CN107334714B - Snail facial mask containing snail secretion filtrate and active peptide and preparation method thereof - Google Patents
Snail facial mask containing snail secretion filtrate and active peptide and preparation method thereof Download PDFInfo
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/494—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
- A61K8/4946—Imidazoles or their condensed derivatives, e.g. benzimidazoles
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
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- A61K8/678—Tocopherol, i.e. vitamin E
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- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
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- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
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- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/99—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from microorganisms other than algae or fungi, e.g. protozoa or bacteria
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- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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Abstract
The invention belongs to the field of cosmetics, and particularly relates to a preparation method of a snail facial mask containing snail secretion filtrate and active peptide. The components of the facial mask comprise water, glycerol, propylene glycol, snail secretion filtrate, lactobacillus fermentation lysate, hexapeptide-1, tocopherol, hyaluronic acid, dipotassium glycyrrhizinate, allantoin, EDTA disodium and propyl benzoate which are used as raw materials. The snail facial mask provided by the invention is suitable for the skin with water deficiency, dryness and large pores.
Description
Technical Field
The invention mainly belongs to the field of cosmetics, and particularly relates to a snail facial mask containing snail secretion filtrate and active peptide and a preparation method thereof.
Background
As early as in ancient Hizirca, the father of medicine, "Xibo Kela Zi", has used snails in medical therapy as a dietary therapy for whooping cough and gastric ulcer. The Bascunan family of Chilean (Bascunan family) began to breed snails in the year 1980 and exported in large quantities to Europe as a cooking holy. However, in handling the snails, they found that the skin of the worker became soft, and, when the worker was cut by the snail cage, it was very surprising to find that the wound healed quickly and did not infect, nor did the worker leave scars. At this time, the person who is one member of the bethan family-feinanduo bethan (ferando basicnan) is a student of medical department, and accurate scientific research for 15 years is carried out on chile 'Helix Aspersa Muller spiral snail', so that the extract can promote the repair of the skin and soften the skin; and applied for world patent, officially listed in Chile in 1995, and has raised a wind tide of 'natural regeneration' in various countries. Recently, snail mucus and snail enzyme have been widely used in cosmetics because of the natural collagen, elastin, allantoin, protein, multivitamins, glycolic acid, natural antimicrobial agents, etc.
However, most of the snail mucus and helicase used in the existing cosmetics are obtained by making the snail climb on a rough surface to secrete more mucus. There is a problem that the mucus obtained by this method contains a small amount of enzyme species and is poor in the effect of use. In addition, in the existing facial mask preparation process, only the snail mucus and the snail enzyme are simply mixed and stirred with other components, and the obtained facial mask liquid cannot be uniformly emulsified, or even if the intermolecular combination of the components of the obtained emulsion is poor, the mixing state is unstable, the components are easy to decompose and deteriorate, and the use effect is seriously influenced.
Disclosure of Invention
In order to solve the problems, the invention provides a snail facial mask containing snail secretion filtrate and active peptide and a preparation method thereof.
The invention is realized by the following technical scheme:
the invention has the beneficial technical effects that:
(1) the snail secretion filtrate of the present invention is obtained by stimulating the treble sacs and digestive tract of snails, and contains more enzymes and has a higher nutritional value than snail mucus obtained by snails crawling on rough surfaces.
(2) The preparation method of the invention controls the temperature, the stirring strength and the stirring time in the process of mixing and stirring the snail secretion filtrate and other components, so that the snail mucus and other components are fully emulsified, and the components are stably combined with each other.
Drawings
FIG. 1 is a schematic flow chart of a preparation method of the invention.
Detailed Description
In order to make the objects, technical solutions and advantages of the present invention more apparent, the present invention is described in further detail below with reference to the accompanying drawings and embodiments. It should be understood that the specific embodiments described herein are merely illustrative of the invention and are not intended to limit the invention.
On the contrary, the invention is intended to cover alternatives, modifications, equivalents and alternatives which may be included within the spirit and scope of the invention as defined by the appended claims. Furthermore, in the following detailed description of the present invention, certain specific details are set forth in order to provide a better understanding of the present invention. It will be apparent to one skilled in the art that the present invention may be practiced without these specific details.
Example 1
A preparation method of a snail mask containing snail secretion filtrate and active peptide comprises the following steps:
heating and stirring: mixing water, glycerol, propylene glycol, snail secretion filtrate, lactobacillus fermentation lysate, hexapeptide-1, tocopherol, hyaluronic acid, dipotassium glycyrrhizinate, allantoin, EDTA disodium and propyl benzoate in proportion, stirring under vacuum condition, controlling temperature to rise from room temperature to 60-80 deg.C during stirring process, and raising temperature rate to 0.1-1 deg.C/min;
stirring at constant temperature: stirring for 2-5h at 60-80 deg.C;
degassing and stirring: degassing the mixed solution, and cooling to 30-40 deg.C;
and (3) continuously stirring: stirring at 30-40 deg.C for 0.5-3 h;
standing and aging: cooling to room temperature, and standing for 12-48 h.
