CN107616938A - A kind of preparation method of agalloch eaglewood stoste - Google Patents

A kind of preparation method of agalloch eaglewood stoste Download PDF

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Publication number
CN107616938A
CN107616938A CN201710894175.5A CN201710894175A CN107616938A CN 107616938 A CN107616938 A CN 107616938A CN 201710894175 A CN201710894175 A CN 201710894175A CN 107616938 A CN107616938 A CN 107616938A
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parts
weight
pots
agalloch eaglewood
added
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CN201710894175.5A
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唐文君
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Shenzhen Tianxiang Fu Biotechnology Co Ltd
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Shenzhen Tianxiang Fu Biotechnology Co Ltd
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Priority to CN201710894175.5A priority Critical patent/CN107616938A/en
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  • Medicines Containing Plant Substances (AREA)

Abstract

The invention discloses a kind of preparation method of agalloch eaglewood stoste, comprise the following steps:A, precise yeast extract, golden yellow camomile extract, glycerine, allantoin add A pots, warming while stirring;Weigh Lignum Aquilariae Resinatum extract, water, Sodium Hyaluronate, oat peptide, glucan and add B pots, warming while stirring;B, when A pot temperatures are warming up to 90 DEG C, and B pots are warming up to 85 DEG C, and A pots are added in vacuum emulsification pot with B pot mixtures and stirred;C, start homogeneous to make a call to 5 minutes;D, butanediol, propane diols, carbomer, trideceth, hydroxyethyl cellulose, tocopherol, niacinamide, triethanolamine, decoyl hydroximic acid is added after logical cooling water temperature to stir;E, the filtering and discharging when temperature is down to 35 DEG C, product is obtained after standing.Lignum Aquilariae Resinatum extract and other active ingredients can organically be combined by the inventive method, enable agalloch eaglewood stoste using when give full play to the effect of Lignum Aquilariae Resinatum extract.

