CN109288716A - A kind of toner - Google Patents
A kind of toner Download PDFInfo
- Publication number
- CN109288716A CN109288716A CN201811467991.9A CN201811467991A CN109288716A CN 109288716 A CN109288716 A CN 109288716A CN 201811467991 A CN201811467991 A CN 201811467991A CN 109288716 A CN109288716 A CN 109288716A
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- CN
- China
- Prior art keywords
- water
- oat
- toner
- oat composition
- composition
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/35—Ketones, e.g. benzophenone
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4906—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/645—Proteins of vegetable origin; Derivatives or degradation products thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/65—Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9728—Fungi, e.g. yeasts
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
Abstract
The present invention relates to a kind of toner, which is made using glycerol, propylene glycol, oat composition, UVNUL MS-40, trehalose, dried tremella extract, Rosmarinus officinalis extract, water-solubleazone, collagen, preservative, essence and water by raw material.Toner of the invention has efficient Scavenging ability, is excellent in anti-aging aspect of performance, and is suitable for all kinds of skins.
Description
Technical field
The present invention relates to cosmetic field, in particular to a kind of toner.
Background technique
With the raising of quality of the life, consumer increasingly payes attention to skin nursing, and cosmetics are increasingly becoming current consumption
Product, for moisturizing, whitening, Sage Extract, anti-oxidant, wherein anti-oxidant particularly important.The aging of medical field studies have shown that 80%
Phenomenon is because of caused by " free radical " in environment, due to the destruction of free radical, make the cell for maintaining skin-balance be destroyed and
It reduces, Skin Cell immunocompetence declines rapidly, so as to cause skin aging and lesion.
Oat component is often used to be added in cosmetics, if oat polypeptide is for removing free radical, avenabeta glucosan
For cell repair etc..But the use both in Traditional makeup formula is simply to pass through mixing addition as raw material
Into cosmetics, so the Scavenging ability of cosmetics can be limited by the Scavenging ability of oat polypeptide itself, very
Hardly possible breakthrough achievees the effect that more efficient.
Summary of the invention
In order to overcome the deficiencies of the prior art, the purpose of the present invention is to provide a kind of toners, and the toner is by following matter
The group of amount percentages is grouped as:
Glycerol 1.0-5.0%
Propylene glycol 0.5-3.0%
Oat composition 2.0-6.0%
UVNUL MS-40 0.5%
Trehalose 1.0-3.0%
Dried tremella extract 2.0-4.0%
Rosmarinus officinalis extract 0.1-0.4%
Water-solubleazone 0.5-1.0%
Collagen 0.1-0.5%
Preservative 0.2%
Essence 0-0.05%
Surplus is water.
Wherein, the oat composition is prepared by following methods: avenin, avenabeta glucosan being taken to be dissolved in water
In, heating carries out Maillard reaction, when grafting degree reaches 10-15%, controls feed liquid temperature to the operative temperature of protease, adds
Enter protease, be stirred enzymatic hydrolysis, is then heated to boiling enzyme deactivation 15min, removal solid insoluble, freezing are separated by solid-liquid separation after cooling
It is dried to obtain oat composition；Avenin, avenabeta glucosan and the water adds according to the mass ratio of 1:0.2-5:10-50
Add；The Maillard reaction temperature is 40-100 DEG C, preferably 45-50 DEG C.
The preservative is selected from parabens or Jie Ma-BP.
The present invention also provides the preparation method of above-mentioned toner, the preparation method the following steps are included:
(1) water is preheated to 70-80 DEG C, be added under stirring condition glycerol, propylene glycol, oat composition, UVNUL MS-40, trehalose,
Dried tremella extract, Rosmarinus officinalis extract are cooled to 50-60 DEG C of formation A phase until each raw material is completely dissolved；
(2) collagen, water-solubleazone, preservative and essence are sequentially added in 50-60 DEG C of A phase, the process of charging is protected
Stirring is held, after each raw material is completely dissolved into pellucidity, is cooled to 40 DEG C or less；
(3) toner finished product is dispensed to obtain.
