CN109106613B - Preparation method of mask containing moringa oil and hawthorn polysaccharide - Google Patents

Preparation method of mask containing moringa oil and hawthorn polysaccharide Download PDF

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Publication number
CN109106613B
CN109106613B CN201811216133.7A CN201811216133A CN109106613B CN 109106613 B CN109106613 B CN 109106613B CN 201811216133 A CN201811216133 A CN 201811216133A CN 109106613 B CN109106613 B CN 109106613B
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parts
oil
polysaccharide
hawthorn
semi
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Expired - Fee Related
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CN201811216133.7A
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CN109106613A (en
Inventor
熊华斌
高定烽
张言
李思敏
石峰
高云涛
李晓芬
杨志
胡成婷
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Yunnan Minzu University
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Yunnan Minzu University
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/02Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/04Dispersions; Emulsions
    • A61K8/042Gels
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • A61K8/735Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9706Algae
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9794Liliopsida [monocotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/08Anti-ageing preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions
    • A61K2800/5922At least two compounds being classified in the same subclass of A61K8/18

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  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Veterinary Medicine (AREA)
  • Public Health (AREA)
  • Animal Behavior & Ethology (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Engineering & Computer Science (AREA)
  • Biotechnology (AREA)
  • Mycology (AREA)
  • Microbiology (AREA)
  • Botany (AREA)
  • Dermatology (AREA)
  • Chemical & Material Sciences (AREA)
  • Gerontology & Geriatric Medicine (AREA)
  • Dispersion Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Cosmetics (AREA)
  • Medicines Containing Plant Substances (AREA)

Abstract

The invention relates to a preparation method of a mask containing moringa oil and hawthorn polysaccharide, which is characterized in that 10-15 parts of hawthorn polysaccharide, 5-10 parts of seaweed extract, 5-10 parts of aloe extract, 5-10 parts of moringa oil, 2-5 parts of sodium hyaluronate, 1-3 parts of prinsepia utilis royle oil, 1-3 parts of rose hip oil, 3-7 parts of glycerin monostearate, 1-4 parts of carbomer, 3-5 parts of shea butter, 1-3 parts of lavender essential oil, 3-6 parts of sodium cocoyl sulfate, 0.2-1 part of preservative, a proper amount of distilled water and other raw materials are matched to prepare the spreadable gel mask, and the mask has the effects of moisturizing, oxidation resistance and the like on skin.

