CN105342914A - Spot-removing whitening astringent toner and preparation method thereof - Google Patents

Spot-removing whitening astringent toner and preparation method thereof Download PDF

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Publication number
CN105342914A
CN105342914A CN201510793626.7A CN201510793626A CN105342914A CN 105342914 A CN105342914 A CN 105342914A CN 201510793626 A CN201510793626 A CN 201510793626A CN 105342914 A CN105342914 A CN 105342914A
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extract
preparation
freckle removing
cosmetic water
whitening cosmetic
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樊利平
关美玲
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/64Proteins; Peptides; Derivatives or degradation products thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/02Preparations for care of the skin for chemically bleaching or whitening the skin

Abstract

The present invention belongs to the technical field of cosmetics, and in particular relates to spot-removing whitening astringent toner and a preparation method thereof, and the spot-removing whitening astringent toner includes water, glycerin, dipropylene glycol, butylene glycol, oat beta-glucan, milk protein, mulberry leaf extract, gastrodia elata extract, ophiopogon root extract, purslane extract, sodium hyaluronate, methylparaben, ethylparaben and flavorings and the like. The spot-removing whitening astringent toner is mild, skin- friendly, safe and non-stimulating, can effectively moisturize, hydrate, fade pigments, remove spots and whiten, make skin moist and smooth and elastic, and can be used for long term.

Description

A kind of freckle removing and whitening cosmetic water and preparation method thereof
Technical field
The present invention relates to cosmetic technical field, be specifically related to a kind of freckle removing and whitening cosmetic water and preparation method thereof.
Background technology
Bright and clean, pale, ruddy skin is that Nails is pursued always, the fashion of China and the state such as Japan, Southeast Asia women high praise in recent years especially, affect by it, whitening, Freckle removing cosmetics market are increasingly active, production marketing grows with each passing day, one of main flow kind having become skin protection cosmetics.Mottle is the representative of the melanin pigmentation that face is easily seen, comprises freckle, senile plaque, postinflammatory pigmentation etc.The reason that mottle is formed: human epidermal lower floor is distributed with many pigment celles, the catalytic oxidation of pigment cell's tryrosinase in body and form melanin, in skin, melanin increases and uneven gathering and form mottle.Want the object reaching whitening, speckle dispelling, by following two main paties: a kind of is the generation preventing pigment; Another kind of then be that to impel the chromocrinia of generation to go out external, wherein suppress and get rid of the main way that melanin is whitening, cosmetics adopts.Melanic generation needs to carry out under the effect of enzyme, and wherein tryrosinase is most important one.Many whitenings of selling in the market, speckle dispelling product are all achieved with restraint of tyrosinase, and by using some skin cell renewal promoter in formula, as fruit acid, vitamin etc., impel the pigment generated to excrete.
At present, many famous cosmetics companies and research institution drop into the exploitation that a large amount of manpower and materials carry out novel whitening speckle dispelling additive.Cosmetic water can, as clean the product that secondary is clean afterwards, also be lock the most important step of water moisturizing in skin care.But cosmetic water at present on the market, often owing to adding the problems such as chemicals, strong acid and strong base, chemical preservative, not only can not reach the object fundamentally protecting skin, skin also can be made to produce dependency or have intense stimulus to skin.Therefore, be necessary to develop a kind of freckle removing and whitening, the cosmetic water that replenishing water and preserving moisture effect is good, meet the demand in market.
Summary of the invention
In order to overcome the deficiencies in the prior art, the object of the present invention is to provide a kind of freckle removing and whitening cosmetic water, its gentle pro-skin, easily absorbs, safe and non-stimulating, and moisturizing, moistening effect are good, effectively suppress chromogenesis, and promote metabolism of pigment, freckle removing and whitening, can life-time service.