Toner of the invention has the advantage that
(1) two kinds of raw materials of oat polypeptide and avenabeta glucosan are often used in traditional toner formula, each serve as removing freely
Base and the effect for carrying out cell repair, and present invention uses the oat compositions being prepared through special process, although also with
Avenabeta glucosan is raw material, and the structure containing oat polypeptide, but oat composition ratio of the invention is by oat polysaccharide and swallow
Wheat beta glucan is directly added as raw material has higher free radical scavenging ability, shows in terms of anti-aging powerful excellent
Gesture；
(2) further, the oat composition in the present invention is the technique preparation by protease hydrolyzed after first Maillard reaction
It obtains, on the one hand, avenin and avenabeta glucosan are first carried out Maillard reaction grafting by the preparation process, are then carried out again
Enzymatic hydrolysis, rather than Maillard reaction is first carried out again to avenin enzymatic hydrolysis, it can be with effective protection by digesting the polypeptide structure generated
Bioactivity, comparison discovery, the free radical scavenging ability for first digesting again the oat composition of Maillard reaction only have Shen of the present invention
The 1/2-3/4 of oat composition please, conjecture is the possible reason is the oat polypeptide structure for first digesting generation is drawn in subsequent beauty
Cause the active structure of polypeptide to be destroyed due to taking part in reaction etc. hygrothermal environment and active function groups in moral reaction, leads
Cause free radical scavenging ability relatively low.On the other hand the preparation process digested after first Maillard reaction also helps oat combination
The control of object Maillard reaction degree, because the deeper Maillard reaction degree not the better, the too deep extent of reaction makes oat group
Closing the solvability of object in water reduces, and molecular weight is big, is unfavorable for the osmotic absorption of skin.And protease hydrolyzed makes oat
Albumen exposes more aminoterminals, is easy to participate in Maillard reaction, to be unfavorable for the control of the extent of reaction.The most most
Excellent effect, Maillard reaction stage grafting degree are controlled in 10-15%, and oat composition is enabled to have efficient freedom again
While base Scavenging activity, rapid osmotic skin, effectively progress cell repair；
(3) it in addition, the present invention is when being formulated design, is sent out after oat composition is carried out compatible use with Rosmarinus officinalis extract
Synergistic effect is waved, hence it is evident that enhance radicals scavenging effect, skin care effect, which is significantly better than, is individually added into rosemary
Extract, oat polypeptide, oat composition toner.
Specific embodiment
Below in conjunction with specific example, the following further describes the technical solution of the present invention.
Embodiment 1
Oat composition in the embodiment is prepared as follows: avenin, avenabeta glucosan and water are according to 1:0.2:
10 mass ratio mixing, is heated to 50 DEG C of progress Maillard reactions, until grafting degree 12.3%, reduces temperature to 45 DEG C, albumen is added
Enzyme is stirred enzymatic hydrolysis to degree of hydrolysis and reaches 10%, is heated to boiling enzyme deactivation 15min, it is insoluble that removal solid is separated by solid-liquid separation after cooling
Object, freeze-drying obtain oat composition.
As control, the present embodiment has also been prepared as follows oat composition reference material: avenin and water according to
The mass ratio of 1:10 mixes, and is preheated to 45 DEG C, and addition protease, which is digested to degree of hydrolysis, reaches 10%, is heated to boiling enzyme deactivation
15min reduces temperature to 50 DEG C, based on the quality of the avenin of original addition, gathers according to avenin and oat β-Portugal
Avenabeta glucosan is added in the mass ratio of sugared 1:0.2, carries out Maillard reaction, equally reaches 12.3% to grafting degree, after cooling admittedly
Liquid separation removal solid insoluble, freeze-drying obtain oat composition reference material.
It is purged the measurement of DPPH ability, the IC50 of oat composition is the 3/4 of oat composition reference material IC50, it is seen that
The free radical scavenging ability of oat composition reference material about only has the 3/4 of oat composition.
The present embodiment toner and reference examples skin toner is made according to table 1 in oat composition and oat composition reference material
Water, after tested, the free radical scavenging ability of embodiment are 1.3 times of reference examples.
1 embodiment of table, 1 skin toner water constituent forms table
The toner of embodiment and reference examples is prepared as follows:
(1) water is preheated to 70-80 DEG C, and glycerol, propylene glycol, oat composition are added under stirring condition, and (reference examples add oat group
Close object reference material), UVNUL MS-40, trehalose, dried tremella extract, Rosmarinus officinalis extract be cooled to until each raw material is completely dissolved
50-60 DEG C of formation A phase；
(2) collagen, water-solubleazone, propylben and essence, the mistake of charging are sequentially added in 50-60 DEG C of A phase
Journey is kept stirring, and after each raw material is completely dissolved into pellucidity, is cooled to 40 DEG C or less；
(3) toner finished product is dispensed to obtain.
Embodiment 2
Oat composition in the embodiment is prepared as follows: avenin, avenabeta glucosan and water are according to 1:1:20
Mass ratio mixing, be heated to 50 DEG C of progresss Maillard reactions, until grafting degree 11.0%, reduce temperature to 45 DEG C, addition albumen
Enzyme is stirred enzymatic hydrolysis to degree of hydrolysis and reaches 10%, is heated to boiling enzyme deactivation 15min, it is insoluble that removal solid is separated by solid-liquid separation after cooling
Object, freeze-drying obtain oat composition.
The present embodiment and the skin toner water constituent of reference examples are formed in ratio shown in table 2.
