CN107260576A - A kind of facial mask congealed fat containing Dendrobium officinale polysaccharide body and preparation method thereof - Google Patents

A kind of facial mask congealed fat containing Dendrobium officinale polysaccharide body and preparation method thereof Download PDF

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CN107260576A
CN107260576A CN201710378463.5A CN201710378463A CN107260576A CN 107260576 A CN107260576 A CN 107260576A CN 201710378463 A CN201710378463 A CN 201710378463A CN 107260576 A CN107260576 A CN 107260576A
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extract
parts
facial mask
dendrobium officinale
officinale polysaccharide
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CN107260576B (en
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陈永刚
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Hangzhou Qiandao hufuxi Industrial Co.,Ltd.
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Metal And Stone Bio Tech Ltd Zhejiang
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL, OR TOILET PURPOSES
    • A61K8/00Cosmetics or similar toilet preparations
    • A61K8/18Cosmetics or similar toilet preparations characterised by the composition
    • A61K8/96Cosmetics or similar toilet preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toilet preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL, OR TOILET PURPOSES
    • A61K8/00Cosmetics or similar toilet preparations
    • A61K8/18Cosmetics or similar toilet preparations characterised by the composition
    • A61K8/19Cosmetics or similar toilet preparations characterised by the composition containing inorganic ingredients
    • A61K8/29Titanium; Compounds thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL, OR TOILET PURPOSES
    • A61K8/00Cosmetics or similar toilet preparations
    • A61K8/18Cosmetics or similar toilet preparations characterised by the composition
    • A61K8/30Cosmetics or similar toilet preparations characterised by the composition containing organic compounds
    • A61K8/31Hydrocarbons
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL, OR TOILET PURPOSES
    • A61K8/00Cosmetics or similar toilet preparations
    • A61K8/18Cosmetics or similar toilet preparations characterised by the composition
    • A61K8/30Cosmetics or similar toilet preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toilet preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • A61K8/345Alcohols containing more than one hydroxy group
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL, OR TOILET PURPOSES
    • A61K8/00Cosmetics or similar toilet preparations
    • A61K8/18Cosmetics or similar toilet preparations characterised by the composition
    • A61K8/30Cosmetics or similar toilet preparations characterised by the composition containing organic compounds
    • A61K8/46Cosmetics or similar toilet preparations characterised by the composition containing organic compounds containing sulfur
    • A61K8/463Cosmetics or similar toilet preparations characterised by the composition containing organic compounds containing sulfur containing sulfuric acid derivatives, e.g. sodium lauryl sulfate
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL, OR TOILET PURPOSES
    • A61K8/00Cosmetics or similar toilet preparations
    • A61K8/18Cosmetics or similar toilet preparations characterised by the composition
    • A61K8/30Cosmetics or similar toilet preparations characterised by the composition containing organic compounds
    • A61K8/46Cosmetics or similar toilet preparations characterised by the composition containing organic compounds containing sulfur
    • A61K8/466Cosmetics or similar toilet preparations characterised by the composition containing organic compounds containing sulfur containing sulfonic acid derivatives; Salts
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL, OR TOILET PURPOSES
    • A61K8/00Cosmetics or similar toilet preparations
    • A61K8/18Cosmetics or similar toilet preparations characterised by the composition
    • A61K8/30Cosmetics or similar toilet preparations characterised by the composition containing organic compounds
    • A61K8/49Cosmetics or similar toilet preparations characterised by the composition containing organic compounds containing heterocyclic compounds
    • A61K8/494Cosmetics or similar toilet preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL, OR TOILET PURPOSES
    • A61K8/00Cosmetics or similar toilet preparations
    • A61K8/18Cosmetics or similar toilet preparations characterised by the composition
    • A61K8/30Cosmetics or similar toilet preparations characterised by the composition containing organic compounds
    • A61K8/64Proteins; Peptides; Derivatives or degradation products thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL, OR TOILET PURPOSES
    • A61K8/00Cosmetics or similar toilet preparations
    • A61K8/18Cosmetics or similar toilet preparations characterised by the composition
