CN106963683A - A kind of essence containing raspberry - Google Patents
A kind of essence containing raspberry Download PDFInfo
- Publication number
- CN106963683A CN106963683A CN201710218664.9A CN201710218664A CN106963683A CN 106963683 A CN106963683 A CN 106963683A CN 201710218664 A CN201710218664 A CN 201710218664A CN 106963683 A CN106963683 A CN 106963683A
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- CN
- China
- Prior art keywords
- raspberry
- extract
- essence
- parts
- fruit
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Classifications
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/35—Ketones, e.g. benzophenone
- A61K8/355—Quinones
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/494—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
- A61K8/4946—Imidazoles or their condensed derivatives, e.g. benzimidazoles
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
Abstract
The invention provides a kind of essence containing raspberry.Present invention research is found, after raspberry Anthocyanin-rich Extract, raspberry fruit oil and the component compatibility use such as raspberry polysaccharide, with good whitening, moisturizing, anti-aging, it is sun-proof the effects such as.
Description
Technical field
The present invention relates to a kind of essence containing raspberry.
Background technology
Raspberry (Rubus idaeus L.) also known as Rubus corchorifolius, raspberry, raspberry etc., belong to rose family rubus.Raspberry master
Northern Hemisphere temperate zone and frigid zone are distributed in, its fruit is starches small aggregate fruit more, and taste sweet tea is slightly sour.Raspberry contains fruit oil, organic acid, Huang
Ketone, anthocyanidin, the various active composition such as polyphenol, vitamin, mineral element, volatile oil, tannin, with high nutritive value and
Medical care effect, is described as " gold fruit ".
At present, it yet there are no the report of the various active components compatibility utilization of raspberry.
The content of the invention
The invention provides a kind of essence containing raspberry, it contains the component of following quality proportioning：
Wherein, raspberry Anthocyanin-rich Extract is selected selected from 3.0~5.0 parts, the grease separation of raspberry fruit from 1.0~3.0 parts, raspberry polysaccharide
From 5.0~10.0 parts, 1.0~3.0 parts of Lycium chinense fruit aqueous extract, 1.0~3.0 parts of rose wate extract.Such as one tool of the present invention
In body embodiment, emulsion has following component to match：
Proportioning one：
Preparation method is ibid.
Proportioning two：
Proportioning three：
Proportioning four：
Proportioning five：
Further, raspberry Anthocyanin-rich Extract be selected from 4.0 ± 0.5 parts, the grease separation of raspberry fruit from 2.0 ± 0.5 parts, raspberry it is many
Sugar selected from 8.0 ± 0.5 parts, 2.0 ± 0.5 parts of Lycium chinense fruit aqueous extract, 2.0 ± 0.5 parts of rose wate extract.The present invention actually makes
Found during, if each position of raspberry is combined according to the proportioning with Lycium chinense fruit aqueous extract and rose wate extract to be made
With its skin effect is significantly better than other compatibility relationships.
Wherein, the raspberry is the fruit of rose family rubus plant.
Raspberry Anthocyanin-rich Extract used in the present invention, raspberry fruit oil, raspberry polysaccharide, Lycium chinense fruit aqueous extract and rose
Water extract can be bought in commercial goods, can also be prepared according to presently disclosed technology, and the present invention one is specific real
Apply in mode, the preparation method of the raspberry Anthocyanin-rich Extract is as follows：Take macroreticular resin on raspberry, extracting in water, water extract
Post, is first washed with water removal of impurities, then with 60~80%v/v ethanol elutions, collect alcohol elution, be drying to obtain.
Wherein, the preparation method of the raspberry polysaccharide is as follows：Take after raspberry, petroleum ether or ether defatting, with 75%~
95%v/v ethanol is extracted, filtering, filter residue extracting in water, after water intaking extract concentration, plus ethanol or hydrous ethanol to alcohol content reach
70%~85%v/v, it is raspberry polysaccharide to take solid content.
Wherein, the preparation method of the raspberry fruit oil is as follows：Raspberry is taken, using supercritical CO2Extraction is extracted, and is extracted
Afterwards, then through two-stage decompression separation raspberry fruit oil is obtained；Wherein, extraction conditions is as follows：Extraction kettle pressure is 15~45Mpa, temperature
For 30~55 DEG C, CO2Flow is that 20~60L/h, extraction time are 40~120min；Two-stage decompression separation condition is as follows：To press
Power be 5~7Mpa, temperature be 40~50 DEG C as one-level decompression separation, by 3~5Mpa of pressure, temperature be 30~40 DEG C as
Second depressurized is separated.
Lycium chinense fruit aqueous extract, i.e., be heated to 50~70 DEG C using water and extracted, extract solution is concentrated under reduced pressure, and is drying to obtain.
Rose wate extract, i.e., be heated to 50~70 DEG C using water and extracted, extract solution is concentrated under reduced pressure, and is drying to obtain.