Further, the preparation method of the snail secretion filtrate comprises the following steps:
stimulation of snail mucus secretion: the snail is placed in a box body to collect mucus, various pictures with sharp objects are arranged around the box body, or the box body is made of transparent materials, various objects with sharp parts are arranged around the outside of the box body, the snail is stimulated to secrete the mucus under the condition of not damaging the snail, and the mucus is collected;
extracting filtrate: collecting mucus, centrifuging at high speed to break mucus cell, and collecting supernatant to obtain snail secretion filtrate containing snail active enzyme.
Furthermore, during the preparation of the snail secretion filtrate, the temperature of mucus needs to be kept within 0-5 ℃, and during the centrifugation, the temperature needs to be kept below-3-6 ℃ to avoid the temperature rise during the centrifugation.
Further, the storage temperature of the collected mucus is within 0-5 ℃.
Further, the stimulating snail secretes mucus: the snail is placed in a box body to collect mucus, and the box body vibrates to stimulate the snail to secrete the mucus.
A snail facial mask containing snail secretion filtrate and polypeptide, each facial mask contains 30ml facial mask solution containing water, glycerol, propylene glycol, snail secretion filtrate, lactobacillus fermentation lysate, hexapeptide-1, tocopherol, hyaluronic acid, dipotassium glycyrrhizinate, allantoin, disodium EDTA, and propyl benzoate.
The using method comprises the following steps:
(1) cleaning facial skin, soaking a towel in hot water, wringing to dry, applying to facial skin, and holding for 2-3 min to remove towel;
(2) applying 5-6 drops of essential oil on facial skin, gently massaging for 3-5 min in a manner of making a loop on finger and abdomen, pressing with palm for 20-30 min, and cleaning with warm water.
The preparation method of the snail secretion filtrate comprises the following steps: stimulating snail to secrete mucus by physical method, collecting mucus, centrifuging at high speed to break mucus cell, and collecting supernatant to obtain snail secretion filtrate containing snail active enzyme. It should be noted that during the preparation of the snail secretion filtrate, the temperature of mucus needs to be kept within 0-5 ℃, so that during the centrifugation process, the operation needs to be carried out at minus 3-6 ℃ to avoid the temperature rise during the centrifugation process. Meanwhile, mucus is collected and cannot be refrigerated at low temperature, and partial helicase is easy to lose activity in the processes of refrigeration and subsequent thawing.
Wherein the physical methods include mechanical vibration, electrical stimulation, and the like.
Selecting materials:
glycerol: has the functions of moisture retention and moistening, and also has the special effects of high activity, oxidation resistance, alcoholization promotion and the like.
Propylene glycol: can be used as humectant, softening agent, and solvent in cosmetic.
Lactobacillus fermentation lysate: the modern biological fermentation and extraction technology is utilized, the active ingredients separated from the live bacteria cells of the live lactobacillus can improve the respiratory capacity of skin cells, make the cells more active, enhance ATP synthesis, enhance cell energy, promote the synthesis of collagen and hyaluronic acid of a human body, lighten wrinkles, reduce redness and allergy, diminish inflammation and relieve skin; can improve skin cell quality.
Hexapeptide-1: the active peptide can regulate and repair the skin, improve the elasticity of the skin, tighten and lubricate the skin and delay the generation of fine wrinkles on the skin
And (3) tocopherol: vitamin e (vitamin e) is a fat-soluble vitamin whose hydrolysate is tocopherol, one of the most important antioxidants.
Hyaluronic acid: it is also called as the poruric acid, which can keep the skin moisture, moisten the skin and hair, increase the luster, and prevent chapped skin and wrinkles.
Dipotassium glycyrrhizinate: the dipotassium glycyrrhizinate has multiple effects of bacteriostasis, inflammation diminishing, detoxification, anti-allergy, deodorization and the like.
Allantoin: the allantoin is an amphoteric compound, can combine with multiple substances to form double salt, has the effects of protecting from light, sterilizing, preventing corrosion, relieving pain, resisting oxidation, and keeping skin moisture, moistening and softening.
Disodium EDTA: a complexing agent is added into cosmetic for complexing some metal ions and stabilizing cosmetic.
Propyl benzoate: a preservative for cosmetics.
Example 2
This example is essentially the same as example 1, except for the method of stimulating the snail to secrete mucus.
Through experimental research, the inventor of the application finds that the snail which is stimulated by mechanical vibration or electrical stimulation and the like can not be directly injured by death, but the state of the snail which is stimulated by mechanical vibration or electrical stimulation is obviously changed, and when the stimulated snail and the normal snail are put together for culturing, the stimulated snail is easily eaten by other normal snails. Therefore, the snail after mechanical vibration or electrical stimulation can not be cultured normally, and the utilization rate of the snail is reduced.
