CN105380873B - A kind of replenishing water and preserving moisture essence containing oil of Nitraria seeds - Google Patents
A kind of replenishing water and preserving moisture essence containing oil of Nitraria seeds Download PDFInfo
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- CN105380873B CN105380873B CN201510788524.6A CN201510788524A CN105380873B CN 105380873 B CN105380873 B CN 105380873B CN 201510788524 A CN201510788524 A CN 201510788524A CN 105380873 B CN105380873 B CN 105380873B
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- essence
- oil
- extraction
- nitraria seeds
- nitraria
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/494—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
- A61K8/4946—Imidazoles or their condensed derivatives, e.g. benzimidazoles
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
- A61K8/988—Honey; Royal jelly, Propolis
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
Abstract
The present invention provides a kind of essences containing oil of Nitraria seeds, it is formed by combining by oil of Nitraria seeds, Mel extract.The present invention after the components compatible use such as oil of Nitraria seeds and Mel extract the study found that by synergistic function has been played, hence it is evident that enhances replenishing water and preserving moisture effect, skin care effect is significantly better than the essence for being individually added into Mel extract.
Description
Technical field
The present invention relates to a kind of essences containing oil of Nitraria seeds.
Background technology
White thorn (Nitraria) is the life of zygophyllaceae (Zygophyllceae) drought or super non-irrigated raw Typical Desert plant, is often crawled
Aerial growth, 30~50cm of plant height, multi-branched, small part branch is upright, and bark is faint yellow, sprig canescence, tip thorn-like, branch
Stingless or few thorn.Its resistance is strong, it is drought-resistant it is saline and alkaline, adapt to that high temperature is low cold, and NATURAL DISTRIBUTION is in drying, saline and alkaline, windy, vegetation
It is the excellent shrub checked winds and fixed drifting sand in rare harsh environment.Currently, the natural Bai Cilin of Qinghai-Tibet Caidamu Basin distribution
About 3~40,000 km2。
A large amount of applied basic research work confirms berry of nitraria tangutorum bobr rich in vitamin C, amino acid, polysaccharide, flavones, biology
Alkali etc. has the function of anti-oxidant, reducing blood lipid, prevention Hyperhomocysteinemia.Piercing abundant nutrition and active constituent in vain makes it
As exploitation drug, the quality raw materials of health food and Speciality Foods.
Previous research focuses primarily upon the function of the active constituent of berry of nitraria tangutorum bobr, to the composition Study of oil of Nitraria seeds compared with
It is few, more do not use it for the report of replenishing water and preserving moisture skin care item.
Invention content
Inventor has carried out comprehensive analysis to oil of Nitraria seeds, it is found that oil of Nitraria seeds has the uniqueness on ingredient, performance
Go out containing profuse unsaturated fatty acid, free fatty, sterols, hydrocarbon, squalene, phosphatide and fat-soluble dimension
Raw element E, vitamin A etc..The first six kind compound is most of ingredient in sebum, is easy to be absorbed by the skin, has and be similar to skin
The skin care effect of skin.Sebum ingredient in oil of Nitraria seeds plays skin nutrition with nutritional ingredients such as dimension E therein, dimension A, protects jointly
The function of sheath skin, therefore, oil of Nitraria seeds are a kind of highly desirable natural and green raw material of skin care articles.
For these reasons, the present invention is practical provides a kind of essence containing oil of Nitraria seeds, wherein per 100g essence
The component contained in element is as follows：
In a specific implementation mode of the invention, the component contained in every 100g essences is as follows：
The non-limiting example of preservative includes propylben, Jie Ma-BP etc..The non-limiting reality of essence
Example includes jasmine fragrance, rosemary type, thyme type, mint aroma etc..
The content of unsaturated fatty acid is high in oil of Nitraria seeds, mainly contains linolenic and linoleic, they can be adjusted
The metabolism of moisture in skin；Skin can also be protected not damaged by X-ray, the mechanism of action may be due to cambium
Growth needs, and the repair process of damaged tissues is also required to unsaturated fatty acid.Also contain vitamin E, vitamin in oil of Nitraria seeds
A, the bioactive substances such as phytosterol, they have human body particularly important physiological action, as radioresistance, it is anti-oxidant, disappear
Inflammation effect etc..In addition, unsaturated fatty acid can also further be sent out with nutritional ingredients such as other active components such as amino acid, polysaccharide
Synergistic effect is waved, the function for reaching skin nutrition, protecting skin.
