CN106963690A - A kind of ultra-thin breathable PE chitosan composite facial masks and preparation method thereof - Google Patents
A kind of ultra-thin breathable PE chitosan composite facial masks and preparation method thereof Download PDFInfo
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- CN106963690A CN106963690A CN201710318482.9A CN201710318482A CN106963690A CN 106963690 A CN106963690 A CN 106963690A CN 201710318482 A CN201710318482 A CN 201710318482A CN 106963690 A CN106963690 A CN 106963690A
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- bioactivity
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0212—Face masks
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/494—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
- A61K8/4946—Imidazoles or their condensed derivatives, e.g. benzimidazoles
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4973—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom
- A61K8/498—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom having 6-membered rings or their condensed derivatives, e.g. coumarin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
- A61K8/602—Glycosides, e.g. rutin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/66—Enzymes
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/68—Sphingolipids, e.g. ceramides, cerebrosides, gangliosides
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/731—Cellulose; Quaternized cellulose derivatives
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/008—Preparations for oily skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/70—Biological properties of the composition as a whole
- A61K2800/72—Hypo-allergenic
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/88—Two- or multipart kits
- A61K2800/882—Mixing prior to application
Abstract
The present invention proposes a kind of ultra-thin breathable PE chitosan composite facial masks and preparation method thereof, the composite facial mask includes face mask substrate material, PE films, SOD bioactivity Essences, the PE films are compounded with the face mask substrate material, the present invention is combined PE films with chitin fiber cloth can be such that facial mask reuses 23 times, resource utilization is high, and it is designed as two kinds of forms of dry and wet, market satisfaction is high, the rotten of facial mask can effectively be prevented, the problems such as deformation, in addition, facial mask of the present invention has excellent whitening Firm, effect of anti-inflammation, moisture absorption goes oiliness good, free radical can effectively be removed, keep skin wet gloss flexible, inherently improve the immunity of skin.
Description
Technical field
The present invention relates to facial mask preparing technical field, and in particular to a kind of ultra-thin breathable PE chitosans composite facial mask and its system
Preparation Method.
Background technology
Chitosan is mainly derived from marine crustacean, is also largely present in the materials such as mushroom, with good suppression
Bacterium property, the physicochemical property for adsorbing the uniqueness such as sequestering, biocompatibility, biological safety and biodegradability.It applies ten
Divide extensive, have its in the fields such as cosmetics, health products, medicine, food industry, chemical industry, papermaking, agricultural, environmental protection, light textile
Figure.Chitosan skincare product have become the main component of current internationally recognized senior medicine adornment, for pulsed light, radio frequency, dot matrix,
The medical cosmetologies such as tartaric acid are postoperative, can play a part of similar natural antibiotics, and quickly repair substrate fire damage, are quickly cured
Close wound, repair epidermal barrier.Meanwhile, Chitosan skincare product also have stronger absorption chelation, are very suitable for as facial mask
Carrier.It is well known that cosmetics contain heavy metal mostly, heavy metal can not only influence skin, even more cutaneous lesions a weight
Inducement is wanted, and a significant properties of chitosan is high adsorption capacity, the material of many low molecule amounts, such as metal ion, courage
Sterol, triglycerides, cholic acid and organic mercury etc. also have some artificial colors to be effectively adsorbed.Therefore be badly in need of research and development it is a kind of with
Chitosan is the beauty mask of carrier.
The content of the invention
For above-mentioned problem, the present invention proposes a kind of ultra-thin breathable PE chitosans composite facial mask and its preparation side
Method, being combined PE films with chitin fiber cloth can be such that facial mask reuses 2-3 times, and resource utilization is high, and is designed as dry and wet two
Kind of form, market satisfaction is high, can effectively prevent the problems such as the rotten of facial mask, deformation, in addition, facial mask of the present invention have it is excellent
Effect of whitening Firm, anti-inflammation, moisture absorption goes oiliness good, can effectively remove free radical, keeps skin wet gloss flexible,
Inherently improve the immunity of skin.
