CN113786371A - Composition for preparing blueberry seaweed mask, mask and preparation method - Google Patents
Composition for preparing blueberry seaweed mask, mask and preparation method Download PDFInfo
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- CN113786371A CN113786371A CN202110755485.5A CN202110755485A CN113786371A CN 113786371 A CN113786371 A CN 113786371A CN 202110755485 A CN202110755485 A CN 202110755485A CN 113786371 A CN113786371 A CN 113786371A
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- mask
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- sodium
- blueberry
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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Abstract
The invention relates to the field of cosmetic preparations, and provides a composition for preparing a blueberry seaweed mask, which comprises nutritional ingredients, additives and a solvent; wherein the nutrient components comprise plant extract; the plant extract comprises cowberry fruit ferment extract and brown algae whole substance extract. The invention also provides a facial mask containing the composition and a preparation method. Has the advantages that: 1. the addition amount of the preservative can be effectively controlled by using the conventional simple mask manufacturing process. 2. The mask and the mask composition provided by the invention have more obvious effects of resisting oxidation and aging, replenishing water and moisturizing, and can effectively remove active oxygen free radicals, strengthen capillary vessels, moisturize and lock water and repair damaged cells. 3. The invention improves the utilization rate of raw materials such as cowberry peel residue, marine brown algae and the like, saves resources and reduces the production cost of the mask. The mask provided by the invention is simple in production process, simple in equipment required by production, and suitable for large-scale industrial production.
Description
Technical Field
The invention relates to the field of toilet preparations, in particular to a composition for preparing a facial mask, the facial mask prepared by using the composition and a preparation method thereof; in particular to a composition for preparing a blueberry seaweed mask, the mask and a preparation method.
Background
With the continuous improvement of the standard of life of people, modern urban people pay more and more attention to skin maintenance and beauty treatment, people wake and pursue beauty treatment, and the blowout type development of the cosmetic industry in China is enabled to appear. The mask as a representative skin care product is changed from the original special care product to the current fast-absorption product, and occupies a very important share of the beauty market.
The beginning of the 'mask year' is called by the cosmetics industry in 2012, and the mask is a basic skin care product which is 3 days after the cream, the lotion and the hand cream, and becomes a 4 th-day consumer product, and the market growth rate is far higher than that of other products. The brand number of new masks in the market is increased by about 8 times, and at least more than 400 mask varieties are provided. According to the Nielson retail research data, the sales scale of the facial mask market in China in 2012 reaches 78.5 million yuan RMB, the composite growth rate exceeds 21.9% in 3 consecutive years, the scale and the brand of the facial mask market in China are rapidly increased from 2012 to the present, and the market scale breaks through 500 million yuan. According to the grand idea of the general manager of the mask ODM Bohao group in China, the annual conservative estimation increases by 15 percent, and the market scale of the mask industry in China breaks 1000 million yuan in 2021. Roughly estimated, by 2018, the permeability is still at a low level when 0.03 mask is used every week by the elderly people (18-50 years old) in China. While korean and japanese facial masks use 0.08 and 0.17 facial masks, respectively, 2.7 and 5.7 times per week as much as china, so it is expected that the chinese facial mask market still has a huge promotion space.
The facial mask is divided into a plurality of types according to different physical forms and using methods, and the types of the facial mask comprise a peeling type facial mask, a wiping or washing type facial mask and a cloth pasting type facial mask. The specific action principle of any facial mask is approximately similar, namely the facial mask covers the horny layer of the skin, provides moisture for the horny layer, and enables the horny layer to be fully hydrated so as to improve the appearance and the elasticity of the skin; contains humectant, emollient and nutrients, and has effects in blocking skin, reducing water loss of skin, softening horny layer, and promoting absorption of nutrients through skin.
More preservatives are required to be added in the traditional mask preparation to ensure that the product has a longer shelf life, but the preservatives have greater harm to people, and particularly, under the condition that the skin directly contacts the preservatives for a long time, even if the amount of the preservatives is less, adverse reactions such as damage, allergy and the like generated by sensitive skin can be easily caused. Some preservative-free mask products are mainly manufactured by using a special process, such as a moist heat sterilization method or an irradiation method, and have a disadvantage in that important nutrients in the mask composition are damaged, thereby reducing the practical utility.
Therefore, there is a need for a new technical solution to ensure that the use of preservatives with more harmful properties is minimized or avoided without significantly reducing the shelf life of the product while effectively moisturizing the skin.
Disclosure of Invention
The present invention is directed to solving the following problems, and provides several new solutions to solve the problems.
The problems to be solved by the invention mainly comprise:
1. the problem that the existing facial masks contain too much preservative;
2. the problem of wasting nutrient substances in the existing preservative-free mask in the manufacturing process is solved;
3. at present, the known facial mask mostly acts on the skin cells on the surface layer of the human face, but rarely solves the problem of improving the blood vessels in the deep layer of the human face.