Oil of Nitraria seeds is with after other base starting materials and additive compound in formula, and replenishing water and preserving moisture effect is more preferable, such as thoroughly
Bright matter acid, allantoin, Mel extract.Hyaluronic acid is ideal natural moisturizing factor (NMF), it can improve skin-nourishing
Metabolism, make skin it is tender, it is smooth, go wrinkle, increase elasticity, prevent aging, be good Transdermal absorption rush again while moisturizing
It into agent, is used cooperatively with other nutritional ingredients, the more preferable effect for promoting nutrient absorption can be played.Allantoin has sterilization anti-
Rotten, oxidation resistant effect can make skin keep moisture, while can also promote tissue growth and cell metabolism, cutin-softening
Layer has the function of moist, soft skin.Mel extract has preferable moisture regulation effect and hygroscopicity, it can be straight
The aquation for participating in cuticula is connect, the moisture loss of cuticula is supplemented, there is long-term moistening effect, the extract is more
It is used in a product, such as ZL201210183745.7, ZL201310355139.3.
Wherein, the oil of Nitraria seeds is to use supercritical CO2What extraction was prepared.
Further, the supercritical CO2Extraction conditions is：30~60 DEG C, 10~30MPa of extracting pressure of extraction temperature,
CO2Flow is 35~40kg/h, 60~180min of extraction time.
Further, the supercritical CO2Extraction conditions is：45 DEG C of extraction temperature, extracting pressure 20MPa, CO2Flow
For 35~40kg/h, extraction time 120min.
The present invention also provides the preparation methods of above-mentioned essence, it includes following operating procedure：
(1) sodium ethylene diamine tetracetate, allantoin, Sodium Hyaluronate, 1,3- pentanediols are sufficiently mixed, make ethylenediamine tetrem
Sour sodium, allantoin, Sodium Hyaluronate are uniformly dispersed, and are heated to 60~100 (preferably 80) DEG C, stir evenly；
(2) triethanolamine, rilanit special are being added into above-mentioned solution, are maintaining temperature in 60~100 (preferably 80)
DEG C, it stirs evenly；
(3) methyl hydroxybenzoate and 1,3-BDO are heated, makes to be completely dissolved, is added in above-mentioned mixed liquor；
(4) Carbopol 941 is added, adds the water of surplus, stirs evenly；
(5) 50~30 (preferably 40) DEG C are cooled to, oil of Nitraria seeds, Mel extract, preservative, essence is added, continues
Stirring；
(6) continue to be down to room temperature, dispense.
The present invention also provides above-mentioned essences to prepare the purposes in having effects that the skin care item of replenishing water and preserving moisture.
The present invention also provides oil of Nitraria seeds to have effects that the skin care item of replenishing water and preserving moisture or as replenishing water and preserving moisture in preparation
The purposes of the complementary ingredient of skin care item.
Wherein, at least contain Mel extract in the skin care item.
Further, allantoin, Sodium Hyaluronate are also contained in the skin care item.
The present invention after the components compatible use such as oil of Nitraria seeds and Mel extract the study found that by synergistic work has been played
With, hence it is evident that replenishing water and preserving moisture effect is enhanced, skin care effect is significantly better than the essence for being individually added into Mel extract.
The present invention can make the long-acting moisturizing of skin, supplement amino acid, abundant maintenance dry low and deep sub-health state, excite
Skin water vigor opens infiltration lane for skin, and osmotrophy substance accelerates the self-regeneration of skin, strengthens skin update
Ability, so that skin is restored, water is tender, compacts, ruddy glossy, high resilience.Especially oil of Nitraria seeds extract also has nti-freckle beautiful
In vain, anti-oxidant, anti-aging effect.The present invention does not add artificial color, using natural biological extract as active material, plays
Its given efficacy, permanence operation is apparent, and manufacture craft is simple, best in quality, and safety is without side-effects.
