CN106580762B - Have effects that comfort the crease-resistant composite skin care product of line, eye cream and preparation method thereof - Google Patents
Have effects that comfort the crease-resistant composite skin care product of line, eye cream and preparation method thereof Download PDFInfo
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
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Abstract
It is described to have effects that comforting the crease-resistant composite skin care product of line includes following components: Atlas cedar bark extract, nipa palm seed extract and astaxanthin the present invention relates to having effects that comfort the crease-resistant composite skin care product of line, eye cream and preparation method thereof；The mass ratio of the Atlas cedar bark extract, nipa palm seed extract and astaxanthin is 0.2-5:0.1-5:0.01-0.5.The present invention has effects that comfort the crease-resistant composite skin care product of line and applies and can provide more nutritional ingredients to eye skin on the whole in the formula of eye cream, it is easy to absorb, and stimulation to eye skin can be effectively reduced, eye wrinkle-removing is effectively removed or alleviated, skin moisturization and elasticity are improved.
Description
Technical field
The present invention relates to cosmetic fields, have effects that comfort the crease-resistant skin care item group compound of line, eye more particularly to a kind of
Frost and preparation method thereof.
Background technique
Wrinkle refers to that skin is influenced by external environment, forms free free radical, and free radical destroys normal cell membrane tissue
Interior collagen, active material, oxidative cell and the small microgroove, the wrinkle that are formed.Facial wrinkles are divided into atrophy wrinkle and hypertrophy
Wrinkle two types.Atrophy wrinkle refers to the wrinkle appeared on thin, easy jackknifing and dry skin, such as those nothings of circumference of eyes
The tiny wrinkle of number；Loose wrinkle refers to the wrinkle appeared in Oily, and quantity is few, and texture is close and deep.Wherein, eye
Skin is the most thin skin of human body, very careful and fragile, it is easy to come to harm.
In addition, existing eye cream ingredient emulsifier mainly based on emulsification system, can be added during preparing eye cream will
Oily to be mutually fused together with water phase, the emulsifier used on the market is largely artificial synthetic emulsifier, is easy to cause skin
The problems such as stimulation, allergy.Eye part skin can be more sensitive to stimulation, and researching and developing a mild non-stimulated eye cream has certain city
Field value.
Summary of the invention
Based on this, it is necessary to which providing a kind of has effects that comfort the crease-resistant composite skin care product of line, eye cream and preparation method thereof.
Specific technical solution is as follows:
It is a kind of to have effects that comfort the crease-resistant composite skin care product of line, it include following components: Atlas cedar bark extract, sea
Jujube seed extract and astaxanthin；The mass ratio of the Atlas cedar bark extract, nipa palm seed extract and astaxanthin is 0.2-
5:0.1-5:0.01-0.5.
It is described to have effects that comforting the crease-resistant composite skin care product of line further includes acetyl group six in wherein some embodiments
One of peptide -8, phytosterol, artemia extract or yeast extractive from fermentative are a variety of.
In wherein some embodiments, the Atlas cedar bark extract, nipa palm seed extract, astaxanthin and yeast hair
The mass ratio of ferment extract is 0.2-5:0.1-5:0.01-0.5:0.5-1.
In wherein some embodiments, the Atlas cedar bark extract, nipa palm seed extract, astaxanthin and yeast hair
The mass ratio of ferment extract is 1.2:1.5:0.2:0.8.
It is above-mentioned to have effects that comfort the crease-resistant composite skin care product of line has effects that comfort the crease-resistant skin care item of line or change in preparation
Application in cosmetic.
It is a kind of to have effects that comfort the crease-resistant eye cream of line, it is prepared by auxiliary material acceptable in above-mentioned composite skin care product and eye cream
It forms.
In wherein some embodiments, the eye cream comfort with line by the raw material preparation of following mass percent and
At: the described in any item composite skin care product 0.8%-8% of Claims 1-4, plant source wedding agent 2%-5%, antioxidant
0.1%-3%, moisturizer 1%-5%, thickener 0.2%-1%, vegetable oil 5%-10% and surplus deionized water.
In wherein some embodiments, the plant source wedding agent is selected from lecithin, alkyl glucoside, inulin ester or lemon
One of acid esters is a variety of；
The thickener is selected from one of Sodium Polyacrylate, xanthan gum, hydroxyethyl cellulose or methylcellulose or more
Kind；
The vegetable oil be selected from jojoba oil, Sweet Almond Oil, olive oil, camellia seed oil, wheat-germ oil, safflower seed oil,
One of grape seed oil or white pond flower seed oil are a variety of；
The antioxidant is in tocopherol, Co-Q10, beta carotene, lycopene, tea polyphenols or vitamin C
It is one or more；
The moisturizer is selected from Sodium Hyaluronate, pyrrolidone sodium carboxylate, ceramide, marine algae extract, amino acid and protects
One of humectant, glycerol caprylate or 1,2- hexylene glycol are a variety of.
