CN107157797A - A kind of preparation technology of Application of Collagen from Fish Scales facial mask - Google Patents
A kind of preparation technology of Application of Collagen from Fish Scales facial mask Download PDFInfo
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- CN107157797A CN107157797A CN201710471002.2A CN201710471002A CN107157797A CN 107157797 A CN107157797 A CN 107157797A CN 201710471002 A CN201710471002 A CN 201710471002A CN 107157797 A CN107157797 A CN 107157797A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/65—Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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Abstract
The present invention relates to biological technical field, more particularly to a kind of preparation technology of Application of Collagen from Fish Scales facial mask, the preparation technology of the Application of Collagen from Fish Scales facial mask, comprise the following steps：(1) grass carp scales are soaked in the solvent containing carbonate, then grass carp scales is placed in acid solution, with microwave treatment, then soaked again with alkaline solution, filtered, obtain filtrate 1 and filter residue 1；(2) by the filter residue processing with enzyme preparation in step (1), washing and filtering obtains filtrate 2 and filter residue 2；(3) it is filtrate 1 and filtrate is 2-in-1 simultaneously, with filtering with microporous membrane, filtrate 3 is obtained, dries, obtains Application of Collagen from Fish Scales；(4) Application of Collagen from Fish Scales is well mixed in a solvent with film forming agent, plant extracts, thickener, bleeding agent, obtain Application of Collagen from Fish Scales facial mask, the extraction efficiency of collagen in the present invention in grass carp scales is high, extract and pungent is free of in obtained collagen, it is safe.
Description
Technical field
The present invention relates to biological technical field, more particularly to a kind of preparation technology of Application of Collagen from Fish Scales facial mask.
Background technology
Collagen is protein component main in skin histology, the 70%~80% of skin dry weight is accounted for, in corium
Fibrocyte (Fibroblasts) manufacture, collagen is a kind of white, transparent, branchiess fibrillation, is a kind of in itself
Very firm protein, in youth, health, few by the skin of sun damages, it constitutes the slightly curved fiber of a branch of beam, mutually
With last layer and next layer of formation right-angle array, this makes skin obtain solid effect.But when the years increase, collagen is not
But quantity reduce, and arrangement also become irregular, corium thus it is thinning；Environmental factor is easier to make collagen dissolving disappear
Lose.Cause the aging of skin.Exactly because the loss of collagen causes the collagen peptide bond for supporting skin and elasticated net fracture, its
Spiral net-shaped structure is destroyed immediately, and skin histology is oxidized, atrophy, collapsed, and dryings, wrinkle, loose nothing just occurs in skin
The aging phenomenons such as elasticity.The enough collagens of supplement can stimulate the fibroblast in skin corium voluntarily to carry out collagen
Secretion so that voluntarily generting machanism and metabolic function recover normal to collagen, so effectively the relaxation of delaying skin with it is old
Change.Smeared with the lotion containing collagen after skin, epiderm skin and dermis can effectively improve, and promote skin
The synthesis of interior collagen.Real medical science often carries out beauty with collagen, and collagen can directly act on the impaired of skin corium
Collagenous fibres, make it recover transverse flow fiber configuration rapidly.In the unique triple-helix structure of collagen and collagen molecules
Hydrophilic group, enhances skin primary hydrodynamic force, it is ensured that moisture improves Lymphatic Circulation, made in the circulation of skin surface and deep layer
Skin water profit is full vibrant.But collagen molecules amount is big, and being directly added into cosmetics can not directly be absorbed by skin.
At present, what collagen production was extracted is mainly derived from three class materials：Ossein, deep-sea fish fish-skin, fish scale.Wherein
Ossein is easily obtained essentially from the animals such as pig, ox, sheep, raw material, and raw material source is stable, but the ossein that Animal Bone is extracted contains
Compared with fattiness, ossein purity is slightly lower, and beauty performance is slightly worse, and due to religion and Animal diseases, animal ossein
The market share it is less and less.For producing the deep-sea fish fish-skin predominantly skin deep-sea cod of collagen, fish skin collagen
Protein content is high, function admirable, but cod belongs to cold aqueous demersal fishes, lives in below 300 meters of sea, can not manually enter
Row cultivation, acquisition difficulty is larger, and technical requirements are high.