Description

A kind of preparation method of agalloch eaglewood stoste
Technical field
The present invention relates to daily chemical product field, more particularly to a kind of preparation method of agalloch eaglewood stoste
Background technology
Maintenance product in the market for facial skin is numerous, but contains artificial synthesized composition mostly, long-term use of The problems such as easily causing allergic, inflammation, and poor permeability mostly be present in the product of natural extract, function is single, effect The unconspicuous problem of fruit.
Agalloch eaglewood contains numerous active components, can have positive role to skin cleaning, the elimination of scytitis, but at present Do not occur the skin-protection product about being prepared using agalloch eaglewood also on the market, related preparation technology is also and immature.
The content of the invention
For above-mentioned technical problem, the embodiments of the invention provide a kind of preparation method of agalloch eaglewood stoste
The first aspect of the embodiment of the present invention provides a kind of preparation method of agalloch eaglewood stoste, wherein, methods described include with Lower step:
A, precise 3-5 parts by weight yeast extract, the golden yellow camomile extract of 3-5 parts by weight, 3-5 parts by weight are sweet Oil, 0.01-0.03 parts by weight allantoin are added in A pots, warming while stirring;
Precise 10-20 parts by weight Lignum Aquilariae Resinatum extract, 5-10 parts by weight water, 5-7 parts by weight Sodium Hyaluronate, 2-3 weights Measure part oat peptide, 0.2-0.5 parts by weight glucan is added in B pots, warming while stirring;
B, when A kettle temperatures are warming up to 90 DEG C, and 85 DEG C are warming up in B pots, by mixture in mixture in A pots and B pots It is added in vacuum emulsification pot and mixes;
C, start homogeneous and make a call to 5 minutes temperature at 90 DEG C;
D, 1-2 parts by weight butanediol, 0.1-0.3 parts by weight of propylene glycol, 0.02-0.04 weight are added after leading to cooling water temperature Part carbomer, 0.03-0.05 parts by weight trideceth, 0.01-0.02 parts by weight hydroxyethyl cellulose, 0.03-0.05 weights Measure part tocopherol, 0.04-0.06 parts by weight niacinamide, 0.01-0.02 parts by weight triethanolamine, 5-10 parts by weight decoyl hydroximic acids Stir;
E, filtering and discharging is shut down when temperature is down to 35 DEG C, product is obtained after then standing.
The preparation method of described agalloch eaglewood stoste, wherein, in the A pots mixture before vacuum emulsification pot is added 90 DEG C insulation 10 minutes;Mixture is incubated 10 minutes before vacuum emulsification pot is added at 85 DEG C in the B pots.
The preparation method of described agalloch eaglewood stoste, wherein, mixture in A pots and mixture in B pots are added in the step B Enter into vacuum emulsification pot to mix and be specially:First mixture in B pots is added in vacuum emulsification pot, then will be mixed in A pots Thing adds, and is mixed at a temperature of 95 DEG C.
The preparation method of described agalloch eaglewood stoste, wherein, cooling water is led in the step D makes temperature be down to 40 DEG C.
The preparation method of described agalloch eaglewood stoste, wherein, standing 24h is needed in the step E after filtering and discharging.
The preparation method of described agalloch eaglewood stoste, wherein, the agalloch eaglewood stoste is composed of the following components:
Beneficial effect:Lignum Aquilariae Resinatum extract and other active ingredients can be organically attached to one by the inventive method Rise, enable agalloch eaglewood stoste using when give full play to the effect of Lignum Aquilariae Resinatum extract, and the inventive method is simple and practical, beneficial to big rule Mould is promoted.Agalloch eaglewood stoste of the present invention has extremely strong permeability, while has the effect of anti-inflammatory toxin expelling again, and agalloch eaglewood stoste can penetrate into Skin bottom, promote the reparation of inflammation and the discharge of toxin.In addition, agalloch eaglewood stoste also has the function that to calm the nerves, it is commonly used, energy It is effectively improved sleep quality.
Embodiment
Technical solution of the present invention is clearly and completely described below by embodiment, it is clear that described embodiment Only part of the embodiment of the present invention, rather than whole embodiments.Based on the embodiment in the present invention, people in the art The every other embodiment that member is obtained under the premise of creative work is not made, belongs to the scope of protection of the invention.
The present invention provides a kind of preparation method of agalloch eaglewood stoste, wherein, it the described method comprises the following steps:
A, precise 3-5 parts by weight yeast extract, the golden yellow camomile extract of 3-5 parts by weight, 3-5 parts by weight are sweet Oil, 0.01-0.03 parts by weight allantoin are added in A pots, warming while stirring;
Precise 10-20 parts by weight Lignum Aquilariae Resinatum extract, 5-10 parts by weight water, 5-7 parts by weight Sodium Hyaluronate, 2-3 weights Measure part oat peptide, 0.2-0.5 parts by weight glucan is added in B pots, warming while stirring.
B, when A kettle temperatures are warming up to 90 DEG C, and 85 DEG C are warming up in B pots, by mixture in mixture in A pots and B pots It is added in vacuum emulsification pot and mixes.
Wherein, mixture is incubated 10 minutes before vacuum emulsification pot is added at 90 DEG C in the A pots;Mixed in the B pots Compound is incubated 10 minutes before vacuum emulsification pot is added at 85 DEG C.
It is preferred that mixture in A pots and mixture in B pots are added to mix in vacuum emulsification pot being specially: First mixture in B pots is added in vacuum emulsification pot, then mixture in A pots is added, is mixed at a temperature of 95 DEG C.
C, start homogeneous and make a call to 5 minutes temperature at 90 DEG C.