Present invention also offers the preparation method of above-mentioned essence, it includes following behaviour
Make step：
(1) sodium ethylene diamine tetracetate, Sodium Hyaluronate, 1,3- pentanediols are sufficiently mixed, make sodium ethylene diamine tetracetate, thoroughly
The sour sodium of bright matter is uniformly dispersed, and is heated to 60~90 DEG C, stirs；
(2) triethanolamine, rilanit special are being added into above-mentioned solution, is maintaining temperature at 60~90 DEG C, stir；
(3) methyl hydroxybenzoate or ethyl ester and 1,3-BDO are heated, makes to be completely dissolved, be added in above-mentioned mixed liquor；
(4) carbomer, water are added, is stirred；
(5) 30~50 DEG C are cooled to, raspberry Anthocyanin-rich Extract, raspberry fruit oil, raspberry polysaccharide, fruit of Chinese wolfberry water extraction is added
Thing, rose wate extract, continue to stir；
(6) continue to be down to room temperature, dispense.
Present invention also offers above-mentioned essence prepare with replenishing water and preserving moisture, whitening and anti-aging, sun-proof function skin care
Purposes in product.
Present invention research is found, after the component compatibility uses such as raspberry Anthocyanin-rich Extract, raspberry fruit oil and raspberry polysaccharide,
With good whitening, moisturizing, anti-aging, it is sun-proof the effects such as.
In addition, some known skin care materials, such as pearl can also be added on the basis of the present invention, in composition or emulsion
Powder, allantoin, Co-Q10 etc..
In addition, the auxiliary materials such as appropriate natural antiseptic agent, antioxidant can also be added in composition or emulsion.
Embodiment
The preparation of the essence of the present invention of embodiment 1 and efficacy study
Technological process：
(1) sodium ethylene diamine tetracetate, Sodium Hyaluronate, 1,3- pentanediols are sufficiently mixed, make sodium ethylene diamine tetracetate, thoroughly
The sour sodium of bright matter is uniformly dispersed, and is heated to 60~90 DEG C, stirs；
(2) triethanolamine, rilanit special are being added into above-mentioned solution, is maintaining temperature at 60~90 DEG C, stir；
(3) methyl hydroxybenzoate or ethyl ester and 1,3-BDO are heated, makes to be completely dissolved, be added in above-mentioned mixed liquor；
(4) Carbopol 941, water are added, is stirred；
(5) 30~50 DEG C are cooled to, raspberry Anthocyanin-rich Extract, raspberry fruit oil, raspberry polysaccharide, Lycium chinense fruit aqueous extract is added
With rose wate extract, continue to stir；
(6) continue to be down to room temperature, dispense.
In order to test the moistening effect of the present invention, investigation experiment on probation has been carried out：
1. respondent：Choose aspiration trier totally 86 people of the different skin quality of areal；
2. control time：Continuous 30 days
Use product：A products：Essence prepared by the embodiment of the present invention 1；B products are reference examples essence：Reference examples essence
The only following parts of Hua Suzhong are different from embodiment 1：Raspberry Anthocyanin-rich Extract 5.0g, raspberry fruit oil 4.0g, raspberry polysaccharide 5.0g,
Remaining be the same as Example 1.
3. method of testing：43 people use A products, and remaining 43 people uses B products, halfway without exiting example.Each group trier is clear
After clean face, A, B product are applied to left and right both sides facial skin respectively, observes and investigates using effect, trier's validity period
Between do not know each group of composition proportion, using once before sleeping every night.
4. test result statistics is as follows：
Table 1
* it is good：Trier thinks that skin improves significantly effect；Typically：Trier's skin has improvement, but feels
Effect is not to protrude very much；Without influence：Trier thinks that skin is without any improvement.
5. feed back conclusion：
Trier represents that the formation for suppressing melanin of two kinds of products of A, B can freckle removing and whitening, anti-aging, moisturizing
Moisturizing, makes skin gloss high resilience.
In addition, A product whitening anti-agings moistening effect is very well, continuous just occurred in that using skin after two weeks is substantially changed
Kind, microgroove is reduced, and skin is flexible and gloss, and whitening effect is fabulous.B products have certain wrinkle resistant moistening effect, face
Microgroove has been reduced, but whitening and anti-aging and moistening effect are but not as good as A products.
The preparation of the essence of the present invention of embodiment 2 and efficacy study
Preparation method is ibid.
The preparation of the essence of the present invention of embodiment 3 and efficacy study
Preparation method is ibid
The preparation of the essence of the present invention of embodiment 4 and efficacy study
Preparation method is ibid.