In wherein some embodiments, the plant source wedding agent be selected from soybean lecithin, cetearyl glucoside and
The mixture of inulin lauryl carbamate: the vegetable oil is selected from the mixed of jojoba oil, safflower seed oil and Bai Chi flower seed oil
Close object；The antioxidant is selected from the mixture of Co-Q10, lycopene and tea polyphenols；The moisturizer is selected from hyaluronic acid
Sodium, ceramide, glycerol caprylate and 1,2- hexylene glycol mixture；The thickener is selected from Sodium Polyacrylate and xanthan gum
Mixture.
It is above-mentioned to have effects that comfort the preparation method of the crease-resistant eye cream of line, composite skin care product described above and auxiliary material are passed through
Be mixed system cream to get.
The invention has the following beneficial effects:
Through the long-term experience accumulation of inventor and a large amount of experimental study, it is of the present invention have effects that comfort line it is crease-resistant
Composite skin care product includes Atlas cedar bark extract, nipa palm seed extract and astaxanthin, and triplicity has good association
With crease-resistant effect.
The present invention by screen natural, mild above-mentioned composite skin care product, moisturizer, plant source wedding agent and
The compounding of vegetable oil makes not adding artificial synthesized oil, essence and preservative in the formula system of eye cream, is free of acrylamide list
Body provides more nutritional ingredients to eye skin on the whole, is easy to absorb, and can effectively reduce the thorn to eye skin
Swash, improve the moisture content of eye cuticula, improve moisturizing and it is compact go wrinkle effect, enhance skin elasticity, can effectively reduce pair
The stimulation of eye skin, and there is salubrious skin sense, effectively remove or alleviate eye wrinkle-removing.
The preparation process comfort with the crease-resistant eye cream of line of the invention is simple, reliable, and the eye cream of preparation being capable of heatproof
Degree variation, stability is good, is suitble to industrialized production.
Detailed description of the invention
Nothing.
Specific embodiment
Have effects that comfort the crease-resistant composite skin care product of line, eye cream and its system to of the invention below in conjunction with specific embodiment
Preparation Method is further described in detail.
Raw material sources
Atlas cedar bark extract, hundred Hao Bo Co., Ltd of Guangzhou
Nipa palm seed extract, hundred Hao Bo Co., Ltd of Guangzhou
Argireline, celestial graceful (world) Co., Ltd
Phytosterol, Guangzhou You Ran Biotechnology Co., Ltd
Astaxanthin, Guangzhou day of snow of oozing use Chemical Co., Ltd.
Artemia extract, Guangzhou Rong Dao Chemical Co., Ltd.
Yeast extractive from fermentative, celestial graceful (world) Co., Ltd
Other auxiliary materials are also commercial product.
Embodiment 1
There is provided it is a kind of have effects that comfort the formula of the crease-resistant eye cream of line, be shown in Table 1.
The formula table of the eye cream of 1 embodiment 1 of table
Eye cream is prepared according to the formula in the following table 1, is included the following steps:
(1) A phase component is added in oily phase pot and will be warming up to 80 DEG C, keep the temperature 10min, obtained and oily mix liquid；
(2) B phase component is sequentially added and is warming up to 85 DEG C, homogeneous 5min in water phase pot, keep the temperature 30min, obtain water phase mixing
Liquid；
(3) the water phase mixed liquor of 3/4 times of amount of above-mentioned total volume is pumped into emulsion pot, opens emulsion pot stirring, stirring
Speed is 1500rap/min, under agitation, slowly mixes after liquid is pumped into emulsion pot oil and emulsifies, then will be remaining overall
The water phase mixed liquor of 1/4 times of long-pending amount is pumped into emulsion pot；
After homogeneous 5min, then 10min is persistently stirred, mixing speed 1500rap/min；
(4) cooling water is opened, after pot temperature to be emulsified is down to 45 DEG C, C phase component is added and stirs 10min, mixing speed
1000rap/min；
(5) be added D phase component stir 10min, be cooled to room temperature, discharging to get.
Embodiment 2
Have effects that comfort the formula of the crease-resistant eye cream of line the present embodiment provides a kind of, is shown in Table 2.This has effects that comfort line crease-resistant
Eye cream preparation method referring to embodiment 1.