D, lead to cooling water make temperature added after being down to 40 DEG C 1-2 parts by weight butanediols, 0.1-0.3 parts by weight of propylene glycol, 0.02-0.04 parts by weight carbomer, 0.03-0.05 parts by weight trideceth, 0.01-0.02 parts by weight hydroxy ethyl fibers Element, 0.03-0.05 parts by weight tocopherol, 0.04-0.06 parts by weight niacinamide, 0.01-0.02 parts by weight triethanolamine, 5-10 weight Amount part decoyl hydroximic acid stirs.
E, filtering and discharging is shut down when temperature is down to 35 DEG C, product is obtained after then standing 24h.
In preferred embodiment, the agalloch eaglewood stoste is composed of the following components:
Lignum Aquilariae Resinatum extract and other active ingredients can organically be combined by the inventive method, make agalloch eaglewood former Liquid using when can give full play to the effect of Lignum Aquilariae Resinatum extract, and the inventive method is simple and practical, beneficial to large-scale promotion.This hair Bright agalloch eaglewood stoste has an extremely strong permeability, while has the effect of anti-inflammatory toxin expelling again, and agalloch eaglewood stoste can penetrate to the skin bottom, promote Enter the reparation of inflammation and the discharge of toxin.In addition, agalloch eaglewood stoste also has the function that to calm the nerves, it is commonly used, can effectively improve and sleep Dormancy quality.
Wherein, the Lignum Aquilariae Resinatum extract is prepared by following steps:
S1, from Edgeworthia chrysantha agalloch eaglewood and cleaned up;
S2, clean agalloch eaglewood is put into supercritical CO2Extraction equipment, extraction equipment vessel space is filled out using wood chip It is full, then extracted, obtain extract.Extraction temperature is set as 45-60 DEG C, extracting pressure 50-60Mpa, extraction time For 4-6 hours, CO2Flow is 25L/h.
Extraction device is put into after impurity in S3, removal extract, separates agilawood essential oil and extract;
S4, extract is filtered to purification, acquisition Lignum Aquilariae Resinatum extract.
The golden yellow camomile extract is prepared by following steps:
H1, the chamomile of 50-65 mass parts is cleaned up and uses crusher machine of squeezing the juice, the dense of mass parts such as then use Spend and soak 30-50min for the ethanol water of 50-65 parts;
H2, the chamomile liquid after immersion be put into centrifuge under 1000-1500r/min centrifuge 10-15min, obtain from Heart liquid;
H3,0.8 normal atmosphere pressure of centrifugate is distilled and collects extract solution, extract solution is used to the screen cloth of 320 mesh Filtering carries out screen filtration, and 30-45 mass parts concentration is added into filtrate as the ethanol solution of 75-80 parts and is well mixed;
H4, filtrate mixed liquor distilled at 0.9 standard atmospheric pressure, 90-100 DEG C, remove distillate, obtain residue As camomile extract.
The preparation method of oat peptide is as follows:Oat is cleaned, oat is put into container, 18 times of amount of water, with alkali protease As hydrolysis enzyme, enzyme addition is 1.0%, heating, 50 DEG C of reaction temperature, obtains oat polypeptide, membrane filtration is standby after purification.
Using the inventive method can rapid, high volume prepare agalloch eaglewood stoste, prepared agalloch eaglewood stoste has repair function, Its permeability is strong, while has good antiinflammation, and stoste can penetrate to the skin bottom, promotes reparation and the toxin of inflammation Discharge.Meanwhile agalloch eaglewood stoste plays the role of to calm the nerves, and is commonly used, and can effectively improve sleep quality.
The inventive method, which prepares agalloch eaglewood stoste, has isolation, antianaphylaxis function.It is the antiallergy of agalloch eaglewood stoste, radioresistance, anti- Oxidation, the effect of isolation can be effectively isolated the skin damage that color make-up is brought.Meanwhile sensitivity, water shortage can be improved, dry decortication Skin, increase skin elasticity, can also treat the scytitises such as skin eczema, running sore, acne, promote skin repair and regeneration.
The inventive method, which prepares agalloch eaglewood stoste, has Glycerin, vegetative cell, the growth hair for promoting skin histology health The effect of educating.Containing the bioactive ingredients that can largely suppress tyrosinase activity in agalloch eaglewood stoste, can effectively press down The progress of redox reaction in melanin forming process processed, the formation of melanin is reduced, desalinate color spot, kept pale beautiful Skin.Stoste can effectively remove free radical simultaneously, reduce injury of the free radical to Skin Cell, reduce the appearance of wrinkle, Desalinate color spot, keep skin high resilience and gloss.Not only have and remove the effect of free radical is crease-resistant, the also spy with anti-irritant Property, especially when ultraviolet Irradiation on Skin produces detrimental effect, it is general red that agalloch eaglewood stoste can effectively remove skin table, to anaphylaxis skin Skin has excellent nursing role.
Agalloch eaglewood stoste prepared by the inventive method can increase and promote cuticula hydratability, it is combined the ability of water and increase Add, reduce moisture loss, make skin become it is smooth, wetting and it is flexible, can alleviate and treat xerodermia, skin care.Together When, agalloch eaglewood stoste can make water and active principle rapid osmotic effectively to improve skin base layer water shortage to skin bottom, from Fundamentally solves the water shortage problem of skin.
The above embodiments are merely illustrative of the technical solutions of the present invention, rather than its limitations;Although with reference to the foregoing embodiments The present invention is described in detail, it will be understood by those within the art that:It still can be to foregoing each implementation Technical scheme described in example is modified, or carries out equivalent substitution to which part technical characteristic;And these modification or Replace, the essence of appropriate technical solution is departed from the spirit and scope of various embodiments of the present invention technical scheme.