Specifically, the present invention provides a series of technical solutions, including:
technical scheme 1, a composition for preparing a blueberry seaweed mask comprises nutritional ingredients, additives and a solvent; wherein the additive comprises one or more of humectant, film forming agent, plasticizer, volatility regulator, antiseptic, pH regulator, essence, colorant, stabilizer and viscosity regulator; the solvent comprises water; the nutrient components comprise plant extracts; the plant extract is characterized by comprising a cowberry ferment extract and a brown algae whole substance extract.
The key element for solving the technical problem 1 is to find a substance which can be directly applied to the mask and has a certain antiseptic effect and is not harmful to human, and the substance is particularly good when the substance is a nutrient substance. The cowberry fruit is plant of Vaccinium of Ericaceae, and contains large amount of flavonoids, wherein anthocyanins are main components. Anthocyanins (also called anthocyanidins) are water-soluble natural pigments widely present in plants in nature, and are colored aglycones obtained by hydrolyzing anthocyanins. The anthocyanin can be used as a nutrition enhancer and can be used as a preservative to replace synthetic preservatives such as toluic acid and the like in the fields of food and the like. The invention formally utilizes the characteristics of the anthocyanin and skillfully replaces the preservative which is required to be added in the conventional technology, and the replacement degree can be full replacement or partial replacement. The technical problem 2, namely the loss of nutrients during the production of the current preservative-free products due to process factors, is thus also solved. Meanwhile, the anthocyanin belongs to a bioflavonoid substance, so that the anthocyanin has very strong free radical scavenging capacity and oxidation resistance, wherein the oxidation resistance is 50 times higher than that of VE and 20 times higher than that of VC; the anthocyanin also has the functions of reducing enzyme activity, resisting variation and the like, and data show that the extract with a certain anthocyanin concentration can effectively prevent canceration at different stages; the anthocyanin has the effects of strengthening capillary vessels, improving blood circulation, preventing thrombosis, reducing arteriosclerosis occurrence frequency, deeply improving human facial skin, reducing excessive dependence of human on nutrient substances of a conventional mask, and reducing the problems of eye bags, dark yellow faces and the like caused by long-term dark eye circles and edema of the faces due to unsmooth blood microcirculation.
In order to effectively and comprehensively utilize the cowberry, the cowberry fruit can be used as a basic raw material, and waste cowberry peel and residue obtained after industrial treatment of the cowberry can also be used as the basic raw material, so that the social resource waste condition is reduced, the environmental pollution is reduced, the waste treatment intensity is reduced, and the comprehensive utilization rate of the cowberry is improved.
The seaweed is an alga growing in the sea, which contains not only common nutrient substances such as abundant amino acids, vitamins, proteins and mineral substances, but also active substances with special regulating functions such as phytohormone, polyphenol, oligosaccharide, polysaccharide, carbohydrate gum and the like. When the blueberry nutrient solution is used together with the blueberry, the blueberry nutrient solution and the blueberry can form a synergistic effect, and the nourishing effect of the original fixed and measured nutrient substances is effectively improved. The seaweed cultivation industry is developed in China, in addition, a large amount of algae are generated by seaweed tide, the seaweed is adopted as a basic raw material, the stable, high-quality and cheap resource supply is ensured, and the comprehensive utilization rate of the marine brown algae is improved.
According to the technical scheme 2 obtained by optimizing the technical scheme 1, the cowberry enzyme extract is prepared from cowberry fruit. The cowberry has a plurality of subspecies around the world, including more than 400 varieties such as vaccinium myrtillus, vaccinium americanum, siberian vaccinium myrtillus, ovular vaccinium myrtillus, blueberry and the like, wherein the vaccinium myrtillus produced by Sweden, Finland, Norway, Austria and Switzerland is better in anthocyanin content, and other nutrient substances are more suitable for the direct contact nutrition of the skin.
According to the technical scheme 3 obtained by optimizing the technical scheme 1, the plant extract further comprises one or more of aloe barbadensis leaf extract, green tea extract, ginseng radix extract, licorice extract, gherkin extract, cactus flower extract, oat extract and angelica sinensis extract.
The aloe vera leaf extract is one of aloe extracts, and is particularly suitable for being used in the fields of cosmetics, OTC medicines and the like. The main components include polysaccharides, anthraquinone compounds, proteins, vitamins, minerals, etc. Can comprehensively repair the damaged tissues of the human body, quickly eliminate various toxins in the human body, enhance the immunity of the organism, delay the aging of the skin, decompose fat, reduce the weight, whiten the skin and improve simple obesity.
The green tea extract contains tea polyphenols, has remarkable antioxidant, anti-inflammatory and anti-aging effects, and has effects of inhibiting tyrosinase and catalase activities which cause skin blackening, freckle, chloasma and senile plaque, and thus preventing dullness and whitening skin.
The main nutrient substance in the ginseng extract is eighteen ginseng monomer saponins, and has the effects of removing freckles, reducing wrinkles, activating skin cells and enhancing skin elasticity.