Description

Preparation method of mask containing moringa oil and hawthorn polysaccharide
Technical Field
The invention belongs to the technical field of skin care products, and particularly relates to a preparation method of a smearing type gel mask containing moringa oil and hawthorn polysaccharide.
Background
The skin is natural coat of people, particularly the facial skin, the basic requirement of facial skin care is to keep healthy and beautiful, the personal confidence can be increased, the charm of people can be improved, and the daily facial mask becomes the most basic facial care tool. At present, in the traditional facial masks in the market, non-woven fabrics, silks, cottons and the like are often used as the materials of the patch type facial mask, and the materials are essentially soaked in essence, so that the effects of moisturizing, whitening and nourishing and repairing facial skin are achieved; however, the patch type mask has obvious defects that the deep cleaning effect on the skin is poor, the attachment degree of the patch type mask is high, pressure is easily caused on the skin, and if the time for pasting the mask is too long, the skin is easily stuffy and slightly itchy. The smearing type facial mask can well clean the skin, is more free to use, can adjust the using amount according to the requirements of users, and is very convenient for regional nursing.
Moringa oleifera oil, also called ' native oil ' or ' Bei ' on oil ', is a non-drying oil with light yellow color extracted from seeds of Moringa oleifera, compared with other vegetable oil, the Moringa oleifera oil has excellent inoxidizability, does not need to add any synergist or preservative in the storage process, can be stored for about 1 year at normal temperature without deterioration, rancidity or rancidity, and has the effects of sterilization, ultraviolet resistance, skin moistening, hair nourishing, moisture preservation and the like in cosmetics.
The hawthorn polysaccharide applied to the cosmetics has the advantages that the hawthorn polysaccharide can rapidly enter the skin to replenish water and enter subcutaneous capillaries, the blood circulation of the skin capillaries is promoted, the metabolism of skin cells is accelerated, and particularly, in an extracellular matrix, the polysaccharide, other polysaccharide components in the skin and fibrous protein jointly form an extracellular colloidal matrix containing a large amount of water so as to provide water for the skin; the existing research shows that the hawthorn polysaccharide has the efficacy of removing free radicals of human bodies, and has small toxic and side effects and high safety performance.
The moringa oil and the hawthorn polysaccharide are combined in the mask, so that respective efficacy characteristics can be effectively exerted, the complementary advantages are achieved, the antioxidation of the moringa oil can protect and repair the skin of a human body when the moringa oil and the hawthorn polysaccharide are combined, the hawthorn polysaccharide can achieve the functions of moisturizing, stabilizing, improving the skin color, resisting aging and the like, and the high molecular polysaccharide has no toxic or side effect.
Disclosure of Invention
The invention aims to provide a gel type mask containing moringa oil and hawthorn polysaccharide, which can supplement water, preserve moisture, balance grease, improve the oxidation resistance of skin, enhance the immunity of skin and slow down the aging of skin.
A mask preparation containing moringa oil and hawthorn polysaccharide comprises the following raw materials in parts by weight: 10-15 parts of hawthorn polysaccharide, 5-10 parts of seaweed extract, 5-10 parts of aloe extract, 5-10 parts of moringa oil, 2-5 parts of glycerol, 2-5 parts of sodium hyaluronate, 1-3 parts of prinsepia utilis royle oil, 1-3 parts of rosehip oil, 3-7 parts of glyceryl monostearate, 1-4 parts of carbomer, 1-4 parts of xanthan gum, 3-5 parts of shea butter, 1-3 parts of lavender essential oil, 3-6 parts of sodium coco oil sulfate, 2 parts of disodium lauryl alcohol sulfosuccinate, 0.2-1 part of preservative and a proper amount of distilled water.
A preparation method of a mask containing moringa oil and hawthorn polysaccharide comprises the following steps:
(1) feeding shea butter, glycerol, glyceryl monostearate, sodium cocoyl sulfate and distilled water in a predetermined weight ratio into a homogenizing and emulsifying machine for homogenizing and emulsifying for 10-14h, and mixing and emulsifying to obtain a semi-finished product for later use;
(2) adding the hawthorn polysaccharide, the seaweed extract, the aloe extract, the moringa oil, the glycerol, the sodium hyaluronate and the rose fruit oil in a predetermined weight ratio into a semi-finished product after a homogeneous emulsification reaction, heating and uniformly mixing the mixture through a heating and stirring tank at 50-80 ℃, naturally cooling the mixture to below 50 ℃, adding the preservative, uniformly stirring the mixture at the speed of 1000 plus materials and 1200r/min, and completely naturally cooling the mixture to obtain the gelatinous mask containing the moringa oil and the hawthorn polysaccharide.
The invention has the following beneficial effects:
the hawthorn polysaccharide is natural plant polysaccharide, is a high molecular polyhydroxy polymer, molecular chains of the polysaccharide are interwoven into a net shape, and polar groups are combined with hydrogen bonds of water to play a strong water retention role. In addition, due to the combination of the hawthorn polysaccharide and the moringa oil, compared with a pure moisturizing smearing type mask on the market, the oil essence on the inner side can better keep moisture for the skin, and the sebum layer is repaired and protected. In the whole process of preparing the mask of the moringa oil and the hawthorn polysaccharide, the extraction method of the hawthorn polysaccharide is simple, efficient, easy to operate and environment-friendly.
Detailed Description
In order to better understand the present invention, the following examples are further provided to illustrate the present invention, but the present invention is not limited to the following examples.
The invention discloses a preparation method of a mask containing moringa oil and hawthorn polysaccharide, which accurately weighs various raw materials according to the following proportion: 12 parts of hawthorn polysaccharide, 7 parts of aloe extract, 5 parts of moringa oil, 2 parts of glycerol, 3 parts of sodium hyaluronate, 1 part of rose hip oil, 4 parts of carbomer, 4 parts of shea butter, 3 parts of sodium coco oil sulfate, 2 parts of disodium lauryl sulfosuccinate, 0.6 part of phenoxyethanol and 30 parts of distilled water.
Extracting the hawthorn crude polysaccharide: accurately weighing 50g of fresh hawthorn, cleaning, slicing, freeze-drying, crushing by using a crusher, sieving by using a 60-mesh sieve, and placing into a constant-temperature water bath kettle, wherein the extraction process comprises the following steps: the water bath temperature is 70 ℃, and the material-liquid ratio is 1: 40. extracting for 150min, naturally cooling after leaching, centrifuging for 10min at 5000r/min, taking the filtrate, concentrating to 1/5 of the original volume, adding 3 times of ethanol for precipitation, standing overnight, centrifuging again to obtain crude polysaccharide, freeze-drying at low temperature to obtain the hawthorn polysaccharide, crushing by using a crusher again, sieving with a 100-mesh sieve, and adding deionized water to 70 ℃ to completely dissolve the hawthorn polysaccharide.
2 parts of glycerol, 3 parts of sodium cocoanut oil alcohol sulfate, 2 parts of disodium lauryl sulfosuccinate and 30 parts of distilled water in a predetermined weight ratio are sent to a homogenizing and emulsifying machine for homogenizing and emulsifying for 10-14h, and the mixture is emulsified into a semi-finished product for standby;
12 parts of hawthorn polysaccharide, 7 parts of aloe extract, 5 parts of moringa oil, 3 parts of sodium hyaluronate, 1 part of rose oil, 4 parts of carbomer, 4 parts of shea butter and 0.6 part of phenoxyethanol in a predetermined weight ratio are added into the homogenized and emulsified semi-finished product obtained in the previous step, the semi-finished product is heated in a heating and stirring tank at 50-80 ℃, the semi-finished product is uniformly stirred at the speed of 1000 plus materials and 1200r/min, and after the semi-finished product is completely and naturally cooled, the gelatinous mask containing the moringa oil and the hawthorn polysaccharide is obtained.
Testing water replenishing and moisture preserving performance: searching a 23-year-old female volunteer, cleaning the inner side of the arm of the female volunteer before testing, marking the inner side of the arm, wherein the interval of each testing area is 1cm, and each testing area is 5cm by 5 cm; on the test day, the test subject sits still in a room temperature environment for 30min without any skin care product, then the moisture value of the test area is measured by using a capacitance method skin moisture meter (SG-5D), the content of collagen fiber and the elasticity index of the skin are measured by using a 200 ten thousand pixel CCD50X portable high-definition intelligent skin detector (EH-800U), and the data are recorded. Uniformly coating the mask containing the moringa oil and the hawthorn polysaccharide in an arm test area, wherein the coating thickness is about 0.2-1.0nm, observing and measuring the tested area after 30min, and parallelly measuring for 3 times to obtain the average value of the moisture, collagen and fiber contents of the tested object, continuously measuring the tested area for one week, coating the tested area for 30min under the same condition every day, and observing and measuring.
The results showed that after six consecutive days, the average moisture content of the inner arm of the subject increased by 26.2%, 25.7% and 26.5%, the collagen fiber content increased by 52.2%, 51.8% and 52.4%, and the elasticity increased by 13.8%, 14.2% and 14.3%, respectively.
The above description is only for the purpose of illustrating the preferred embodiments of the present invention and is not to be construed as limiting the invention, and any modifications, equivalents, improvements and the like that fall within the spirit and principle of the present invention are intended to be included therein.