The formula table of the eye cream of 2 embodiment 2 of table
Embodiment 3
Have effects that comfort the formula of the crease-resistant eye cream of line the present embodiment provides a kind of, is shown in Table 3.This has effects that comfort line crease-resistant
Eye cream preparation method referring to embodiment 1.
The formula table comfort with the crease-resistant eye cream of line of 3 embodiment 3 of table
Embodiment 4
Have effects that comfort the formula of the crease-resistant eye cream of line the present embodiment provides a kind of, is shown in Table 4.This has effects that comfort line crease-resistant
Eye cream preparation method referring to embodiment 1.
The formula table comfort with the crease-resistant eye cream of line of 4 embodiment 4 of table
Embodiment 5
Have effects that comfort the formula of the crease-resistant eye cream of line the present embodiment provides a kind of, is shown in Table 5.This has effects that comfort line crease-resistant
Eye cream preparation method referring to embodiment 1.
The formula table comfort with the crease-resistant eye cream of line of 5 embodiment 5 of table
Embodiment 6
Have effects that comfort the formula of the crease-resistant eye cream of line the present embodiment provides a kind of, is shown in Table 6.This has effects that comfort line crease-resistant
Eye cream preparation method referring to embodiment 1.
The formula table comfort with the crease-resistant eye cream of line of 6 embodiment 6 of table
Embodiment 7
Have effects that comfort the formula of the crease-resistant eye cream of line the present embodiment provides a kind of, is shown in Table 7.This has effects that comfort line crease-resistant
Eye cream preparation method referring to embodiment 1.
The formula table comfort with the crease-resistant eye cream of line of 7 embodiment 7 of table
Embodiment 8
Stability analysis is carried out to embodiment 1-7, standard is executed with reference to moisturizing cream QB/T 1857-2013 and carries out, statistics
It the results are shown in Table 8.
(1) resistance to Thermal test
What Example 1-7 was produced, which have effects that comfort the crease-resistant eye cream of line, is placed under 48 DEG C of environment, observes after standing 90 days.
(2) it resists cold and tests
What Example 1-7 was produced, which have effects that comfort the crease-resistant eye cream of line, is placed under -10 DEG C of environment, sees after standing 90 days
It examines.
(3) fever and chills loop test:
What Example 1-7 was produced, which have effects that comfort the crease-resistant eye cream of line, is placed under 48 DEG C of environment, stands 12h；It again will be real
The crease-resistant eye cream of line that has effects that comfort that a 1-7 is produced is applied to be placed under -10 DEG C of environment；Continuously repeat this circulation three times.
Table 8 has effects that comfort the stability study of the crease-resistant eye cream of line
As shown in Table 8, what prepared by embodiment 1-7, which has effects that comfort the crease-resistant eye cream of line, low temperature resistant to change with high temperature,
Stability is good.
Embodiment 9
Hypersensitive test
Taking healthy albino guinea-pig, weight 250-300g, male and female dual-purpose rejects two sides dorsal body setae before testing, every 3 × 3cm of side, with
Machine is divided into test group 1 to 7, blank control group and positive controls.Test group 1 to 7 uses the eye cream of the embodiment of the present invention 1 to 7；
Positive controls 2,4-dinitrochlorobenzene, sensitization are 1% using its mass concentration, and excitation is 0.1% using its mass concentration.
Take the eye cream of the embodiment of the present invention 1 to 7 to be applied to back and go to hair-fields, the next day 1 time, totally 3 times.14 after last contact
It, at back, the same area smears the eye cream, observed at once after removing drug after 6h, and in for 24 hours, whether there is or not mistakes for 48h, 72h observation
Quick reaction.Blank control group and the same method of positive controls excite contact and observe.
Test result:
There is localized erythema and slight oedema after sensitization 1h in the animal skin of positive controls, allergic reaction for 24 hours
Exacerbation of symptoms, sensitization rate are 100%.Test group and blank control group animal skin do not occur any symptoms of allergic, cause
Quick rate is 0%.
The experimental results showed that the formula comfort with the crease-resistant eye cream of line of the invention is mild, non-stimulated.
10 eye cream measure of merit of embodiment
(1) the crease-resistant measure of merit of line is comforted
The eye cream of user's above-described embodiment 1 to 7 is measured respectively using after 60d, and statistics is using irritation incidence and resists
Effect of wrinkling is efficient, and statistical result is shown in Table 9.Its criterion of therapeutical effect is as follows:
Effective: skin smooth high resilience, wrinkle are obviously desalinated, and small microgroove disappears；
Effective: skin is relatively smooth, and elasticity makes moderate progress, and small microgroove is obviously desalinated, but wrinkle still remains；
Invalid: small microgroove, wrinkle still remain, or even have the tendency that intensification.