The present invention is by following technical solution to realize above-mentioned purpose:
A kind of freckle removing and whitening cosmetic water, comprises the raw material of following weight percent meter: water 75 ~ 85%, glycerol 1 ~ 4%, dipropylene glycol 1 ~ 2%, butanediol 2 ~ 4%, avenabeta glucosan 0.8 ~ 2%, milk protein 0.6 ~ 2%, Folium Mori extract 1 ~ 2%, Rhizoma Gastrodiae extract 1 ~ 4%, Radix Ophiopogonis extract 2 ~ 4%, Herba portulacae extract 2 ~ 4%, hyaluronate sodium 0.08 ~ 2%, methyl hydroxybenzoate 0.02 ~ 1%, ethyl hydroxybenzoate 0.02 ~ 1%, triethanolamine 0.6 ~ 1%, disodium edetate 0.4 ~ 1% and essence 0.008% ~ 0.2%.
As the preferred embodiment of the present invention, described freckle removing and whitening cosmetic water is made up of the raw material of following weight percent meter: glycerol 2%, dipropylene glycol 1%, butanediol 2%, avenabeta glucosan 1%, milk protein 1%, Folium Mori extract 2%, Rhizoma Gastrodiae extract 2%, Radix Ophiopogonis extract 4%, Herba portulacae extract 2%, hyaluronate sodium 1%, methyl hydroxybenzoate 0.8%, ethyl hydroxybenzoate 0.6%, triethanolamine 0.6%, disodium edetate 0.4%, essence 0.06%, and surplus is water.
Milk protein of the present invention contains hydrophilic moisturizing ingredient can protect skin total moisture to prevent from running off; several amino acids composition can promote the quick reparation of injured skin; the content of albumen in skin can be enriched; the intensity of connective tissue can be strengthened simultaneously; can promote that skin generates albumen; prevent and reduce wrinkle, making skin plentiful and flexible.
Described Folium Mori extract is rich in flavonoid substances, ecdysterone, rutin, the compositions such as alkaloid, effectively can prevent oxidative damage by scavenging free radicals, improve the activity of superoxide dismutase in body, stop the generation of harmful substance in body, the activity of restraint of tyrosinase, suppress the formation of pigment, thus reduction pigmentation, produce freckle removing and whitening, the effect of slow down aging.
Described Rhizoma Gastrodiae extract is rich in the compositions such as gastrodine, vitamin A, sterols, vanillyl alcohol, vanillin, gastrodia elata polysaccharide, and have calmness to central nervous system, hypnosis, antidotal effect, having obvious skin moistens foster, the effect of crease-resistant and mottle of dispelling.
Described Radix Ophiopogonis extract is rich in polysaccharide, steroidal saponin, homoisoflavone class, aminoacid, the compositions such as cupreol, stigmasterol, glycocide compound, CYCLIC DIPEPTIDES compounds, amides compound, polyhydrony fatty acid and phenolic acid compound, blood circulation promoting, improve the colour of skin, increase the synthesis of collagen protein simultaneously, make skin tender and lovely flexible.
Described Herba portulacae extract is rich in a large amount of flavonoid, polysaccharide, vitamin, and the compositions such as aminoacid have antiinflammatory, antiallergic, anti-acne, antioxidative effect.
Containing Folium Mori extract, Rhizoma Gastrodiae extract, Radix Ophiopogonis extract, Herba portulacae extract four kinds of natural extracts in freckle removing and whitening cosmetic water of the present invention, to skin supply nutrition, promote skin metabolism, desalination mottle, whitening makes skin water tender flexible, then in conjunction with milk protein, improves moist, the whitening of freckle removing and whitening cosmetic water of the present invention further, promote skin color and luster and brightness, strengthening speckle dispelling ability; Coordinate the basic materials such as avenabeta glucosan, glycerol, hyaluronate sodium, the efficacy exertion of freckle removing and whitening cosmetic water of the present invention is stablized, and stable system safety, gentle hypoallergenic, is easily absorbed by the skin, can life-time service.
Present invention also offers the preparation method of above-mentioned freckle removing and whitening cosmetic water, specifically comprise the following steps:
S1. water, glycerol, dipropylene glycol, butanediol, avenabeta glucosan, hyaluronate sodium, disodium edetate are added in agitated kettle, homogenizing 10 ~ 20min, be heated to 70 ~ 80 DEG C, be stirred to material dissolution complete;
S2. continue to stir cooling and be down to 45 ~ 55 DEG C, add milk protein, Folium Mori extract, Rhizoma Gastrodiae extract, Radix Ophiopogonis extract, Herba portulacae extract, be stirred to system even;
S3. finally add methyl hydroxybenzoate, ethyl hydroxybenzoate, triethanolamine and essence, stir, get final product discharging, obtain freckle removing and whitening cosmetic water.