In order to realize above-mentioned purpose, the present invention uses following technical scheme：
A kind of ultra-thin breathable PE chitosan composite facial masks, including face mask substrate material, PE films, SOD bioactivity Essences, it is described
The PE films are compounded with face mask substrate material.
It is preferred that, the face mask substrate material be using chitin fiber as raw material, the chitosan produced by water jet process without
Spin cloth.
It is preferred that, the SOD bioactivity Essence is made including following components：Yeast dextran 13-17%, ursin
3-4%, modification SOD 0.01-0.5%, trehalose 1-1.3%, ceramide 0.5-0.6%, Tea Polyphenols 1.5-3%, natto gum
0.02-0.5%, polyethylene glycol-800 9-10%, Hippophate flavone extract SOD 1-1.2%, acetyl group hexapeptide 1.5-2%, carboxylic
Methylcellulose 0-0.1%, allantoin 1-1.5%, double imidazolidinyl urea 0.02-0.05%, deionized water surplus.
It is preferred that, the SOD bioactivity Essence also includes rose pectin 0.2-1%, olive extract 0.5-
0.7%th, licorice 0.5-2%.
It is preferred that, the modification SOD is La-SOD, and enzymatic activity is 300-3000u/ml.
It is preferred that, the acetyl group hexapeptide is mass ratio 1:1.5 acetyl group hexapeptide -3 and the combination of Argireline
Thing.
It is preferred that, ultra-thin breathable PE chitosan composite facial masks, preparation process is as follows：
(1) preparation of SOD bioactivity Essence
Raw material is weighed in proportion, and natto gum, polyethylene glycol-800, carboxymethyl cellulose, deionized water blending are heated to
50-60 DEG C, 15-20min is incubated under stirring condition, then yeast dextran, Tea Polyphenols, acetyl group hexapeptide are added thereto, stirred
Mix after 3-4min, uniform decrease in temperature is sequentially added wherein under agitation to 35 DEG C, then by remaining ingredient, after the completion of addition, after
Continuous stirring 30-35min, is then cooled to 25 DEG C, stands insulation 30min, filters, discharging, is stored at room temperature to obtain SOD bioactivity essence
Magnificent liquid, then dispenses SOD bioactivity Essences into spray bottle；
(2) preparation of composite facial mask
By face mask substrate material and medical ultra-thin PE films compound sticking, it is then placed in mask packaging bag, is placed in ultraviolet sterilization case
Middle sterilization treatment 5-6h, by mask packaging bag packaging corresponding with spray bottle after the completion of sterilizing, or obtained SOD biologies is living
Property Essence infiltration composite facial mask after pack jointly.
It is preferred that, it is heated to be heating water bath in SOD bioactivity Essence preparation process.
It is preferred that, the composite facial mask is divided into dry, wet two kinds of packagings.
Due to using above-mentioned technical scheme, the beneficial effects of the invention are as follows：The present invention is combined PE with chitin fiber cloth
Film can be such that facial mask reuses 2-3 times, and resource utilization is high, and be designed as two kinds of forms of dry and wet, and market satisfaction is high, can have
Effect prevents the problems such as the rotten of facial mask, deformation.Specifically, dry packaging separately matches somebody with somebody SOD bioactivity Essence inhalator jar hydrojets, use
During facial mask, the packaging bag of dried noodle film is opened, Essence is sprayed into dried noodle film in facial mask bag, after full penetration, face, facial mask is sticked
Repeat 2~3 times and use.In addition, facial mask of the present invention uses SOD bioactivity Essences, with excellent whitening Firm, antibacterial
The effects such as anti-inflammatory, moisture absorption goes oiliness good, can effectively remove free radical, keeps skin wet gloss flexible, inherently improves
The immunity of skin.SOD after modification coordinates yeast dextran, the trehalose of high bioactivity to significantly improve facial mask
Whitening spot-removing, the active ingredient of antibacterial smoothing wrinkle are generally natural extraction raw material in skin effect, and the present invention, safe, to skin
Skin does not have any stimulation.
