CN108567647A - A kind of preparation method of the Whitening, spot lotion containing Gotu Kola P.E - Google Patents
A kind of preparation method of the Whitening, spot lotion containing Gotu Kola P.E Download PDFInfo
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- CN108567647A CN108567647A CN201810829875.0A CN201810829875A CN108567647A CN 108567647 A CN108567647 A CN 108567647A CN 201810829875 A CN201810829875 A CN 201810829875A CN 108567647 A CN108567647 A CN 108567647A
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- whitening
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/06—Emulsions
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/732—Starch; Amylose; Amylopectin; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/82—Preparation or application process involves sonication or ultrasonication
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Abstract
A kind of preparation method of the Whitening, spot lotion containing Gotu Kola P.E, belongs to facial treatment milk preparing technical field, the present invention includes：Gotu Kola P.E is prepared, licorice is prepared, prepares Maca extract, extraction buckwheat starch, graininess cold water solubles buckwheat starch is prepared, prepares lotion.The present invention is using plant extracts as active constituent, Gotu Kola P.E is a kind of natural whiting additive of better performances, has effects that Whitening, spot, Radix Glycyrrhizae main active is glycyrrhizic acid and flavones, with excellent Whitening, spot and anti-aging function, maca contains polysaccharide composition, the compositions such as hyaluronic acid, glucan, biological carbohydrate gum, these ingredients have good moisture-keeping efficacy, and maca has excellent white-skinned face function rich in a variety of amino acid.
Description
Technical field
The present invention relates to facial treatment milk preparing technical fields, and in particular to a kind of Whitening, spot breast containing Gotu Kola P.E
The preparation method of liquid.
Background technology
Lotion is the most basic step of skin care, and the active ingredients such as moisturizing, whitening and anti-aging in lotion being capable of better quilt
Percutaneous absorption possesses many lotions that one bottle of good lotion is extremely important, and now occurs in the market, all contains a large amount of chemistry and closes
At object, long-time service will produce skin certain side effect so that the nutritional ingredient in lotion is not easy to be absorbed, or even can draw
The adverse reactions such as scytitis are sent out, if selection is improper to will result in immeasurable loss, many lotions are making on the market
When, the selection of chemical substance and dosage are there are prodigious problem, and natural component is less, and skin effect is bad, need further
It improves.
Invention content
According to problems of the prior art, the present invention provides a kind of Whitening, spot lotion containing Gotu Kola P.E
Preparation method, natural component is high, and Whitening, spot effect is good.
The present invention uses following technical scheme：
A kind of preparation method of the Whitening, spot lotion containing Gotu Kola P.E, includes the following steps：
Step 1：Centella is weighed, is cleaned, drying is ground, and is sent into percolator, the ethyl alcohol with 10-13 times of weight is water-soluble
The processing of liquid diacolation, obtains percolate and diacolation residue, and the ethanol water of 2-3 times of weight is added into diacolation residue, impregnates 6-
10h, ultrasonic wave extraction 50-60min obtain ultrasonic extract and ultrasonic wave extraction residue, by ultrasonic extract and diacolation
Liquid merges, filtering, and filtrate decompression is concentrated by evaporation the 10-15% for original volume to get Gotu Kola P.E, the ethanol water
The mass concentration of solution is 50-60%；
Step 2：10g Radix Glycyrrhizaes are crushed, sieving, obtain Radix Glycyrrhizae powder, and the NaOH that mass concentration is 0.2mol/L is added
Aqueous solution is 1 by solid-liquid mass ratio:10 ratios mix, and the hot dipping extraction 2h at 80 DEG C repeats extraction 2 times, filtering, and filtrate is closed
And and be added mass concentration be 3% hydrochloric acid tune pH value to 1-2.5, centrifuged under the rotating speed of 4000r/min, collect supernatant
Liquid obtains licorice after filtering；