9 anti-wrinkle effect statistical form of table
| Group | Effective number | Efficiently individual quantity | Invalid number | It is efficient |
| Embodiment 1 | 5 | 10 | 5 | 75% |
| Embodiment 2 | 6 | 11 | 3 | 85% |
| Embodiment 3 | 7 | 8 | 5 | 75% |
| Embodiment 4 | 6 | 9 | 5 | 75% |
| Embodiment 5 | 6 | 12 | 4 | 80% |
| Embodiment 6 | 9 | 10 | 1 | 95% |
| Embodiment 7 | 1 | 8 | 11 | 45% |
(2) eye part skin moisturizing and skin elasticity measure of merit
Age is met to tested standard volunteer between 30-35 years old, is randomly assigned to be 7 groups, every group 20.Volunteer is every
Sooner or later face is cleaned day later according to correct gimmick smearing eye cream.
User is measured respectively the 0th week and 4th week, the water content of eye part skin, use moisture of skin tester (Germany
CK, CM825-MDD), room temperature is 20 DEG C~25 DEG C when measuring indices, and humidity is 35%~70%, and is required tested
Person shifts to an earlier date 30min and enters test environment, and the measurement of indices is carried out after rest.Every group of embodiment is averaged, statistics knot
Fruit is shown in Table 10.
10 moistening effect statistical form of table
| Group | Water content of stratum corneum the 0th week | Water content of stratum corneum the 4th week |
| Embodiment 1 | 60.17 | 65.21 |
| Embodiment 2 | 61.23 | 67.81 |
| Embodiment 3 | 60.88 | 66.08 |
| Embodiment 4 | 62.01 | 67.45 |
| Embodiment 5 | 61.55 | 66.10 |
| Embodiment 6 | 60.96 | 70.05 |
| Embodiment 7 | 60.46 | 64.72 |
User is measured respectively the 0th week and 4th week, the water content of eye part skin, using skin elasticity tester
Cutometer MPA580 (German CK company) tests the volunteer of every group of embodiment, and statistical result is shown in Table 11.
11 skin elasticity effect statistical form of table
| Group | Water content of stratum corneum the 0th week | Water content of stratum corneum the 4th week |
| Embodiment 1 | 57.41 | 68.69 |
| Embodiment 2 | 58.02 | 71.23 |
| Embodiment 3 | 56.98 | 70.10 |
| Embodiment 4 | 57.11 | 70.91 |
| Embodiment 5 | 57.36 | 69.02 |
| Embodiment 6 | 56.67 | 73.59 |
| Embodiment 7 | 57.86 | 63.50 |
By table 9 to table 11 it is found that compared with Example 7, the crease-resistant eye cream of line that has effects that comfort of embodiment 1-6 all has
Good moistening effect can effectively enhance the elasticity of eye part skin, hence it is evident that have the effect of it is compact go wrinkle, smooth skin.
Each technical characteristic of embodiment described above can be combined arbitrarily, for simplicity of description, not to above-mentioned reality
It applies all possible combination of each technical characteristic in example to be all described, as long as however, the combination of these technical characteristics is not deposited
In contradiction, all should be considered as described in this specification.
The embodiments described above only express several embodiments of the present invention, and the description thereof is more specific and detailed, but simultaneously
It cannot therefore be construed as limiting the scope of the patent.It should be pointed out that coming for those of ordinary skill in the art
It says, without departing from the inventive concept of the premise, various modifications and improvements can be made, these belong to protection of the invention
Range.Therefore, the scope of protection of the patent of the invention shall be subject to the appended claims.
Claims (9)
1. a kind of have effects that comfort the crease-resistant composite skin care product of line, which is characterized in that include following components: Atlas cedar bark
Extract, nipa palm seed extract, astaxanthin and yeast extractive from fermentative；The Atlas cedar bark extract, nipa palm seed extract
The mass ratio of object, astaxanthin and yeast extractive from fermentative is 0.2-5:0.1-5:0.01-0.5:0.5-1.
2. according to claim 1 have effects that comfort the crease-resistant composite skin care product of line, which is characterized in that including acetyl group
One of hexapeptide -8, phytosterol and artemia extract are a variety of.
3. according to claim 1 have effects that comfort the crease-resistant composite skin care product of line, which is characterized in that the north African snow
Pine Bark, nipa palm seed extract, astaxanthin and yeast extractive from fermentative mass ratio be 1.2:1.5:0.2:0.8.
Line is comforted 4. having effects that comfort the crease-resistant composite skin care product of line described in any one of claims 1 to 3 and having in preparation
The skin care item of crease-resistant effect or the application in cosmetics.