Claims (6)

1. a kind of preparation method of agalloch eaglewood stoste, it is characterised in that the described method comprises the following steps:
A, precise 3-5 parts by weight yeast extract, the golden yellow camomile extract of 3-5 parts by weight, 3-5 parts by weight of glycerin, 0.01-0.03 parts by weight allantoin is added in A pots, warming while stirring;
Precise 10-20 parts by weight Lignum Aquilariae Resinatum extract, 5-10 parts by weight water, 5-7 parts by weight Sodium Hyaluronate, 2-3 parts by weight Oat peptide, 0.2-0.5 parts by weight glucan are added in B pots, warming while stirring;
B, when A kettle temperatures are warming up to 90 DEG C, and 85 DEG C are warming up in B pots, mixture in mixture in A pots and B pots is added Mixed in vacuum emulsification pot;
C, start homogeneous and make a call to 5 minutes temperature at 90 DEG C;
D, 1-2 parts by weight butanediol, 0.1-0.3 parts by weight of propylene glycol, 0.02-0.04 parts by weight cards are added after leading to cooling water temperature Ripple nurse, 0.03-0.05 parts by weight trideceth, 0.01-0.02 parts by weight hydroxyethyl cellulose, 0.03-0.05 parts by weight Tocopherol, 0.04-0.06 parts by weight niacinamide, 0.01-0.02 parts by weight triethanolamine, the stirring of 5-10 parts by weight decoyls hydroximic acid Uniformly;
E, filtering and discharging is shut down when temperature is down to 35 DEG C, product is obtained after then standing.
2. the preparation method of agalloch eaglewood stoste according to claim 1, it is characterised in that mixture is adding in the A pots Before vacuum emulsification pot 10 minutes are incubated at 90 DEG C;Mixture is incubated before vacuum emulsification pot is added at 85 DEG C in the B pots 10 minutes.
3. the preparation method of agalloch eaglewood stoste according to claim 1, it is characterised in that will be mixed in the step B in A pots Thing is added to mix in vacuum emulsification pot with mixture in B pots:Mixture in B pots is first added into vacuum emulsification pot It is interior, then mixture in A pots is added, mixed at a temperature of 95 DEG C.
4. the preparation method of agalloch eaglewood stoste according to claim 1, it is characterised in that leading to cooling water in the step D makes Temperature is down to 40 DEG C.
5. the preparation method of agalloch eaglewood stoste according to claim 1, it is characterised in that in the step E after filtering and discharging 24h need to be stood.
6. the preparation method of agalloch eaglewood stoste according to claim 1, it is characterised in that the agalloch eaglewood stoste is by following components Composition:
CN201710894175.5A 2017-09-28 2017-09-28 A kind of preparation method of agalloch eaglewood stoste Pending CN107616938A (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108852974A (en) * 2018-08-22 2018-11-23 吴华 A kind of agalloch eaglewood facial mask and preparation method thereof
CN111877023A (en) * 2020-07-08 2020-11-03 潘嘉红 Agilawood silk quilt and manufacturing method thereof
CN113016820A (en) * 2021-02-09 2021-06-25 百色学院 Inducer for promoting agaric tree to produce fragrance

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104357217A (en) * 2014-11-06 2015-02-18 孙广娥 Eaglewood stock solution as well as preparation process and application thereof
CN104825351A (en) * 2015-04-24 2015-08-12 东莞波顿香料有限公司 Eaglewood whitening facial cleanser and preparation method thereof

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104357217A (en) * 2014-11-06 2015-02-18 孙广娥 Eaglewood stock solution as well as preparation process and application thereof
CN104825351A (en) * 2015-04-24 2015-08-12 东莞波顿香料有限公司 Eaglewood whitening facial cleanser and preparation method thereof

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
深圳市天香赋生物科技有限公司: "《http://125.35.6.80:8181/ftban/itownet/hzp_ba/fw/pz.jsp?processid=20160511135040wiq9a&nid=20160511135040wiq9a》", 11 May 2016 *

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108852974A (en) * 2018-08-22 2018-11-23 吴华 A kind of agalloch eaglewood facial mask and preparation method thereof
CN111877023A (en) * 2020-07-08 2020-11-03 潘嘉红 Agilawood silk quilt and manufacturing method thereof
CN113016820A (en) * 2021-02-09 2021-06-25 百色学院 Inducer for promoting agaric tree to produce fragrance
CN113016820B (en) * 2021-02-09 2021-11-16 百色学院 Inducer for promoting agaric tree to produce fragrance

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Application publication date: 20180123