, mixing and stirring until the mixture is completely dissolved, and heating to 60-80 ℃ to form a water phase;
(2) sequentially adding glycerol, butanediol and beeswax into a stirring kettle, mixing and stirring, heating to 60-80 ℃, and stirring for 10-20 min to form an oil phase;
(3) and adding the oil phase into the water phase at the temperature of 60-80 ℃, mixing and stirring for 10-30 min at the stirring speed of 2000-10000 r/min, adding hydroxyethyl cellulose, stirring for 10-20 min, and cooling to room temperature to obtain the anti-allergy skin-soothing essence.
10. The preparation method of the anti-allergy skin-soothing essence according to claim 9, wherein the stirring speed in the steps (1) and (2) is 500-3000 r/min; and (3) when the oil phase is added into the water phase, the stirring speed is 2000-10000 r/min, and the stirring speed after the hydroxyethyl cellulose is added is 500-3000 r/min.
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Application publication date: 20200214 |