CN105395443A - Anti-aging eye cream and preparation method thereof - Google Patents
Anti-aging eye cream and preparation method thereof Download PDFInfo
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- CN105395443A CN105395443A CN201510799141.9A CN201510799141A CN105395443A CN 105395443 A CN105395443 A CN 105395443A CN 201510799141 A CN201510799141 A CN 201510799141A CN 105395443 A CN105395443 A CN 105395443A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
- A61K8/988—Honey; Royal jelly, Propolis
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/005—Preparations for sensitive skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
Abstract
The invention belongs to the technical field of cosmetics and particularly relates to anti-aging eye cream and a preparation method thereof. The anti-aging eye cream is prepared from glycerol, propylene glycol, hyaluronic acid, polydimethylsiloxane, palmitic acid ethyl ester, C20-22 alcohol phosphate, methylparaben, polyacrylamide, horseradish tree leaf extract, ginkgo leaf extract, mulberry leaf extract, purslane extract, honey, butyrospermum parkii butter, triethanolamine and the like. The anti-aging eye cream is good in permeability and easy to absorb, pigment deposition is reduced, dark circles are relieved, eye bags are eliminated, the elasticity of the skin around the eyes is enhanced, dryness and looseness phenomena are relieved, damaged or in-nutritive cells are restored, skin aging is obviously delayed, the skin around the eyes are restored to be full and mellow, and the bright and lustrous eyes are regained.
Description
Technical field
The present invention relates to cosmetic technical field, be specifically related to a kind of defying age eye cream and preparation method thereof.
Background technology
Skin aging is the outstanding behaviours of whole body aging, wherein facial skin is aging particularly evident, in human body, fibroblastic quantity reduces gradually, the collagen protein of its secretion and elastic fibers albumen are also because oxidizedly to reduce gradually, rupture, just disappear to the supporting role of epidermis, cause inhomogenous subsiding, skin corium starts thinning, skin elasticity is deteriorated, and wrinkle also starts to produce gradually.Eye skin is the thinnest skin of human body, is again activity position the most frequently simultaneously, but also is pull the maximum place of skin number of times in making up, and is very easy to grow wrinkle, and is just difficult to eliminate once grow.
Eye cream, one of skin type cosmetic product, be used to the skin protecting around eyes thinner, it has moist effect, has certain effect to eye pouch, black eye, crows-feet, dry stricture of vagina, microgroove etc.Eye cream product has much in the market, but ubiquity poor permeability, not easily absorbs, the problems such as result of use is not obvious, and meanwhile, the skin of eye is very careful and fragile, easily comes to harm, and therefore, eye cream needs gentleness, do not stimulate, hypoallergenic.Chinese patent CN102552065B discloses a kind of carboxymethyl yeast dextran eye cream, it comprises the mixture of water, cetearyl alcohol and C12 ~ 20 alkyl androstanediol, PEG-20 methyl sesquistearate, caprylic/capric triglyceride, squalane, polydimethylsiloxane, Cyclomethicone, mass percentage concentration are 1% carboxymethyl yeast dextran pure water solution, propylene glycol, xanthan gum, carbomer, hydroxyethyl-cellulose, pantothenylol, methyl hydroxybenzoate, EDETATE SODIUM, triethanolamine, essence and phenoxyethanol.But along with growth in the living standard, people are more and more higher for the diversified requirement of cosmetics, also more and more higher to the quality requirements of cosmetics, need the new product providing multiple high-quality.
Summary of the invention
In order to overcome the deficiencies in the prior art, the object of the present invention is to provide a kind of defying age eye cream, it nourishes composition containing multiple natural extract, effectively can infiltrate dermal tissue, improve the collagen structure of skin corium more fast, reduce pigmentation, alleviate black eye, strengthen skin around the eyes elastic force and improve drying, relaxation, repair impaired or innutritive cell, obvious continuity skin aging, makes skin around the eyes recover plentiful and mellow and full, regains bright two pupil of beautiful gloss.
