CN105168112A - Anti-wrinkle toner and preparation method thereof - Google Patents
Anti-wrinkle toner and preparation method thereof Download PDFInfo
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- CN105168112A CN105168112A CN201510674410.9A CN201510674410A CN105168112A CN 105168112 A CN105168112 A CN 105168112A CN 201510674410 A CN201510674410 A CN 201510674410A CN 105168112 A CN105168112 A CN 105168112A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8129—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an alcohol, ether, aldehydo, ketonic, acetal or ketal radical; Compositions of hydrolysed polymers or esters of unsaturated alcohols with saturated carboxylic acids; Compositions of derivatives of such polymers, e.g. polyvinylmethylether
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/41—Amines
- A61K8/416—Quaternary ammonium compounds
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/42—Amides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/494—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
- A61K8/4946—Imidazoles or their condensed derivatives, e.g. benzimidazoles
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/65—Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/99—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from microorganisms other than algae or fungi, e.g. protozoa or bacteria
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
Abstract
The invention belongs to the technical field of cosmetics, and particularly relates to an anti-wrinkle toner and a preparation method thereof. The anti-wrinkle toner consists of water, glycerin, propylene glycol, polyglycerol-10, butanediol, oat Beta-glucan, lycine, hydroxyethylurea, milk protein, lactobacillus/pomegranate fruit fermentation product extract, starfish essence, allantoin, sodium hyaluronate, preservative and essence. The anti-wrinkle toner is mild, skin-friendly, safe and non-irritating, can effectively moisturize, preserve moisture, resist aging, repair wrinkles and ensures that skin is moist, smooth and elastic, and can be used for a long term.
Description
Technical field
The present invention relates to cosmetic technical field, be specifically related to a kind of crease-resistant cosmetic water and preparation method thereof.
Background technology
Along with growth in the living standard, people more and more focus on the maintenance of skin, but the reason such as inherent and external causes various skin problem.Immanent cause: be wrinkle, crows-feet, microgroove, temporal wrinkle be all because the inhomogenous contraction of skin epidermis is subsided and caused.First, skin is made up of three-decker, epidermal area, skin corium, subcutaneous fat respectively, skin corium contains collagen protein, elastin and other fibers and constitutes the skeleton supporting skin, also be that skin that these elements make seems smooth youth, these elements are also the damages being subject to UVA, UVB and ozone or other oxidative factors equally.Extrinsic factor: modern's life stress is large, overtime work is stayed up late, long-time to computer, smoking, do not have enough sleep, stay in air-conditioned room for a long time, drink, excess eye-using etc. becomes life normality, adds air pollution.According to the U.S. beautiful scientific center research of Dior Christian Dior, every day, the each layer of skin can accumulate the cellular elements toxin in a large number caused by inherent or extrinsic factor, skin cell can be caused to suffocate, and have impact on the Dusuqing removing solid capacity of skin self, thus just create the worries such as the colour of skin is obscure, shortage gloss, tired state are showed fully, increase the weight of the burden of skin, accelerate skin aging.Therefore, the cosmetics for the various problems of skin existence also arise at the historic moment.Cosmetic water also claims firming lotion, astringent etc., and its effect is just the pH-value again cleaning to recover skin surface, and nurses one's health horny layer, and skin is absorbed better, and prepares for application maintenance product.So after washed, use cosmetic water, can keep the skin wet rapidly.
" hydropenia " is that skin becomes more poor and more poor and one of aging main arch-criminal, replenishing water and preserving moisture is not the patent of responsive skin, various skin all can because of factors such as environment, age, nutrition, health hydropenia, when human body skin horny layer moisture lower than 10% time, skin will lose fine and soft, elasticity, then becomes coarse, dry, occur various skin abnormality, correct if can not get for a long time, skin easily aging, long speckle becomes responsive, so also will note moisturizing while anti-ageing.Chinese patent application 104000759A discloses a kind of active cosmetic water, and it comprises: glycerol, propylene glycol, allantoin, xanthan gum, hyaluronate sodium, glycyrrhizic acid diformazan, α arbutin, water soluble vitamin, Gherkin extract, Argireline, VC ethylether, Radix Hamamelidis Mollis extracting solution, tartaric acid, phenoxyethanol and deionized water.This cosmetic water can solve and cause that sensitivity is high due to air pollution to the skin of people, corse sweat pore, skin are dim and the problem such as xerosis cutis hydropenia, but its moisturizing and anti-aging effects need to improve.
