CN112336668A

CN112336668A - Deep sea fish collagen peptide seaweed rejuvenating facial mask and preparation method thereof

Info

Publication number: CN112336668A
Application number: CN201910721340.6A
Authority: CN
Inventors: 彭健; 方素云; 胡晓珂; 闵军; 张海坤; 李岩; 刘卫; 王彩霞
Original assignee: Yantai Institute of Coastal Zone Research of CAS
Current assignee: Yantai Institute of Coastal Zone Research of CAS
Priority date: 2019-08-06
Filing date: 2019-08-06
Publication date: 2021-02-09

Abstract

The invention relates to the field of beauty cosmetics, and particularly relates to a deep sea fish collagen peptide seaweed rejuvenating mask and a preparation method thereof. The facial mask comprises a facial mask base cloth and essence; wherein, the supporting amount of the essence is 15-30%; the mask disclosed by the invention is prepared from natural components, and has the effects of resisting oxidation and aging, whitening and moisturizing, promoting cell metabolism, delaying cell aging, repairing damaged cells and the like. The production process of the deep sea fish collagen peptide seaweed mask greatly improves the utilization rate of the skin, the bone and the seaweed of the deep sea fish, saves resources, reduces the production cost of the mask and improves the production efficiency.

Description

Deep sea fish collagen peptide seaweed rejuvenating facial mask and preparation method thereof

Technical Field

The invention relates to the field of beauty cosmetics, and particularly relates to a deep sea fish collagen peptide seaweed rejuvenating mask prepared from deep sea fish collagen peptide and seaweed serving as main raw materials and a preparation method of the deep sea fish collagen peptide seaweed rejuvenating mask.

Background

With the continuous improvement of the standard of life of people, modern urban people pay more and more attention to skin maintenance and beauty treatment, people wake and pursue beauty treatment, and the blowout type development of the cosmetic industry in China is enabled to appear. The mask as a representative skin care product is changed from the original special care product to the current fast-absorption product, and occupies a very important share of the beauty market.

The beginning of the 'mask year' is called by the cosmetics industry in 2012, and the mask is a basic skin care product which is 3 days after the cream, the lotion and the hand cream, and becomes a 4 th-day consumer product, and the market growth rate is far higher than that of other products. The brand number of new masks in the market is increased by about 8 times, and at least more than 400 mask varieties are provided. According to the Nielson retail research data, the sales scale of the Chinese mask market in 2012 reaches 78.5 million yuan RMB, the composite growth rate exceeds 21.9% in 3 consecutive years, the scale and brand of the Chinese mask market are rapidly increased from 2012 to the present, and the market scale breaks through 500 million yuan. According to the grand idea of the general manager of the mask ODM Bohao group in China, the annual conservative estimation increases by 15 percent, and the market scale of the mask industry in China breaks 1000 million yuan in 2021. Roughly estimated, by 2018, the permeability is still at a low level when 0.03 mask is used every week by the elderly people (18-50 years old) in China. While korean and japanese facial masks use 0.08 and 0.17 facial masks, respectively, 2.7 and 5.7 times per week as much as china, so it is expected that the chinese facial mask market still has a huge promotion space.

Most of the existing facial masks are added with chemical synthetic medicaments, and the long-term use of the facial masks can cause harm to health. The development of the green natural environment-friendly mask becomes the current mainstream trend.

Disclosure of Invention

The invention provides a mask which has the effects of removing wrinkles, resisting oxidation, whitening skin, protecting skin, supplementing water and moisturizing and is prepared by taking deep sea fish skin, fishbone and seaweed as raw materials and a preparation method thereof aiming at the existing mask development technology.

In order to achieve the purpose, the technical scheme of the invention is as follows:

a deep sea fish collagen peptide seaweed rejuvenating mask comprises a mask base cloth and essence; wherein, the supporting amount of the essence is 15-30%; the essence comprises, by weight, 4-10% of deep sea fish collagen peptide, 2-6% of seaweed extract, 1-8% of rose hydrosol, 2-8% of aloe juice, 0.01-0.04% of trehalose, 0.2-0.6% of sodium hyaluronate, 0.5-3% of sodium benzoate, 0.001-0.01% of allantoin, 0.04-0.1% of xanthan gum, 0.1-0.9% of disodium EDTA, 0.01-0.05% of tocopherol, 0.1-0.6% of sodium PCA, 0.1-0.4% of sodium alginate, 0.01-0.1% of 1, 2-pentanediol, 0.01-0.1% of citric acid, 0.01-0.06% of sodium lactate and the balance of water.