Further, the rotating speed of described homogenizing is 2000 ~ 3000rpm.
Further, the mixing speed of described stirring is 40 ~ 60r/min.
Further, the preparation method of described Folium Mori extract is: pulverize after getting Folium Mori cleaning, drying, cross 90-100 mesh sieve, adding its weight 6-10 times amount volume fraction is the ethanol of 70-85%, soaks 3-6 hour, supersound extraction twice at 45-65 DEG C of temperature, each 30-60 minute, supersonic frequency is 25-35kHz, filters, merging filtrate, during filtrate reduced in volume to 60 DEG C, relative density is the extractum of 1.05-1.25, to obtain final product.
Further, the preparation method of described Rhizoma Gastrodiae extract is: get Rhizoma Gastrodiae, wash away impurity, crushed after being dried, cross 60-80 mesh sieve, adding Rhizoma Gastrodiae gross weight 6-8 times amount volume fraction is the ethanol of 60-80%, microwave extraction 8-15 minute, and microwave power is 240-300W, Extracting temperature is 45-65 DEG C, filter, survey the extractum that relative density is 1.20-1.25 at filtrate reduced in volume to 60 DEG C, to obtain final product.
Further, the preparation method of described Radix Ophiopogonis extract is: get Radix Ophiopogonis, wash away impurity, crushed after being dried, cross 60-80 mesh sieve, adding Radix Ophiopogonis gross weight 6-8 times amount volume fraction is the ethanol of 60-80%, microwave extraction 8-15 minute, and microwave power is 240-300W, Extracting temperature is 45-65 DEG C, filter, survey the extractum that relative density is 1.20-1.25 at filtrate reduced in volume to 60 DEG C, to obtain final product.
Further, the preparation method of described Herba portulacae extract is: get Herba Portulacae, wash away impurity, crushed after being dried, cross 60-80 mesh sieve, adding medical material gross weight 6-10 times amount volume fraction is the ethanol of 70-85%, microwave extraction 10-20 minute, and microwave power is 250-300W, Extracting temperature is 45-65 DEG C, filter, survey the extractum that relative density is 1.10-1.25 at filtrate reduced in volume to 60 DEG C, to obtain final product.
Therefore, compared with prior art, advantage of the present invention is:
(1) freckle removing and whitening cosmetic water of the present invention contains the multiple natural extracts such as Folium Mori extract, Rhizoma Gastrodiae extract, Radix Ophiopogonis extract, Herba portulacae extract, can efficiently moisturizing, moisturizing, to skin supply nutrition, promote skin metabolism, reduce chromogenesis, promote metabolism of pigment, desalination mottle, whitening and long-acting moisturizing, make skin beauty water moisten smooth, high resilience.
(2) freckle removing and whitening cosmetic water safety and stability of the present invention, gentle pro-skin, does not stimulate, and skin easily absorbs, and uses rear face salubrious not sticky; And freckle removing and whitening cosmetic water cost of material of the present invention is low, preparation method is simple, and condition is controlled, process stabilizing, can be applicable.
Detailed description of the invention
Further describe the present invention below by way of detailed description of the invention, but the present invention is not limited only to following examples.Within the scope of the invention or not departing from content of the present invention, spirit and scope, freckle removing and whitening cosmetic water of the present invention is suitably improved, replaces the identical component of effect, will become apparent to those skilled in the art that they are all deemed to be included within scope of the present invention.