Step 3：Maca is washed, is placed at aeration-drying and is air-dried after washing, the maca after air-drying is set
In micro-wave oven, moderate heat dries 4min, and the maca after drying is put into pulverizer and is crushed, the maca after crushing is crossed 60 mesh
Sieve, obtains pueraria root powder；
Step 4：Pueraria root powder 10g, water 100g are weighed, is added to the container, extraction 100min is decocted at 90 DEG C, by container
In substance all take out, be cooled to room temperature, with cryogenic freezing centrifuge filter, rotating speed 3000r/min, centrifugation time
5min collects supernatant, and Maca extract is obtained after filtering；
Step 5：According to the mass fraction, by 3 parts of Gotu Kola P.Es, 3 parts of licorices, 3 parts of Maca extracts, 10
Part glycerine, 4 parts of propylene glycol, 0.4 part of triethanolamine are added in 78 parts of deionized waters, and 80 DEG C of heating stirrings are made until dissolving
Water phase liquid；
Step 6：According to the mass fraction, by 2 parts of methyl-silicone oils, 3 parts of monoglycerides, 1.2 parts of polyoxyethylene sorbitan lists
Oil phase liquid is made in laurate, 0.4 part of xanthan gum, uniform stirring 15min under the conditions of 80 DEG C；
Step 7：By buckwheat fine powder with bath raio 1:2.5 are added in the sodium sulfite aqueous solution that mass concentration is 2%, 50 DEG C
2h is impregnated, mixed solution is obtained；
Step 8：Mixed solution at 4000r/min is centrifuged into 10min with centrifuge, wipes upper layer dark matter off, it is heavy to take
It forms sediment and washes one time, cleaned 3 times with the sodium hydroxide solution of mass concentration 0.2% after filtering, wash 2 times, filtered again after filtering
Filter, is dried overnight, crushing sieves with 100 mesh sieve, and obtains buckwheat starch in 45 DEG C of baking oven；
Step 9：By bath raio 1:Buckwheat starch is mixed to obtain starch suspension by 20 with 80% ethanol solution of volumetric concentration,
It is placed in 70 DEG C of thermostat water baths, while the sodium hydroxide solution of a concentration of 10.5g/100mL is slowly dropped to starch suspension
In liquid, so that starch suspension pH value is remained at 7-7.5, and be stirred continuously, is filtered after reacting 80min；
Step 10：Gained starch will be filtered and be neutralized to neutrality with the hydrochloric acid solution of 3mol/L, with the second of volumetric concentration 70%
Alcoholic solution cleaning is primary, supernatant is discarded after precipitation, then cleaned once with the ethanol solution of volumetric concentration 85%, is discarded after precipitation
Supernatant is finally cleaned once with 95% ethanol solution of volumetric concentration again, is dried in 45 DEG C of baking ovens after suction filtration, be crushed 100 mesh
Sieve, obtains graininess cold water solubles buckwheat starch；
Step 11：Under conditions of being stirred continuously, oil phase liquid made from step 6 is added slowly to step 5 system
In the water phase liquid obtained, 5min is stirred using high speed disperser, the graininess cold water solubles buckwheat starch of 4 mass parts is then added,
It is continuing with high speed disperser stirring 6min, cooling discharging both obtains lotion.
Preferably, the mixing speed of a step ten high speed disperser is 5000-6000r/min.
Preferably, the filtering in the step two and step 4 is three layers of filtered through gauze.
Preferably, it is filtered using the membrane filter in 0.2 μm of aperture after three layers of filtered through gauze.
Preferably, grinding and sieving was 40 mesh sieve in the step two.
Preferably, the water in the step four is deionized water.
The beneficial effects of the present invention are：
1) using plant extracts as active constituent, Gotu Kola P.E is a kind of natural whiting addition of better performances
Agent has effects that Whitening, spot.
2) Radix Glycyrrhizae main active is glycyrrhizic acid and flavones, has excellent Whitening, spot and anti-aging function, and
Radix Glycyrrhizae is safe as traditional Chinese medicine ingredients, without side-effects.
3) maca contains polysaccharide composition, and compositions, these ingredients such as hyaluronic acid, glucan, biological carbohydrate gum have good
Moisture-keeping efficacy, and maca rich in a variety of amino acid have excellent white-skinned face function.