Specific implementation mode
Specific embodiments of the present invention are described in detail below：
In the present invention, oil of Nitraria seeds can be obtained by buying commercial product, can also be extracted by supercritical carbon dioxide
Technology is taken to prepare, extraction conditions is exemplified below：45 DEG C of extraction temperature, extracting pressure 20MPa, CO2Flow is 35~40kg/h,
Extraction time 120min.
In the present invention, Mel extract can obtain (being purchased in the specific embodiment of the invention by buying commercial product
The brand bought is German BASF).
The preparation of 1 essence of the present invention of embodiment and efficacy study
Table 1
Technological process：
(1) precise sodium ethylene diamine tetracetate 0.05, allantoin 0.05, Sodium Hyaluronate 0.05,1,3- pentanediols
3.0, it is sufficiently mixed, sodium ethylene diamine tetracetate, allantoin, Sodium Hyaluronate is made to be uniformly dispersed, be heated to 80 DEG C, stirring is equal
It is even；
(2) triethanolamine 0.16, rilanit special 0.3 are accurately being added into above-mentioned solution, are maintaining temperature at 80 DEG C, stirs
It mixes uniformly；
(3) precise methyl hydroxybenzoate 0.1 and 1,3-BDO 3.0 are slightly warm, make it completely dissolved, and are added to above-mentioned
In mixed liquor；
(4) last accurate addition card wave 941 15.0, adds the water 77.1 of surplus, stirs evenly；
(5) 40 DEG C are cooled to, it is accurate that oil of Nitraria seeds 1.0, Mel extract 0.5, preservative 0.2, essence 0.03 is added, after
Continuous stirring (replacing oil of Nitraria seeds with Mel extract in reference examples)；
(6) continue to be down to room temperature, discharge, packing.
In order to test the moistening effect of the present invention, investigation experiment on probation has been carried out：
1. respondent：Choose the dry skin of areal, neutral skin volunteers each 10 people of trier；
2. control time：Continuous two months
3. using product：A products are the embodiment of the present invention, and B products are reference examples；
4. test method：After each group trier cleans face, A, B product are applied to left and right both sides facial skin respectively,
Using effect is observed and investigates, trier does not know each group of composition proportion during use；
5. test result statistics is as follows：
Table 2
6. feeding back conclusion：
Trier indicates that embodiment product can not only moisturizing, moreover it is possible to moisturize the skin, improve skin quality, reduce microgroove, use
When there is no heavy feeling, without irritation, and there is no allergic phenomena；And the moisturizing effect of 1 product of reference examples is not so good as embodiment
Significantly, 80% trier recommends product of the present invention, and thinks that product of the present invention is better than reference examples 1.
Product quality detects：
1. organoleptic detection：Color and luster is orange bright, and modest viscosity, fragrance is comfortable, salubrious non-greasy.
2. Physico-chemical tests：Ph：4.5-8.5 methanol ＜ 1000ppm.
3. microorganism detection：Total number of bacteria ＜ 500/g；Fecal coliform, Pseudomonas aeruginosa and staphylococcus aureus are not examined
Go out, meets cosmetic standard.
4. heavy metal analysis：Mercury ＜ 1ppm, lead ＜ 40ppm, arsenic ＜ 10ppm, in cosmetic standard range.
Safety testing：
Oral Acute Toxicity experiment, Skin Irritation Test and eye irritant test, knot are carried out by method as defined in QB-963-85
Fruit shows that emulsion Oral Acute Toxicity made of white thorn moisturizing essence using the present invention is practical to be nontoxic, to normal human
The stimulus intensity of skin and mucous membrane be it is non-stimulated, it is safe to use.
Claims (10)
1. a kind of essence containing oil of Nitraria seeds, it is characterised in that：The component contained in per 100g essences is as follows：
2. essence according to claim 1, it is characterised in that：The component contained in per 100g essences is as follows：
3. essence according to claim 1 or 2, it is characterised in that：The oil of Nitraria seeds is to use supercritical CO2Extraction
It is prepared.
4. essence according to claim 3, it is characterised in that：The supercritical CO2Extraction conditions is：Extraction temperature 30
~60 DEG C, extracting pressure 10~30MPa, CO2Flow is 35~40kg/h, 60~180min of extraction time.