In the cosmetic water of freckle removing and whitening described in the embodiment of the present invention, the information such as producer and article No. of part material is as follows:
Raw material and the proportioning (by weight percentage) of the embodiment of the present invention 1 ~ 3 and comparative example 1 ~ 2 freckle removing and whitening cosmetic water are as follows:
The preparation method of the embodiment of the present invention 1 ~ 3 freckle removing and whitening cosmetic water is as follows:
S1. water, glycerol, dipropylene glycol, butanediol, avenabeta glucosan, hyaluronate sodium, disodium edetate are added in agitated kettle, homogenizing 20min, be heated to 75 DEG C, be stirred to material dissolution complete;
S2. continue to stir cooling and be down to 45 DEG C, add milk protein, Folium Mori extract, Rhizoma Gastrodiae extract, Radix Ophiopogonis extract, Herba portulacae extract, be stirred to system even;
S3. finally add methyl hydroxybenzoate, ethyl hydroxybenzoate, triethanolamine and essence, stir, get final product discharging, obtain freckle removing and whitening cosmetic water.
Wherein, the rotating speed of described homogenizing is 2500rpm; The mixing speed of described stirring is 45r/min;
The preparation method of described Folium Mori extract is: get Folium Mori and clean, crushed after being dried, cross 90 mesh sieves, adding its weight 6 times amount volume fraction is the ethanol of 75%, soak 4 hours, supersound extraction twice at 45 DEG C of temperature, each 40 minutes, supersonic frequency was 25kHz, filter, merging filtrate, during filtrate reduced in volume to 60 DEG C, relative density is the extractum of 1.05, to obtain final product;
The preparation method of described Rhizoma Gastrodiae extract is: get Rhizoma Gastrodiae, wash away impurity, crushed after being dried, cross 70 mesh sieves, adding Rhizoma Gastrodiae gross weight 6 times amount volume fraction is the ethanol of 75%, microwave extraction 10 minutes, microwave power is 250W, and Extracting temperature is 50 DEG C, filters, survey the extractum that relative density is 1.20 at filtrate reduced in volume to 60 DEG C, to obtain final product;
The preparation method of described Radix Ophiopogonis extract is: get Radix Ophiopogonis, wash away impurity, crushed after being dried, cross 60 mesh sieves, adding Radix Ophiopogonis gross weight 6 times amount volume fraction is the ethanol of 75%, microwave extraction 10 minutes, microwave power is 250W, and Extracting temperature is 45 DEG C, filters, survey the extractum that relative density is 1.20 at filtrate reduced in volume to 60 DEG C, to obtain final product;
The preparation method of described Herba portulacae extract is: get Herba Portulacae, wash away impurity, crushed after being dried, cross 60 mesh sieves, adding medical material gross weight 6 times amount volume fraction is the ethanol of 75%, microwave extraction 20 minutes, microwave power is 250W, and Extracting temperature is 45 DEG C, filters, survey the extractum that relative density is 1.10 at filtrate reduced in volume to 60 DEG C, to obtain final product.
The preparation method of the preparation method reference embodiment of the present invention of comparative example 1 ~ 2.
Meet the pertinent regulations requirement of QB/T1857-2013 through inspection embodiment 1 ~ 3 product, sense index (color and luster, fragrance, structure) meets industry regulation, and physical and chemical index (pH, heat-resisting, cold-resistant, active matter) meets industry regulation.
test example one, Product Safety evaluation (experiment of human body skin patch)
One, trial target: the freckle removing and whitening cosmetic water that embodiment 1 ~ 3, comparative example 1 ~ 2 prepare
Two, tested crowd's data and grouping: 100 routine skin healths, the tested volunteer of the women without dermatosis allergies, 35 ~ 55 years old, 40 years old mean age, is divided into 5 groups at random, often organizes 20 people.
Three, patch method: select qualified speckle examination device, with closed patch experiment method, tested material being about 0.015mL ~ 0.030mL drips in speckle examination device, external special adhesive tape is covered on experimenter back, tested material is removed after 24 hours, within after removing respectively 0.5,6,12,24,48 hour, observe dermoreaction, according to its result of dermoreaction grade scale record in " cosmetics health specification ".
Four, experimental result: human skin patch result shows: each group experimenter is by the patch test of the freckle removing and whitening cosmetic water of embodiment 1 ~ 3, comparative example 1 ~ 2, dermoreaction is observed at 0.5,6,12,24,48 hour, there is skin adverse reaction in equal nothing, the freckle removing and whitening cosmetic water use safety described in explanation.
test example two, product effect assessment
part I:
One, trial target: the freckle removing and whitening cosmetic water that embodiment 1 ~ 3, comparative example 1 ~ 2 prepare
Two, tested crowd's data and grouping: 100 routine skin healths, the tested volunteer of the women without dermatosis allergies, 25 ~ 55 years old, 30 years old mean age, is divided into 5 groups at random, often organizes 20 people.