5. a kind of have effects that comfort the crease-resistant eye cream of line, which is characterized in that the skin care as described in any one of claims 1 to 3
Acceptable auxiliary material is prepared in product composition and eye cream.
6. the eye cream for comforting the crease-resistant effect of line stated according to claim 5, which is characterized in that by the raw material system of following mass percent
It is standby to form: the described in any item composite skin care product 0.8%-8% of claims 1 to 3, plant source wedding agent 2%-5%, antioxygen
Agent 0.1%-3%, moisturizer 1%-5%, thickener 0.2%-1%, vegetable oil 5%-10% and surplus deionized water.
7. comforting the eye cream of the crease-resistant effect of line as claimed in claim 6, which is characterized in that the plant source wedding agent is selected from lecithin
One of rouge, alkyl glucoside, inulin ester or citrate are a variety of；
The thickener is selected from one of Sodium Polyacrylate, xanthan gum, hydroxyethyl cellulose or methylcellulose or a variety of；
The vegetable oil is selected from jojoba oil, Sweet Almond Oil, olive oil, camellia seed oil, wheat-germ oil, safflower seed oil, grape
One of seed oil or white pond flower seed oil are a variety of；
The antioxidant in tocopherol, Co-Q10, beta carotene, lycopene, tea polyphenols or vitamin C one
Kind is a variety of；
The moisturizer be selected from Sodium Hyaluronate, pyrrolidone sodium carboxylate, ceramide, marine algae extract, amino acid humectant,
One of glycerol caprylate or 1,2- hexylene glycol are a variety of.
8. comforting the eye cream of the crease-resistant effect of line as claimed in claim 7, which is characterized in that the plant source wedding agent is selected from soybean
The mixture of lecithin, cetearyl glucoside and inulin lauryl carbamate: the vegetable oil be selected from jojoba oil,
The mixture of safflower seed oil and Bai Chi flower seed oil；The antioxidant is selected from the mixing of Co-Q10, lycopene and tea polyphenols
Object；The moisturizer is selected from the mixture of Sodium Hyaluronate, ceramide, glycerol caprylate and 1,2- hexylene glycol；The thickening
Agent is selected from the mixture of Sodium Polyacrylate and xanthan gum.
9. having effects that comfort the preparation method of the crease-resistant eye cream of line described in any one of claim 5 to 8, which is characterized in that
By the described in any item composite skin care products of claims 1 to 3 and auxiliary material be mixed system cream to get.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611200901.0A CN106580762B (en) | 2016-12-22 | 2016-12-22 | Have effects that comfort the crease-resistant composite skin care product of line, eye cream and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611200901.0A CN106580762B (en) | 2016-12-22 | 2016-12-22 | Have effects that comfort the crease-resistant composite skin care product of line, eye cream and preparation method thereof |
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| CN108785136B (en) * | 2017-05-04 | 2022-08-09 | 伽蓝（集团）股份有限公司 | Application of cedar essential oil |
| CN107184442A (en) * | 2017-06-01 | 2017-09-22 | 四川惠泰农业科技有限公司 | Anti-aging anti-wrinkle moisture retention water rich in beta glucan and preparation method thereof |
| CN107496245B (en) * | 2017-09-15 | 2020-04-03 | 澳宝化妆品（惠州）有限公司 | Anti-aging liposome composition and preparation method and application thereof |
| CN108703927A (en) * | 2018-07-25 | 2018-10-26 | 宁波博睿修存生物科技有限公司 | Anti-age corrective eye treatment cream |
| CN110179684B (en) * | 2019-07-01 | 2022-05-10 | 日照职业技术学院 | Natural astaxanthin eye cream capable of being efficiently absorbed and preparation method thereof |
| CN111514085B (en) * | 2020-05-18 | 2021-05-11 | 高宝化妆品（中国）有限公司 | Moisturizing composition containing date seed extract and mask |
| CN113413338A (en) * | 2021-06-30 | 2021-09-21 | 广州市科能化妆品科研有限公司 | Eye repairing composition and preparation method and application thereof |
| CN113576934B (en) * | 2021-08-23 | 2023-05-30 | 上海晶典化妆品有限公司 | Fresh skin and muscle activation essence stock solution and preparation method thereof |
| CN113456532A (en) * | 2021-08-24 | 2021-10-01 | 广州莱倩化妆品有限公司 | Zero-pore makeup front cream without silicone oil and preparation method thereof |
| CN116531309B (en) * | 2023-06-25 | 2023-11-28 | 天地慈(东莞)生物科技有限公司 | Anti-wrinkle smoothing composition and preparation method thereof |
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