Claims (1)

1. A preparation method of a mask containing moringa oil and hawthorn polysaccharide is characterized by comprising the following steps:
(1) accurately weighing the following raw materials in parts by weight: 10-15 parts of hawthorn polysaccharide, 5-10 parts of seaweed extract, 5-10 parts of aloe extract, 5-10 parts of moringa oil, 2-5 parts of glycerol, 2-5 parts of sodium hyaluronate, 1-3 parts of prinsepia utilis royle oil, 1-3 parts of rosehip oil, 3-7 parts of glyceryl monostearate, 1-4 parts of carbomer, 1-4 parts of xanthan gum, 3-5 parts of shea butter, 1-3 parts of lavender essential oil, 3-6 parts of sodium cocoalcohol sulfate, 0.2-1 part of preservative and a proper amount of distilled water; the preservative is one or a combination of more of cason, nipagin ester, phenoxyethanol, sodium benzoate, potassium sorbate, iodopropynyl butyl carbamate, benzoic acid and benzyl alcohol, and the content of the preservative is 0.2-1 part of the weight of the whole mask;
(2) feeding shea butter, glycerol, glyceryl monostearate, sodium cocoyl sulfate and distilled water in a predetermined weight ratio into a homogenizing and emulsifying machine for homogenizing and emulsifying for 10-14h, and mixing and emulsifying to obtain a semi-finished product for later use;
(3) and (3) adding hawthorn polysaccharide, moringa oil, seaweed extract, aloe extract, glycerol, sodium hyaluronate, rose hip oil and preservative in a predetermined weight ratio into the semi-finished product obtained in the step (2) after the homogeneous emulsification reaction, heating the semi-finished product in a heating and stirring tank at 50-80 ℃, uniformly stirring the semi-finished product at the speed of 1000-1200r/min, and completely and naturally cooling the semi-finished product to obtain the gelatinous mask containing the moringa oil and the hawthorn polysaccharide.
CN201811216133.7A 2018-10-18 2018-10-18 Preparation method of mask containing moringa oil and hawthorn polysaccharide Expired - Fee Related CN109106613B (en)

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111374927B (en) * 2020-04-03 2022-09-06 广州环亚化妆品科技股份有限公司 Stick-shaped facial mask and preparation method thereof

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR101558967B1 (en) * 2015-04-21 2015-10-12 신영미 Facial mask pack
CN106265456A (en) * 2016-09-30 2017-01-04 中国热带农业科学院农产品加工研究所 A kind of Moringa facial film and preparation method thereof
CN107260576A (en) * 2017-05-16 2017-10-20 浙江金石生物科技有限公司 A kind of facial mask congealed fat containing Dendrobium officinale polysaccharide body and preparation method thereof
CN108186679A (en) * 2018-02-07 2018-06-22 中国科学院化学研究所 A kind of acne-removing composition

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR101558967B1 (en) * 2015-04-21 2015-10-12 신영미 Facial mask pack
CN106265456A (en) * 2016-09-30 2017-01-04 中国热带农业科学院农产品加工研究所 A kind of Moringa facial film and preparation method thereof
CN107260576A (en) * 2017-05-16 2017-10-20 浙江金石生物科技有限公司 A kind of facial mask congealed fat containing Dendrobium officinale polysaccharide body and preparation method thereof
CN108186679A (en) * 2018-02-07 2018-06-22 中国科学院化学研究所 A kind of acne-removing composition

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
邓旭坤 等.山楂多糖的成分测定及其单糖组分分析研究.《中南民族大学学报(自然科学版)》.2017,第36卷(第3期),第52-56页. *
郑朋朋 等.山楂多糖的提取及其抗氧化性作用.《中国酿造》.2015,第34卷(第6期),第107-113页. *

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