Three, method of testing: experimenter uses Fes Kai Er SK-III skin moisture detector to test the moisture of forehead, left face, right face and chin skin respectively after using clean water face, and get arithmetic mean of instantaneous value, experimenter re-uses above-mentioned crease-resistant cosmetic water, uniform application is in face, pat gently, by the skin moisture content of skin moisture tester test forehead, left face, right face and the same position of chin after 20min, and get arithmetic mean of instantaneous value, re-use skin moisture tester after 6h and test one time.Often organize 10 experimenters and tested result is got arithmetic mean of instantaneous value.
Four, test result is as following table 1.
Wherein, skin average moisture before skin average moisture-use cosmetic water is used after cosmetic water 20min after skin moisture content gradient=use cosmetic water 20min;
To use after cosmetic water 6h after skin moisture content gradient=use cosmetic water 6h skin average moisture before skin average moisture-use cosmetic water.
Table 1 skin moisture content table with test results
From upper table 1: after using the freckle removing and whitening cosmetic water 20min of embodiment 1 ~ 3, can not only skin moisture content be significantly improved, also can pin moisture, make skin keep long-acting water to moisten, still keep good water supplement function after 6h.And use the moisturizing that the cosmetic water of comparative example 1,2 produces, moistening effect is not as good as embodiment 1 ~ 3, illustrate and use freckle removing and whitening cosmetic water of the present invention, moisture of skin can be pinned well, keep skin beauty water profit, and comparative example 1,2 cosmetic water all lacks some component in freckle removing and whitening cosmetic water formula of the present invention, its result of use is all not as embodiment 1 ~ 3, illustrate that freckle removing and whitening cosmetic water formula of the present invention is not obtained by the simple combination of each component, then further illustrate between each component of formula of the present invention and there is synergism.As can be seen here, this freckle removing and whitening cosmetic water has the effect increasing skin elasticity, moisturizing moisturizing.
part II:
One, trial target: embodiment 1 ~ 3, freckle removing and whitening cosmetic water prepared by comparative example 1 ~ 2
Two, tested crowd's data and grouping: 150 routine skin healths, the tested volunteer of the women without dermatosis allergies, 30 ~ 55 years old, 35 years old mean age, is divided into 5 groups at random, often organizes 30 people.
Three, method of testing: respectively use-case 1 ~ 3, freckle removing and whitening cosmetic water prepared by comparative example 1 ~ 2, observes and experiences result of use.Using method: after experimenter cleans face, by above-mentioned freckle removing and whitening cosmetic water uniform application in face, pat gently to skin and all absorb, the every day of each use sooner or later once, adhere to use one month, at least check weekly once to understand with or without whole body and local untoward reaction, and itemized record result.
Four, testing evaluation result is as follows:
(one month) on probation feedback conclusive table of table 2 embodiment 1 freckle removing and whitening cosmetic water
(one month) on probation feedback conclusive table of table 3 embodiment 2 freckle removing and whitening cosmetic water
(one month) on probation feedback conclusive table of table 4 embodiment 3 freckle removing and whitening cosmetic water
(one month) on probation feedback conclusive table of table 5 comparative example 1 freckle removing and whitening cosmetic water
(one month) on probation feedback conclusive table of table 6 comparative example 2 freckle removing and whitening cosmetic water
From upper table 2 ~ 6, the gentle pro-skin of the freckle removing and whitening cosmetic water of embodiment 1 ~ 3, easily to absorb, use rear face salubrious not sticky, moisturizing, moistening effect are good, to skin supply nutrition, promote skin metabolism, reduce the formation of pigment, promote the metabolism of pigment, reduce mottle, make skin lightening glossy, and long-acting moisturizing, skin beauty water is moistened smooth, flexible.Wherein the degree of recognition of embodiment 1 freckle removing and whitening cosmetic water is the highest, and therefore embodiment 1 is preferred embodiment.And comparative example 1,2 cosmetic water all lacks some component in freckle removing and whitening cosmetic water formula of the present invention, the effect of its freckle removing and whitening, replenishing water and preserving moisture, all not as embodiment 1 ~ 3, illustrates that formula components of the present invention is worked in coordination with mutually, plays better effect.Do not have people to occur the allergic phenomenas such as skin pruritus, twinge, redness in whole experimenter, therefore, the gentle safety of freckle removing and whitening cosmetic water of the present invention, can life-time service simultaneously.