Therefore, be necessary to research and develop a kind of crease-resistant cosmetic water, its moisturizing, moistening effect are good, and effectively repair skin wrinkle, delay skin aging.
Summary of the invention
In order to overcome the deficiencies in the prior art, the object of the present invention is to provide a kind of crease-resistant cosmetic water, its gentle pro-skin, easily absorbs, safe and non-stimulating, and moisturizing, moistening effect are good, and effectively repair skin wrinkle, delay skin aging, can life-time service.
The present invention is by following technical solution to realize above-mentioned purpose:
A kind of crease-resistant cosmetic water, comprises the raw material of following weight percent meter: water 72 ~ 85%, glycerol 2 ~ 5%, propylene glycol 2 ~ 5%, Natrulon H-10 2 ~ 5%, butanediol 2 ~ 5%, avenabeta glucosan 0.5 ~ 2%, betanin 0.2 ~ 1%, ethoxy urea 0.2 ~ 1%, milk protein 0.3 ~ 1.5%, lactobacillus/Punica granatum L. tunning extract 0.3 ~ 1%, Asterias amurensis Lutken elite 0.3 ~ 1%, allantoin 0.05 ~ 0.2%, hyaluronate sodium 0.01 ~ 0.05%, antiseptic 0.2 ~ 1% and essence 0.01 ~ 0.02%.
Further, described crease-resistant cosmetic water also comprise the leaf of Herb Gynostemmae Pentaphylli extract 0.3 ~ 1% of weight percent meter, arctic Ascophyllum nodosum elite 0.3 ~ 1% and the youth algae 0.3 ~ 1%.
Further, described antiseptic is the compositions of methyl hydroxybenzoate and phenoxyethanol, and the weight ratio of described methyl hydroxybenzoate and phenoxyethanol is 1:5.
As the preferred embodiment of the present invention, described crease-resistant cosmetic water is made up of the raw material of following weight percent meter: water 79.37%, glycerol 4%, propylene glycol 3%, Natrulon H-10 4%, butanediol 3%, avenabeta glucosan 1%, betanin 0.6%, ethoxy urea 0.5%, milk protein 1%, lactobacillus/Punica granatum L. tunning extract 0.6%, Asterias amurensis Lutken elite 0.5%, leaf of Herb Gynostemmae Pentaphylli extract 0.6%, arctic Ascophyllum nodosum elite 0.6%, the youth algae 0.5%, allantoin 0.1%, hyaluronate sodium 0.02%, antiseptic 0.6% and essence 0.01%.
Milk protein of the present invention contains hydrophilic moisturizing ingredient can protect skin total moisture to prevent from running off; several amino acids composition can promote the quick reparation of injured skin; the content of albumen in skin can be enriched; the intensity of connective tissue can be strengthened simultaneously; can promote that skin generates albumen; prevent and reduce wrinkle, making skin plentiful and flexible.
Described lactobacillus/Punica granatum L. tunning extract contains a large amount of ellagic acids, polyphenol and anthocyanidin, and its non-oxidizability is strong, can effectively in and free radical, enhance metabolism, reduce visible microgroove.
Described Asterias amurensis Lutken elite can promote the metabolism of skin, increase epidermal barrier regeneration, more increase the synthesis of glycosaminoglycan (GAGS) and III, type Ⅳ collagen albumen simultaneously, help skin effectively to anti-wrinkle, make skin water tender flexible, and without any side effect and zest.
Described leaf of Herb Gynostemmae Pentaphylli extract can improve the function of the aquaporin in Skin Cell, promotes to produce aquaporin, imports moisture to cell interior, brings skin water profit from cell interior.Cell has been moistened, and skin also can become water profit thereupon.
Described arctic Ascophyllum nodosum elite is rich in algin body, brown algae polyphenols, sodium alginate, algae carotene and ocean trace element, skin thickness can be increased, improve the mechanical performance of skin, improve barrier function, promote collagen protein and elastin laminin with become, suppress digestive enzyme, thus improve the texture of skin, color and luster and brightness.