In addition, some otch can be opened up on face mask substrate material of the present invention, PE films from edge to center in position, it is easy to apply
The comfortableness in face, it is to avoid fold.
Embodiment
To make the purpose, technical scheme and advantage of the embodiment of the present invention clearer, below in conjunction with the embodiment of the present invention,
Technical scheme in the embodiment of the present invention is clearly and completely described.Based on embodiments of the invention, the common skill in this area
The every other embodiment that art personnel are obtained under the premise of creative work is not made, belongs to the model that the present invention is protected
Enclose.
Embodiment 1：
A kind of ultra-thin breathable PE chitosan composite facial masks, including face mask substrate material, PE films, SOD bioactivity Essences, it is described
The PE films are compounded with face mask substrate material, the face mask substrate material is, using chitin fiber as raw material, to be produced by water jet process
Chitosan non-woven fabrics.
The SOD bioactivity Essence is made including following components：Yeast dextran 14%, ursin 3.5%, modification
SOD 0.3%, trehalose 1.2%, ceramide 0.55%, Tea Polyphenols 1.5%, natto gum 0.3%, polyethylene glycol
8009.5%th, Hippophate flavone extract SOD 3.8%, acetyl group hexapeptide 1.8%, carboxymethyl cellulose 0%, allantoin 1.2%,
Double imidazolidinyl urea 0.05%, in addition to rose pectin 0.2%, olive extract 0.6%, licorice 1.5%, go from
Sub- water surplus.
Ultra-thin breathable PE chitosan composite facial masks, preparation process is as follows：
(1) preparation of SOD bioactivity Essence
Raw material is weighed in proportion, and natto gum, polyethylene glycol-800, carboxymethyl cellulose, deionized water blending are heated to 55
DEG C, 15min is incubated under stirring condition, then yeast dextran, Tea Polyphenols, acetyl group hexapeptide is added thereto, after stirring 3min,
Uniform decrease in temperature is sequentially added wherein under agitation to 35 DEG C, then by remaining ingredient, after the completion of addition, continues to stir 30min,
Then 25 DEG C are cooled to, insulation 30min is stood, filters, discharging is stored at room temperature to obtain SOD bioactivity Essences, then by SOD
Bioactivity Essence is dispensed into spray bottle；
(2) preparation of composite facial mask
By face mask substrate material and medical ultra-thin PE films compound sticking, it is then placed in mask packaging bag, is placed in ultraviolet sterilization case
Middle sterilization treatment 5.5h, by mask packaging bag packaging corresponding with spray bottle after the completion of sterilizing, or obtained SOD biologies is living
Property Essence infiltration composite facial mask after pack jointly.
Embodiment 2：
A kind of ultra-thin breathable PE chitosan composite facial masks, including face mask substrate material, PE films, SOD bioactivity Essences, it is described
The PE films are compounded with face mask substrate material, the face mask substrate material is, using chitin fiber as raw material, to be produced by water jet process
Chitosan non-woven fabrics.
The SOD bioactivity Essence is made including following components：Yeast dextran 16%, ursin 3.2%, modification
SOD 0.5%, trehalose 1.1%, ceramide 0.58%, Tea Polyphenols 2.5%, natto gum 0.5%, polyethylene glycol-800 10%,
Hippophate flavone extract SOD 3.6%, acetyl group hexapeptide 2%, carboxymethyl cellulose 0%, allantoin 1.3%, double imidazolidinyls
Urea 0.03%, in addition to rose berry extract 1%, olive extract 0.7%, licorice 0.5%, more than deionized water
Amount.
