CN108653034A - A kind of preparation method of the moisturizing emulsion containing fibroin - Google Patents
A kind of preparation method of the moisturizing emulsion containing fibroin Download PDFInfo
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- CN108653034A CN108653034A CN201810827438.5A CN201810827438A CN108653034A CN 108653034 A CN108653034 A CN 108653034A CN 201810827438 A CN201810827438 A CN 201810827438A CN 108653034 A CN108653034 A CN 108653034A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/925—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of animal origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/981—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of mammals or bird
- A61K8/986—Milk; Derivatives thereof, e.g. butter
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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Abstract
A kind of preparation method of the moisturizing emulsion containing fibroin, belongs to facial treatment milk preparing technical field, including：Fibroin aqueous solution is prepared, the newborn whey of camel is prepared, prepares Maca extract, prepare water phase liquid, prepare oil phase liquid, prepare soluble buckwheat starch, prepare lotion.The present invention uses fibroin as excellent cosmetic humectant, for moisturizing significant effect.With fresh camel breast for raw material, the whey in camel breast is extracted, has effects that excellent nourishing moisturizing, and be better than cow's milk whey.Oviductus ranae contains abundant bioactive ingredients, such as abundant collagen and amino acid, a variety of estrogenic components, a large amount of unsaturated fatty acids, nucleic acid, vitamin, these active constituents are easily absorbed by the skin, and can effectively prevent dry skin, nourishes skin.
Description
Technical field
The present invention relates to facial treatment milk preparing technical fields, and in particular to a kind of preparation of the moisturizing emulsion containing fibroin
Method.
Background technology
Lotion is the most basic step of skin care, and the active ingredients such as moisturizing, whitening and anti-aging in lotion being capable of better quilt
Percutaneous absorption possesses many lotions that one bottle of good lotion is extremely important, and now occurs in the market, all contains a large amount of chemistry and closes
At object, long-time service will produce skin certain side effect so that the nutritional ingredient in lotion is not easy to be absorbed, or even can draw
The adverse reactions such as scytitis are sent out, if selection is improper to will result in immeasurable loss, many lotions are making on the market
When, the selection of chemical substance and dosage are there are prodigious problem, and natural component is less, and skin effect is bad, need further
It improves.
Invention content
According to problems of the prior art, the present invention provides a kind of preparation side of the moisturizing emulsion containing fibroin
Method, natural component is high, and it is good to nourish moistening effect.
The present invention uses following technical scheme：
A kind of preparation method of the moisturizing emulsion containing fibroin, includes the following steps：
Step 1：By silk cocoon with bath raio 1:200 are added the Na that mass concentration is 0.5%2CO3In aqueous solution, boil 1 hour
The silk after degumming is taken out in degumming, and rubbing washing is until clarification of water, the white shape of silk, are used in combination deionized water to impregnate 2 in water
To 3 times, 3 minutes every time, the silk that deionized water was impregnated is paved and is put into baking oven, after being dried 2 hours under the conditions of 50 DEG C -60 DEG C
It takes out, silk is immersed in the LiBr aqueous solutions of 9.3mol/L with mass concentration 10%, stirring and dissolving 3 hours under the conditions of 70 DEG C
Until silk is completely dissolved, the silk solution dissolved is filtered with 8 layers of gauze, filtered solution is cooled to room temperature
After introduce bag filter, be then placed in deionized water bathtub and dialyse, after 1h, 4h, 8h, 12h, replace for 24 hours with 48h it is primary
Deionized water obtains fibroin aqueous solution until conductivity values are constant；
Step 2：With fresh camel breast for raw material, the absolute ethyl alcohol of mass percent 25% is added in hunchbacked breast, uniformly mixes
Static 1h afterwards, centrifuge filtering, rotating speed 3000r/min, centrifugation time 5min collect supernatant, obtain hunchbacked newborn whey；
Step 3：Maca is washed, is placed at aeration-drying and is air-dried after washing, the maca after air-drying is set
In micro-wave oven, moderate heat dries 4min, and the maca after drying is put into pulverizer and is crushed, the maca after crushing is crossed 60 mesh