The quick new life of skin corium Collagen material can be promoted in described youth algae exclusive " also virgin albumen ", strengthen the elasticity of epidermis and degree of compacting, relax face's lines, revise face mask.
Containing milk protein, lactobacillus/Punica granatum L. tunning extract and Asterias amurensis Lutken elite three kinds of natural extracts in the crease-resistant cosmetic water of the present invention, to skin supply nutrition, promote skin metabolism, repair skin wrinkle to regenerate anti-wrinkle simultaneously, make skin water tender flexible, then in conjunction with leaf of Herb Gynostemmae Pentaphylli extract, arctic Ascophyllum nodosum elite and the youth algae, improve further the moisturizing of the crease-resistant cosmetic water of the present invention, moisture retention, promote skin color and luster and brightness, strengthening oxidation resistance; Coordinate the basic materials such as avenabeta glucosan, betanin, allantoin, hyaluronate sodium, the efficacy exertion of the crease-resistant cosmetic water of the present invention is stablized, and stable system safety, gentle hypoallergenic, is easily absorbed by the skin, can life-time service.
Present invention also offers the preparation method of above-mentioned crease-resistant cosmetic water, specifically comprise the following steps:
S1. water, glycerol, propylene glycol, butanediol, avenabeta glucosan, betanin, ethoxy urea, allantoin, Natrulon H-10 and hyaluronate sodium are added in agitated kettle, homogenizing 5 ~ 10min, be heated to 75 ~ 85 DEG C, be stirred to material dissolution complete;
S2. continue to stir cooling and be down to 40 ~ 50 DEG C, add milk protein, lactobacillus/Punica granatum L. tunning extract and Asterias amurensis Lutken elite, be stirred to system even;
S3. finally add the mixture of antiseptic and essence, stir, get final product discharging, obtain crease-resistant cosmetic water.
Further, described S2 also comprise add leaf of Herb Gynostemmae Pentaphylli extract, arctic Ascophyllum nodosum elite and the youth algae.
Therefore, compared with prior art, advantage of the present invention is:
(1) the crease-resistant cosmetic water of the present invention contains milk protein, lactobacillus/multiple natural extract such as Punica granatum L. tunning extract and Asterias amurensis Lutken elite, can efficiently moisturizing, moisturizing, to skin supply nutrition, promote skin metabolism, effective minimizing wrinkle, delay skin aging, and long-acting moisturizing, skin beauty water is moistened smooth, high resilience.
(2) the crease-resistant cosmetic water safety and stability of the present invention, gentle pro-skin, does not stimulate, and skin easily absorbs, and uses rear face salubrious not sticky; And the present invention's crease-resistant cosmetic water cost of material is low, preparation method is simple, and condition is controlled, process stabilizing, can be applicable.
Detailed description of the invention
Further describe the present invention below by way of detailed description of the invention, but the present invention is not limited only to following examples.Within the scope of the invention or not departing from content of the present invention, spirit and scope, crease-resistant cosmetic water of the present invention is suitably improved, replaces the identical component of effect, will become apparent to those skilled in the art that they are all deemed to be included within scope of the present invention.
In crease-resistant cosmetic water described in the embodiment of the present invention, the information such as producer and article No. of part material is as follows:
embodiment 1, the crease-resistant cosmetic water of the present invention and preparation thereof
formula:be made up of the raw material of following weight percent meter: water 79.89%, glycerol 2%, propylene glycol 2%, Natrulon H-10 5%, butanediol 5%, avenabeta glucosan 2%, betanin 0.2%, ethoxy urea 1%, milk protein 0.3%, lactobacillus/Punica granatum L. tunning extract 1%, Asterias amurensis Lutken elite 1%, allantoin 0.05%, hyaluronate sodium 0.05%, antiseptic 0.5% and essence 0.01%.