Ultra-thin breathable PE chitosan composite facial masks, preparation process is as follows：
(1) preparation of SOD bioactivity Essence
Raw material is weighed in proportion, and natto gum, polyethylene glycol-800, carboxymethyl cellulose, deionized water blending are heated to 50
DEG C, 20min is incubated under stirring condition, then yeast dextran, Tea Polyphenols, acetyl group hexapeptide is added thereto, after stirring 4min,
Uniform decrease in temperature is sequentially added wherein under agitation to 35 DEG C, then by remaining ingredient, after the completion of addition, continues to stir 35min,
Then 25 DEG C are cooled to, insulation 30min is stood, filters, discharging is stored at room temperature to obtain SOD bioactivity Essences, then by SOD
Bioactivity Essence is dispensed into spray bottle；
(2) preparation of composite facial mask
By face mask substrate material and medical ultra-thin PE films compound sticking, it is then placed in mask packaging bag, is placed in ultraviolet sterilization case
Middle sterilization treatment 6h, by mask packaging bag packaging corresponding with spray bottle after the completion of sterilizing, or by obtained SOD bioactivity
Packed jointly after Essence infiltration composite facial mask.
Embodiment 3：
A kind of ultra-thin breathable PE chitosan composite facial masks, including face mask substrate material, PE films, SOD bioactivity Essences, it is described
The PE films are compounded with face mask substrate material, the face mask substrate material is, using chitin fiber as raw material, to be produced by water jet process
Chitosan non-woven fabrics.
The SOD bioactivity Essence is made including following components：Yeast dextran 17%, ursin 4%, modification
SOD 0.01%, trehalose 1.3%, ceramide 0.55%, Tea Polyphenols 3%, natto gum 0.02%, polyethylene glycol-800 9%,
Hippophate flavone extract SOD 3.5%, acetyl group hexapeptide 2%, carboxymethyl cellulose 0.1%, allantoin 1.5%, double imidazolidines
Base urea 0.02%, in addition to rose berry extract 0.5%, olive extract 0.5%, licorice 2%, more than deionized water
Amount.
Ultra-thin breathable PE chitosan composite facial masks, preparation process is as follows：
(1) preparation of SOD bioactivity Essence
Raw material is weighed in proportion, and natto gum, polyethylene glycol-800, carboxymethyl cellulose, deionized water blending are heated to 50
DEG C, 20min is incubated under stirring condition, then yeast dextran, Tea Polyphenols, acetyl group hexapeptide is added thereto, after stirring 4min,
Uniform decrease in temperature is sequentially added wherein under agitation to 35 DEG C, then by remaining ingredient, after the completion of addition, continues to stir 35min,
Then 25 DEG C are cooled to, insulation 30min is stood, filters, discharging is stored at room temperature to obtain SOD bioactivity Essences, then by SOD
Bioactivity Essence is dispensed into spray bottle；
(2) preparation of composite facial mask
By face mask substrate material and medical ultra-thin PE films compound sticking, it is then placed in mask packaging bag, is placed in ultraviolet sterilization case
Middle sterilization treatment 6h, by mask packaging bag packaging corresponding with spray bottle after the completion of sterilizing, or by obtained SOD bioactivity
Packed jointly after Essence infiltration composite facial mask.
Embodiment 4：
A kind of ultra-thin breathable PE chitosan composite facial masks, including face mask substrate material, PE films, SOD bioactivity Essences, it is described
The PE films are compounded with face mask substrate material, the face mask substrate material is, using chitin fiber as raw material, to be produced by water jet process
Chitosan non-woven fabrics.
The SOD bioactivity Essence is made including following components：Yeast dextran 13%, ursin 3%, modification
SOD 0.1%, trehalose 1%, ceramide 0.6%, Tea Polyphenols 3%, natto gum 0.1%, polyethylene glycol-800 9%, sea-buckthorn are yellow
Ketone extract SOD 3.5%, acetyl group hexapeptide 1.5%, carboxymethyl cellulose 0.05%, allantoin 1%, double imidazolidinyl urea
0.02%, in addition to rose berry extract 0.6%, olive extract 0.6%, licorice 1%, deionized water surplus.