The extract of Cucumis sativus is rich in nutrients such as minerals, amino acids, glycoprotein, and tannin, which are easily absorbed by human body, and has softening, refreshing, astringing and moisturizing effects. The Chinese medicinal composition has the effects of clearing away heat and toxic materials, promoting blood circulation, whitening skin, reducing wrinkles and enhancing skin immunity, can repair the problems of whelks, acnes, eczema, wrinkles, scalds, freckles, senile plaques, rough skin and the like, and has a good heat-clearing effect on inflamed skin.
The licorice extract has whitening, sunscreen and antioxidant effects, and is mainly used for inhibiting the activity of tyrosinase and dopachrome tautomerase (TRP-2) and inhibiting the polymerization of 5, 6-dihydroxyindole (DHl), so as to prevent the formation of melanin. The molecular structure of the flavone compound has conjugation property, and the flavone compound has strong absorption to ultraviolet light and visible light and releases harmless low-energy rays.
The cactus flower extract has obvious bacteriostasis and antiphlogosis effects, and has inhibition effect on staphylococcus aureus, proteus, colibacillus, bacillus subtilis and bacillus cereus.
The oat extract is a whole plant extract of gramineous plant oat, mainly contains beta-glucan, flavonoid compounds and various antioxidant substances, has excellent anti-aging effect, can smooth fine wrinkles and improve skin texture, has obvious curative effect on allergic skin, can improve skin lubricity, relieves irritation of severe environment to the skin and pain and itch of the skin caused by eczema, and has excellent effect on treating senile skin.
The radix Angelicae sinensis extract has effects in dilating skin capillary, promoting blood circulation, and nourishing skin and preventing pachylosis due to abundant microelements.
The technical scheme 4 obtained by optimizing the technical scheme 1 is characterized in that the nutrient components further comprise one or more of allantoin, tocopherol and vitamin D.
Allantoin has physiological functions of promoting cell growth, accelerating wound healing, softening keratin and the like, is a good healing agent and anti-ulcer agent for skin wounds, and can be used for relieving and treating xeroderma, squamous skin diseases and skin ulcer. Has obvious effects on protecting skin tissues, being hydrophilic, absorbing water, preventing water from dispersing, promoting tissue growth and cell metabolism and softening cuticle protein.
The tocopherol is the hydrolysate of vitamin E, and the natural tocopherol is d-tocopherol (D-type), which has 8 isomers such as alpha, beta, gamma, delta and the like, wherein the activity of the alpha-tocopherol is strongest. Can increase cell antioxidation, maintain and promote reproductive function, has obvious anti-aging effect on skin, and can improve lipid metabolism of facial skin.
The vitamin D has obvious effect of promoting the growth of skin cells and has good effect of repairing facial skin injury.
In the technical scheme 5 obtained by optimizing the technical scheme 1, the solvent further comprises 1, 2-pentanediol.
The 1, 2-pentanediol has excellent moisturizing properties and can be used as a moisturizing agent of a facial mask. And has preservative effect to a certain extent, and has positive significance for preparing preservative-free or low-dose preservative products. Meanwhile, the 1, 2-pentanediol can dissolve part of the insoluble active ingredients, so that the composition can be used as a solvent of the facial mask.
Technical solution 6 obtained by optimizing technical solution 1, wherein the humectant is one or a combination of several selected from glycerin, propylene glycol, 1, 3-butylene glycol, sorbitol, polyethylene glycol, polysaccharides, sodium PCA, trehalose, sodium hyaluronate, amino acids, collagen, and aloe; the film forming agent is selected from one or a combination of more of polyvinyl alcohol, PVP, CMC, polyvinylpyrrolidone, pectin, gelatin and xanthan gum; the plasticizer is selected from one or a combination of more of polyethylene glycol, glycerol, propylene glycol and water-soluble lanolin; the volatility regulator is selected from ethanol and/or isopropanol; the preservative is selected from one or a combination of more of methyl hydroxybenzoate, diazolidinyl urea, phenoxyethanol, methylisothiazolinone, iodopropynyl butylcarbamate, propylhydroxybenzoate, DMDM hydantoin, methylchloroisothiazolinone, 2-bromo-2-nitropropane-1, 3-diol, imidazolidinyl urea, ethylparaben, potassium sorbate, benzyl alcohol, sodium benzoate, butanediol, octylglycol, phenethyl alcohol, sodium salicylate, chlorphenesin, methylparaben, deoxyacetic acid, ethylhexylglycerol, p-hydroxyphenyl esters, chlorphenesin, quaternary ammonium salt-15 and sodium dehydroacetate; the pH regulator is selected from one or more of triethanolamine, citric acid, potassium hydroxide, lactic acid, sodium hydroxide, sodium citrate, sodium lactate, arginine and glutamic acid; the essence is selected from natural essence and/or synthetic essence; the colorant is selected from inorganic pigment and/or natural pigment; the stabilizer comprises disodium EDTA; the viscosity regulator is selected from one or more of sodium alginate, carbomer, xanthan gum, hydroxyethyl cellulose and acrylic acid (ester);
technical scheme 7 obtained by optimizing any one of technical schemes 1 to 6 includes, in terms of weight percent: 4-30% of cowberry enzyme extract, 2-16% of brown algae whole extract, 1-8% of glycerol, 0-18% of aloe, 0-0.04% of trehalose, 0-0.6% of sodium hyaluronate, 0-0.01% of allantoin, 0-0.1% of xanthan gum, 0-0.9% of EDTA disodium, 0-0.05% of tocopherol, 0-0.6% of sodium PCA, 0-0.4% of sodium alginate, 0-0.05% of vitamin D0, 0-0.1% of 1, 2-pentanediol, 0-0.1% of citric acid, 0-0.06% of sodium lactate, 0-3% of sodium benzoate and the balance of water.