Sieve, obtains pueraria root powder, weighs pueraria root powder 10g, water 100g, be added to the container, and extraction 100min is decocted at 90 DEG C, will be in container
Substance all takes out, and is cooled to room temperature, is filtered with cryogenic freezing centrifuge, rotating speed 3000r/min, centrifugation time 5min, receives
Collect supernatant, Maca extract is obtained after filtering；
Step 4：According to the mass fraction, by 2 parts of fibroin aqueous solutions, 2 parts of Maca extracts, 10 parts of glycerine, 4 part third
Glycol, 0.4 part of triethanolamine are added in 78 parts of deionized waters, and water phase liquid is made until dissolving in 80 DEG C of heating stirrings；
Step 5：According to the mass fraction, by the newborn wheys of 10 parts of camels, 2 parts of Rana amurensis ovary powders, 2 parts of methyl-silicone oils, 3 parts of monoglycerides,
1.2 parts of polyoxyethylene sorbitan monolaurates, 0.4 part of xanthan gum, uniform stirring 15min under the conditions of 80 DEG C are made
Oil phase liquid；
Step 6：By buckwheat fine powder with bath raio 1:2.5 are added in the sodium sulfite aqueous solution that mass concentration is 2%, 50 DEG C
2h is impregnated, mixed solution is obtained；
Step 7：Mixed solution at 4000r/min is centrifuged into 10min with centrifuge, wipes upper layer dark matter off, it is heavy to take
It forms sediment and washes one time, cleaned 3 times with the sodium hydroxide solution of mass concentration 0.2% after filtering, wash 2 times, filtered again after filtering
Filter, is dried overnight, crushing sieves with 100 mesh sieve, and obtains buckwheat starch in 45 DEG C of baking oven；
Step 8：By bath raio 1:Buckwheat starch is mixed to obtain starch suspension by 20 with 80% ethanol solution of volumetric concentration,
It is placed in 70 DEG C of thermostat water baths, while the sodium hydroxide solution of a concentration of 10.5g/100mL is slowly dropped to starch suspension
In liquid, so that starch suspension pH value is remained at 7-7.5, and be stirred continuously, is filtered after reacting 80min；
Step 9：Gained starch will be filtered and be neutralized to neutrality with the hydrochloric acid solution of 3mol/L, with the second of volumetric concentration 70%
Alcoholic solution cleaning is primary, supernatant is discarded after precipitation, then cleaned once with the ethanol solution of volumetric concentration 85%, is discarded after precipitation
Supernatant is finally cleaned once with 95% ethanol solution of volumetric concentration again, is dried in 45 DEG C of baking ovens after suction filtration, be crushed 100 mesh
Sieve, obtains graininess cold water solubles buckwheat starch；
Step 10：Under conditions of being stirred continuously, oil phase liquid made from step 5 is added slowly to step 4 and is made
Water phase liquid in, using high speed disperser stir 5min, the graininess cold water solubles buckwheat starch of 2 mass parts is then added, after
Continuous to stir 6min using high speed disperser, cooling discharging both obtains lotion.
Preferably, the Rana amurensis ovary powder is that oviductus ranae dry product smashes it through 40 mesh sieve.
Preferably, the mixing speed of the step ten high speed disperser is 5000-6000r/min.
Preferably, three layers of filtered through gauze are filtered into the step three.
Preferably, it is filtered using the membrane filter in 0.2 μm of aperture after three layers of filtered through gauze.
Preferably, the water in the step three is deionized water.
The beneficial effects of the present invention are：
1) present invention uses fibroin as excellent cosmetic humectant, for moisturizing significant effect.
2) present invention extracts the whey in camel breast, has effects that excellent nourishing moisturizing with fresh camel breast for raw material, and
Better than cow's milk whey.
3) oviductus ranae is the fallopian tubal of female wood frog, and volume energy expands 15-20 times after meeting water, and be translucent gel,
With good retentiveness and elasticity, main component is protein, accounts for about 50% of total amount or more, also contains abundant biology
Active constituent, such as abundant collagen and amino acid, a variety of estrogenic components, a large amount of unsaturated fatty acids, nucleic acid, dimension life
Element, carrotene, minerals and steroid etc., these active constituents are easily absorbed by the skin, and skin can be helped to dissolve hair
The sebum and aging cutin accumulated in hole accelerate cell turnover speed, reduce melanin production, can effectively prevent dry skin,
Nourish skin.
4) protein of buckwheat seed, fat content are higher than rice and wheat, and vitamin B2 content is higher than other grains
4-24 times, and contain chlorophyll and rutin, there is the effect of moistening and repairing skin for making lotion；Buckwheat starch is as wherein
A kind of natural biological macromolecular, resourceful and cheap, easily biological-degradable will not pollute, and be that a kind of green is former
Material.