In response to this problem, the present inventors tried other methods to stimulate the snail to secrete mucus. The observation shows that the snail walks on or near the sharp object and easily secretes mucus, and further shows that
The snail secretes mucus easily when seeing a sharp object.
Therefore, the method for stimulating the snail to secrete mucus in the embodiment is as follows:
the snail is placed in a box to collect the mucus. Various pictures with sharp objects are arranged around the box body, or
The box body is made of transparent material, and various objects with sharp parts, such as roses, cactus, thorns and the like, are arranged around the outside of the box body.
The method can stimulate snail to secrete mucus without damaging snail, and the collected snail can be further cultured normally.
Claims (1)
1. A preparation method of snail facial mask containing snail secretion filtrate and active peptide is characterized in that the components of the facial mask contain water, glycerol, propylene glycol, snail secretion filtrate, lactobacillus fermentation lysate, hexapeptide-1, tocopherol, hyaluronic acid, dipotassium glycyrrhizinate, allantoin, EDTA disodium and propyl benzoate;
the preparation method of the snail secretion filtrate comprises the following steps:
stimulation of snail mucus secretion: the snail is placed in a box body to collect mucus, various pictures with sharp objects are arranged around the box body, or the box body is made of transparent materials, various objects with sharp parts are arranged around the outside of the box body, the snail is stimulated to secrete the mucus under the condition of not damaging the snail, and the mucus is collected;
extracting filtrate: collecting mucus, centrifuging at high speed to break mucus cell, and collecting supernatant to obtain snail secretion filtrate containing snail active enzyme;
the preparation method of the snail mask comprises the following steps:
heating and stirring: mixing water, glycerol, propylene glycol, snail secretion filtrate, lactobacillus fermentation lysate, hexapeptide-1, tocopherol, hyaluronic acid, dipotassium glycyrrhizinate, allantoin, EDTA disodium and propyl benzoate in proportion, stirring under vacuum condition, controlling the temperature to rise from room temperature to T1 in the stirring process, wherein the temperature rise rate is 0.1-1 ℃/min;
stirring at constant temperature: stirring for 2-5h at the temperature of T1;
degassing and stirring: degassing the mixed solution, and cooling to T2 temperature;
and (3) continuously stirring: stirring for 0.5-3h at the temperature of T2;
standing and aging: cooling to room temperature, and standing for 12-48 h;
wherein T1 is 60-80 ℃; t2 is 30-40 ℃;
keeping the mucus within 0-5 ℃ in the preparation process of the snail secretion filtrate, and operating at-3 to-6 ℃ in the centrifugation process to avoid temperature rise in the centrifugation process;
the mucus is collected and stored at the temperature of 0-5 ℃.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201710502342.7A CN107334714B (en) | 2017-06-27 | 2017-06-27 | Snail facial mask containing snail secretion filtrate and active peptide and preparation method thereof |
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| CN201710502342.7A CN107334714B (en) | 2017-06-27 | 2017-06-27 | Snail facial mask containing snail secretion filtrate and active peptide and preparation method thereof |
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| CN107334714B true CN107334714B (en) | 2021-05-04 |
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| CN108852968A (en) * | 2018-08-09 | 2018-11-23 | 广州市瓷颜化妆品有限公司 | A kind of maintenance Essence and preparation method thereof of the filtrate of secretion containing snail |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20110027221A1 (en) * | 2002-07-01 | 2011-02-03 | Tianjin Sinobiotech Ltd. | Skincare Composition Comprising HSA Fusion Protein, Preparation Method And Uses Thereof |
| CN103860451A (en) * | 2014-04-01 | 2014-06-18 | 广东伊茗药业有限公司 | Functional skin care product containing snail mucus extractive and preparation method thereof |
| CN105496919A (en) * | 2015-12-21 | 2016-04-20 | 太仓张根木生物科技有限公司 | Snail mask with repairing and wrinkle reducing effects |
| CN106047517A (en) * | 2016-05-31 | 2016-10-26 | 太仓协大申泰羊毛衫有限公司 | Woolen sweater washing liquid containing snail extracting solution |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH02211143A (en) * | 1989-02-10 | 1990-08-22 | Shimada Phys & Chem Ind Co Ltd | Artificial internal ear |
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Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20110027221A1 (en) * | 2002-07-01 | 2011-02-03 | Tianjin Sinobiotech Ltd. | Skincare Composition Comprising HSA Fusion Protein, Preparation Method And Uses Thereof |
| CN103860451A (en) * | 2014-04-01 | 2014-06-18 | 广东伊茗药业有限公司 | Functional skin care product containing snail mucus extractive and preparation method thereof |
| CN105496919A (en) * | 2015-12-21 | 2016-04-20 | 太仓张根木生物科技有限公司 | Snail mask with repairing and wrinkle reducing effects |
| CN106047517A (en) * | 2016-05-31 | 2016-10-26 | 太仓协大申泰羊毛衫有限公司 | Woolen sweater washing liquid containing snail extracting solution |
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