Technical scheme 8 obtained by optimizing technical scheme 7 includes, in weight percent: 4-10% of cowberry enzyme extract, 2-6% of brown algae whole extract, 1-8% of glycerol, 2-8% of aloe, 0.01-0.04% of trehalose, 0.2-0.6% of sodium hyaluronate, 0.001-0.01% of allantoin, 0.04-0.1% of xanthan gum, 0.1-0.9% of disodium EDTA, 0.01-0.05% of tocopherol, 0.1-0.6% of sodium PCA, 0.1-0.4% of sodium alginate, 0.01-0.05% of vitamin D, 0.01-0.1% of 1, 2-pentanediol, 0.01-0.1% of citric acid, 0.01-0.06% of sodium lactate, 0.1-3% of sodium benzoate and the balance of water.
Trehalose is also called rhaponticum and mycose, and is a non-reducing disaccharide composed of two glucose molecules. The structural formula is alpha-D-glucopyranosyl-alpha-D-glucopyranoside, often in the presence of dihydrate, the formula C12H22O11·2H2And O, a unique protective film can be formed on the cell surface under severe environmental conditions of high temperature, high cold, high osmotic pressure, drying and dehydration and the like, so that the biomolecular structure is effectively protected from being damaged. Has obvious effects of moisturizing, sun-screening and ultraviolet-proof when in use.
Sodium hyaluronate of the formula (C)14H20NO11Na)nIs an inherent component in the human body, is a glucuronic acid, and is free ofSpecies specificity, which is widely existed in tissues such as placenta, amniotic fluid, crystalline lens, articular cartilage, skin dermis and the like; it is distributed in cytoplasm and intercellular substance, and has lubricating and nourishing effects on cells and cell organs contained therein. The moisturizing effect of sodium hyaluronate in skin tissues is one of the most important physiological functions of sodium hyaluronate, and sufficient moisture can make skin smooth and fine. The highest moisture absorption at low relative humidity (33%) and the lowest moisture absorption at high relative humidity (75%) are suitable for the skin moisture retention requirements of cosmetics in different seasons and different ambient humidity, and have no greasy feeling and pore blocking feeling. Further, it is known that the skin moisture level is closely related to the hyaluronic acid content, and as the skin ages, the hyaluronic acid content decreases, so that the water retention function of the skin is weakened, thereby generating wrinkles. The sodium hyaluronate aqueous solution has strong viscoelasticity and lubricity, and can form a layer of moisture-preserving breathable film when being coated on the surface of skin, so that the skin is kept moist and bright. Meanwhile, the micromolecular hyaluronic acid can permeate into the dermis to promote blood microcirculation, is beneficial to the absorption of skin on nutrient substances, and plays a role in beautifying, resisting wrinkles and protecting health.
Xanthan gum (Xanthan gum), also known as Xanthan gum, is a microbial extracellular polysaccharide with wide action produced by fermentation engineering of Xanthomonas campestris (Xanthomonas campestris) with carbohydrate as main raw material. The molecules contain a large number of hydrophilic groups, are good surface active substances, and have the effects of resisting oxidation, preventing skin aging and the like.
Disodium EDTA, also known as disodium edetate, is a good complexing agent and stabilizer in chemistry, used to complex metal ions and separate metals.
Sodium PCA, also known as sodium pyrrolidone carboxylate, is a naturally occurring substance in the skin and is an amino acid derivative of formula C5H6O3NNa is soluble in water and ethanol, insoluble in oil, has strong hygroscopicity, is mainly used as a humectant in the field of facial masks, and has stronger moisturizing capability than glycerin, propylene glycol and sorbitol.
Sodium alginate is a byproduct after iodine and mannitol are extracted from brown algae such as kelp or gulfweed, the molecule of the sodium alginate is formed by connecting beta-D-mannuronic acid (beta-D-mannuronic acid, M) and alpha-L-guluronic acid (alpha-L-guluronic acid, G) according to a (1 → 4) bond, and the sodium alginate is a natural polysaccharide and has stability, solubility, viscosity and safety required by pharmaceutical preparation auxiliary materials. Effectively adjust the viscosity of the facial mask essence product.
Citric acid, also known as citric acid, having the molecular formula C6H8O7It is an important organic acid, colorless crystal, odorless, strongly sour and easily soluble in water. Not only has the function of adjusting the pH value of a component system, but also has a certain antiseptic function, thereby reducing the actual usage amount of other preservatives.
Sodium lactate having the molecular formula of C3H5O3And (4) Na. A colorless or nearly colorless transparent liquid with molecular weight of 112.06, which can be dissolved in water, ethanol, and glycerol. Mainly for adjusting the PH of the ingredient system.