Specific implementation mode
With reference to embodiments, the technical solution in the present invention is clearly and completely described.Based in the present invention
Embodiment, every other embodiment obtained by those of ordinary skill in the art without making creative efforts, all
Belong to the scope of protection of the invention.
A kind of preparation method of the moisturizing emulsion containing fibroin, includes the following steps：
Step 1：By silk cocoon with bath raio 1:200 are added the Na that mass concentration is 0.5%2CO3In aqueous solution, boil 1 hour
The silk after degumming is taken out in degumming, and rubbing washing is until clarification of water, the white shape of silk, are used in combination deionized water to impregnate 2 in water
To 3 times, 3 minutes every time, the silk that deionized water was impregnated is paved and is put into baking oven, after being dried 2 hours under the conditions of 50 DEG C -60 DEG C
It takes out, silk is immersed in the LiBr aqueous solutions of 9.3mol/L with mass concentration 10%, stirring and dissolving 3 hours under the conditions of 70 DEG C
Until silk is completely dissolved, the silk solution dissolved is filtered with 8 layers of gauze, filtered solution is cooled to room temperature
After introduce bag filter, be then placed in deionized water bathtub and dialyse, after 1h, 4h, 8h, 12h, replace for 24 hours with 48h it is primary
Deionized water obtains fibroin aqueous solution until conductivity values are constant；
Step 2：With fresh camel breast for raw material, the absolute ethyl alcohol of mass percent 25% is added in hunchbacked breast, uniformly mixes
Static 1h afterwards, centrifuge filtering, rotating speed 3000r/min, centrifugation time 5min collect supernatant, obtain hunchbacked newborn whey；
Step 3：Maca is washed, is placed at aeration-drying and is air-dried after washing, the maca after air-drying is set
In micro-wave oven, moderate heat dries 4min, and the maca after drying is put into pulverizer and is crushed, the maca after crushing is crossed 60 mesh
Sieve, obtains pueraria root powder, weighs pueraria root powder 10g, water 100g, be added to the container, and extraction 100min is decocted at 90 DEG C, will be in container
Substance all takes out, and is cooled to room temperature, is filtered with cryogenic freezing centrifuge, rotating speed 3000r/min, centrifugation time 5min, receives
Collect supernatant, Maca extract is obtained after filtering；
Step 4：According to the mass fraction, by 2 parts of fibroin aqueous solutions, 2 parts of Maca extracts, 10 parts of glycerine, 4 part third
Glycol, 0.4 part of triethanolamine are added in 78 parts of deionized waters, and water phase liquid is made until dissolving in 80 DEG C of heating stirrings；
Step 5：According to the mass fraction, by the newborn wheys of 10 parts of camels, 2 parts of Rana amurensis ovary powders, 2 parts of methyl-silicone oils, 3 parts of monoglycerides,
1.2 parts of polyoxyethylene sorbitan monolaurates, 0.4 part of xanthan gum, uniform stirring 15min under the conditions of 80 DEG C are made
Oil phase liquid；
Step 6：By buckwheat fine powder with bath raio 1:2.5 are added in the sodium sulfite aqueous solution that mass concentration is 2%, 50 DEG C
2h is impregnated, mixed solution is obtained；
Step 7：Mixed solution at 4000r/min is centrifuged into 10min with centrifuge, wipes upper layer dark matter off, it is heavy to take
It forms sediment and washes one time, cleaned 3 times with the sodium hydroxide solution of mass concentration 0.2% after filtering, wash 2 times, filtered again after filtering
Filter, is dried overnight, crushing sieves with 100 mesh sieve, and obtains buckwheat starch in 45 DEG C of baking oven；
Step 8：By bath raio 1:Buckwheat starch is mixed to obtain starch suspension by 20 with 80% ethanol solution of volumetric concentration,
It is placed in 70 DEG C of thermostat water baths, while the sodium hydroxide solution of a concentration of 10.5g/100mL is slowly dropped to starch suspension
In liquid, so that starch suspension pH value is remained at 7-7.5, and be stirred continuously, is filtered after reacting 80min；
Step 9：Gained starch will be filtered and be neutralized to neutrality with the hydrochloric acid solution of 3mol/L, with the second of volumetric concentration 70%
Alcoholic solution cleaning is primary, supernatant is discarded after precipitation, then cleaned once with the ethanol solution of volumetric concentration 85%, is discarded after precipitation
Supernatant is finally cleaned once with 95% ethanol solution of volumetric concentration again, is dried in 45 DEG C of baking ovens after suction filtration, be crushed 100 mesh
Sieve, obtains graininess cold water solubles buckwheat starch；
Step 10：Under conditions of being stirred continuously, oil phase liquid made from step 5 is added slowly to step 4 and is made
Water phase liquid in, using high speed disperser stir 5min, the graininess cold water solubles buckwheat starch of 2 mass parts is then added, after
Continuous to stir 6min using high speed disperser, cooling discharging both obtains lotion.