To achieve these goals, technical scheme of the present invention is as follows:
A kind of defying age eye cream, comprises the component of following weight percent meter: glycerol 4 ~ 10%, propylene glycol 2 ~ 8%, hyaluronic acid 4 ~ 8%, polydimethylsiloxane 0.4 ~ 2%, ethylhexyl palmitate 2 ~ 6%, C20-22 alcohol phosphate ester 1 ~ 4%, methyl hydroxybenzoate 0.5 ~ 2%, polyacrylamide 0.5 ~ 2%, moringa oleifera leaf extractive 2 ~ 8%, Folium Ginkgo extract 4 ~ 8%, Folium Mori extract 2 ~ 6%, Herba portulacae extract 2 ~ 4%, Mel 0.4 ~ 2%, Butyrospermum parkii fruit fat 1 ~ 4%, triethanolamine 0.4 ~ 2%, essence 0.002 ~ 0.04% and water 40 ~ 65%.
As the preferred embodiment of the present invention, described defying age eye cream is made up of the component of following weight percent meter: glycerol 4%, propylene glycol 2%, hyaluronic acid 8%, polydimethylsiloxane 1%, ethylhexyl palmitate 2%, C20-22 alcohol phosphate ester 2%, methyl hydroxybenzoate 1%, polyacrylamide 1%, moringa oleifera leaf extractive 4%, Folium Ginkgo extract 6%, Folium Mori extract 4%, Herba portulacae extract 2%, Mel 0.8%, Butyrospermum parkii fruit fat 2%, triethanolamine 0.8%, essence 0.01%, surplus is water.
In technical solution of the present invention, described moringa oleifera leaf extractive is rich in several mineral materials, vitamin, aminoacid, antioxygen element, and its non-oxidizability is strong, effectively eliminates free radical, enhances metabolism, and desalination mottle, eliminates microgroove.
Described Folium Ginkgo extract is rich in the compositions such as pyrite glycoside, terpene lactones, organic acid, separating Ginkgo phenolic acids, alkyl phenol, alkyl phenolic acid, and non-oxidizability is strong, improves microcirculation, thus improves the texture of skin, color and luster and brightness.
Described Folium Mori extract is rich in flavonoid substances, ecdysterone, rutin, the compositions such as alkaloid, effectively can prevent oxidative damage by scavenging free radicals, improve the activity of superoxide dismutase in body, stop the generation of harmful substance in body, reduce pigmentation, slow down aging.
Described Herba portulacae extract is rich in a large amount of flavonoid, polysaccharide, vitamin, and the compositions such as aminoacid have antiinflammatory, antiallergic, anti-acne, antioxidative effect.Described Mel is rich in the compositions such as multiple organic acid, enzyme, colloidal substance, aromatic substance, and eye strain of releiving, minimizing eye edema, improve black eye.
The humectant properties of the unsaturated fatty acid that described Butyrospermum parkii fruit fat contains is very similar to the sebaceous gland of human body skin, it is natural emollient, it has extraordinary penetration, skin bottom can be penetrated into fast after contact skin, skin water loss can be prevented, increase skin defence capability and compliance.
Defying age eye cream of the present invention contains moringa oleifera leaf extractive, Folium Ginkgo extract, Folium Mori extract, the multiple natural plant composition such as Herba portulacae extract, again in conjunction with Mel of the present invention, Butyrospermum parkii fruit fat, glycerol, propylene glycol, hyaluronic acid, polydimethylsiloxane, the basic materials such as ethylhexyl palmitate, each component is worked in coordination with, make defying age eye cream good penetrability of the present invention, easy absorption, deep water supplement moisturizing, nourish maintenance skin, strengthen skin around the eyes elastic force and improve drying, relaxation, reduce pigmentation, alleviate black eye, repair impaired or innutritive cell, obvious continuity skin aging, skin around the eyes is replied plentiful and mellow and full, regain bright two pupil of beautiful gloss.