    • A61K8/72Cosmetics or similar toilet preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • A61K8/732Starch; Amylose; Amylopectin; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL, OR TOILET PURPOSES
    • A61K8/00Cosmetics or similar toilet preparations
    • A61K8/18Cosmetics or similar toilet preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILET PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08BPOLYSACCHARIDES; DERIVATIVES THEREOF
    • C08B37/00Preparation of polysaccharides not provided for in groups C08B1/00 - C08B35/00; Derivatives thereof
    • C08B37/0003General processes for their isolation or fractionation, e.g. purification or extraction from biomass
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL, OR TOILET PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/54Polymers characterized by specific structures/properties
    • A61K2800/548Associative polymers
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL, OR TOILET PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/84Products or compounds obtained by lyophilisation, freeze-drying

Abstract

The present invention relates to a kind of facial mask congealed fat containing Dendrobium officinale polysaccharide body and preparation method thereof, the Dendrobium officinale polysaccharide fibroin matched by specified weight, marine algae extract, aloe extract, chlorophyll, cuke extract, Ganodenna Lucidum P.E, fiddlehead dish root extract, extractive of olive growing leaves, anise seed extract, camellia oil extract, ginkgo biloba p.e, poplar flower extract, beta glucan, cocounut oil acyl isethionic acid ester sodium, shea butter, glycerine, dendrobium candidum flower essential oil, laruyl alcohol sulfosuccinate disodium, lauric alcohol sodium sulfovinate, wheaten starch, paraffin, titanium dioxide, and appropriate distilled water, can be in the case where modification agent need not be dosed, produce softness, toughness is good, moisturizing, tender skin, the facial mask congealed fat of skin care, due to containing the polysaccharide body for being derived from dendrobium candidum, there is the tender skin of moisturizing, skin care, releive skin the effect of.

Description

A kind of facial mask congealed fat containing Dendrobium officinale polysaccharide body and preparation method thereof
Technical field
The present invention relates to facial mask manufacture field, more particularly to a kind of facial mask congealed fat containing Dendrobium officinale polysaccharide body and Its preparation method.
Background technology
Facial mask has increasingly been popularized as facial-care instrument in the crowd that likes to be beautiful, and in general, traditional facial mask is included One layer with the layer of cloth obtained by the materials such as cotton or chemical fibre, and the beautifying liquid or Essence being coated in the layer of cloth.By In the layer of cloth using being difficult to fit entirely with skin so that skin surface there are considerable the air gap with the cloth interlayer, Therefore cause the effect of percutaneous absorption beautifying liquid or Essence poor, form the harmful effects such as waste.
In order to improve this problem, so-called jelly facial mask or colloid facial mask are occurred in that on the market.But such facial mask is needed The plastics modification agent for promoting hardness is added, although this plastics modification agent can be unlikely to deform the facial mask manufactured, The degraded toughness of facial mask can be made, also easily because pull and fragmentation, and consumer skin's allergy may be caused, can not be careless.
The content of the invention
It is an object of the invention to provide a kind of facial mask congealed fat containing Dendrobium officinale polysaccharide body and preparation method thereof, Neng Gou In the case of modification agent need not being added, with softness, good toughness, moisturizing, tender skin, skin care and releive skin the effects such as.
Technical scheme
A kind of facial mask congealed fat containing Dendrobium officinale polysaccharide body, including following weight raw material composition:Dendrobium candidum Polysaccharide 2,5-8 parts, 2.0-6.5 parts of fibroin, 4 parts of marine algae extract, 2 parts of aloe extract, 1 part of chlorophyll, cuke carry 0.5 part of thing, 0.5 part of Ganodenna Lucidum P.E, 0.5 part of fiddlehead dish root extract, 0.5 part of extractive of olive growing leaves, anise seed is taken to extract 0.5 part of thing, 0.6 part of camellia oil extract, 0.5 part of ginkgo biloba p.e, 0.5 part of poplar flower extract, 3 parts of β-glucan, coconut palm 25 parts of oleoyl isethionic acid ester sodium, 5 parts of shea butter, 5 parts of glycerine, 0.8 part of dendrobium candidum flower essential oil, laruyl alcohol sulfosuccinic acid 4-10 parts of ester disodium, 3-6 parts of lauric alcohol sodium sulfovinate, 8 parts of wheaten starch, 0.5-2.5 parts of paraffin, 0.1-0.3 parts of titanium dioxide, And appropriate distilled water.