Sodium benzoate, also known as sodium benzoate, of formula C7H5NaO2White granular or crystalline powder, odorless or slightly benzoin-smelling, slightly sweet taste, astringent taste, relative molecular mass of 144.12, stable in air, and easily soluble in water, wherein the pH of the aqueous solution is 8, and is soluble in ethanol. The sterilizing and bacteriostatic effects are enhanced along with the increase of the acidity of the medium, and the sterilizing and bacteriostatic effects are lost in an alkaline medium. The optimum pH value for corrosion prevention is 2.5-4.0.
By the composition formula related to the types and the contents of the components, the dosage of the preservative can be effectively reduced under the condition of efficiently nourishing the facial skin.
Technical scheme 9, a blueberry seaweed mask containing the composition mentioned in any one of the technical schemes is provided.
Compared with the prior art, the invention has the beneficial effects that:
1. the addition amount of the preservative can be effectively controlled by using the conventional simple mask manufacturing process.
2. The mask and the mask composition provided by the invention have more obvious effects of resisting oxidation and aging, replenishing water and moisturizing, and can effectively remove active oxygen free radicals, strengthen capillary vessels, moisturize and lock water and repair damaged cells.
3. The invention improves the utilization rate of raw materials such as cowberry peel residue, marine brown algae and the like, saves resources and reduces the production cost of the mask.
4. The mask provided by the invention is simple in production process, simple in equipment required by production, and suitable for large-scale industrial production.
Drawings
Fig. 1 is a data diagram of an instrumental skin test using a skin tester on a human subject before the mask of the present invention is used.
Fig. 2 is a data diagram of an instrumental skin test using a skin tester for a human subject after the mask of the present invention is applied.
Detailed Description
For further explanation, the present invention is provided so that those skilled in the art can clearly understand the gist of the present invention. It should be noted that the following embodiments are not intended to limit the technical solutions of the present invention, and those skilled in the art can analyze and understand the embodiments and make a series of modifications and equivalent substitutions on the technical solutions provided by the present invention in combination with the prior knowledge, and the new technical solutions obtained by the modifications and equivalent substitutions are also included in the present invention.
Since the present invention cannot be exhaustive, some preferred features and preferred embodiments may be reasonably replaced or combined with each other, and thus the new embodiments are also encompassed by the present invention.
For the reader to better understand the subject matter of the present invention, a series of experimental data are specifically exemplified. The reader should have the general technical knowledge in the field when reading to facilitate an accurate understanding of the logical relationships included in the data.
Example 1
The preparation method of the blueberry seaweed mask comprises the following steps:
(1) according to the weight percentage, 30 percent of wild bilberry enzyme extract, 2 percent of brown algae whole extract, 1 percent of glycerin, 2 percent of aloe juice, 0.01 percent of trehalose, 0.2 percent of sodium hyaluronate, 0.001 percent of allantoin, 0.04 percent of xanthan gum, 0.1 percent of EDTA disodium, 0.01 percent of tocopherol, 0.1 percent of sodium PCA, 0.1 percent of sodium alginate, 0.01 percent of vitamin D, 0.01 percent of 1, 2-pentanediol, 0.01 percent of citric acid, 0.01 percent of sodium lactate and the balance of water are prepared.
(2) Weighing and putting the glycerol, the sodium hyaluronate, the EDTA disodium, the PCA sodium, the ammonium alginate, the 1, 2-pentanediol, the citric acid and the sodium lactate according to the formula ratio into a pot, heating to 65 ℃ (the temperature is selected to be 60-70 ℃, 65 ℃ is selected in the embodiment 1), and stirring for dissolving; keeping the temperature for 30min (the temperature keeping time is 25-40 min, in this example 1 for 30min), slowly cooling to 30 ℃ (the temperature is 25-35 ℃, in this example 1 for 30 ℃), weighing trehalose, allantoin, xanthan gum, tocopherol, and vitamin D in the formula amount, slowly adding into a pot, and uniformly stirring for 15min (the stirring time is 10-30 min, in this example 1 for 15 min); weighing the wild bilberry enzyme extract, the brown algae whole-material extract and the aloe juice in the formula ratio, and stirring for 5min (the stirring time is selected to be 2-8 min, and the stirring time is selected to be 5min in the embodiment 1); folding the facial mask paper, putting the facial mask paper into a facial mask bag, injecting the prepared essence into the facial mask bag by using a clean injector, and then sealing the facial mask bag. Then, the packaged mask is placed in a 70 ℃ (the temperature range can be selected to be 65-75 ℃), in this embodiment 1, 70 ℃) water bath is kept for 30min (the time is selected to be 20-35 min, in this embodiment 1, 30min), and then is rapidly cooled to 4 ℃ (the temperature is selected to be 4-6 ℃, in this embodiment 1, 4 ℃).