Present invention also offers the preparation method of above-mentioned defying age eye cream, specifically comprise the following steps:
S1, by polydimethylsiloxane, ethylhexyl palmitate, C20-22 alcohol phosphate ester, methyl hydroxybenzoate, Mel, Butyrospermum parkii fruit fat be placed in oil phase pot, stir and be heated to 80 ~ 90 DEG C, being stirred to material and dissolving completely, obtain material A;
Put into water in S2, main cooker, open homogenizing, by glycerol, propylene glycol, hyaluronic acid, polyacrylamide, be stirred to evenly, be heated to 80 ~ 90 DEG C, insulation 20 ~ 30min;
S3, by material A suction main cooker, then add triethanolamine, open homogenizing, homogenizing 10 ~ 15min, obtains material B, and material B carries out insulation froth breaking;
S4, after material B bubble-free, be cooled to 40 ~ 45 DEG C, add moringa oleifera leaf extractive, Folium Ginkgo extract, Folium Mori extract, Herba portulacae extract and essence, be stirred to evenly, namely discharging obtains defying age eye cream.
Further, the rotating speed of described homogenizing is 2500 ~ 4000rpm.
Further, the mixing speed of described stirring is 50 ~ 60r/min.
Further, the preparation method of described moringa oleifera leaf extractive is: get leaf of Moringa, pulverize after cleaning, drying, cross 80-100 mesh sieve, adding medical material total amount 8-12 times amount volume fraction is the ethanol of 50-70%, then adds the Snailase of medical material total amount 1.5-3%, lixiviate 1-2 hour at 38-45 DEG C, then at 85-95 DEG C of reflux, extract, 1-2 hour, filter, at filtrate reduced in volume to 60 DEG C, relative density is the extractum of 1.10-1.25, to obtain final product.
Further, the preparation method of described Folium Ginkgo extract is: get Folium Ginkgo, wash away impurity, crushed after being dried, crosses 60-80 mesh sieve, obtains coarse powder; Coarse powder is placed in supercritical carbon dioxide extraction apparatus, and adding coarse powder total amount 30-45% volume fraction is the ethanol of 70-85%, and regulation and control carbon dioxide flow is 15 ~ 20L/h, extracting pressure is 15 ~ 20MPa, and extraction temperature is 40 ~ 60 DEG C, and extraction time is 1.5 ~ 2h, decompression separation, to obtain final product.
Further, the preparation method of described Folium Mori extract is: pulverize after getting Folium Mori cleaning, drying, cross 90-100 mesh sieve, adding its weight 6-10 times amount volume fraction is the ethanol of 70-85%, soaks 3-6 hour, supersound extraction twice at 45-65 DEG C of temperature, each 30-60 minute, supersonic frequency is 25-35kHz, filters, merging filtrate, during filtrate reduced in volume to 60 DEG C, relative density is the extractum of 1.05-1.25, to obtain final product.
Further, the preparation method of described Herba portulacae extract is: get Herba Portulacae, wash away impurity, crushed after being dried, cross 60-80 mesh sieve, adding medical material gross weight 6-10 times amount volume fraction is the ethanol of 70-85%, microwave extraction 10-20 minute, and microwave power is 250-300W, Extracting temperature is 45-65 DEG C, filter, survey the extractum that relative density is 1.10-1.25 at filtrate reduced in volume to 60 DEG C, to obtain final product.
Therefore, compared with prior art, advantage of the present invention is:
(1) defying age eye cream of the present invention contains the multiple active skull cap components such as moringa oleifera leaf extractive, Folium Ginkgo extract, Folium Mori extract, Herba portulacae extract, Mel, Butyrospermum parkii fruit fat, deep water supplement moisturizing, nourish maintenance skin, strengthen skin around the eyes elastic force and improve drying, relaxation, reducing pigmentation, alleviate black eye, repair impaired or innutritive cell, obvious continuity skin aging, makes skin around the eyes reply plentiful and mellow and full, regains bright two pupil of beautiful gloss.