Described antiseptic is made up of according to weight ratio 1:5 methyl hydroxybenzoate and phenoxyethanol.
preparation method:s1. water, glycerol, propylene glycol, butanediol, avenabeta glucosan, betanin, ethoxy urea, allantoin, Natrulon H-10 and hyaluronate sodium are added in agitated kettle, homogenizing 5min, be heated to 75 DEG C, be stirred to material dissolution complete;
S2. continue to stir cooling and be down to 40 DEG C, add milk protein, lactobacillus/Punica granatum L. tunning extract and Asterias amurensis Lutken elite, be stirred to system even;
S3. finally add the mixture of antiseptic and essence, stir, get final product discharging, obtain crease-resistant cosmetic water.
embodiment 2, the crease-resistant cosmetic water of the present invention and preparation thereof
formula:be made up of the raw material of following weight percent meter: water 81.17%, glycerol 5%, propylene glycol 5%, Natrulon H-10 2%, butanediol 2%, avenabeta glucosan 0.5%, betanin 1%, ethoxy urea 0.2%, milk protein 1.5%, lactobacillus/Punica granatum L. tunning extract 0.3%, Asterias amurensis Lutken elite 0.3%, allantoin 0.2%, hyaluronate sodium 0.01%, antiseptic 0.8% and essence 0.02%.
Described antiseptic is made up of according to weight ratio 1:5 methyl hydroxybenzoate and phenoxyethanol.
preparation method:s1. water, glycerol, propylene glycol, butanediol, avenabeta glucosan, betanin, ethoxy urea, allantoin, Natrulon H-10 and hyaluronate sodium are added in agitated kettle, homogenizing 10min, be heated to 85 DEG C, be stirred to material dissolution complete;
S2. continue to stir cooling and be down to 50 DEG C, add milk protein, lactobacillus/Punica granatum L. tunning extract and Asterias amurensis Lutken elite, be stirred to system even;
S3. finally add the mixture of antiseptic and essence, stir, get final product discharging, obtain crease-resistant cosmetic water.
embodiment 3, the crease-resistant cosmetic water of the present invention and preparation thereof
formula:be made up of the raw material of following weight percent meter: water 81.07%, glycerol 4%, propylene glycol 3%, Natrulon H-10 4%, butanediol 3%, avenabeta glucosan 1%, betanin 0.6%, ethoxy urea 0.5%, milk protein 1%, lactobacillus/Punica granatum L. tunning extract 0.6%, Asterias amurensis Lutken elite 0.5%, allantoin 0.1%, hyaluronate sodium 0.02%, antiseptic 0.6% and essence 0.01%.
Described antiseptic is made up of according to weight ratio 1:5 methyl hydroxybenzoate and phenoxyethanol.
preparation method:s1. water, glycerol, propylene glycol, butanediol, avenabeta glucosan, betanin, ethoxy urea, allantoin, Natrulon H-10 and hyaluronate sodium are added in agitated kettle, homogenizing 8min, be heated to 80 DEG C, be stirred to material dissolution complete;
S2. continue to stir cooling and be down to 45 DEG C, add milk protein, lactobacillus/Punica granatum L. tunning extract and Asterias amurensis Lutken elite, be stirred to system even;
S3. finally add the mixture of antiseptic and essence, stir, get final product discharging, obtain crease-resistant cosmetic water.
embodiment 4, the crease-resistant cosmetic water of the present invention and preparation thereof
formula:be made up of the raw material of following weight percent meter: water 79.37%, glycerol 4%, propylene glycol 3%, Natrulon H-10 4%, butanediol 3%, avenabeta glucosan 1%, betanin 0.6%, ethoxy urea 0.5%, milk protein 1%, lactobacillus/Punica granatum L. tunning extract 0.6%, Asterias amurensis Lutken elite 0.5%, leaf of Herb Gynostemmae Pentaphylli extract 0.6%, arctic Ascophyllum nodosum elite 0.6%, the youth algae 0.5%, allantoin 0.1%, hyaluronate sodium 0.02%, antiseptic 0.6% and essence 0.01%.
Described antiseptic is made up of according to weight ratio 1:5 methyl hydroxybenzoate and phenoxyethanol.
preparation method:s1. water, glycerol, propylene glycol, butanediol, avenabeta glucosan, betanin, ethoxy urea, allantoin, Natrulon H-10 and hyaluronate sodium are added in agitated kettle, homogenizing 8min, be heated to 80 DEG C, be stirred to material dissolution complete;
S2. continue stir cooling be down to 45 DEG C, add milk protein, lactobacillus/Punica granatum L. tunning extract, Asterias amurensis Lutken elite, leaf of Herb Gynostemmae Pentaphylli extract, arctic Ascophyllum nodosum elite and the youth algae, be stirred to system even;
S3. finally add the mixture of antiseptic and essence, stir, get final product discharging, obtain crease-resistant cosmetic water.