Example 2
The preparation method of the blueberry seaweed mask comprises the following steps:
(1) according to weight percentage, preparing 4 percent of wild bilberry enzyme extract, 16 percent of brown algae whole extract, 1 percent of glycerin, 18 percent of aloe juice, 0.01 percent of trehalose, 0.2 percent of sodium hyaluronate, 0.001 percent of allantoin, 0.04 percent of xanthan gum, 0.1 percent of EDTA disodium, 0.01 percent of tocopherol, 0.1 percent of sodium PCA, 0.1 percent of sodium alginate, 0.01 percent of vitamin D, 0.01 percent of 1, 2-pentanediol, 0.01 percent of citric acid, 0.01 percent of sodium lactate, 3 percent of sodium benzoate and the balance of water.
(2) Weighing and putting the glycerol, the sodium hyaluronate, the sodium benzoate, the EDTA disodium, the PCA sodium, the ammonium alginate, the 1, 2-pentanediol, the citric acid and the sodium lactate according to the formula ratio into a pot, heating to 60 ℃, and stirring for dissolving; keeping the temperature for 40min, slowly cooling to 35 deg.C, slowly adding trehalose, allantoin, xanthan gum, tocopherol, and vitamin D in formula amount into the pan, and stirring at constant speed for 30 min; weighing wild Vaccinium myrtillus enzyme extract, brown algae whole-material extract and Aloe juice in formula amount, adding and stirring for 8 min; folding the facial mask paper, putting the facial mask paper into a facial mask bag, injecting the prepared essence into the facial mask bag by using a clean injector, and then sealing the facial mask bag. Then placing the packaged facial mask in 65 deg.C water bath kettle, maintaining for 35min, and rapidly cooling to 5 deg.C.
Example 3
The preparation method of the blueberry seaweed mask comprises the following steps:
(1) according to weight percentage, 6 percent of wild bilberry enzyme extract, 3 percent of brown algae whole extract, 2 percent of glycerol, 3 percent of aloe juice, 0.02 percent of trehalose, 0.3 percent of sodium hyaluronate, 0.004 percent of allantoin, 0.06 percent of xanthan gum, 0.3 percent of EDTA disodium, 0.03 percent of tocopherol, 0.2 percent of sodium PCA, 0.1 percent of sodium alginate, 0.03 percent of vitamin D, 0.05 percent of 1, 2-pentanediol, 0.02 percent of citric acid, 0.02 percent of sodium lactate, 1 percent of sodium benzoate and the balance of water are prepared.
(2) Weighing and putting the glycerol, the sodium hyaluronate, the sodium benzoate, the EDTA disodium, the PCA sodium, the ammonium alginate, the 1, 2-pentanediol, the citric acid and the sodium lactate according to the formula ratio into a pot, heating to 70 ℃, and stirring for dissolving; keeping the temperature for 25min, slowly cooling to 25 deg.C, slowly adding trehalose, allantoin, xanthan gum, tocopherol, and vitamin D in formula amount into the pan, and stirring at constant speed for 10 min; weighing wild Vaccinium myrtillus enzyme extract, brown algae whole-material extract and Aloe juice in formula amount, adding and stirring for 4 min; folding the facial mask paper, putting the facial mask paper into a facial mask bag, injecting the prepared essence into the facial mask bag by using a clean injector, and then sealing the facial mask bag. Then placing the packaged facial mask in 75 deg.C water bath, maintaining for 20min, and rapidly cooling to 6 deg.C.
Example 4
The preparation method of the blueberry seaweed mask comprises the following steps:
(1) according to weight percentage, 8 percent of wild bilberry enzyme extract, 4 percent of brown algae whole extract, 6 percent of glycerin, 5 percent of aloe juice, 0.03 percent of trehalose, 0.2 percent of sodium hyaluronate, 0.001 percent of allantoin, 0.04 percent of xanthan gum, 0.1 percent of EDTA disodium, 0.01 percent of tocopherol, 0.1 percent of sodium PCA, 0.1 percent of sodium alginate, 0.01 percent of vitamin D, 0.01 percent of 1, 2-pentanediol, 0.01 percent of citric acid, 0.01 percent of sodium lactate, 3 percent of sodium benzoate and the balance of water are prepared.
(2) Weighing and putting the glycerol, the sodium hyaluronate, the sodium benzoate, the EDTA disodium, the PCA sodium, the ammonium alginate, the 1, 2-pentanediol, the citric acid and the sodium lactate according to the formula ratio into a pot, heating to 60 ℃, and stirring for dissolving; keeping the temperature for 40min, slowly cooling to 35 deg.C, slowly adding trehalose, allantoin, xanthan gum, tocopherol, and vitamin D in formula amount into the pan, and stirring at constant speed for 30 min; weighing wild Vaccinium myrtillus enzyme extract, brown algae whole-material extract and Aloe juice in formula amount, adding and stirring for 8 min; folding the facial mask paper, putting the facial mask paper into a facial mask bag, injecting the prepared essence into the facial mask bag by using a clean injector, and then sealing the facial mask bag. Then placing the packaged facial mask in 65 deg.C water bath kettle, maintaining for 35min, and rapidly cooling to 5 deg.C.