Ultra-thin breathable PE chitosan composite facial masks, preparation process is as follows：
(1) preparation of SOD bioactivity Essence
Raw material is weighed in proportion, and natto gum, polyethylene glycol-800, carboxymethyl cellulose, deionized water blending are heated to 50
DEG C, 20min is incubated under stirring condition, then yeast dextran, Tea Polyphenols, acetyl group hexapeptide is added thereto, after stirring 3min,
Uniform decrease in temperature is sequentially added wherein under agitation to 35 DEG C, then by remaining ingredient, after the completion of addition, continues to stir 30min,
Then 25 DEG C are cooled to, insulation 30min is stood, filters, discharging is stored at room temperature to obtain SOD bioactivity Essences, then by SOD
Bioactivity Essence is dispensed into spray bottle；
(2) preparation of composite facial mask
By face mask substrate material and medical ultra-thin PE films compound sticking, it is then placed in mask packaging bag, is placed in ultraviolet sterilization case
Middle sterilization treatment 5h, by mask packaging bag packaging corresponding with spray bottle after the completion of sterilizing, or by obtained SOD bioactivity
Packed jointly after Essence infiltration composite facial mask.
Embodiment 5：
A kind of ultra-thin breathable PE chitosan composite facial masks, including face mask substrate material, PE films, SOD bioactivity Essences, it is described
The PE films are compounded with face mask substrate material, the face mask substrate material is, using chitin fiber as raw material, to be produced by water jet process
Chitosan non-woven fabrics.
The SOD bioactivity Essence is made including following components：Yeast dextran 15%, ursin 3.5%, modification
SOD 0.05%, trehalose 1.2%, ceramide 0.5%, Tea Polyphenols 2.5%, natto gum 0.4%, polyethylene glycol-800 10%,
Hippophate flavone extract SOD 3.6%, acetyl group hexapeptide 1.5%, carboxymethyl cellulose 0.04%, allantoin 1%, double imidazolidines
Base urea 0.04%, deionized water surplus.
Ultra-thin breathable PE chitosan composite facial masks, preparation process is as follows：
(1) preparation of SOD bioactivity Essence
Raw material is weighed in proportion, and natto gum, polyethylene glycol-800, carboxymethyl cellulose, deionized water blending are heated to 60
DEG C, 15min is incubated under stirring condition, then yeast dextran, Tea Polyphenols, acetyl group hexapeptide is added thereto, after stirring 3min,
Uniform decrease in temperature is sequentially added wherein under agitation to 35 DEG C, then by remaining ingredient, after the completion of addition, continues to stir 35min,
Then 25 DEG C are cooled to, insulation 30min is stood, filters, discharging is stored at room temperature to obtain SOD bioactivity Essences, then by SOD
Bioactivity Essence is dispensed into spray bottle；
(2) preparation of composite facial mask
By face mask substrate material and medical ultra-thin PE films compound sticking, it is then placed in mask packaging bag, is placed in ultraviolet sterilization case
Middle sterilization treatment 5h, by mask packaging bag packaging corresponding with spray bottle after the completion of sterilizing, or by obtained SOD bioactivity
Packed jointly after Essence infiltration composite facial mask.
Embodiment 6：
A kind of ultra-thin breathable PE chitosan composite facial masks, including face mask substrate material, PE films, SOD bioactivity Essences, it is described
The PE films are compounded with face mask substrate material, the face mask substrate material is, using chitin fiber as raw material, to be produced by water jet process
Chitosan non-woven fabrics.