(2) defying age eye cream safety and stability of the present invention, good penetrability, easily absorbs, and uses rear skin salubrious not sticky; And the preparation method of defying age eye cream of the present invention is simple, condition is controlled, process stabilizing, can be applicable.
Detailed description of the invention
Further describe the present invention below by way of detailed description of the invention, but the present invention is not limited only to following examples.Within the scope of the invention or not departing from content of the present invention, spirit and scope, defying age eye cream of the present invention is suitably improved, replaces the identical component of effect, will become apparent to those skilled in the art that they are all deemed to be included within scope of the present invention.
In the eye cream of defying age described in the embodiment of the present invention, the information such as producer and article No. of part material is as follows:
Raw material and the proportioning (by weight percentage) of the embodiment of the present invention 1 ~ 3 and comparative example 1,2 defying age eye cream are as follows:
The preparation method of the embodiment of the present invention 1 ~ 3 defying age eye cream is as follows:
S1, by polydimethylsiloxane, ethylhexyl palmitate, C20-22 alcohol phosphate ester, methyl hydroxybenzoate, Mel, Butyrospermum parkii fruit fat be placed in oil phase pot, stir and be heated to 90 DEG C, being stirred to material and dissolving completely, obtain material A;
Put into water in S2, main cooker, open homogenizing, by glycerol, propylene glycol, hyaluronic acid, polyacrylamide, be stirred to evenly, be heated to 90 DEG C, insulation 20min;
S3, by material A suction main cooker, then add triethanolamine, open homogenizing, homogenizing 15min, obtains material B, and material B carries out insulation froth breaking;
S4, after material B bubble-free, be cooled to 45 DEG C, add moringa oleifera leaf extractive, Folium Ginkgo extract, Folium Mori extract, Herba portulacae extract and essence, be stirred to evenly, namely discharging obtains defying age eye cream.
Wherein, the rotating speed of described homogenizing is 3000rpm; The mixing speed of described stirring is 60r/min;
The preparation method of described moringa oleifera leaf extractive is: get leaf of Moringa, clean, crushed after being dried, cross 80 mesh sieves, adding medical material total amount 8 times amount volume fraction is the ethanol of 60%, add the Snailase of medical material total amount 2% again, lixiviate 2 hours at 40 DEG C, then 90 DEG C of reflux, extract, 1 hour, filters, at filtrate reduced in volume to 60 DEG C, relative density is the extractum of 1.10, to obtain final product;
The preparation method of described Folium Ginkgo extract is: get Folium Ginkgo, wash away impurity, crushed after being dried, crosses 60 mesh sieves, obtains coarse powder; Coarse powder is placed in supercritical carbon dioxide extraction apparatus, and adding coarse powder total amount 45% volume fraction is the ethanol of 70%, and regulation and control carbon dioxide flow is 20L/h, and extracting pressure is 20MPa, and extraction temperature is 50 DEG C, and extraction time is 2h, and decompression separation, to obtain final product;
The preparation method of described Folium Mori extract is: get Folium Mori and clean, crushed after being dried, cross 90 mesh sieves, adding its weight 8 times amount volume fraction is the ethanol of 80%, soak 4 hours, supersound extraction twice at 50 DEG C of temperature, each 40 minutes, supersonic frequency was 30kHz, filter, merging filtrate, during filtrate reduced in volume to 60 DEG C, relative density is the extractum of 1.05, to obtain final product;
The preparation method of described Herba portulacae extract is: get Herba Portulacae, wash away impurity, crushed after being dried, cross 60 mesh sieves, adding medical material gross weight 8 times amount volume fraction is the ethanol of 80%, microwave extraction 15 minutes, microwave power is 300W, and Extracting temperature is 50 DEG C, filters, survey the extractum that relative density is 1.25 at filtrate reduced in volume to 60 DEG C, to obtain final product.