Relative to ossein, fish skin collagen, scale collagen has the advantage of the two concurrently；And pass through detection, scale collagen egg
White hydroxyproline content is higher than other raw materials, because collagen peptide is similar to the structure of application on human skin collagen in fish scale, compatible
Good, the collagen product prepared by fish scale of property, it is easier to be absorbed by the skin.But do not utilize grass carp fish also in the prior art
The method that squama prepares facial mask.
The content of the invention
In view of the shortcomings of the prior art, the main object of the present invention is to provide a kind of system of Application of Collagen from Fish Scales facial mask
The extraction efficiency of collagen is high in standby technique, the technique, and extracts in obtained collagen without pungent, safety
Property it is high.
To solve the above problems, the invention provides a kind of preparation technology of Application of Collagen from Fish Scales facial mask, including with
Lower step：
(1) grass carp scales are taken, after cleaning, grass carp scales 3~5h are soaked into the solution containing carbonate, then by grass
Fish fish scale is placed in acid solution, with microwave treatment, is then soaked 3~12h with alkaline solution again, is washed out to neutrality, mistake
Filter, obtains filtrate 1 and filter residue 1；
(2) by the filter residue processing with enzyme preparation in step (1), washing and filtering obtains filtrate 2 and filter residue 2；
(3) it is filtrate 1 and filtrate is 2-in-1 simultaneously, with filtering with microporous membrane, filtrate 3 is obtained, filtrate 3 is spray-dried, obtained
To Application of Collagen from Fish Scales；
(4) Application of Collagen from Fish Scales is mixed in a solvent with film forming agent, plant extracts, thickener, bleeding agent
It is even, that is, obtain Application of Collagen from Fish Scales facial mask.
According to the present invention, the present invention is first handled the solution of grass carp scales carbonate, and carbonate solution can be loose
Fine and close collagen fabric in fish scale, so as to facilitate subsequent treatment, improves the efficiency of subsequent treatment, it is preferred that described to contain
The solution of carbonate is the aqueous solution of the aqueous solution, preferably sodium carbonate and/or potassium carbonate of carbonate.
According to the present invention, in step (1), the acid solution is any solvent that pH is extremely less than 7, can be sour water
Solution, the aqueous solution of strong acid weak base salt, phenol and its derivatives solution, are preferably the aqueous solution of acid, due to being extracted in the present invention
Collagen be finally to be fabricated to facial mask, apply on the face, the acid is preferably harmless acid, and preferably concentration is less than
At least one of 0.1M hydrochloric acid, citric acid, acetic acid, lactic acid.
According to the present invention, microwave treatment can be destroyed the triple-helix structure of collagen, hydrogen bond therein and hydrophobic
Key is broken, by increasing capacitance it is possible to increase the efficiency of acid dissolving, it is preferred that in step (1), and the power of the microwave treatment is 400~900W；
The time of the microwave treatment is 0.5~15min.
It is preferred that, in step (1), the alkaline solution is alkali metal hydroxide and/or alkaline earth metal hydroxide
The aqueous solution.
It is preferred that, in the step (2), the processing with enzyme preparation is concretely comprised the following steps：Jia 15 in filter residue in step (1)
~20 times of amount water, regulation control ph, at 45~55 DEG C, adds enzyme preparation 1, the enzyme preparation 1 and filter residue in 6.5~7.5, temperature
Ratio is (0.5~3.0): 100,0.5~1.5h is stirred, 1~4h is incubated, enzyme preparation 1 is then inactivated；Control ph 1.0~
3.0th, temperature adds enzyme preparation 2 at 55~70 DEG C, and the enzyme preparation 2 is (0.1~3.0) with filter residue ratio: 100, stir 1~3h
Afterwards, fire extinguishing enzyme preparation 2.