2 embodiment of table, 2 skin toner water constituent forms table
The free radical scavenging ability of embodiment and cell repair ability are set to 1, the free radical scavenging ability of each reference examples such as table 3
It is shown:
3 embodiment of table is compared with the ability of reference examples
It can be seen that from the comparison of embodiment and reference examples 1 and compare oat polypeptide in free radical scavenging ability using oat composition
There is significant sexual clorminance with avenabeta glucosan, and cell repair ability is also basic with the reference examples of addition avenabeta glucosan
Unanimously.
It can be seen that oat composition from the comparison of embodiment, reference examples 2, reference examples 3 and reference examples 4 or oat be more
Peptide and rosemary carry out compatible use, have significant synergy in terms of free radical scavenging ability, have anti-ageing well
Old ability.
Claims (4)
1. a kind of toner, it is characterised in that be grouped as by the group of following mass percent meter:
Glycerol 1.0-5.0%
Propylene glycol 0.5-3.0%
Oat composition 2.0-6.0%
UVNUL MS-40 0.5%
Trehalose 1.0-3.0%
Dried tremella extract 2.0-4.0%
Rosmarinus officinalis extract 0.1-0.4%
Water-solubleazone 0.5-1.0%
Collagen 0.1-0.5%
Preservative 0.2%
Essence 0-0.05%
Surplus is water；
The oat composition is successively prepared through Maillard reaction and protease hydrolyzed by avenin and avenabeta glucosan
It obtains.
2. toner according to claim 1, it is characterised in that the preservative is parabens or Jie Ma-BP.
3. toner according to claim 1, it is characterised in that the oat composition is prepared by following methods:
Take avenin, avenabeta glucosan soluble in water, heating carries out Maillard reaction, when grafting degree reaches 10-15%,
The operative temperature of feed liquid temperature to protease is controlled, protease is added, is stirred enzymatic hydrolysis, is then heated to boiling enzyme deactivation 15min,
Removal solid insoluble is separated by solid-liquid separation after cooling, freeze-drying obtains oat composition；The avenin, oat β-Portugal are poly-
Sugar and water are added according to the mass ratio of 1:0.2-5:10-50；The Maillard reaction temperature is 40-100 DEG C, preferably 45-50
℃。
4. a kind of preparation method of toner as described in claim 1, feature the following steps are included:
(1) water is preheated to 70-80 DEG C, be added under stirring condition glycerol, propylene glycol, oat composition, UVNUL MS-40, trehalose,
Dried tremella extract, Rosmarinus officinalis extract are cooled to 50-60 DEG C of formation A phase until each raw material is completely dissolved；
(2) collagen, water-solubleazone, preservative and essence are sequentially added in 50-60 DEG C of A phase, the process of charging is protected
Stirring is held, after each raw material is completely dissolved into pellucidity, is cooled to 40 DEG C or less；
(3) toner finished product is dispensed to obtain.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811467991.9A CN109288716A (en) | 2018-12-03 | 2018-12-03 | A kind of toner |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811467991.9A CN109288716A (en) | 2018-12-03 | 2018-12-03 | A kind of toner |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109288716A true CN109288716A (en) | 2019-02-01 |
Family
ID=65142368
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811467991.9A Withdrawn CN109288716A (en) | 2018-12-03 | 2018-12-03 | A kind of toner |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109288716A (en) |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105168112A (en) * | 2015-10-19 | 2015-12-23 | 广州科玛生物科技有限公司 | Anti-wrinkle toner and preparation method thereof |
| CN106176276A (en) * | 2016-09-27 | 2016-12-07 | 广东丸美生物技术股份有限公司 | A kind of have defying age and the skin matrix of antiallergic effect and preparation and application thereof |
-
2018
- 2018-12-03 CN CN201811467991.9A patent/CN109288716A/en not_active Withdrawn
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105168112A (en) * | 2015-10-19 | 2015-12-23 | 广州科玛生物科技有限公司 | Anti-wrinkle toner and preparation method thereof |
| CN106176276A (en) * | 2016-09-27 | 2016-12-07 | 广东丸美生物技术股份有限公司 | A kind of have defying age and the skin matrix of antiallergic effect and preparation and application thereof |
Non-Patent Citations (3)
| Title |
|---|
| 孔保华等: ""美拉德反应产物抗氧化机理及影响因素的研究进展"", 《东北农业大学学报》 * |
| 王建新: "《化妆品植物原料大全》", 30 June 2012, 中国纺织出版社 * |
| 陈世超: ""燕麦蛋白质与β-葡聚糖在不同体系中美拉德反应的研究"", 《中国优秀硕士学位论文全文数据库 工程科技Ⅰ辑》 * |
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| WW01 | Invention patent application withdrawn after publication |
Application publication date: 20190201 |
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