A kind of facial mask congealed fat preparation method containing Dendrobium officinale polysaccharide body, is comprised the steps of:
Step is 1.:Sieving is placed into hot water and extracted 3-6 times after being smashed after dendrobium candidum is freeze-dried by disintegrating machine, By centrifuging and taking liquid and filtered, then reduced vacuum is concentrated into after the 1/10 of original volume, alcohol precipitation by centrifuging simultaneously Dendrobium officinale polysaccharide is obtained after frozen drying standby;
Step is 2.:Dendrobium candidum flower raw material freeze-drying is weighed after sieving, filled by disintegrating machine grinding and sieving Material, then extracts that discrete after essential oil condensation to obtain dendrobium candidum flower essential oil finished product standby by steam distillation;
Step is 3.:Laruyl alcohol sulfosuccinate disodium, lauric alcohol sodium sulfovinate, the wheat that predetermined weight is matched form sediment Powder, paraffin, glycerine, titanium dioxide and the smart matter emulsification of distilled water feeding homogeneous emulsifying machine, mixing and emulsifying is into semi-finished product for standby;
Step is 4.:Fibroin that predetermined weight is matched, marine algae extract, aloe extract, chlorophyll, cuke carry Take thing, Ganodenna Lucidum P.E, fiddlehead dish root extract, extractive of olive growing leaves, poplar flower extract, anise seed extract, camellia The iron sheet of oil extract, ginkgo biloba p.e, beta glucan, cocounut oil acyl isethionic acid ester sodium, shea butter, step 1. middle extraction After the dendrobium candidum flower essential oil finished product of dendrobium polysaccharide, step 2. middle extraction, the smart matter emulsion reaction obtained in adding step 3. Semi-finished product, mixing stand after by high-speed stirred and penetrating final molding in a mold after heating tank diameter heating;
Step is 5.:Finished product after ejection formation is prevented to carry out air drying in hothouse.
Further, step 1. in, hot water temperature is 55-100 DEG C, solid-liquid ratio is 1: 15~1: 50, when extracting every time Between be 2-4 hours, sifting step is after dendrobium candidum is crushed:First 100 mesh sieve coarse filtration, then cross 150 mesh refined filtrations.
Further, step 2. in, dendrobium candidum flower raw material sifting step be:First 50 mesh sieve coarse filtration, then cross 80 mesh Refined filtration.
Further, step 3. in, the smart matter emulsion reaction time be 12-48 hours.
Further, step 4. in, mixing time is 40-120 minute, and time of repose is 1-4 hour.
Further, step 4. in, during heating stirring, mixing speed is 500-1500 per minute turn, and heating-up temperature is 55-75 DEG C, time control is projected at 1.5-3.5 seconds.
Further, step 5. in, time of air drying is 2-4 days.
Further, the weight distribution ratio of the distilled water is 10-50 parts.
Beneficial effect
It is of the invention compared with present technology, with following significant effect:
Dendrobium officinale polysaccharide is polyhydroxyl polymer, and its polar group can form hydrogen bond with hydrone and combine water Point.Meanwhile, polysaccharide molecule chain, which is also interleaved with each other, to be reticulated, and plays very strong water retention with the Hydrogenbond of water in addition.In addition, In extracellular matrix, polysaccharide collectively constitutes the extracellular glue containing large quantity of moisture with the other polysaccharide components and celloglobulin in skin Shape matrix, moisture is provided for skin.On the other hand, it is because polysaccharide good filming performance in itself, can be formed in skin surface One layer of uniform film, so as to reduce the moisture evaporation of skin surface, preserves itself moisture so that moisture is from substrate microstructure Mass To cuticula, the further aquation of cuticula is induced, skin itself moisture is preserved, and then complete moisturizing effect.Therefore, the height of polysaccharide Degree water absorbing properties are ideally combined with good filming performance, and good moistening effect can be provided for skin.