Preferably, the carrying amount of the essence is 20% -25%; the essence comprises the following raw materials in percentage by weight: 5-9% of deep sea fish collagen peptide, 2-5% of seaweed extract, 2-6% of rose hydrosol, 3-6% of aloe juice, 0.01-0.04% of trehalose, 0.3-0.5% of sodium hyaluronate, 0.8-2% of sodium benzoate, 0.004-0.008% of allantoin, 0.05-0.08% of xanthan gum, 0.3-0.8% of disodium EDTA, 0.02-0.08% of tocopherol, 0.2-0.5% of sodium PCA, 0.2-0.4% of sodium alginate, 0.03-0.08% of 1, 2-pentanediol, 0.02-0.05% of citric acid, 0.02-0.05% of sodium lactate and the balance of water.

More preferably, the essence comprises, by weight, 5-8% of deep sea fish collagen peptide, 3-5% of seaweed whole extract, 3-5% of rose hydrosol, 4-5% of aloe juice, 0.02-0.03% of trehalose, 0.4-0.5% of sodium hyaluronate, 1-2% of sodium benzoate, 0.005-0.007% of allantoin, 0.06-0.07% of xanthan gum, 0.4-0.7% of disodium EDTA, 0.03-0.06% of tocopherol, 0.3-0.4% of sodium PCA, 0.3-0.4% of sodium alginate, 0.04-0.06% of 1, 2-pentanediol, 0.03-0.04% of citric acid, 0.03-0.04% of sodium lactate and the balance of water.

The deep sea fish collagen peptide: selecting fish heads, fish skins (scales) and fish bones of deep-sea fish as raw materials, cleaning the raw materials by using sterile water, crushing the cleaned raw materials, putting the crushed raw materials into an enzymolysis reaction tank, carrying out heat preservation enzymolysis, and then inactivating enzyme at high temperature; removing fishy smell with activated carbon, centrifuging, and collecting supernatant to obtain fish collagen peptide.

Selecting deep sea fish heads, fish skins (scales) and fish bones as raw materials to remove impurities, cleaning the raw materials by using sterile water, crushing the raw materials to 50-150 meshes for later use by using a crusher, transferring crushed raw material powder into an enzymolysis reaction tank, adding 10-20 times of distilled water of the raw materials, fully stirring the raw materials uniformly, adding enzyme to carry out enzymolysis on the raw materials, carrying out centrifugation after enzyme deactivation to obtain a crude fish collagen extract, adding activated carbon into the crude extract, stirring the mixture for 30-40min, and filtering the mixture to obtain a deep sea fish collagen peptide clear solution; wherein the enzyme accounts for 0.05-0.15% of the raw material powder.

The deep sea is deep sea cod or deep sea bass

The enzyme is alkaline protease, and the enzymolysis reaction step comprises the following steps: adjusting the pH value of the system to be 7-9, adding alkaline protease for enzymolysis at 50-60 ℃ for 3-5 h, and stirring at 85-95 ℃ for 40-50 min to inactivate enzyme.

The seaweed full-quality extract is prepared by cleaning fresh seaweed for later use, smashing the seaweed and uniformly mixing the smashed seaweed with deionized water and an organic solvent; adding wetting penetrant, and soaking at 30-40 deg.C for 36-48 h; distilling to remove the organic solvent, and carrying out pressure filtration on the distilled mixture to obtain a filtrate, wherein the filtrate is a seaweed extracting solution; wherein the distillation temperature is 50-60 ℃, and the distillation pressure is-0.5 to-1.2 Mpa; the mass ratio of the seaweed, the deionized water, the organic solvent and the wetting agent is 5-25:12-70:12-70: 1-7.