The preparation method of the preparation method reference embodiment of the present invention of comparative example 1,2.
Meet the pertinent regulations requirement of QB/T1857-2013 through inspection embodiment 1 ~ 3 product, sense index (color and luster, fragrance, structure) meets industry regulation, and physical and chemical index (pH, heat-resisting, cold-resistant, active matter) meets industry regulation.
test example one, Product Safety evaluation (experiment of human body skin patch)
One, trial target: the defying age eye cream that embodiment 1 ~ 3 and comparative example 1 ~ 2 prepare
Two, tested crowd's data and grouping: 100 routine skin healths, the tested volunteer of the women without dermatosis allergies, 25 ~ 55 years old, 40 years old mean age, is divided into 5 groups at random, often organizes 20 people.
Three, patch method: select qualified speckle examination device, with closed patch experiment method, tested material being about 0.015g ~ 0.020g drips in speckle examination device, external special adhesive tape is covered on experimenter back, tested material is removed after 24 hours, within after removing respectively 0.5,6,12,24,48 hour, observe dermoreaction, according to its result of dermoreaction grade scale record in " cosmetics health specification ".
Four, experimental result: human skin patch result shows: each group experimenter passes through the patch test of the eye cream of embodiment 1 ~ 3 and comparative example 1 ~ 2, dermoreaction is observed at 0.5,6,12,24,48 hour, there is skin adverse reaction in equal nothing, the defying age eye cream use safety described in explanation.
test example two, product effect assessment
part I:
One, trial target: the defying age eye cream that embodiment 1, comparative example 1 ~ 2 prepare
Two, tested crowd's data and grouping: 90 routine skin healths, the tested volunteer of the women without dermatosis allergies, 25 ~ 55 years old, 38 years old mean age, is divided into 3 groups at random, often organizes 30 people.
Three, method of testing: adopt the skin elasticity CotometerMPA580 main frame that German Courage+Khazaka company (German CK company) manufactures, the probe used is ReviscometerRV600 elastic fibrous tissue test probe, surveys and averages for five times.Test zone: skin around the eyes.First measure the blank value (R2, R5, R7) of 30min after tested region clean, then specify that experimenter adheres to using above-mentioned trial target every day sooner or later, test test zone skin elasticity index R2, R5, R7 value (in test process, negative pressure is constant is 450mbar) after 1 week, 2 weeks, 3 weeks, 4 weeks respectively.
Index illustrates: skin elasticity index R2, R5, R7 are more close to 1, and the elasticity of skin is better.
R2=Ua/Uf；R5=Ur/Ue；R7=Ur/Uf
Uf---skin maximum tension amount
Ue---constant negative pressure is added to after on skin, the amount of tension of skin during 0.1 second, positioning elastic part amount of tension.
Ur---cancel after negative pressure, skin will restore to the original state rapidly state, is divided into elastic score value Ur equally, namely cancels negative pressure after 0.1 second, the recovery value of skin and visco-elastic portions value, or claim plastic value.
Ua---from cancelling the recovery value of negative pressure to skin when follow-on test skin surface adds negative pressure more next time.
Four, test result is as following table 1.
Table 1 is group defying age eye cream table with test results respectively
From upper table 1: use embodiment 1, defying age eye cream the 1st week rear R2 of comparative example 1 ~ 2, R5, R7 increases to some extent, the R2 of embodiment 1 after 4th week, R5, R7 all rises obviously, its value all levels off to 1, and comparative example 1, the R2 of 2, R5, R7 ascensional range is not obvious, illustrate and use defying age eye cream, the skin elasticity index of experimenter has very large lifting, and comparative example 1, 2 eye creams all lack some component in defying age eye cream formula of the present invention, its result of use is all not as embodiment 1, illustrate that defying age eye cream formula of the present invention is not obtained by the simple combination of each component, further illustrate again between each component of formula of the present invention and there is synergism.As can be seen here, this defying age eye cream has increases skin elasticity, antidotal effect.
part II:
One, trial target: embodiment 1 ~ 2, defying age eye cream prepared by comparative example 1 ~ 2
Two, tested crowd's data and grouping: 120 routine skin healths, the tested volunteer of the women without dermatosis allergies, 30 ~ 55 years old, 42 years old mean age, is divided into 4 groups at random, often organizes 30 people.