In step (2), the enzyme preparation 1 and enzyme preparation 2 be respectively neutral proteinase, papain, trypsase,
At least one of pepsin.
Due to macromolecular it is difficult to which by percutaneous absorption, the present invention can remove big point in solution by filtering with microporous membrane
Son, it is preferred that in step (3), the miillpore filter is the cellulose mixture miillpore filter that aperture is 20-50 μm.
It is preferred that, in step (4), the film forming agent be polyacrylic acid, polyacrylate sodium, polyvinylpyrrolidone,
At least one of hydroxymethyl cellulose, PVP and polyethylene glycol.
In order to improve the applicability of facial mask, increase the function of facial mask, it is preferred that in step (4), the plant extracts
For gadol extract, marine algae extract, green-tea extract, aloe extract, mint extract, pot marigold extract, gold and silver
Flower extract, Herba Lysimachiae foenumgraeci extract, rose extract, camomile extract, lemon extract, Rosmarinus officinalis extract, sweet basil are carried
Take at least one of thing, grape seed extract, tuckahoe extracts.
Compared with prior art, product beneficial effect of the invention is as follows：
(1) extraction efficiency of the collagen in the present invention in grass carp scales is high, extracts and is free of in obtained collagen
Pungent, it is safe；
(2) collagen that facial mask of the present invention is extracted using in grass carp scales is safe and non-stimulating as main component, and and human body
Compatibility is good, effectively can directly be absorbed by skin, deep layer nourishes rough skin；
(3) grass carp scales belong to domestic refuse, and the present invention realizes the recycling of grass carp scales, improves aquaculture
Added value, while reducing environmental pollution and the wasting of resources.
(4) present invention uses cooperatively fish scale collagen with plant extraction liquid, the effect with Synergistic, and enhancing is anti-
Skin senescence effect, while improving product odour, without adding essence, increase Product Safety and applicability.
Embodiment
In order to make the purpose , technical scheme and advantage of the present invention be clearer, following examples, to present invention progress
It is further described.It should be appreciated that the specific embodiments described herein are merely illustrative of the present invention, it is not used to limit
The present invention.
Embodiment 1
The invention provides a kind of preparation technology of Application of Collagen from Fish Scales facial mask, comprise the following steps：
(1) grass carp scales are taken, after cleaning, grass carp scales is soaked into 4h in sodium carbonate liquor, then grass carp scales are put
In hydrochloric acid solution, with microwave treatment, the power of the microwave treatment is 600W；The time of the microwave treatment is 10min；So
7h is soaked with sodium hydroxide solution again afterwards, is washed out to neutrality, filtering, obtains filtrate 1 and filter residue 1；
(2) 17 times of amount water are added in the filter residue in step (1), regulation control ph, at 50 DEG C, is added neutral in 7, temperature
Protease, the neutral proteinase and filter residue ratio are 1: 100, stir 1h, are incubated 2h, then inactivate neutral proteinase；Control pH
Value adds papain in 2.0, temperature at 60 DEG C, and the papain and filter residue ratio are 1.3: 100, after stirring 2h,
Papain is inactivated, washing and filtering obtains filtrate 2 and filter residue 2；
(3) it is filtrate 1 and filtrate is 2-in-1 simultaneously, with the cellulose mixture filtering with microporous membrane that aperture is 30 μm, filtrate 3 is obtained,
Filtrate 3 is spray-dried, Application of Collagen from Fish Scales is obtained；
(4) by Application of Collagen from Fish Scales and polyacrylic acid, gadol extract, sodium carboxymethyl cellulose thickener, alkane
Base benzene sulfonic acid sodium salt bleeding agent is well mixed in a solvent, that is, obtains Application of Collagen from Fish Scales facial mask.