4) protein of buckwheat seed, fat content are higher than rice and wheat, and vitamin B2 content is higher than other grains
4-24 times, and contain chlorophyll and rutin, there is the effect of moistening and repairing skin for making lotion；Buckwheat starch is as wherein
A kind of natural biological macromolecular, resourceful and cheap, easily biological-degradable will not pollute, and be that a kind of green is former
Material.
Specific implementation mode
With reference to embodiments, the technical solution in the present invention is clearly and completely described.Based in the present invention
Embodiment, every other embodiment obtained by those of ordinary skill in the art without making creative efforts, all
Belong to the scope of protection of the invention.
A kind of preparation method of the Whitening, spot lotion containing Gotu Kola P.E, includes the following steps：
Step 1：Centella is weighed, is cleaned, drying is ground, and is sent into percolator, the ethyl alcohol with 10-13 times of weight is water-soluble
The processing of liquid diacolation, obtains percolate and diacolation residue, and the ethanol water of 2-3 times of weight is added into diacolation residue, impregnates 6-
10h, ultrasonic wave extraction 50-60min obtain ultrasonic extract and ultrasonic wave extraction residue, by ultrasonic extract and diacolation
Liquid merges, filtering, and filtrate decompression is concentrated by evaporation the 10-15% for original volume to get Gotu Kola P.E, the ethanol water
The mass concentration of solution is 50-60%；
Step 2：10g Radix Glycyrrhizaes are crushed, sieving, obtain Radix Glycyrrhizae powder, and the NaOH that mass concentration is 0.2mol/L is added
Aqueous solution is 1 by solid-liquid mass ratio:10 ratios mix, and the hot dipping extraction 2h at 80 DEG C repeats extraction 2 times, filtering, and filtrate is closed
And and be added mass concentration be 3% hydrochloric acid tune pH value to 1-2.5, centrifuged under the rotating speed of 4000r/min, collect supernatant
Liquid obtains licorice after filtering；
Step 3：Maca is washed, is placed at aeration-drying and is air-dried after washing, the maca after air-drying is set
In micro-wave oven, moderate heat dries 4min, and the maca after drying is put into pulverizer and is crushed, the maca after crushing is crossed 60 mesh
Sieve, obtains pueraria root powder；
Step 4：Pueraria root powder 10g, water 100g are weighed, is added to the container, extraction 100min is decocted at 90 DEG C, by container
In substance all take out, be cooled to room temperature, with cryogenic freezing centrifuge filter, rotating speed 3000r/min, centrifugation time
5min collects supernatant, and Maca extract is obtained after filtering；
Step 5：According to the mass fraction, by 3 parts of Gotu Kola P.Es, 3 parts of licorices, 3 parts of Maca extracts, 10
Part glycerine, 4 parts of propylene glycol, 0.4 part of triethanolamine are added in 78 parts of deionized waters, and 80 DEG C of heating stirrings are made until dissolving
Water phase liquid；
Step 6：According to the mass fraction, by 2 parts of methyl-silicone oils, 3 parts of monoglycerides, 1.2 parts of polyoxyethylene sorbitan lists
Oil phase liquid is made in laurate, 0.4 part of xanthan gum, uniform stirring 15min under the conditions of 80 DEG C；
Step 7：By buckwheat fine powder with bath raio 1:2.5 are added in the sodium sulfite aqueous solution that mass concentration is 2%, 50 DEG C
2h is impregnated, mixed solution is obtained；
Step 8：Mixed solution at 4000r/min is centrifuged into 10min with centrifuge, wipes upper layer dark matter off, it is heavy to take
It forms sediment and washes one time, cleaned 3 times with the sodium hydroxide solution of mass concentration 0.2% after filtering, wash 2 times, filtered again after filtering
Filter, is dried overnight, crushing sieves with 100 mesh sieve, and obtains buckwheat starch in 45 DEG C of baking oven；
Step 9：By bath raio 1:Buckwheat starch is mixed to obtain starch suspension by 20 with 80% ethanol solution of volumetric concentration,
It is placed in 70 DEG C of thermostat water baths, while the sodium hydroxide solution of a concentration of 10.5g/100mL is slowly dropped to starch suspension