Above-described embodiment is illustrative principle of the present invention and effect thereof only, but not for limiting the present invention.Any person skilled in the art scholar all without prejudice under spirit of the present invention and category, can modify above-described embodiment or changes.Therefore, such as have in art usually know the knowledgeable do not depart from complete under disclosed spirit and technological thought all equivalence modify or change, must be contained by claim of the present invention.

Claims (9)

1. a freckle removing and whitening cosmetic water, it is characterized in that, comprise the raw material of following weight percent meter: water 75 ~ 85%, glycerol 1 ~ 4%, dipropylene glycol 1 ~ 2%, butanediol 2 ~ 4%, avenabeta glucosan 0.8 ~ 2%, milk protein 0.6 ~ 2%, Folium Mori extract 1 ~ 2%, Rhizoma Gastrodiae extract 1 ~ 4%, Radix Ophiopogonis extract 2 ~ 4%, Herba portulacae extract 2 ~ 4%, hyaluronate sodium 0.08 ~ 2%, methyl hydroxybenzoate 0.02 ~ 1%, ethyl hydroxybenzoate 0.02 ~ 1%, triethanolamine 0.6 ~ 1%, disodium edetate 0.4 ~ 1% and essence 0.008% ~ 0.2%.
2. freckle removing and whitening cosmetic water as claimed in claim 1, it is characterized in that, described freckle removing and whitening cosmetic water is made up of the raw material of following weight percent meter: glycerol 2%, dipropylene glycol 1%, butanediol 2%, avenabeta glucosan 1%, milk protein 1%, Folium Mori extract 2%, Rhizoma Gastrodiae extract 2%, Radix Ophiopogonis extract 4%, Herba portulacae extract 2%, hyaluronate sodium 1%, methyl hydroxybenzoate 0.8%, ethyl hydroxybenzoate 0.6%, triethanolamine 0.6%, disodium edetate 0.4%, essence 0.06%, and surplus is water.
3. prepare a method for freckle removing and whitening cosmetic water as claimed in claim 1, it is characterized in that, comprise the following steps:
S1. water, glycerol, dipropylene glycol, butanediol, avenabeta glucosan, hyaluronate sodium, disodium edetate are added in agitated kettle, homogenizing 10 ~ 20min, be heated to 70 ~ 80 DEG C, be stirred to material dissolution complete;
S2. continue to stir cooling and be down to 45 ~ 55 DEG C, add milk protein, Folium Mori extract, Rhizoma Gastrodiae extract, Radix Ophiopogonis extract, Herba portulacae extract, be stirred to system even;
S3. finally add methyl hydroxybenzoate, ethyl hydroxybenzoate, triethanolamine and essence, stir, get final product discharging, obtain freckle removing and whitening cosmetic water.
4. the preparation method of freckle removing and whitening cosmetic water as claimed in claim 3, it is characterized in that, the rotating speed of described homogenizing is 2000 ~ 3000rpm.
5. the preparation method of freckle removing and whitening cosmetic water as claimed in claim 3, it is characterized in that, the mixing speed of described stirring is 40 ~ 60r/min.
6. the preparation method of freckle removing and whitening cosmetic water as claimed in claim 3, it is characterized in that, the preparation method of described Folium Mori extract is: get Folium Mori and clean, crushed after being dried, cross 90-100 mesh sieve, adding its weight 6-10 times amount volume fraction is the ethanol of 70-85%, soak 3-6 hour, supersound extraction twice at 45-65 DEG C of temperature, each 30-60 minute, supersonic frequency is 25-35kHz, filter, merging filtrate, during filtrate reduced in volume to 60 DEG C, relative density is the extractum of 1.05-1.25, to obtain final product.