Example 5
The preparation method of the blueberry seaweed mask comprises the following steps:
(1) according to weight percentage, 10 percent of wild bilberry enzyme extract, 6 percent of brown algae whole extract, 8 percent of glycerin, 8 percent of aloe juice, 0.04 percent of trehalose, 0.6 percent of sodium hyaluronate, 0.01 percent of allantoin, 0.1 percent of xanthan gum, 0.9 percent of EDTA disodium, 0.05 percent of tocopherol, 0.6 percent of sodium PCA, 0.4 percent of sodium alginate, 0.05 percent of vitamin D, 0.1 percent of 1, 2-pentanediol, 0.1 percent of citric acid, 0.06 percent of sodium lactate, 0.1 percent of sodium benzoate and the balance of water are prepared.
(2) Weighing and putting the glycerol, the sodium hyaluronate, the sodium benzoate, the EDTA disodium, the PCA sodium, the ammonium alginate, the 1, 2-pentanediol, the citric acid and the sodium lactate according to the formula ratio into a pot, heating to 65 ℃, and stirring for dissolving; keeping the temperature for 30min, slowly cooling to 30 deg.C, slowly adding trehalose, allantoin, xanthan gum, tocopherol, and vitamin D in formula amount into the pan, and stirring at constant speed for 15 min; weighing wild Vaccinium myrtillus enzyme extract, brown algae whole-material extract and Aloe juice in formula amount, adding and stirring for 5 min; folding the facial mask paper, putting the facial mask paper into a facial mask bag, injecting the prepared essence into the facial mask bag by using a clean injector, and then sealing the facial mask bag. Then placing the packaged facial mask in 70 deg.C water bath kettle, maintaining for 35min, and rapidly cooling to 6 deg.C.
In the above-mentioned embodiments 1 to 5,
the bilberry enzyme extract is prepared by the following steps:
selecting wild Vaccinium myrtillus peel residue, and removing impurities. The lemons were washed with sterile water (sterilized with 1% sodium hypochlorite for 2min) and cut into uniform slices for use. Mixing white sugar, cowberry peel residue and water at a ratio of 1:8:10, and adding small amount of fresh cowberry fruit. Activating strains (Bifidobacterium, Lactobacillus casei, and Lactobacillus plantarum) with 5% sucrose solution at 37 deg.C for 30min, inoculating 1%, mixing with the raw materials, and placing into a fermentation tank. A layer of lemon is placed in the middle and on the top of the mixture. And sealing the tank body, placing the tank body in a shade place, fermenting at the room temperature of 25-30 ℃, ventilating once every 3d in a sterile operating platform, and standing and fermenting for 15 d. And observing the color and the state of the fermentation liquor every 3 days and recording in real time until no gas is generated and the pH value is 2-4, namely stopping fermentation. Filtering the obtained ferment liquid, and centrifuging at 8000rpm for 15min to obtain wild Vaccinium myrtillus ferment extract.
The brown algae full-quality extract is prepared by the following steps:
selecting and cleaning brown algae, and removing impurities; mixing brown algae and water according to a weight ratio of 2:3, soaking at room temperature for 48h, transferring to a pot, heating and boiling for 1h, and filtering to obtain a filtrate; decolorizing the filtrate, and concentrating according to the volume ratio of 95:1 to obtain the brown algae full-quality extract.
Sensory evaluation was performed on the masks obtained in examples 1 to 5, and the evaluation criteria were as follows: 50 people in different age groups are selected as members of the appraisal group, other conditions are guaranteed to be the same, sensory scoring is carried out, the total score is 10, 4 grades are good, good and acceptable. The corresponding case of scores and grades is: not less than 8 is preferred; <8 > and ≧ 6 are preferred; <6, > 5 is acceptable; <5 was completely unacceptable. There were 4 indices evaluated: the odor, viscosity, color and comfort level experience is respectively 20%, 25%, 10% and 45%. And taking the average score of the scores of each index testee, wherein the weighted scores of all the indexes are the sensory scores. The sensory evaluation is shown in Table 1.
| Index (I) | Score value |
| Smell(s) | 8 |
| Viscosity of the oil | 9 |
| |
10 |
| Comfort experience | 9 |
| Evaluation of Total points | 8.9 |
The skin tester is used for performing instrument skin test on a human subject, data test is respectively performed on the forehead, the eyes and the cheek before and after the wild vaccinium myrtillus seaweed mask is used, the test indexes comprise three aspects of elasticity, oil content and moisture, and the test results are respectively shown in a table 1 and a table 2.
As can be seen from the sensory test data of the mask, the evaluation of the tested population is 8.9 points, which is good for the mask grade condition. The data tested by using a skin tester show that the indexes of elasticity, moisture and oil content of the face before and after the face mask is used have obvious changes, wherein the elasticity coefficient and the moisture coefficient of the skin of the face mask after the face mask is used are obviously increased, and the oil content coefficient of the skin of the face after the face mask is used is greatly reduced, so that the experience effect of the face skin of a human subject after the face mask is used is obvious.