Three, method of testing: respectively use-case 1 ~ 2, defying age eye cream prepared by comparative example 1 ~ 2, observes and experiences result of use.Using method: after experimenter cleans face, get the eye cream of a meter great little, dub in eye all around, with refer to abdomen along near the eyes gently bullet clap until thoroughly absorb, the every day of each use sooner or later once, adhere to use one month, at least check weekly once to understand with or without whole body and local untoward reaction, and itemized record result.
Four, testing evaluation result is as follows:
(one month) on probation feedback conclusive table of table 2 embodiment 1 defying age eye cream
(one month) on probation feedback conclusive table of table 3 embodiment 2 defying age eye cream
(one month) on probation feedback conclusive table of table 4 comparative example 1 defying age eye cream
(one month) on probation feedback conclusive table of table 5 comparative example 2 defying age eye cream
From upper table 2 ~ 5, the defying age eye cream good penetrability of the embodiment of the present invention 1 ~ 2, easy absorption, uses rear skin around the eyes salubrious not sticky, to skin supply nutrition, reduce pigmentation, Vitamin K, promotes skin metabolism, effectively calms down microgroove, reduce dry stricture of vagina and wrinkle, slowing down skin aging.Wherein the degree of recognition of embodiment 1 defying age eye cream is the highest, therefore embodiment 1 is preferred embodiment, and comparative example 1,2 eye cream all lacks some component in defying age eye cream formula of the present invention, its permeability, Vitamin K, calm down microgroove, reduce the effect of dry stricture of vagina and wrinkle all not as embodiment 1 and 2, illustrate that formula components of the present invention is worked in coordination with mutually, play better effect.Do not have people to occur the allergic phenomenas such as skin pruritus, twinge, redness in whole experimenter, therefore, the gentle safety of defying age eye cream of the present invention, can life-time service simultaneously.
Above-described embodiment is illustrative principle of the present invention and effect thereof only, but not for limiting the present invention.Any person skilled in the art scholar all without prejudice under spirit of the present invention and category, can modify above-described embodiment or changes.Therefore, such as have in art usually know the knowledgeable do not depart from complete under disclosed spirit and technological thought all equivalence modify or change, must be contained by claim of the present invention.
Claims (9)
1. a defying age eye cream, it is characterized in that, comprise the component of following weight percent meter: glycerol 4 ~ 10%, propylene glycol 2 ~ 8%, hyaluronic acid 4 ~ 8%, polydimethylsiloxane 0.4 ~ 2%, ethylhexyl palmitate 2 ~ 6%, C20-22 alcohol phosphate ester 1 ~ 4%, methyl hydroxybenzoate 0.5 ~ 2%, polyacrylamide 0.5 ~ 2%, moringa oleifera leaf extractive 2 ~ 8%, Folium Ginkgo extract 4 ~ 8%, Folium Mori extract 2 ~ 6%, Herba portulacae extract 2 ~ 4%, Mel 0.4 ~ 2%, Butyrospermum parkii fruit fat 1 ~ 4%, triethanolamine 0.4 ~ 2%, essence 0.002 ~ 0.04% and water 40 ~ 65%.