embodiment 5, the crease-resistant cosmetic water of the present invention and preparation thereof
formula:be made up of the raw material of following weight percent meter: water 78.07%, glycerol 4%, propylene glycol 3%, Natrulon H-10 4%, butanediol 3%, avenabeta glucosan 1%, betanin 0.6%, ethoxy urea 0.5%, milk protein 1%, lactobacillus/Punica granatum L. tunning extract 0.6%, Asterias amurensis Lutken elite 0.5%, leaf of Herb Gynostemmae Pentaphylli extract 1%, arctic Ascophyllum nodosum elite 1%, the youth algae 1%, allantoin 0.1%, hyaluronate sodium 0.02%, antiseptic 0.6% and essence 0.01%.
Described antiseptic is made up of according to weight ratio 1:5 methyl hydroxybenzoate and phenoxyethanol.
Preparation method is with embodiment 4.
Do testing performance index to the crease-resistant cosmetic water of embodiment 1 ~ 5, its test result is as follows:
1, pH value: 5.5 ~ 7.0;
2, viscosity :≤300mpa;
3, heat-resistant stability investigates (45 DEG C × 24h): qualified;
4, cold-resistant study on the stability (-15 DEG C × 24h): qualified.
comparative example 1,
formula:be made up of the raw material of following weight percent meter: water 81.07%, glycerol 4%, propylene glycol 3%, Natrulon H-10 4%, butanediol 3%, avenabeta glucosan 1%, betanin 0.6%, ethoxy urea 0.5%, milk protein 1%, lactobacillus/Punica granatum L. tunning extract 1.1%, allantoin 0.1%, hyaluronate sodium 0.02%, antiseptic 0.6% and essence 0.01%.
Described antiseptic is made up of according to weight ratio 1:5 methyl hydroxybenzoate and phenoxyethanol.
Preparation method is with reference to embodiment 3.
comparative example 2,
formula:be made up of the raw material of following weight percent meter: water 82.19%, glycerol 4%, propylene glycol 3%, Natrulon H-10 4%, butanediol 3%, betanin 0.6%, ethoxy urea 0.5%, milk protein 1%, lactobacillus/Punica granatum L. tunning extract 0.6%, Asterias amurensis Lutken elite 0.5%, antiseptic 0.6% and essence 0.01%.
Described antiseptic is made up of according to weight ratio 1:5 methyl hydroxybenzoate and phenoxyethanol.
Preparation method is with reference to embodiment 3.
test example one, Product Safety evaluation (experiment of human body skin patch)
One, trial target: the crease-resistant cosmetic water that embodiment 1 ~ 5, comparative example 1 ~ 2 prepare
Tested crowd's number: 70 people, women
Age: between 20 ~ 50 years old
Health status: subjects skin is healthy, without dermatosis allergies, meets experimenter and volunteers inclusion criteria.
Grouping: 7 groups, often organize 10 people, 28 ± 2 years old mean age.
Two, patch method: select qualified speckle examination device, with closed patch experiment method, tested material being about 0.020mL ~ 0.025mL drips in speckle examination device, external special adhesive tape is covered on experimenter back, tested material is removed after 24 hours, within after removing respectively 0.5,6,12,24,48 hour, observe dermoreaction, according to its result of dermoreaction grade scale record in " cosmetics health specification ".
Three, experimental result: human skin patch result shows: each group experimenter is by the patch test of the crease-resistant cosmetic water of embodiment 1 ~ 5, comparative example 1 ~ 2, dermoreaction is observed at 0.5,6,12,24,48 hour, wherein there is skin adverse reaction in 0 example, the crease-resistant cosmetic water use safety described in explanation.
test example two, product effect assessment
part I:
One, trial target: the crease-resistant cosmetic water that embodiment 1 ~ 5, comparative example 1 ~ 2 prepare
Two, tested crowd
Sex number: female, 70 people
Age: between 20 ~ 40 years old
Health status: subjects skin is healthy, without dermatosis allergies, meets experimenter and volunteers inclusion criteria.
Grouping: be divided into 7 groups, often organize 10 people, 28 ± 2 years old mean age.