The Rana amurensis ovary powder is that oviductus ranae dry product smashes it through 40 mesh sieve.
The mixing speed of the step ten high speed disperser is 5000-6000r/min.
It is filtered into three layers of filtered through gauze in the step three.
It is filtered using the membrane filter in 0.2 μm of aperture after three layers of filtered through gauze.
Water in the step three is deionized water.
The present invention is exemplarily described above, it is clear that present invention specific implementation is not subject to the restrictions described above,
As long as using the improvement of the various unsubstantialities of inventive concept and technical scheme of the present invention progress, or not improved this is sent out
Bright design and technical solution directly applies to other occasions, within protection scope of the present invention.The protection of the present invention
Range should be determined by the scope of protection defined in the claims.
Claims (6)
1. a kind of preparation method of the moisturizing emulsion containing fibroin, which is characterized in that include the following steps：
Step 1：By silk cocoon with bath raio 1:200 are added the Na that mass concentration is 0.5%2CO3In aqueous solution, degumming in 1 hour is boiled,
The silk after degumming is taken out, rubbing washing is until clarification of water, the white shape of silk, are used in combination deionized water to impregnate 2 to 3 in water
It is secondary, 3 minutes every time, the silk that deionized water was impregnated is paved and is put into baking oven, taken after being dried 2 hours under the conditions of 50 DEG C -60 DEG C
Go out, silk is immersed in the LiBr aqueous solutions of 9.3mol/L with mass concentration 10%, stirring and dissolving 3 hours is straight under the conditions of 70 DEG C
It is completely dissolved, the silk solution dissolved is filtered with 8 layers of gauze, after filtered solution is cooled to room temperature to silk
Bag filter is introduced, is then placed in deionized water bathtub and dialyses, after 1h, 4h, 8h, 12h, replaces with 48h once go for 24 hours
Ionized water obtains fibroin aqueous solution until conductivity values are constant；
Step 2：With fresh camel breast for raw material, the absolute ethyl alcohol of mass percent 25% is added in hunchbacked breast, it is quiet after evenly mixing
Only 1h, centrifuge filtering, rotating speed 3000r/min, centrifugation time 5min collect supernatant, obtain hunchbacked newborn whey；
Step 3：Maca is washed, is placed at aeration-drying and is air-dried after washing, the maca after air-drying is placed in micro-
In wave stove, moderate heat dries 4min, and the maca after drying is put into pulverizer and is crushed, and the maca after crushing is crossed 60 mesh sieve, is obtained
Pueraria root powder weighs pueraria root powder 10g, water 100g, is added to the container, and extraction 100min is decocted at 90 DEG C, by the substance in container
It all takes out, is cooled to room temperature, filtered with cryogenic freezing centrifuge, rotating speed 3000r/min, centrifugation time 5min, in collection
Clear liquid obtains Maca extract after filtering；
Step 4：According to the mass fraction, by 2 parts of fibroin aqueous solutions, 2 parts of Maca extracts, 10 parts of glycerine, 4 parts of propylene glycol,
0.4 part of triethanolamine is added in 78 parts of deionized waters, and water phase liquid is made until dissolving in 80 DEG C of heating stirrings；
Step 5：According to the mass fraction, by the newborn whey of 10 parts of camels, 2 parts of Rana amurensis ovary powders, 2 parts of methyl-silicone oils, 3 parts of monoglycerides, 1.2
Oil phase is made in part polyoxyethylene sorbitan monolaurate, 0.4 part of xanthan gum, uniform stirring 15min under the conditions of 80 DEG C
Liquid；
Step 6：By buckwheat fine powder with bath raio 1:2.5 are added in the sodium sulfite aqueous solution that mass concentration is 2%, 50 DEG C of immersions
2h obtains mixed solution；
Step 7：Mixed solution at 4000r/min is centrifuged into 10min with centrifuge, upper layer dark matter is wiped off, takes precipitation water
It washes one time, is cleaned 3 times, washed again after filtering 2 times, filtered off with suction with the sodium hydroxide solution of mass concentration 0.2% after filtering,