The SOD bioactivity Essence is made including following components：Yeast dextran 16%, ursin 3.8%, modification
SOD 0.2%, trehalose 1.3%, ceramide 0.5%, Tea Polyphenols 2%, natto gum 0.35%, polyethylene glycol-800 9.5%,
Hippophate flavone extract SOD 3.7%, acetyl group hexapeptide 1.6%, carboxymethyl cellulose 0.08%, allantoin 1.4%, double imidazoles
Ureine 0.05%, deionized water surplus.
Ultra-thin breathable PE chitosan composite facial masks, preparation process is as follows：
(1) preparation of SOD bioactivity Essence
Raw material is weighed in proportion, and natto gum, polyethylene glycol-800, carboxymethyl cellulose, deionized water blending are heated to 60
DEG C, 15min is incubated under stirring condition, then yeast dextran, Tea Polyphenols, acetyl group hexapeptide is added thereto, after stirring 4min,
Uniform decrease in temperature is sequentially added wherein under agitation to 35 DEG C, then by remaining ingredient, after the completion of addition, continues to stir 30min,
Then 25 DEG C are cooled to, insulation 30min is stood, filters, discharging is stored at room temperature to obtain SOD bioactivity Essences, then by SOD
Bioactivity Essence is dispensed into spray bottle；
(2) preparation of composite facial mask
By face mask substrate material and medical ultra-thin PE films compound sticking, it is then placed in mask packaging bag, is placed in ultraviolet sterilization case
Middle sterilization treatment 5h, by mask packaging bag packaging corresponding with spray bottle after the completion of sterilizing, or by obtained SOD bioactivity
Packed jointly after Essence infiltration composite facial mask.
120 female volunteers (are divided into by 6 groups at random and corresponds to 6 using composite facial mask made from the embodiment of the present invention
Individual embodiment product) clinical trial is carried out, by surface application in 2 days once, every composite facial mask is using twice：After one week, wrinkle is obvious
The number of mitigation accounts for 30%, and the enhanced number of skin compactibility accounts for 20%, and the enhanced number of skin moisture-keeping lubricity accounts for 25%；One
After month, the number that wrinkle substantially mitigates is up to 100%, wherein 65% microgroove tends to smooth, the enhanced number of skin compactibility is accounted for
95%, the enhanced number of skin moisture-keeping lubricity is up to 100%.(data above is the average value of six experimental groups)
The above embodiments are merely illustrative of the technical solutions of the present invention, rather than its limitations；Although with reference to the foregoing embodiments
The present invention is described in detail, it will be understood by those within the art that：It still can be to foregoing each implementation
Technical scheme described in example is modified, or carries out equivalent substitution to which part technical characteristic；And these modification or
Replace, the essence of appropriate technical solution is departed from the spirit and scope of various embodiments of the present invention technical scheme.
Claims (9)
1. a kind of ultra-thin breathable PE chitosan composite facial masks, it is characterised in that：Including face mask substrate material, PE films, SOD bioactivity essence
The PE films are compounded with magnificent liquid, the face mask substrate material.
2. ultra-thin breathable PE chitosan composite facial masks according to claim 1, it is characterised in that：The face mask substrate material be with
Chitin fiber is as raw material, the chitosan non-woven fabrics produced by water jet process.
3. ultra-thin breathable PE chitosan composite facial masks according to claim 1, it is characterised in that the SOD bioactivity
Essence is made including following components：Yeast dextran 13-17%, ursin 3-4%, modification SOD 0.01-0.5%, marine alga
Sugared 1-1.3%, ceramide 0.5-0.6%, Tea Polyphenols 1.5-3%, natto gum 0.02-0.5%, polyethylene glycol-800 9-
10%th, Hippophate flavone extract SOD 1-1.2%, acetyl group hexapeptide 1.5-2%, carboxymethyl cellulose 0-0.1%, allantoin 1-
1.5%th, double imidazolidinyl urea 0.02-0.05%, deionized water surplus.