7. the preparation method of freckle removing and whitening cosmetic water as claimed in claim 3, it is characterized in that, the preparation method of described Rhizoma Gastrodiae extract is: get Rhizoma Gastrodiae, wash away impurity, crushed after being dried, cross 60-80 mesh sieve, adding Rhizoma Gastrodiae gross weight 6-8 times amount volume fraction is the ethanol of 60-80%, microwave extraction 8-15 minute, microwave power is 240-300W, and Extracting temperature is 45-65 DEG C, filters, survey the extractum that relative density is 1.20-1.25 at filtrate reduced in volume to 60 DEG C, to obtain final product.
8. the preparation method of freckle removing and whitening cosmetic water as claimed in claim 3, it is characterized in that, the preparation method of described Radix Ophiopogonis extract is: get Radix Ophiopogonis, wash away impurity, crushed after being dried, cross 60-80 mesh sieve, adding Radix Ophiopogonis gross weight 6-8 times amount volume fraction is the ethanol of 60-80%, microwave extraction 8-15 minute, microwave power is 240-300W, and Extracting temperature is 45-65 DEG C, filters, survey the extractum that relative density is 1.20-1.25 at filtrate reduced in volume to 60 DEG C, to obtain final product.
9. the preparation method of freckle removing and whitening cosmetic water as claimed in claim 3, it is characterized in that, the preparation method of described Herba portulacae extract is: get Herba Portulacae, wash away impurity, crushed after being dried, cross 60-80 mesh sieve, adding medical material gross weight 6-10 times amount volume fraction is the ethanol of 70-85%, microwave extraction 10-20 minute, microwave power is 250-300W, and Extracting temperature is 45-65 DEG C, filters, survey the extractum that relative density is 1.10-1.25 at filtrate reduced in volume to 60 DEG C, to obtain final product.
CN201510793626.7A 2015-11-18 2015-11-18 Spot-removing whitening astringent toner and preparation method thereof Withdrawn CN105342914A (en)

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CN107184501A (en) * 2017-04-19 2017-09-22 北海市韩能生物科技有限公司 The preparation method of foster skin water
CN107260641A (en) * 2017-06-24 2017-10-20 皖南医学院 Awake skin dew of a kind of man and preparation method thereof
CN110917056A (en) * 2019-12-29 2020-03-27 广东佰欧斐丝细胞科研中心有限公司 Toner with anti-wrinkle, moisturizing and whitening effects
CN112107498A (en) * 2020-07-17 2020-12-22 重庆珂蓝健康管理集团有限公司 Rapid and safe freckle removing method
CN114259454A (en) * 2022-01-24 2022-04-01 浙江省林业科学研究院 Tear-type Zhejiang radix ophiopogonis whitening mask and preparation method thereof
CN114469826A (en) * 2022-01-24 2022-05-13 浙江省林业科学研究院 Gel type Zhejiang radix ophiopogonis whitening mask and preparation method thereof

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CN107184501A (en) * 2017-04-19 2017-09-22 北海市韩能生物科技有限公司 The preparation method of foster skin water
CN107260641A (en) * 2017-06-24 2017-10-20 皖南医学院 Awake skin dew of a kind of man and preparation method thereof
CN107260641B (en) * 2017-06-24 2020-04-21 皖南医学院 Male refreshing lotion and preparation method thereof
CN110917056A (en) * 2019-12-29 2020-03-27 广东佰欧斐丝细胞科研中心有限公司 Toner with anti-wrinkle, moisturizing and whitening effects
CN112107498A (en) * 2020-07-17 2020-12-22 重庆珂蓝健康管理集团有限公司 Rapid and safe freckle removing method
CN114259454A (en) * 2022-01-24 2022-04-01 浙江省林业科学研究院 Tear-type Zhejiang radix ophiopogonis whitening mask and preparation method thereof
CN114469826A (en) * 2022-01-24 2022-05-13 浙江省林业科学研究院 Gel type Zhejiang radix ophiopogonis whitening mask and preparation method thereof
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