Three, method of testing: experimenter uses Fes Kai Er SK-III skin moisture detector to test the moisture of forehead, left face, right face and chin skin respectively after using clean water face, and get arithmetic mean of instantaneous value, experimenter re-uses above-mentioned crease-resistant cosmetic water, uniform application is in face, pat gently, by the skin moisture content of skin moisture tester test forehead, left face, right face and the same position of chin after 10min, and get arithmetic mean of instantaneous value, re-use skin moisture tester after 12h and test one time.Often organize 10 experimenters and tested result is got arithmetic mean of instantaneous value.
Four, test result is as following table 1.
Wherein, skin average moisture before skin average moisture-use cosmetic water is used after cosmetic water 10min after skin moisture content gradient=use cosmetic water 10min;
To use after cosmetic water 12h after skin moisture content gradient=use cosmetic water 12h skin average moisture before skin average moisture-use cosmetic water.
Table 1 skin moisture content table with test results
From upper table 1:
(1) moisturizing of the crease-resistant cosmetic water of the embodiment of the present invention 1 ~ 5, moistening effect are good, can not only significantly improve skin moisture content, also can pin moisture, make skin keep long-acting water to moisten after using.Wherein with the moisturizing of the crease-resistant cosmetic water of embodiment 4, moistening effect the best.
(2) embodiment 4 and embodiment 5 all containing leaf of Herb Gynostemmae Pentaphylli extract, arctic Ascophyllum nodosum elite and the youth algae, its effect is better than embodiment 1 ~ 3, illustrate leaf of Herb Gynostemmae Pentaphylli extract, arctic Ascophyllum nodosum elite and the youth algae and milk protein, lactobacillus/Punica granatum L. tunning extract, Asterias amurensis Lutken elite etc. there is synergism.
(3) comparative example 1 lacks some component with comparative example 2 compared with embodiment 3, and its moisturizing guarantor, wet effect, all not as embodiment 3, illustrate that each component of the crease-resistant cosmetic water of the present invention is worked in coordination with, play good moisturizing, moistening effect.
part II:
One, trial target: the crease-resistant cosmetic water prepared by embodiment 1 ~ 5, comparative example 1 ~ 2
Two, tested crowd
Sex number: female, 210 people
Age: between 20 ~ 50 years old
Health status: subjects skin is healthy, without dermatosis allergies, meets experimenter and volunteers inclusion criteria.
Grouping: be divided into 7 groups, often organize 30 people, 28 ± 2 years old mean age.
Three, method of testing: respectively use-case 1 ~ 5, crease-resistant cosmetic water prepared by comparative example 1 ~ 2, observes and experiences result of use.Using method: after experimenter cleans face, by above-mentioned crease-resistant cosmetic water uniform application in face, pats gently to skin and all absorbs, the every day of each use sooner or later once, adhere to use one month, at least check weekly once to understand with or without whole body and local untoward reaction, and itemized record result.
Four, testing evaluation result is as follows:
(one month) on probation feedback conclusive table of the crease-resistant cosmetic water of table 2 embodiment 1
(one month) on probation feedback conclusive table of the crease-resistant cosmetic water of table 3 embodiment 2
(one month) on probation feedback conclusive table of the crease-resistant cosmetic water of table 4 embodiment 3
(one month) on probation feedback conclusive table of the crease-resistant cosmetic water of table 5 embodiment 4
(one month) on probation feedback conclusive table of the crease-resistant cosmetic water of table 6 embodiment 5
(one month) on probation feedback conclusive table of table 7 comparative example 1 cosmetic water
(one month) on probation feedback conclusive table of table 8 comparative example 2 cosmetic water
(1) from upper table 2 ~ 6, crease-resistant cosmetic water the liking and approving extensively by experimenter of embodiment 1 ~ 5, illustrates the gentle pro-skin of the crease-resistant cosmetic water of the present invention, easily absorbs, and uses rear face salubrious not sticky, moisturizing, moistening effect are good, to skin supply nutrition, promote skin metabolism, thus effectively reduce wrinkle, delay skin aging, and long-acting moisturizing, skin beauty water is moistened smooth, flexible.In embodiment 1 ~ 5, the degree of recognition of the crease-resistant cosmetic water of embodiment 4 is the highest, and therefore embodiment 4 is preferred embodiment.