4. ultra-thin breathable PE chitosan composite facial masks according to claim 3, it is characterised in that：The SOD bioactivity
Essence also includes rose pectin 0.2-1%, olive extract 0.5-0.7%, licorice 0.5-2%.
5. ultra-thin breathable PE chitosan composite facial masks according to claim 3, it is characterised in that：The modification SOD is the moon
Cinnamic acid Modified Superoxide Dismutase, enzymatic activity is 300-3000u/ml.
6. ultra-thin breathable PE chitosan composite facial masks according to claim 3, it is characterised in that：The acetyl group hexapeptide is
Mass ratio 1:1.5 acetyl group hexapeptide -3 and the composition of Argireline.
7. the ultra-thin breathable PE chitosan composite facial masks according to claim 3 or 4, it is characterised in that ultra-thin breathable PE shells
Glycan composite facial mask preparation process is as follows：
(1) preparation of SOD bioactivity Essence
Raw material is weighed in proportion, and natto gum, polyethylene glycol-800, carboxymethyl cellulose, deionized water blending are heated to 50-60
DEG C, 15-20min is incubated under stirring condition, then yeast dextran, Tea Polyphenols, acetyl group hexapeptide is added thereto, 3- is stirred
After 4min, uniform decrease in temperature is sequentially added wherein under agitation to 35 DEG C, then by remaining ingredient, after the completion of addition, continues to stir
30-35min is mixed, 25 DEG C are then cooled to, insulation 30min is stood, filters, discharging is stored at room temperature to obtain SOD bioactivity elite
Liquid, then dispenses SOD bioactivity Essences into spray bottle；
(2) preparation of composite facial mask
By face mask substrate material and medical ultra-thin PE films compound sticking, it is then placed in mask packaging bag, is placed in ultraviolet sterilization case and goes out
Bacterium handles 5-6h, by mask packaging bag packaging corresponding with spray bottle after the completion of sterilizing, or obtained SOD bioactivity is smart
Packed jointly after magnificent immersion profit composite facial mask.
8. the preparation method of ultra-thin breathable PE chitosan composite facial masks according to claim 7, it is characterised in that：SOD gives birth to
It is heated to be heating water bath in thing activity Essence preparation process.
9. the application of composite facial mask according to made from claim 7 ultra-thin breathable PE chitosan composite facial mask preparation methods, it is special
Levy and be：The composite facial mask is divided into dry, wet two kinds of packagings.
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108078898A (en) * | 2018-01-22 | 2018-05-29 | 唐旭 | A kind of new Post-basking repairing mask |
| CN111203048A (en) * | 2020-03-06 | 2020-05-29 | 西安普草瑞珊生物科技有限责任公司 | Preparation and application of non-woven fabric loaded with nano traditional Chinese medicine self-sterilization purification biological membrane |
| CN116173283A (en) * | 2023-02-02 | 2023-05-30 | 江苏恰瑞生物科技有限公司 | Chitosan-polyvinyl alcohol SOD enzyme hydrogel dressing |
-
2017
- 2017-05-08 CN CN201710318482.9A patent/CN106963690A/en active Pending
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108078898A (en) * | 2018-01-22 | 2018-05-29 | 唐旭 | A kind of new Post-basking repairing mask |
| CN111203048A (en) * | 2020-03-06 | 2020-05-29 | 西安普草瑞珊生物科技有限责任公司 | Preparation and application of non-woven fabric loaded with nano traditional Chinese medicine self-sterilization purification biological membrane |
| CN116173283A (en) * | 2023-02-02 | 2023-05-30 | 江苏恰瑞生物科技有限公司 | Chitosan-polyvinyl alcohol SOD enzyme hydrogel dressing |
| CN116173283B (en) * | 2023-02-02 | 2024-02-27 | 江苏恰瑞生物科技有限公司 | Chitosan-polyvinyl alcohol SOD enzyme hydrogel dressing |
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Application publication date: 20170721 |