The seaweed is one or more of herba Zosterae Marinae, Undaria Pinnatifida, and thallus laminariae; preferably, the kelp, the undaria pinnatifida and the kelp are mixed according to the mass ratio of 3-5: 2-7:1-3.

The organic solvent is pharmaceutical grade ethanol and/or pharmaceutical grade propylene glycol, wherein the pharmaceutical grade ethanol and the pharmaceutical grade propylene glycol are mixed in a mass ratio of 1-2: 1-3;

the wetting penetrant is sodium dodecyl benzene sulfonate and/or sodium dodecyl sulfate, wherein the sodium dodecyl benzene sulfonate and the sodium dodecyl sulfate are mixed in a mass ratio of (2-5): 1-3.

The rose hydrosol is prepared by distilling fresh rose petals with purified water, mainly comprises citronellol, nerol, eugenol and the like, contains 0.3-0.5 thousandth of rose essential oil, retains hydrophilic essence in the rose petals, and nourishes skin. The functional factors in the hydrolat can be fully absorbed by the skin, and can thoroughly remove dirt on the surface of the skin and in pores, thereby achieving the purpose of purifying the skin. The rose hydrosol contains a large amount of aromatic alcohol substances, has strong antibacterial and bactericidal effects, and can promote capillary vasoconstriction. It has effects in delaying skin aging, effectively removing wrinkle, improving black eye, preventing wrinkle and mottle, relieving tension, regulating physiological cycle, and balancing skin pH.

A preparation method of a deep sea fish collagen peptide seaweed whitening mask comprises mixing rose hydrosol, sodium hyaluronate, sodium benzoate, disodium EDTA, sodium PCA, ammonium alginate, 1, 2-pentanediol, citric acid and sodium lactate according to the above proportion, heating to 65-70 deg.C, stirring for dissolving; keeping the temperature for 30-52min, slowly cooling to 30-35 deg.C, adding trehalose, allantoin, xanthan gum and tocopherol, and stirring at constant speed for 15-25 min; mixing, adding deep sea fish collagen peptide, Sargassum whole extract, and Aloe juice, and stirring for 5-10min to obtain essence; adding the facial mask base cloth into the essence, placing in 70-76 deg.C water bath, maintaining for 30-40min, and rapidly cooling to 4-5 deg.C (to achieve low temperature pasteurization) to obtain facial mask.

Compared with the prior art, the invention has the following beneficial effects:

1. the mask provided by the invention has the effects of removing wrinkles, resisting oxidation, whitening and protecting skin, resisting bacteria and diminishing inflammation, replenishing water and moisturizing and repairing damaged cells, and the contained deep sea fish collagen peptide can enhance the skin compactness, promote cell metabolism, delay cell aging and have excellent whitening and moisturizing effects; the seaweed extract can preserve moisture and lock water, protect skin, moisten skin, resist bacteria and diminish inflammation, and repair damaged cells.

2. The deep sea fish collagen peptide seaweed rejuvenating mask provided by the invention optimizes and selects the formula composition of the essence, and has better use feeling and skin care effect. And the utilization rate of the fish skin, the fish bone and the marine algae is greatly improved, the resources are saved, and the production cost of the mask is reduced.

3. The mask provided by the invention is simple in production process, simple in equipment required by production, and suitable for large-scale industrial production.

Drawings

Fig. 1 is a diagram of test results before and after using the mask of the present invention, wherein the test indexes include three aspects of elasticity, oil content and moisture; fig. 1A is before use, and fig. 1B is after use.

The specific implementation mode is as follows:

the technical solution of the present invention is further illustrated below with reference to the following embodiments, and the described embodiments are only a part of the embodiments of the present invention, but the scope of the present invention is not limited thereto.

The deep sea fish collagen peptide seaweed rejuvenating facial mask is prepared by taking fish heads, fish skin (scales), fish bones and seaweed of deep sea fish as raw materials and further improving and optimizing the formula composition of the facial mask essence, has the effects of removing wrinkles, resisting oxidation, whitening and protecting skin, resisting bacteria and diminishing inflammation, replenishing water and moisturizing and the like, greatly improves the comprehensive utilization rate of the fish heads, the fish skin (scales), the fish bones and the seaweed, and saves the production cost of the facial mask.