Embodiment 2
The invention provides a kind of preparation technology of Application of Collagen from Fish Scales facial mask, comprise the following steps：
(1) grass carp scales are taken, after cleaning, grass carp scales is soaked into 3h in sodium carbonate liquor, then grass carp scales are put
In hydrochloric acid solution, with microwave treatment, the power of the microwave treatment is 400W；The time of the microwave treatment is 2min；So
3h is soaked with alkaline solution again afterwards, is washed out to neutrality, filtering, obtains filtrate 1 and filter residue 1；
(2) add 15 times of amount water in the filter residue in step (1), control ph is adjusted in 6.5, temperature at 45 DEG C, in addition
Property protease, the neutral proteinase and filter residue ratio are 2.2: 100, stir 0.5h, are incubated 1h, then inactivate neutral proteinase；
Control ph adds trypsase in 1.0, temperature at 55 DEG C, and the trypsase and filter residue ratio are 0.4: 100, stir 1h
Afterwards, trypsase is inactivated, washing and filtering obtains filtrate 2 and filter residue 2；
(3) it is filtrate 1 and filtrate is 2-in-1 simultaneously, with the cellulose mixture filtering with microporous membrane that aperture is 20 μm, filtrate 3 is obtained,
Filtrate 3 is spray-dried, Application of Collagen from Fish Scales is obtained；
(4) by Application of Collagen from Fish Scales and polyacrylate sodium, marine algae extract, sodium carboxymethyl cellulose thickener,
Sodium alkyl benzene sulfonate bleeding agent is well mixed in a solvent, that is, obtains Application of Collagen from Fish Scales facial mask.
Embodiment 3
The invention provides a kind of preparation technology of Application of Collagen from Fish Scales facial mask, comprise the following steps：
(1) grass carp scales are taken, after cleaning, grass carp scales 5h are soaked into the solution containing potassium carbonate, then by grass carp
Fish scale is placed in citric acid solution, and with microwave treatment, the power of the microwave treatment is 900W；The time of the microwave treatment is
15min；Then 12h is soaked with potassium hydroxide solution again, is washed out to neutrality, filtering, obtains filtrate 1 and filter residue 1；
(2) 20 times of amount water are added in the filter residue in step (1), regulation control ph, at 55 DEG C, adds wood in 7.5, temperature
Melon protease, the papain and filter residue ratio are 3: 100, stir 1.2h, are incubated 2h, then inactivate papain；Control
PH value processed adds neutral proteinase in 2.0, temperature at 60 DEG C, and the neutral proteinase and filter residue ratio are 1.2: 100, stir 2h
Afterwards, neutral proteinase is inactivated, washing and filtering obtains filtrate 2 and filter residue 2；
(3) it is filtrate 1 and filtrate is 2-in-1 simultaneously, with the cellulose mixture filtering with microporous membrane that aperture is 40 μm, filtrate 3 is obtained,
Filtrate 3 is spray-dried, Application of Collagen from Fish Scales is obtained；
(4) by Application of Collagen from Fish Scales and polyacrylate sodium, green-tea extract, xanthans thickener, alkylsurfuric acid
Ester sodium bleeding agent is well mixed in a solvent, that is, obtains Application of Collagen from Fish Scales facial mask.
Embodiment 4
The invention provides a kind of preparation technology of Application of Collagen from Fish Scales facial mask, comprise the following steps：
(1) grass carp scales are taken, after cleaning, grass carp scales is soaked into 4h in sodium carbonate liquor, then grass carp scales are put
In hydrochloric acid solution, with microwave treatment, the power of the microwave treatment is 800W；The time of the microwave treatment is 10min；So
4h is soaked with sodium hydroxide solution again afterwards, is washed out to neutrality, filtering, obtains filtrate 1 and filter residue 1；
(2) 17 times of amount water are added in the filter residue in step (1), regulation control ph, at 50 DEG C, adds pancreas in 7.0, temperature
Protease, the trypsase and filter residue ratio are 2.5: 100, stir 0.6h, are incubated 2h, then inactivate trypsase；Control pH
Value adds pepsin in 2.0, temperature at 60 DEG C, and the pepsin and filter residue ratio are 2.3: 100, after stirring 3h, inactivation
Pepsin, washing and filtering obtains filtrate 2 and filter residue 2；
(3) it is filtrate 1 and filtrate is 2-in-1 simultaneously, with the cellulose mixture filtering with microporous membrane that aperture is 50 μm, filtrate 3 is obtained,
Filtrate 3 is spray-dried, Application of Collagen from Fish Scales is obtained；
(4) by Application of Collagen from Fish Scales and polyacrylate sodium, pot marigold extract, carragheen thickener, secondary alkyl
Sodium sulfovinate bleeding agent is well mixed in a solvent, that is, obtains Application of Collagen from Fish Scales facial mask.