In liquid, so that starch suspension pH value is remained at 7-7.5, and be stirred continuously, is filtered after reacting 80min；
Step 10：Gained starch will be filtered and be neutralized to neutrality with the hydrochloric acid solution of 3mol/L, with the second of volumetric concentration 70%
Alcoholic solution cleaning is primary, supernatant is discarded after precipitation, then cleaned once with the ethanol solution of volumetric concentration 85%, is discarded after precipitation
Supernatant is finally cleaned once with 95% ethanol solution of volumetric concentration again, is dried in 45 DEG C of baking ovens after suction filtration, be crushed 100 mesh
Sieve, obtains graininess cold water solubles buckwheat starch；
Step 11：Under conditions of being stirred continuously, oil phase liquid made from step 6 is added slowly to step 5 system
In the water phase liquid obtained, 5min is stirred using high speed disperser, the graininess cold water solubles buckwheat starch of 4 mass parts is then added,
It is continuing with high speed disperser stirring 6min, cooling discharging both obtains lotion.
The mixing speed of a step ten high speed disperser is 5000-6000r/min.
Filtering in the step two and step 4 is three layers of filtered through gauze.
It is filtered using the membrane filter in 0.2 μm of aperture after three layers of filtered through gauze.
Grinding and sieving was 40 mesh sieve in the step two.
Water in the step four is deionized water.
The present invention is exemplarily described above, it is clear that present invention specific implementation is not subject to the restrictions described above,
As long as using the improvement of the various unsubstantialities of inventive concept and technical scheme of the present invention progress, or not improved this is sent out
Bright design and technical solution directly applies to other occasions, within protection scope of the present invention.The protection of the present invention
Range should be determined by the scope of protection defined in the claims.
Claims (6)
1. a kind of preparation method of the Whitening, spot lotion containing Gotu Kola P.E, which is characterized in that include the following steps：
Step 1：Centella is weighed, is cleaned, drying is ground, and is sent into percolator, is oozed with the ethanol water of 10-13 times of weight
It filters processing, obtains percolate and diacolation residue, the ethanol water of 2-3 times of weight is added into diacolation residue, impregnate 6-10h,
Ultrasonic wave extraction 50-60min obtains ultrasonic extract and ultrasonic wave extraction residue, and ultrasonic extract and percolate are closed
And filter, filtrate decompression is concentrated by evaporation the 10-15% for original volume to get Gotu Kola P.E, the ethanol water
Mass concentration be 50-60%；
Step 2：10g Radix Glycyrrhizaes are crushed, sieving, obtain Radix Glycyrrhizae powder, and it is water-soluble that the NaOH that mass concentration is 0.2mol/L is added
Liquid is 1 by solid-liquid mass ratio:10 ratios mix, and the hot dipping extraction 2h at 80 DEG C repeats extraction 2 times, filtering, and filtrate merges, and
Be added mass concentration be 3% hydrochloric acid tune pH value to 1-2.5, centrifuged under the rotating speed of 4000r/min, collect supernatant, mistake
Licorice is obtained after filter；
Step 3：Maca is washed, is placed at aeration-drying and is air-dried after washing, the maca after air-drying is placed in micro-
In wave stove, moderate heat dries 4min, and the maca after drying is put into pulverizer and is crushed, and the maca after crushing is crossed 60 mesh sieve, is obtained
Pueraria root powder；
Step 4：Pueraria root powder 10g, water 100g are weighed, is added to the container, extraction 100min is decocted at 90 DEG C, it will be in container
Substance all takes out, and is cooled to room temperature, is filtered with cryogenic freezing centrifuge, rotating speed 3000r/min, centrifugation time 5min, receives
Collect supernatant, Maca extract is obtained after filtering；