The essence in the mask adopts deep-sea fish collagen peptide, and has good effects of smoothing wrinkles, repairing cells, whitening and beautifying skin; the seaweed extract can reduce blood lipid on skin surface, and has effects of improving surface skin hematopoiesis function, caring skin, resisting bacteria, and relieving inflammation. Common cosmetics such as lotion, cream, facial mask and the like usually contain collagen or seaweed extract, but the effective active substances of the cosmetics are single in compatibility, the utilization rate of the active ingredients is low, and the effect is not obvious. The deep sea fish collagen and the seaweed extract are mixed and matched with other components for moderation, so that the linked action of repairing damaged cells and providing dense nutritional factors for skin is realized, the deep sea fish collagen and the seaweed extract are easy to absorb, deeply repaired, durably nourished and complemented in efficacy, and the skin quality is further improved.

Example 1

A process for preparing a deep sea fish collagen peptide seaweed rejuvenating facial mask comprises the following steps:

(1) preparing essence: preparing 4% of deep sea fish collagen peptide, 2% of seaweed whole extract, 1% of rose hydrosol, 2% of aloe juice, 0.01% of trehalose, 0.2% of sodium hyaluronate, 0.5% of sodium benzoate, 0.001% of allantoin, 0.04% of xanthan gum, 0.1% of EDTA disodium, 0.01% of tocopherol, 0.1% of sodium PCA, 0.1% of sodium alginate, 0.01% of 1, 2-pentanediol, 0.01% of citric acid, 0.01% of sodium lactate and the balance of water.

(2) Preparing essence: preparing essence: weighing rose hydrosol, sodium hyaluronate, sodium benzoate, EDTA disodium, PCA sodium, ammonium alginate, 1, 2-pentanediol, citric acid and sodium lactate according to the formula ratio, putting into a pot, heating to 65 ℃, and stirring for dissolving; keeping the temperature for 30min, slowly cooling to 30 deg.C, slowly adding trehalose, allantoin, xanthan gum and tocopherol in formula amount into the pan, and stirring at constant speed for 15 min; weighing the deep sea fish collagen peptide, the seaweed whole-material extract and the aloe juice in the formula ratio, adding and stirring for 5 min; folding the facial mask paper, putting the facial mask paper into a facial mask bag, injecting the prepared essence into the facial mask bag by using a clean injector, and then sealing the facial mask bag. Then placing the packaged facial mask in 70 deg.C water bath, maintaining for 30min, and rapidly cooling to 4-5 deg.C.

(3) The deep sea fish collagen peptide is prepared by the following steps:

firstly, selecting the fish head, fish skin (scale) and fish bone of the deep sea cod as raw materials, removing impurities, and cleaning with sterile water.

Crushing the cleaned raw material powder to 100 meshes, transferring the crushed raw material powder to an enzymolysis reaction tank, adding 15 times of distilled water of the raw material, fully stirring to be uniform, adjusting the pH value to be 7-8, adding 0.05% of the mass of the raw material powder, performing enzymolysis at the enzymolysis temperature of 50 ℃ for 5 hours, stirring at 85 ℃ for 50min, inactivating enzyme, and centrifuging to obtain supernatant to obtain the fish collagen crude extract.

Thirdly, adding active carbon into the crude extract, stirring for 30-40min, and filtering to obtain clear liquid, namely the deep sea fish collagen peptide.

(4) The seaweed full-quality extract is prepared by the following steps:

cleaning fresh kelp, undaria pinnatifida and kelp, and mixing the raw materials in a mass ratio of 5: crushing the kelp, the undaria pinnatifida and the kelp at a ratio of 4:3 by using a crusher for later use.

Uniformly mixing the smashed seaweed with deionized water, an organic solvent and a wetting penetrant according to a mass ratio of 5:12:12: 2; soaking at 30 deg.C for 48 h; the organic solvent is medical grade ethanol and medical grade propylene glycol, and the mass ratio is 1: 2. The wetting penetrant is sodium dodecyl benzene sulfonate and sodium dodecyl sulfate, and the mass ratio of the wetting penetrant to the sodium dodecyl benzene sulfonate is 2: 1.