5. essence according to claim 4, it is characterised in that：The supercritical CO2Extraction conditions is：Extraction temperature 45
DEG C, extracting pressure 20MPa, CO2Flow is 35~40kg/h, extraction time 120min.
6. the preparation method of essence described in claims 1 or 2, it is characterised in that：It includes following operating procedure：
(1) sodium ethylene diamine tetracetate, allantoin, Sodium Hyaluronate, 1,3- pentanediols are sufficiently mixed, make ethylenediamine tetra-acetic acid
Sodium, allantoin, Sodium Hyaluronate are uniformly dispersed, and are heated to 60~100 DEG C, stir evenly；
(2) triethanolamine, rilanit special are being added into above-mentioned solution, are maintaining temperature at 60~100 DEG C, stirs evenly；
(3) methyl hydroxybenzoate and 1,3-BDO are heated, makes to be completely dissolved, is added in above-mentioned mixed liquor；
(4) Carbopol 941 is added, adds the water of surplus, stirs evenly；
(5) 50~30 DEG C are cooled to, oil of Nitraria seeds, Mel extract, preservative, essence is added, continues to stir；
(6) continue to be down to room temperature, dispense.
7. preparation method according to claim 6, it is characterised in that：In step (1), it is heated to 80 DEG C.
8. preparation method according to claim 6, it is characterised in that：In step (2), maintain temperature at 80 DEG C.
9. preparation method according to claim 6, it is characterised in that：In step (5), it is cooled to 40 DEG C.
10. essence described in Claims 1 to 5 any one is preparing the purposes in having effects that the skin care item of replenishing water and preserving moisture.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510788524.6A CN105380873B (en) | 2015-11-17 | 2015-11-17 | A kind of replenishing water and preserving moisture essence containing oil of Nitraria seeds |
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| CN201510788524.6A CN105380873B (en) | 2015-11-17 | 2015-11-17 | A kind of replenishing water and preserving moisture essence containing oil of Nitraria seeds |
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| CN105380873A CN105380873A (en) | 2016-03-09 |
| CN105380873B true CN105380873B (en) | 2018-09-07 |
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Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105726448B (en) * | 2016-04-12 | 2018-08-24 | 广州智媛生物科技有限公司 | A kind of skin care item and preparation method thereof of the honeycomb active constituent containing there are many |
| CN105997738A (en) * | 2016-07-12 | 2016-10-12 | 广州丹奇日用化工厂有限公司 | Skincare essence containing tetragonia tetragonioides extract |
| CN106963683A (en) * | 2017-04-05 | 2017-07-21 | 中国科学院西北高原生物研究所 | A kind of essence containing raspberry |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1687340A (en) * | 2005-03-23 | 2005-10-26 | 中国科学院西北高原生物研究所 | Supercritical Co2 extracting technique for oil of Nitraria seeds and application in lowering blood fat thereof |
| CN103565699A (en) * | 2013-11-06 | 2014-02-12 | 中国科学院西北高原生物研究所 | Lycium ruthenicum mill freckle-removing and whitening anti-aging essence and preparation method of essence |
-
2015
- 2015-11-17 CN CN201510788524.6A patent/CN105380873B/en active Active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1687340A (en) * | 2005-03-23 | 2005-10-26 | 中国科学院西北高原生物研究所 | Supercritical Co2 extracting technique for oil of Nitraria seeds and application in lowering blood fat thereof |
| CN103565699A (en) * | 2013-11-06 | 2014-02-12 | 中国科学院西北高原生物研究所 | Lycium ruthenicum mill freckle-removing and whitening anti-aging essence and preparation method of essence |
Non-Patent Citations (3)
| Title |
|---|
| 《唐古特白刺籽油的超临界CO2流体萃取及GC/MS分析》;王洪伦;《中国油脂》;20061020;第31卷(第10期);第61-63页 * |
| 《白刺主要功能性成分及其功效研究进展》;冯云子;《食品工业科技》;20100731;第31卷(第7期);第371-375页 * |
| 冯云子.《白刺主要功能性成分及其功效研究进展》.《食品工业科技》.2010,第31卷(第7期),第371-375页. * |
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