It is dried overnight in 45 DEG C of baking oven, crushing sieves with 100 mesh sieve, and obtains buckwheat starch；
Step 8：By bath raio 1:Buckwheat starch is mixed to obtain starch suspension by 20 with 80% ethanol solution of volumetric concentration, is placed in
In 70 DEG C of thermostat water baths, while the sodium hydroxide solution of a concentration of 10.5g/100mL being slowly dropped in starch suspension,
So that starch suspension pH value is remained at 7-7.5, and be stirred continuously, is filtered after reacting 80min；
Step 9：Gained starch will be filtered and be neutralized to neutrality with the hydrochloric acid solution of 3mol/L, the ethyl alcohol with volumetric concentration 70% is molten
Liquid cleaning is primary, supernatant is discarded after precipitation, then cleaned once with the ethanol solution of volumetric concentration 85%, supernatant is discarded after precipitation
Liquid is finally cleaned once with 95% ethanol solution of volumetric concentration again, is dried in 45 DEG C of baking ovens after suction filtration, and crushing is sieved with 100 mesh sieve, obtained
To graininess cold water solubles buckwheat starch；
Step 10：Under conditions of being stirred continuously, oil phase liquid made from step 5 is added slowly to water made from step 4
In phase liquid, 5min is stirred using high speed disperser, the graininess cold water solubles buckwheat starch of 2 mass parts is then added, continues to make
6min is stirred with high speed disperser, cooling discharging both obtains lotion.
2. a kind of preparation method of moisturizing emulsion containing fibroin according to claim 1, it is characterised in that：Described
Rana amurensis ovary powder is that oviductus ranae dry product smashes it through 40 mesh sieve.
3. a kind of preparation method of moisturizing emulsion containing fibroin according to claim 1, it is characterised in that：Described
The mixing speed of step 10 high speed disperser is 5000-6000r/min.
4. a kind of preparation method of moisturizing emulsion containing fibroin according to claim 1, it is characterised in that：Described
It is filtered into three layers of filtered through gauze in step 3.
5. a kind of preparation method of moisturizing emulsion containing fibroin according to claim 4, it is characterised in that：Described
It is filtered using the membrane filter in 0.2 μm of aperture after three layers of filtered through gauze.
6. a kind of preparation method of moisturizing emulsion containing fibroin according to claim 1, it is characterised in that：Described
Water in step 3 is deionized water.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810827438.5A CN108653034A (en) | 2018-07-25 | 2018-07-25 | A kind of preparation method of the moisturizing emulsion containing fibroin |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810827438.5A CN108653034A (en) | 2018-07-25 | 2018-07-25 | A kind of preparation method of the moisturizing emulsion containing fibroin |
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| Publication Number | Publication Date |
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| CN108653034A true CN108653034A (en) | 2018-10-16 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810827438.5A Withdrawn CN108653034A (en) | 2018-07-25 | 2018-07-25 | A kind of preparation method of the moisturizing emulsion containing fibroin |
Country Status (1)
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| CN (1) | CN108653034A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112656755A (en) * | 2021-01-10 | 2021-04-16 | 潘伟 | High-permeability moisture mask and preparation method thereof |
| CN113372427A (en) * | 2021-04-12 | 2021-09-10 | 陶虎 | A assembly line equipment for preparing fibroin solution |
-
2018
- 2018-07-25 CN CN201810827438.5A patent/CN108653034A/en not_active Withdrawn
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112656755A (en) * | 2021-01-10 | 2021-04-16 | 潘伟 | High-permeability moisture mask and preparation method thereof |
| CN113372427A (en) * | 2021-04-12 | 2021-09-10 | 陶虎 | A assembly line equipment for preparing fibroin solution |
| CN113372427B (en) * | 2021-04-12 | 2023-09-12 | 陶虎 | Assembly line equipment for preparing fibroin solution |
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Application publication date: 20181016 |
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