③ 50 ℃ and-0.5 Mpa to remove the organic solvent by distillation. And carrying out pressure filtration on the distilled mixture to obtain a filtrate, wherein the filtrate is the seaweed extract.

Example 2

(1) preparing essence: preparing 6 percent of deep sea fish collagen peptide, 3 percent of seaweed whole extract, 2 percent of rose hydrosol, 3 percent of aloe juice, 0.02 percent of trehalose, 0.3 percent of sodium hyaluronate, 1 percent of sodium benzoate, 0.004 percent of allantoin, 0.06 percent of xanthan gum, 0.3 percent of EDTA disodium, 0.03 percent of tocopherol, 0.2 percent of sodium PCA, 0.2 percent of sodium alginate, 0.05 percent of 1, 2-pentanediol, 0.02 percent of citric acid, 0.02 percent of sodium lactate and the balance of water.

(3) The deep sea fish collagen peptide is prepared by the following steps:

firstly, selecting the fish head, the fish skin (scale) and the fish bone of the deep sea weever as raw materials, removing impurities, and cleaning the raw materials by using sterile water.

Crushing the cleaned raw material into 150 meshes by using a crusher, transferring the crushed raw material powder into an enzymolysis reaction tank, adding distilled water which is 20 times of the raw material, fully stirring the raw material powder to be uniform, adjusting the pH value to be 8-9, adding alkaline protease which accounts for 0.15% of the raw material powder by mass for enzymolysis, wherein the enzymolysis temperature is 50-60 ℃, the enzymolysis time is 3 hours, stirring the mixture at 95 ℃ for 40min for enzyme deactivation, and centrifuging the mixture to obtain supernatant so as to obtain the fish collagen crude extract.

(4) The seaweed full-quality extract is prepared by the following steps:

cleaning fresh kelp, undaria pinnatifida and kelp, and mixing the raw materials in a mass ratio of (3): and 5, smashing the kelp and the undaria pinnatifida by a grinder for standby.

Uniformly mixing the smashed seaweed with deionized water, an organic solvent and a wetting penetrant according to a mass ratio of 10:25:14: 3; soaking at 40 deg.C for 36 h; the organic solvent is pharmaceutical grade ethanol; the wetting penetrant is sodium dodecyl benzene sulfonate.

③ 60 ℃ and minus 1.0Mpa to distill and remove the organic solvent. And carrying out pressure filtration on the distilled mixture to obtain a filtrate, wherein the filtrate is the seaweed extract.

Example 3

(1) preparing essence: preparing 8% of deep sea fish collagen, 4% of seaweed whole extract, 6% of rose hydrosol, 5% of aloe juice, 0.03% of trehalose, 0.4% of sodium hyaluronate, 2% of sodium benzoate, 0.006% of allantoin, 0.08% of xanthan gum, 0.6% of EDTA disodium, 0.04% of tocopherol, 0.4% of sodium PCA, 0.3% of sodium alginate, 0.08% of 1, 2-pentanediol, 0.04% of citric acid, 0.04% of sodium lactate and the balance of water.

(2) Preparing essence: preparing essence: weighing rose hydrosol, sodium hyaluronate, sodium benzoate, EDTA disodium, PCA sodium, ammonium alginate, 1, 2-pentanediol, citric acid and sodium lactate according to the formula ratio, putting into a pot, heating to 65 ℃, and stirring for dissolving; keeping the temperature for 30min, slowly cooling to 30 deg.C, slowly adding trehalose, allantoin, xanthan gum and tocopherol in formula amount into the pan, and stirring at constant speed for 15 min; weighing deep sea fish collagen, seaweed whole-material extract and aloe juice in the formula ratio, adding and stirring for 5 min; folding the facial mask paper, putting the facial mask paper into a facial mask bag, injecting the prepared essence into the facial mask bag by using a clean injector, and then sealing the facial mask bag. Then placing the packaged facial mask in 70 deg.C water bath, maintaining for 30min, and rapidly cooling to 4-5 deg.C.