Step 5：According to the mass fraction, by 3 parts of Gotu Kola P.Es, 3 parts of licorices, 3 parts of Maca extracts, 10 parts it is sweet
Oil, 4 parts of propylene glycol, 0.4 part of triethanolamine are added in 78 parts of deionized waters, and water phase is made until dissolving in 80 DEG C of heating stirrings
Liquid；
Step 6：According to the mass fraction, by 2 parts of methyl-silicone oils, 3 parts of monoglycerides, 1.2 parts of polyoxyethylene sorbitan list bays
Oil phase liquid is made in acid esters, 0.4 part of xanthan gum, uniform stirring 15min under the conditions of 80 DEG C；
Step 7：By buckwheat fine powder with bath raio 1:2.5 are added in the sodium sulfite aqueous solution that mass concentration is 2%, 50 DEG C of immersions
2h obtains mixed solution；
Step 8：Mixed solution at 4000r/min is centrifuged into 10min with centrifuge, upper layer dark matter is wiped off, takes precipitation water
It washes one time, is cleaned 3 times, washed again after filtering 2 times, filtered off with suction with the sodium hydroxide solution of mass concentration 0.2% after filtering,
It is dried overnight in 45 DEG C of baking oven, crushing sieves with 100 mesh sieve, and obtains buckwheat starch；
Step 9：By bath raio 1:Buckwheat starch is mixed to obtain starch suspension by 20 with 80% ethanol solution of volumetric concentration, is placed in
In 70 DEG C of thermostat water baths, while the sodium hydroxide solution of a concentration of 10.5g/100mL being slowly dropped in starch suspension,
So that starch suspension pH value is remained at 7-7.5, and be stirred continuously, is filtered after reacting 80min；
Step 10：Gained starch will be filtered and be neutralized to neutrality with the hydrochloric acid solution of 3mol/L, the ethyl alcohol with volumetric concentration 70% is molten
Liquid cleaning is primary, supernatant is discarded after precipitation, then cleaned once with the ethanol solution of volumetric concentration 85%, supernatant is discarded after precipitation
Liquid is finally cleaned once with 95% ethanol solution of volumetric concentration again, is dried in 45 DEG C of baking ovens after suction filtration, and crushing is sieved with 100 mesh sieve, obtained
To graininess cold water solubles buckwheat starch；
Step 11：Under conditions of being stirred continuously, oil phase liquid made from step 6 is added slowly to made from step 5
In water phase liquid, 5min is stirred using high speed disperser, the graininess cold water solubles buckwheat starch of 4 mass parts is then added, is continued
6min is stirred using high speed disperser, cooling discharging both obtains lotion.
2. a kind of preparation method of Whitening, spot lotion containing Gotu Kola P.E according to claim 1, feature exist
In：The mixing speed of a step ten high speed disperser is 5000-6000r/min.
3. a kind of preparation method of Whitening, spot lotion containing Gotu Kola P.E according to claim 1, feature exist
In：Filtering in the step two and step 4 is three layers of filtered through gauze.
4. a kind of preparation method of Whitening, spot lotion containing Gotu Kola P.E according to claim 3, feature exist
In：It is filtered using the membrane filter in 0.2 μm of aperture after three layers of filtered through gauze.
5. a kind of preparation method of Whitening, spot lotion containing Gotu Kola P.E according to claim 1, feature exist
In：Grinding and sieving was 40 mesh sieve in the step two.
6. a kind of preparation method of Whitening, spot lotion containing Gotu Kola P.E according to claim 1, feature exist
In：Water in the step four is deionized water.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115998636A (en) * | 2023-03-24 | 2023-04-25 | 江苏亨瑞生物医药科技有限公司 | Gel mask containing recombinant humanized collagen and preparation method thereof |
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2018
- 2018-07-25 CN CN201810829875.0A patent/CN108567647A/en not_active Withdrawn
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115998636A (en) * | 2023-03-24 | 2023-04-25 | 江苏亨瑞生物医药科技有限公司 | Gel mask containing recombinant humanized collagen and preparation method thereof |
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Application publication date: 20180925 |