In addition Dendrobium officinale polysaccharide is to belong to polysaccharide body material, when being applied to skin, can produce calmness, moisturizing, tender skin, shield Effect of skin and skin of releiving, and because dendrobium candidum extract is extracted via biotechnology technology, in addition to quite natural Also it is quite environmentally friendly, will not more harmful effect be produced to human body skin.
Embodiment
For a better understanding of the present invention, with reference to the embodiment content that the present invention is furture elucidated, but the present invention Content is not limited solely to the following examples.
The invention discloses a kind of facial mask congealed fat containing Dendrobium officinale polysaccharide body, including following weight raw material group Into:
2.5-8 parts of Dendrobium officinale polysaccharide,
2.0-6.5 parts of fibroin,
4 parts of marine algae extract,
2 parts of aloe extract,
1 part of chlorophyll,
0.5 part of cuke extract,
0.5 part of Ganodenna Lucidum P.E,
0.5 part of fiddlehead dish root extract,
0.5 part of extractive of olive growing leaves,
0.5 part of anise seed extract,
0.6 part of camellia oil extract,
0.5 part of ginkgo biloba p.e,
0.5 part of poplar flower extract,
3 parts of beta glucan,
25 parts of cocounut oil acyl isethionic acid ester sodium,
5 parts of shea butter,
5 parts of glycerine,
0.8 part of dendrobium candidum flower essential oil,
4-10 parts of laruyl alcohol sulfosuccinate disodium,
3-6 parts of lauric alcohol sodium sulfovinate,
8 parts of wheaten starch,
0.5-2.5 parts of paraffin,
0.1-0.3 parts of titanium dioxide,
10-50 parts of distilled water.
A kind of facial mask congealed fat preparation method containing Dendrobium officinale polysaccharide body, is comprised the steps of:
Step is 1.
Sieving is placed into hot water and extracted 3-6 times after being smashed after dendrobium candidum is freeze-dried by disintegrating machine, solid-liquid ratio For 1: 15~1: 50;
By centrifuging and taking liquid and filtered, then reduced vacuum be concentrated into after the 1/10 of original volume, alcohol precipitation by from The heart is separated and that Dendrobium officinale polysaccharide is obtained after frozen drying is standby;
Wherein hot water temperature be 55-100 DEG C, each extraction time be 2-4 hours, dendrobium candidum crush after sifting step For:First 100 mesh sieve coarse filtration, then cross 150 mesh refined filtrations.
Step is 2.
By dendrobium candidum flower raw material freeze-drying, by disintegrating machine grinding and sieving, (first 50 mesh sieve coarse filtration, then cross 80 mesh Refined filtration);
Weighed, fed after sieving;
Then extract that discrete after essential oil condensation to obtain dendrobium candidum flower essential oil finished product standby by steam distillation.
Step is 3.
Laruyl alcohol sulfosuccinate disodium that predetermined weight is matched, lauric alcohol sodium sulfovinate, wheaten starch, paraffin, Glycerine, titanium dioxide and distilled water send into homogeneous emulsifying machine smart matter emulsion reaction 12-48 hours, and mixing and emulsifying is standby into semi-finished product With.
Step is 4.
Predetermined weight is matched
Fibroin,
Marine algae extract,
Aloe extract,
Chlorophyll,
Cuke extract,
Ganodenna Lucidum P.E,
Fiddlehead dish root extract,
Extractive of olive growing leaves,
Poplar flower extract,
Anise seed extract,
Camellia oil extract,
Ginkgo biloba p.e,
Beta glucan,
Cocounut oil acyl isethionic acid ester sodium,
Shea butter,
Step 1. the Dendrobium officinale polysaccharide of middle extraction,
The dendrobium candidum flower essential oil finished product of step 2. middle extraction,
Step 3. in semi-finished product after obtained smart matter emulsion reaction,
Above-mentioned raw materials are mixed and stand 1-4 hour.Then 35-75 DEG C is heated to by heat tank diameter, with every point The rotating speed that clock 500-1500 turns quickly stirs to penetrate after 40-120 minutes to be molded in a mold, projects time control in 1.5-3.5 Second.