(3) The deep sea fish collagen peptide is prepared by the following steps:

Crushing the cleaned raw material into 80-mesh powder by using a crusher, transferring the crushed raw material powder into an enzymolysis reaction tank, adding distilled water which is 10 times of the raw material, fully stirring the mixture to be uniform, adjusting the pH value to be 7-8, adding alkaline protease which accounts for 0.08 percent of the mass of the raw material powder for enzymolysis, wherein the enzymolysis temperature is 55 ℃, the enzymolysis time is 4 hours, stirring the mixture at 90 ℃ for 45min for enzyme deactivation, and centrifuging the mixture to obtain supernatant to obtain the crude fish collagen extract.

(4) The seaweed full-quality extract is prepared by the following steps:

cleaning fresh kelp, undaria pinnatifida and kelp, and mixing the raw materials in a mass ratio of 4: crushing the kelp, the undaria pinnatifida and the kelp at a ratio of 5:1 by using a crusher for later use.

Uniformly mixing the smashed seaweed with deionized water, an organic solvent and a wetting penetrant according to a mass ratio of 8:30:40: 7; soaking at 35 deg.C for 40 h; the organic solvent is medical grade ethanol and medical grade propylene glycol, and the mass ratio is 1: 1. The wetting penetrant is sodium dodecyl benzene sulfonate and sodium dodecyl sulfate, and the mass ratio of the wetting penetrant to the sodium dodecyl benzene sulfonate is 2: 3.

③ 55 ℃ and-0.5 Mpa to remove the organic solvent by distillation. And carrying out pressure filtration on the distilled mixture to obtain a filtrate, wherein the filtrate is the seaweed extract.

Example 4

(1) preparing essence: preparing 10% of deep sea fish collagen, 6% of seaweed whole extract, 8% of rose hydrosol, 8% of aloe juice, 0.04% of trehalose, 0.6% of sodium hyaluronate, 3% of sodium benzoate, 0.01% of allantoin, 0.1% of xanthan gum, 0.9% of EDTA disodium, 0.05% of tocopherol, 0.6% of sodium PCA, 0.4% of sodium alginate, 0.1% of 1, 2-pentanediol, 0.1% of citric acid, 0.06% of sodium lactate and the balance of water.

(3) The deep sea fish collagen peptide is prepared by the following steps:

Crushing the cleaned raw material into 120 meshes by using a crusher, transferring the crushed raw material powder into an enzymolysis reaction tank, adding 18 times of distilled water of the raw material, fully stirring the mixture to be uniform, adjusting the pH value to 8-9, adding 0.12% of the mass of the raw material powder into the mixture for enzymolysis, wherein the enzymolysis temperature is 50 ℃, the enzymolysis time is 4 hours, stirring the mixture at 88 ℃ for 45min for enzyme deactivation, and centrifuging the mixture to obtain supernatant to obtain the crude fish collagen extract.

(4) The seaweed full-quality extract is prepared by the following steps:

cleaning fresh undaria pinnatifida and kelp, and mixing the fresh undaria pinnatifida and the kelp according to a mass ratio of 4:3, crushing the kelp, the undaria pinnatifida and the kelp by a crusher for standby.

Uniformly mixing the smashed seaweed with deionized water, an organic solvent and a wetting penetrant according to a mass ratio of 15:60:40: 3; soaking at 38 deg.C for 44 h; the organic solvent is medical-grade propylene glycol. The wetting penetrant is sodium dodecyl sulfate.

③ 60 ℃ and-0.5 Mpa to remove the organic solvent by distillation. And carrying out pressure filtration on the distilled mixture to obtain a filtrate, wherein the filtrate is the seaweed extract.