(2) from upper table 7 ~ 8, the result of use of comparative example 1 and comparative example 2 cosmetic water is all not as embodiment 1 ~ 5, illustrate that the present invention's crease-resistant cosmetic water formula is not obtained by the simple combination of each component, then further illustrate between each component of formula of the present invention and there is synergism.
There is not people to occur allergic phenomena in whole experimenter simultaneously, all do not occur the situations such as skin pruritus, twinge, redness yet.Therefore, the gentle safety of the crease-resistant cosmetic water of the present invention, can life-time service.
Above-described embodiment is illustrative principle of the present invention and effect thereof only, but not for limiting the present invention.Any person skilled in the art scholar all without prejudice under spirit of the present invention and category, can modify above-described embodiment or changes.Therefore, such as have in art usually know the knowledgeable do not depart from complete under disclosed spirit and technological thought all equivalence modify or change, must be contained by claim of the present invention.
Claims (6)
1. a crease-resistant cosmetic water, it is characterized in that, comprise the raw material of following weight percent meter: water 72 ~ 85%, glycerol 2 ~ 5%, propylene glycol 2 ~ 5%, Natrulon H-10 2 ~ 5%, butanediol 2 ~ 5%, avenabeta glucosan 0.5 ~ 2%, betanin 0.2 ~ 1%, ethoxy urea 0.2 ~ 1%, milk protein 0.3 ~ 1.5%, lactobacillus/Punica granatum L. tunning extract 0.3 ~ 1%, Asterias amurensis Lutken elite 0.3 ~ 1%, allantoin 0.05 ~ 0.2%, hyaluronate sodium 0.01 ~ 0.05%, antiseptic 0.2 ~ 1% and essence 0.01 ~ 0.02%.
2. crease-resistant cosmetic water as claimed in claim 1, is characterized in that, described crease-resistant cosmetic water also comprise the leaf of Herb Gynostemmae Pentaphylli extract 0.3 ~ 1% of weight percent meter, arctic Ascophyllum nodosum elite 0.3 ~ 1% and the youth algae 0.3 ~ 1%.
3. crease-resistant cosmetic water as claimed in claim 1, is characterized in that, described antiseptic is the compositions of methyl hydroxybenzoate and phenoxyethanol, and the weight ratio of described methyl hydroxybenzoate and phenoxyethanol is 1:5.
4. crease-resistant cosmetic water as claimed in claim 2, it is characterized in that, described crease-resistant cosmetic water is made up of the raw material of following weight percent meter: water 79.37%, glycerol 4%, propylene glycol 3%, Natrulon H-10 4%, butanediol 3%, avenabeta glucosan 1%, betanin 0.6%, ethoxy urea 0.5%, milk protein 1%, lactobacillus/Punica granatum L. tunning extract 0.6%, Asterias amurensis Lutken elite 0.5%, leaf of Herb Gynostemmae Pentaphylli extract 0.6%, arctic Ascophyllum nodosum elite 0.6%, the youth algae 0.5%, allantoin 0.1%, hyaluronate sodium 0.02%, antiseptic 0.6% and essence 0.01%.
5. prepare a method for crease-resistant cosmetic water as claimed in claim 1, it is characterized in that, comprise the following steps:
S1. water, glycerol, propylene glycol, butanediol, avenabeta glucosan, betanin, ethoxy urea, allantoin, Natrulon H-10 and hyaluronate sodium are added in agitated kettle, homogenizing 5 ~ 10min, be heated to 75 ~ 85 DEG C, be stirred to material dissolution complete;
S2. continue to stir cooling and be down to 40 ~ 50 DEG C, add milk protein, lactobacillus/Punica granatum L. tunning extract and Asterias amurensis Lutken elite, be stirred to system even;
S3. finally add the mixture of antiseptic and essence, stir, get final product discharging, obtain crease-resistant cosmetic water.
6. the preparation method of crease-resistant cosmetic water as claimed in claim 5, is characterized in that, also comprise in described step S2 add leaf of Herb Gynostemmae Pentaphylli extract, arctic Ascophyllum nodosum elite and the youth algae.
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| CN110711166A (en) * | 2019-11-03 | 2020-01-21 | 广州悦荟化妆品有限公司 | Toner with oil control and moisture retention effects |
| CN114344202A (en) * | 2022-03-02 | 2022-04-15 | 法国科兰黎化妆品实验室 | Anti-aging composition, skin care product and cosmetic |
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