Claims (9)
1. a kind of essence containing raspberry, it is characterised in that：It contains the component of following quality proportioning：
2. the essence according to claim 1 containing raspberry, it is characterised in that：Raspberry Anthocyanin-rich Extract is selected from 3.0
~5.0 parts, the grease separation of raspberry fruit from 1.0~3.0 parts, raspberry polysaccharide be selected from 5.0~10.0 parts, Lycium chinense fruit aqueous extract 1.0~3.0
Part, 1.0~3.0 parts of rose wate extract.
3. the essence according to claim 2 containing raspberry, it is characterised in that：Raspberry Anthocyanin-rich Extract is selected from 4.0
± 0.5 part, the grease separation of raspberry fruit from 2.0 ± 0.5 parts, raspberry polysaccharide be selected from 8.0 ± 0.5 parts, 2.0 ± 0.5 parts of Lycium chinense fruit aqueous extract,
2.0 ± 0.5 parts of rose wate extract.
4. the essence according to claim 1 containing raspberry, it is characterised in that：The raspberry is rose family rubus
The fruit of plant.
5. the essence containing raspberry according to Claims 1 to 4 any one, it is characterised in that：The raspberry pattern
The preparation method of glucoside extract is as follows：
Macroporous resin column on raspberry, extracting in water, water extract is taken, removal of impurities is first washed with water, then with 60~80%v/v ethanol elutions,
Alcohol elution is collected, is drying to obtain.
6. the essence containing raspberry according to Claims 1 to 4 any one, it is characterised in that：The raspberry polysaccharide
Preparation method it is as follows：
Take after raspberry, petroleum ether or ether defatting, extracted with 75%~95%v/v ethanol, filtering, filter residue extracting in water, water intaking
After extract concentration, plus ethanol or hydrous ethanol to alcohol content reach 70%~85%v/v, and it is raspberry polysaccharide to take solid content.
7. the essence containing raspberry according to Claims 1 to 4 any one, it is characterised in that：The raspberry fruit oil
Preparation method it is as follows：
Raspberry is taken, using supercritical CO2Extraction is extracted, after extraction, then obtains raspberry fruit oil through two-stage decompression separation；Wherein,
Extraction conditions is as follows：Extraction kettle pressure is that 15~45Mpa, temperature are 30~55 DEG C, CO2Flow is 20~60L/h, extraction time
For 40~120min；Two-stage decompression separation condition is as follows：By 5~7Mpa of pressure, temperature is 40~50 DEG C and depressurized as one-level
Separation, by 3~5Mpa of pressure, temperature is 30~40 DEG C and separated as second depressurized.
8. the preparation method of essence described in claim 1, it is characterised in that：It includes following operating procedure：
(1) sodium ethylene diamine tetracetate, Sodium Hyaluronate, 1,3- pentanediols are sufficiently mixed, make sodium ethylene diamine tetracetate, hyalomitome
Sour sodium is uniformly dispersed, and is heated to 60~90 DEG C, stirs；
(2) triethanolamine, rilanit special are being added into above-mentioned solution, is maintaining temperature at 60~90 DEG C, stir；
(3) methyl hydroxybenzoate or ethyl ester and 1,3-BDO are heated, makes to be completely dissolved, be added in above-mentioned mixed liquor；
(4) carbomer, water are added, is stirred；
(5) 30~50 DEG C are cooled to, raspberry Anthocyanin-rich Extract, raspberry fruit oil, raspberry polysaccharide, Lycium chinense fruit aqueous extract, rose is added
Rare colored water extract, continues to stir；
(6) continue to be down to room temperature, dispense.
9. essence described in claim 1~7 any one is being prepared with replenishing water and preserving moisture, whitening and anti-aging, sun-proof function
Purposes in skin care item.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710218664.9A CN106963683A (en) | 2017-04-05 | 2017-04-05 | A kind of essence containing raspberry |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710218664.9A CN106963683A (en) | 2017-04-05 | 2017-04-05 | A kind of essence containing raspberry |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106963683A true CN106963683A (en) | 2017-07-21 |
Family
ID=59336613
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|---|---|---|---|
| CN201710218664.9A Pending CN106963683A (en) | 2017-04-05 | 2017-04-05 | A kind of essence containing raspberry |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108783138A (en) * | 2018-07-05 | 2018-11-13 | 青岛海芬生态科技有限公司 | A kind of women face-nourishing health-care beverage and preparation method thereof |
| CN112521521A (en) * | 2020-12-09 | 2021-03-19 | 青海大学 | Polysaccharide SM-W and anti-tumor product prepared from same |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108783138A (en) * | 2018-07-05 | 2018-11-13 | 青岛海芬生态科技有限公司 | A kind of women face-nourishing health-care beverage and preparation method thereof |
| CN112521521A (en) * | 2020-12-09 | 2021-03-19 | 青海大学 | Polysaccharide SM-W and anti-tumor product prepared from same |
| CN112521521B (en) * | 2020-12-09 | 2021-11-05 | 青海大学 | Polysaccharide SM-W and anti-tumor product prepared from same |
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