Evaluation of the deep sea fish collagen peptide seaweed rejuvenation mask obtained in the above example:

1) sensory evaluation was performed on the deep sea fish collagen peptide seaweed rejuvenating facial mask obtained in the above examples: the evaluation criteria are as follows: 50 people in different age groups are selected as members of the appraisal group, other conditions are guaranteed to be the same, sensory scoring is carried out, the total score is 10, 4 grades are good, good and acceptable. The corresponding case of scores and grades is: not less than 8 is preferred; <8 > and ≧ 6 are preferred; <6, > 5 is acceptable; <5 was completely unacceptable. There were 4 indices evaluated: the odor, viscosity, color and comfort level experience is respectively 20%, 25%, 10% and 45%. And taking the average score of the scores of each index testee, wherein the weighted scores of all the indexes are the sensory scores. The sensory evaluation is shown in Table 1.

TABLE 1

Index (I)	Score value
		Smell(s)	8
Viscosity of the oil	9
		Color	10
Comfort experience	9
		Evaluation ofTotal score	8.9

2) Skin measurement before and after using the mask

Performing instrument skin test on a human subject by using a skin tester, and performing data test on the deep sea fish collagen peptide seaweed glowing facial mask before use, and after use, on the forehead, eyes and cheeks respectively, wherein the test indexes comprise three aspects of elasticity, oil content and moisture, and test results (see figure 1)

As can be seen from the sensory test data of the mask shown in Table 1, the evaluation score of the tested population was 8.9 points, which is good for the mask grade. Fig. 1 shows that, as shown in the test data of the skin measuring apparatus, the elasticity, moisture and oil indexes of the face before and after the face mask is used have obvious changes, wherein, the elasticity coefficient and the moisture coefficient of the face mask skin after the face mask is refitted by the deep sea fish collagen peptide seaweed are obviously increased, while the oil coefficient of the face skin after the face mask is used is greatly reduced, so that the experience effect of the face skin of a human subject after the face mask is used is obvious.

The above description is only for the preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art should be able to cover the technical scope of the present invention and the equivalent alternatives or modifications according to the technical solution and the inventive concept of the present invention within the technical scope of the present invention.

Claims

1. The deep sea fish collagen peptide seaweed face-refreshing mask is characterized by comprising the following components in parts by weight: the facial mask comprises a facial mask base cloth and essence; wherein, the supporting amount of the essence is 15-30%; the essence comprises, by weight, 4-10% of deep sea fish collagen peptide, 2-6% of seaweed extract, 1-8% of rose hydrosol, 2-8% of aloe juice, 0.01-0.04% of trehalose, 0.2-0.6% of sodium hyaluronate, 0.5-3% of sodium benzoate, 0.001-0.01% of allantoin, 0.04-0.1% of xanthan gum, 0.1-0.9% of disodium EDTA, 0.01-0.05% of tocopherol, 0.1-0.6% of sodium PCA, 0.1-0.4% of sodium alginate, 0.01-0.1% of 1, 2-pentanediol, 0.01-0.1% of citric acid, 0.01-0.06% of sodium lactate and the balance of water.

2. The deep sea fish collagen peptide seaweed rejuvenating mask as claimed in claim 1, wherein: the essence comprises the following raw materials in percentage by weight: 5-9% of deep sea fish collagen peptide, 2-5% of seaweed extract, 2-6% of rose hydrosol, 3-6% of aloe juice, 0.01-0.04% of trehalose, 0.3-0.5% of sodium hyaluronate, 0.8-2% of sodium benzoate, 0.004-0.008% of allantoin, 0.05-0.08% of xanthan gum, 0.3-0.8% of disodium EDTA, 0.02-0.08% of tocopherol, 0.2-0.5% of sodium PCA, 0.2-0.4% of sodium alginate, 0.03-0.08% of 1, 2-pentanediol, 0.02-0.05% of citric acid, 0.02-0.05% of sodium lactate and the balance of water.

3. The deep sea fish collagen peptide seaweed rejuvenating mask as claimed in claim 2, wherein: the essence comprises, by weight, 5-8% of deep sea fish collagen peptide, 3-5% of seaweed extract, 3-5% of rose hydrosol, 4-5% of aloe juice, 0.02-0.03% of trehalose, 0.4-0.5% of sodium hyaluronate, 1-2% of sodium benzoate, 0.005-0.007% of allantoin, 0.06-0.07% of xanthan gum, 0.4-0.7% of disodium EDTA, 0.03-0.06% of tocopherol, 0.3-0.4% of sodium PCA, 0.3-0.4% of sodium alginate, 0.04-0.06% of 1, 2-pentanediol, 0.03-0.04% of citric acid, 0.03-0.04% of sodium lactate and the balance of water.