Claims (10)
1. A composition for preparing cowberry seaweed facial mask comprises nutritional components, additives and solvent; wherein,
the additive comprises one or more of a humectant, a film forming agent, a plasticizer, a volatile regulator, a preservative, a pH regulator, essence, a coloring agent, a stabilizer and a viscosity regulator;
the solvent comprises water;
the nutrient components comprise plant extracts;
the plant extract is characterized by comprising a cowberry ferment extract and a brown algae whole substance extract.
2. The composition for preparing a blueberry seaweed mask as claimed in claim 1, wherein the blueberry enzyme extract is prepared from vaccinium myrtillus.
3. The composition for preparing the blueberry seaweed mask as claimed in claim 1, wherein the plant extract further comprises one or more of aloe barbadensis leaf extract, green tea extract, ginseng extract, licorice extract, gherkin extract, cactus flower extract, oat extract, and angelica sinensis extract.
4. The composition for preparing the mask of blueberry seaweed as claimed in claim 1, wherein the nutrient components further comprise one or more of allantoin, tocopherol and vitamin D.
5. The composition for preparing a blueberry seaweed mask as set forth in claim 1, wherein the solvent further comprises 1, 2-pentanediol.
6. The composition for preparing the blueberry seaweed mask as claimed in claim 1, wherein the moisturizer is one or more selected from the group consisting of glycerin, propylene glycol, 1, 3-butylene glycol, sorbitol, polyethylene glycol, polysaccharides, sodium PCA, trehalose, sodium hyaluronate, amino acids, collagen, and aloe;
the film forming agent is selected from one or a combination of more of polyvinyl alcohol, PVP, CMC, polyvinylpyrrolidone, pectin, gelatin and xanthan gum;
the plasticizer is selected from one or a combination of more of polyethylene glycol, glycerol, propylene glycol and water-soluble lanolin;
the volatility regulator is selected from ethanol and/or isopropanol;
the preservative is selected from one or a combination of more of methyl hydroxybenzoate, diazolidinyl urea, phenoxyethanol, methylisothiazolinone, iodopropynyl butylcarbamate, propylhydroxybenzoate, DMDM hydantoin, methylchloroisothiazolinone, 2-bromo-2-nitropropane-1, 3-diol, imidazolidinyl urea, ethylparaben, potassium sorbate, benzyl alcohol, sodium benzoate, butanediol, octylglycol, phenethyl alcohol, sodium salicylate, chlorphenesin, methylparaben, deoxyacetic acid, ethylhexylglycerol, p-hydroxyphenyl esters, chlorphenesin, quaternary ammonium salt-15 and sodium dehydroacetate;
the pH regulator is selected from one or more of triethanolamine, citric acid, potassium hydroxide, lactic acid, sodium hydroxide, sodium citrate, sodium lactate, arginine and glutamic acid;
the essence is selected from natural essence and/or synthetic essence;
the colorant is selected from inorganic pigment and/or natural pigment;
the stabilizer comprises disodium EDTA;
the viscosity regulator is selected from one or more of sodium alginate, carbomer, xanthan gum, hydroxyethyl cellulose and acrylic acid (ester).
7. The composition for preparing the blueberry seaweed mask as set forth in any one of claims 1 to 6, which comprises the following components in percentage by weight: 4-30% of cowberry enzyme extract, 2-16% of brown algae whole extract, 1-8% of glycerol, 0-18% of aloe, 0-0.04% of trehalose, 0-0.6% of sodium hyaluronate, 0-0.01% of allantoin, 0-0.1% of xanthan gum, 0-0.9% of disodium EDTA, 0-0.05% of tocopherol, 0-0.6% of sodium PCA, 0-0.4% of sodium alginate, 0-0.05% of vitamin D, 0-0.1% of 1, 2-pentanediol, 0-0.1% of citric acid, 0-0.06% of sodium lactate, 0-3% of sodium benzoate and the balance of water.
8. The composition for preparing a blueberry seaweed mask as set forth in claim 7, which comprises, in weight percent: 4 to 10 percent of cowberry enzyme extract, 2 to 6 percent of brown algae whole extract, 1 to 8 percent of glycerol, 2 to 8 percent of aloe, 0.01 to 0.04 percent of trehalose, 0.2 to 0.6 percent of sodium hyaluronate, 0.001 to 0.01 percent of allantoin, 0.04 to 0.1 percent of xanthan gum, 0.1 to 0.9 percent of disodium EDTA, 0.01 to 0.05 percent of tocopherol, 0.1 to 0.6 percent of sodium PCA, 0.1 to 0.4 percent of sodium alginate, 0.01 to 0.05 percent of vitamin D, 0.01 to 0.1 percent of 1, 2-pentanediol, 0.01 to 0.1 percent of citric acid, 0.01 to 0.06 percent of sodium lactate, 0.1 to 3 percent of sodium benzoate and the balance of water.
9. A blueberry seaweed mask comprising the composition of any one of claims 1 to 8.
10. The method for preparing the blueberry seaweed mask as claimed in claim 9, wherein the composition for preparing the blueberry seaweed mask is attached to a mask paper and then packaged to obtain the blueberry seaweed mask.
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Application publication date: 20211214 |