Embodiment 5
The invention provides a kind of preparation technology of Application of Collagen from Fish Scales facial mask, comprise the following steps：
(1) grass carp scales are taken, after cleaning, grass carp scales is soaked 3 in sodium carbonate liquor, then grass carp scales are placed in
In acetum, with microwave treatment, the power of the microwave treatment is 500W；The time of the microwave treatment is 5min；Then
6h is soaked with potassium hydroxide solution again, is washed out to neutrality, filtering, obtains filtrate 1 and filter residue 1；
(2) add 20 times of amount water in the filter residue in step (1), control ph is adjusted in 7.5, temperature at 55 DEG C, in addition
Property protease, the neutral proteinase and filter residue ratio are 2.3: 100, stir 1h, are incubated 2h, then inactivate neutral proteinase；Control
PH value processed adds papain in 3.0, temperature at 70 DEG C, and the papain and filter residue ratio are 2: 100, stir 3h
Afterwards, papain is inactivated, washing and filtering obtains filtrate 2 and filter residue 2；
(3) it is filtrate 1 and filtrate is 2-in-1 simultaneously, with the cellulose mixture filtering with microporous membrane that aperture is 25 μm, filtrate 3 is obtained,
Filtrate 3 is spray-dried, Application of Collagen from Fish Scales is obtained；
(4) by Application of Collagen from Fish Scales and hydroxymethyl cellulose, Honegsukle flower P.E, pectate thickener, sulphation castor
Sesame oil bleeding agent is well mixed in a solvent, that is, obtains Application of Collagen from Fish Scales facial mask.
Foregoing description is only the description to section Example of the present invention, not to any restriction of the scope of the invention, one's own profession
The those of ordinary skill of industry can make improvement according to the present invention or change to above-described embodiment, but belong to present invention protection model
Enclose.
Claims (9)
1. a kind of preparation technology of Application of Collagen from Fish Scales facial mask, it is characterised in that comprise the following steps：
(1) grass carp scales are taken, after cleaning, grass carp scales 3~5h are soaked into the solution containing carbonate, then by grass carp fish
Squama is placed in acid solution, with microwave treatment, then soaks 3~12h with alkaline solution again, is washed out to neutrality, filtering, is obtained
To filtrate 1 and filter residue 1；
(2) by the filter residue processing with enzyme preparation in step (1), washing and filtering obtains filtrate 2 and filter residue 2；
(3) it is filtrate 1 and filtrate is 2-in-1 simultaneously, with filtering with microporous membrane, filtrate 3 is obtained, filtrate 3 is spray-dried, grass is obtained
Fish fish scale collagen；
(4) Application of Collagen from Fish Scales is well mixed in a solvent with film forming agent, plant extracts, thickener, bleeding agent, i.e.,
Obtain Application of Collagen from Fish Scales facial mask.
2. the preparation technology of Application of Collagen from Fish Scales facial mask according to claim 1, it is characterised in that in step (1)
In, the acid solution is the aqueous solution of acid, and the acid is at least one of hydrochloric acid, citric acid, acetic acid, lactic acid.
3. the preparation technology of Application of Collagen from Fish Scales facial mask according to claim 1, it is characterised in that in step (1)
In, the power of the microwave treatment is 400~900W；The time of the microwave treatment is 0.5~15min.
4. the preparation technology of the Application of Collagen from Fish Scales facial mask according to claim 1 or 3, it is characterised in that in step
(1) in, the alkaline solution is the aqueous solution of alkali metal hydroxide and/or alkaline earth metal hydroxide.