4. The deep sea fish collagen peptide seaweed rejuvenating mask according to any one of claims 1 to 3, characterized in that: the deep sea fish collagen peptide: selecting fish heads, fish skins (scales) and fish bones of deep-sea fish as raw materials, cleaning the raw materials by using sterile water, crushing the cleaned raw materials, putting the crushed raw materials into an enzymolysis reaction tank, carrying out heat preservation enzymolysis, and then inactivating enzyme at high temperature; removing fishy smell with activated carbon, centrifuging, and collecting supernatant to obtain fish collagen peptide.

5. The deep sea fish collagen peptide seaweed rejuvenating mask as claimed in claim 4, wherein: selecting deep sea fish heads, fish skins (scales) and fish bones as raw materials to remove impurities, cleaning the raw materials by using sterile water, crushing the raw materials to 50-150 meshes for later use by using a crusher, transferring crushed raw material powder into an enzymolysis reaction tank, adding 10-20 times of distilled water of the raw materials, fully stirring the raw materials uniformly, adding enzyme to carry out enzymolysis on the raw materials, carrying out centrifugation after enzyme deactivation to obtain a crude fish collagen extract, adding activated carbon into the crude extract, stirring the mixture for 30-40min, and filtering the mixture to obtain a deep sea fish collagen peptide clear solution; wherein the enzyme accounts for 0.05-0.15% of the raw material powder.

6. The deep sea fish collagen peptide seaweed rejuvenating mask as claimed in claim 5, wherein: the enzyme is alkaline protease, and the enzymolysis reaction step comprises the following steps: adjusting the pH value of the system to be 7-9, adding alkaline protease for enzymolysis at 50-60 ℃ for 3-5 h, and stirring at 85-95 ℃ for 40-50 min to inactivate enzyme.

7. The deep sea fish collagen peptide seaweed rejuvenating mask according to any one of claims 1 to 3, characterized in that: the seaweed full-quality extract is prepared by cleaning fresh seaweed for later use, smashing the seaweed and uniformly mixing the smashed seaweed with deionized water and an organic solvent; adding wetting penetrant, and soaking at 30-40 deg.C for 36-48 h; distilling to remove the organic solvent, and carrying out pressure filtration on the distilled mixture to obtain a filtrate, wherein the filtrate is a seaweed extracting solution; wherein the distillation temperature is 50-60 ℃, and the distillation pressure is-0.5 to-1.2 Mpa; the mass ratio of the seaweed, the deionized water, the organic solvent and the wetting agent is 5-25:12-70:12-70: 1-7.

8. The deep sea fish collagen peptide seaweed rejuvenating mask according to claim 7, wherein: the seaweed is one or more of herba Zosterae Marinae, Undaria Pinnatifida, and thallus laminariae;

the organic solvent is pharmaceutical grade ethanol and/or pharmaceutical grade propylene glycol;

the wetting penetrant is sodium dodecyl benzene sulfonate or sodium dodecyl sulfate.

9. The preparation method of the deep sea fish collagen peptide seaweed rejuvenating mask as claimed in claim 1, which is characterized in that: mixing rose hydrosol, sodium hyaluronate, sodium benzoate, EDTA disodium, PCA sodium, ammonium alginate, 1, 2-pentanediol, citric acid and sodium lactate according to the above proportion, heating to 65-70 deg.C, stirring for dissolving; keeping the temperature for 30-52min, slowly cooling to 30-35 deg.C, adding trehalose, allantoin, xanthan gum and tocopherol, and stirring at constant speed for 15-25 min; mixing, adding deep sea fish collagen peptide, Sargassum whole extract, and Aloe juice, and stirring for 5-10min to obtain essence; adding the facial mask base cloth into the essence, placing in 70-76 deg.C water bath, maintaining for 30-40min, and rapidly cooling to 4-5 deg.C to obtain facial mask.