2. defying age eye cream as claimed in claim 1, it is characterized in that, be made up of the component of following weight percent meter: glycerol 4%, propylene glycol 2%, hyaluronic acid 8%, polydimethylsiloxane 1%, ethylhexyl palmitate 2%, C20-22 alcohol phosphate ester 2%, methyl hydroxybenzoate 1%, polyacrylamide 1%, moringa oleifera leaf extractive 4%, Folium Ginkgo extract 6%, Folium Mori extract 4%, Herba portulacae extract 2%, Mel 0.8%, Butyrospermum parkii fruit fat 2%, triethanolamine 0.8%, essence 0.01%, surplus is water.
3. prepare a method for defying age eye cream as claimed in claim 1, it is characterized in that, comprise the following steps:
S1, by polydimethylsiloxane, ethylhexyl palmitate, C20-22 alcohol phosphate ester, methyl hydroxybenzoate, Mel, Butyrospermum parkii fruit fat be placed in oil phase pot, stir and be heated to 80 ~ 90 DEG C, being stirred to material and dissolving completely, obtain material A;
Put into water in S2, main cooker, open homogenizing, by glycerol, propylene glycol, hyaluronic acid, polyacrylamide, be stirred to evenly, be heated to 80 ~ 90 DEG C, insulation 20 ~ 30min;
S3, by material A suction main cooker, then add triethanolamine, open homogenizing, homogenizing 10 ~ 15min, obtains material B, and material B carries out insulation froth breaking;
S4, after material B bubble-free, be cooled to 40 ~ 45 DEG C, add moringa oleifera leaf extractive, Folium Ginkgo extract, Folium Mori extract, Herba portulacae extract and essence, be stirred to evenly, namely discharging obtains defying age eye cream.
4. the preparation method of defying age eye cream as claimed in claim 3, it is characterized in that, the rotating speed of described homogenizing is 2500 ~ 4000rpm.
5. the preparation method of defying age eye cream as claimed in claim 3, is characterized in that, the mixing speed 50 ~ 60r/min of described stirring.
6. the preparation method of defying age eye cream as claimed in claim 3, it is characterized in that, the preparation method of described moringa oleifera leaf extractive is: get leaf of Moringa, clean, crushed after being dried, cross 80-100 mesh sieve, adding medical material total amount 8-12 times amount volume fraction is the ethanol of 50-70%, add the Snailase of medical material total amount 1.5-3% again, lixiviate 1-2 hour at 38-45 DEG C, then at 85-95 DEG C of reflux, extract, 1-2 hour, filters, at filtrate reduced in volume to 60 DEG C, relative density is the extractum of 1.10-1.25, to obtain final product.
7. the preparation method of defying age eye cream as claimed in claim 3, it is characterized in that, the preparation method of described Folium Ginkgo extract is: get Folium Ginkgo, wash away impurity, crushed after being dried, crosses 60-80 mesh sieve, obtains coarse powder; Coarse powder is placed in supercritical carbon dioxide extraction apparatus, and adding coarse powder total amount 30-45% volume fraction is the ethanol of 70-85%, and regulation and control carbon dioxide flow is 15 ~ 20L/h, extracting pressure is 15 ~ 20MPa, and extraction temperature is 40 ~ 60 DEG C, and extraction time is 1.5 ~ 2h, decompression separation, to obtain final product.
8. the preparation method of defying age eye cream as claimed in claim 3, it is characterized in that, the preparation method of described Folium Mori extract is: get Folium Mori and clean, crushed after being dried, cross 90-100 mesh sieve, adding its weight 6-10 times amount volume fraction is the ethanol of 70-85%, soak 3-6 hour, supersound extraction twice at 45-65 DEG C of temperature, each 30-60 minute, supersonic frequency is 25-35kHz, filter, merging filtrate, during filtrate reduced in volume to 60 DEG C, relative density is the extractum of 1.05-1.25, to obtain final product.