5. the preparation technology of Application of Collagen from Fish Scales facial mask according to claim 1, it is characterised in that in step (2)
In, the processing with enzyme preparation is concretely comprised the following steps：
Jia 15 in filter residue in step (1)~20 times of amount water, adjust control ph in 6.5~7.5, temperature at 45~55 DEG C,
Enzyme preparation 1 is added, the enzyme preparation 1 is (0.5~3.0) with filter residue ratio: 100,0.5~1.5h is stirred, 1~4h is incubated, then
Inactivate enzyme preparation 1；Control ph adds enzyme preparation 2 in 1.0~3.0, temperature at 55~70 DEG C, the enzyme preparation 2 and filter residue ratio
Example is (0.1~3.0): after 100,1~3h of stirring, enzyme preparation 2 of putting out a fire.
6. the preparation technology of Application of Collagen from Fish Scales facial mask according to claim 5, it is characterised in that in step (2)
In, the enzyme preparation 1 and enzyme preparation 2 are respectively in neutral proteinase, papain, trypsase, pepsin at least
It is a kind of.
7. the preparation technology of Application of Collagen from Fish Scales facial mask according to claim 1, it is characterised in that in step (3)
In, the miillpore filter is the cellulose mixture miillpore filter that aperture is 20-50 μm.
8. the preparation technology of Application of Collagen from Fish Scales facial mask according to claim 1, it is characterised in that in step (4)
In, the film forming agent is polyacrylic acid, polyacrylate sodium, polyvinylpyrrolidone, hydroxymethyl cellulose, PVP and poly- second
At least one of glycol.
9. the preparation technology of Application of Collagen from Fish Scales facial mask according to claim 1, it is characterised in that in step (4)
In, the plant extracts be gadol extract, marine algae extract, green-tea extract, aloe extract, mint extract,
Pot marigold extract, Honegsukle flower P.E, Herba Lysimachiae foenumgraeci extract, rose extract, camomile extract, lemon extract, fan
Repeatedly at least one of fragrant extract, Ocimum sanctum P.E, grape seed extract, tuckahoe extracts.
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Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN107714615A (en) * | 2017-11-21 | 2018-02-23 | 常州市阿曼特化工有限公司 | A kind of bath foam |
| CN108042388A (en) * | 2018-01-16 | 2018-05-18 | 青岛海洋生物医药研究院股份有限公司 | A kind of moisturizing and skin rejuvenating facial mask and preparation method thereof |
| CN110074998A (en) * | 2019-05-23 | 2019-08-02 | 华南理工大学 | A kind of high-hydroscopicity can wire drawing apply face dried noodle film and preparation method thereof |
| CN110760080A (en) * | 2019-10-10 | 2020-02-07 | 浙江海洋大学 | Method for preparing preservative film by using fish scales |
| CN111329794A (en) * | 2020-04-27 | 2020-06-26 | 杭州协合医疗用品有限公司 | Fish scale collagen nourishing and repairing mask and application thereof |
| CN111467255A (en) * | 2020-04-21 | 2020-07-31 | 江苏更美科技有限公司 | Preparation method and device of VC collagen anti-wrinkle essence capable of preventing skin aging |
| CN112314935A (en) * | 2020-11-19 | 2021-02-05 | 华中农业大学 | Preparation method of collagen-polysaccharide composite hydrogel and product thereof |
| CN112891247A (en) * | 2021-01-29 | 2021-06-04 | 青岛蓝色康典海洋生物科技有限公司 | Fish scale collagen invisible mask and preparation method thereof |
| CN113332217A (en) * | 2021-05-31 | 2021-09-03 | 美卓(杭州)医疗科技有限公司 | Composite collagen composition for repairing neck shrinkage and sagging |
| CN114573681A (en) * | 2020-12-01 | 2022-06-03 | 山东国际生物科技园发展有限公司 | Mild and simple high-purity fish scale collagen extraction process |
| CN117402929A (en) * | 2023-10-27 | 2024-01-16 | 广州市缇梵化妆品有限公司 | Collagen peptide for delaying aging and preparation method and application thereof |
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Application publication date: 20170915 |