9. the preparation method of defying age eye cream as claimed in claim 3, it is characterized in that, the preparation method of described Herba portulacae extract is: get Herba Portulacae, wash away impurity, crushed after being dried, cross 60-80 mesh sieve, adding medical material gross weight 6-10 times amount volume fraction is the ethanol of 70-85%, microwave extraction 10-20 minute, microwave power is 250-300W, and Extracting temperature is 45-65 DEG C, filters, survey the extractum that relative density is 1.10-1.25 at filtrate reduced in volume to 60 DEG C, to obtain final product.
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| CN201510799141.9A CN105395443A (en) | 2015-11-18 | 2015-11-18 | Anti-aging eye cream and preparation method thereof |
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| CN201510799141.9A CN105395443A (en) | 2015-11-18 | 2015-11-18 | Anti-aging eye cream and preparation method thereof |
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| CN105395443A true CN105395443A (en) | 2016-03-16 |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105902469A (en) * | 2016-05-30 | 2016-08-31 | 刘志彬 | Anti-mark firming eye cream and preparation method thereof |
| CN106137925A (en) * | 2016-08-24 | 2016-11-23 | 秦艳红 | A kind of defying age eye cream |
| CN107041862A (en) * | 2017-04-05 | 2017-08-15 | 中国科学院西北高原生物研究所 | A kind of eye cream containing raspberry |
| CN107184447A (en) * | 2017-04-27 | 2017-09-22 | 林俊生 | A kind of eye cream of activated water molecule |
| CN108078893A (en) * | 2017-12-30 | 2018-05-29 | 黄旭东 | A kind of anti-aging eye cream |
| CN110755310A (en) * | 2019-11-15 | 2020-02-07 | 上海曜爱生物科技有限公司 | Active composition for promoting skin microcirculation and preparation method and application thereof |
| CN113925801A (en) * | 2021-11-26 | 2022-01-14 | 上海琴馨文化科技有限公司 | Ginkgo leaf extract eye skin gel water for improving eye skin and preparation thereof |
| CN114748385A (en) * | 2022-04-08 | 2022-07-15 | 广州优理氏生物科技有限公司 | Composition and eye cream with effects of resisting wrinkles, removing dark eye circles and improving eye bags |
-
2015
- 2015-11-18 CN CN201510799141.9A patent/CN105395443A/en not_active Withdrawn
Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105902469A (en) * | 2016-05-30 | 2016-08-31 | 刘志彬 | Anti-mark firming eye cream and preparation method thereof |
| CN106137925A (en) * | 2016-08-24 | 2016-11-23 | 秦艳红 | A kind of defying age eye cream |
| CN107041862A (en) * | 2017-04-05 | 2017-08-15 | 中国科学院西北高原生物研究所 | A kind of eye cream containing raspberry |
| CN107184447A (en) * | 2017-04-27 | 2017-09-22 | 林俊生 | A kind of eye cream of activated water molecule |
| CN108078893A (en) * | 2017-12-30 | 2018-05-29 | 黄旭东 | A kind of anti-aging eye cream |
| CN110755310A (en) * | 2019-11-15 | 2020-02-07 | 上海曜爱生物科技有限公司 | Active composition for promoting skin microcirculation and preparation method and application thereof |
| CN110755310B (en) * | 2019-11-15 | 2022-04-15 | 上海曜爱生物科技有限公司 | Active composition for promoting skin microcirculation and preparation method and application thereof |
| CN113925801A (en) * | 2021-11-26 | 2022-01-14 | 上海琴馨文化科技有限公司 | Ginkgo leaf extract eye skin gel water for improving eye skin and preparation thereof |
| CN114748385A (en) * | 2022-04-08 | 2022-07-15 | 广州优理氏生物科技有限公司 | Composition and eye cream with effects of resisting wrinkles, removing dark eye circles and improving eye bags |
| CN114748385B (en) * | 2022-04-08 | 2022-12-09 | 广州优理氏生物科技有限公司 | Composition and eye cream with effects of resisting wrinkles, removing dark eye circles and improving eye bags |
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