Step is 5.:Finished product after ejection formation is prevented to carry out air drying in hothouse, the time of air drying is 2-4 My god.
It is of the invention compared with present technology, with following significant effect:
Dendrobium officinale polysaccharide is polyhydroxyl polymer, and its polar group can form hydrogen bond with hydrone and combine water Point.Meanwhile, polysaccharide molecule chain, which is also interleaved with each other, to be reticulated, and plays very strong water retention with the Hydrogenbond of water in addition.In addition, In extracellular matrix, polysaccharide collectively constitutes the extracellular glue containing large quantity of moisture with the other polysaccharide components and celloglobulin in skin Shape matrix, moisture is provided for skin.
On the other hand, be because polysaccharide good filming performance in itself, can in one layer of uniform broad film of skin surface formation, So as to reduce the moisture evaporation of skin surface, itself moisture is preserved so that moisture induces angle from substrate microstructure Mass to cuticula Matter layer further aquation, preservation skin itself moisture, and then complete moisturizing effect.
Therefore, the high moisture absorption performance of polysaccharide is ideally combined with good filming performance, can be provided for skin well Moistening effect.
In addition Dendrobium officinale polysaccharide is to belong to polysaccharide body material, when being applied to skin, can produce calmness, moisturizing, tender skin, shield Effect of skin and skin of releiving, and because dendrobium candidum extract is extracted via biotechnology technology, in addition to quite natural Also it is quite environmentally friendly, will not more harmful effect be produced to human body skin.
Specifically, the present invention carries out following prepare according to above-mentioned preparation method.
First 100 mesh sieve coarse filtration are smashed by disintegrating machine after dendrobium candidum is freeze-dried, 150 mesh refined filtrations are then crossed, it is fixed Solid-liquid ratio 1: 50, extraction time 2.5h, extraction time are 3 times, and single factor test is done to Dendrobium officinale polysaccharide yield with Extracting temperature Experiment.Design Extracting temperature be 60,70,80,90,100 DEG C, the results are shown in Table one.
The influence of table one, extraction temperature to Dendrobium officinale polysaccharide yield
Temperature (DEG C) 60 70 80 90 100
Yield (%) 30.4 35.6 38.9 34.1 36.3
As shown in Table 1, for dendrobium candidum, extracted in the hot water in 60~100 DEG C, with the rise of temperature, yield Rise, begun to decline after reaching maximum at 80 DEG C;As temperature is further raised, yield has risen again, due to temperature Rise causes par-tial polysaccharide to be degraded, peak when yield is not less than 70 DEG C in 100 DEG C of maximum temperature, the choosing of optimum extraction temperature Select more suitable at 80 DEG C or so.
Further, 150 mesh dendrobium candidums are set, fixed solid-liquid ratio 1: 50, Extracting temperature are 80 DEG C, extraction time is equal For 3 times, design extraction time be 1.0,1.5,2.0,2.5,3.0h, the results are shown in Table two.
The influence of table two, extraction time to Dendrobium officinale polysaccharide yield
Time (h) 1.0 1.5 2.0 2.5 3.0
Yield (%) 26.1 28.2 31.9 28.4 29.7
As shown in Table 2, for dendrobium candidum, in 1.0~2.0h, with the extension of time, yield is continuously increased, Have falling at 2.5h, slightly go up afterwards, but yield not less than 2.0h when.Therefore, optimum extraction selection of time 2.0h or so compared with To be suitable.
Further, the dendrobium candidum after 150 mesh fine screens, fixed solid-liquid ratio 1: 40,2 hours extraction times, extraction are chosen Temperature is 80 DEG C, and design extraction time is 1,2,3,4,5, the results are shown in Table three.
The influence of table three, extraction time to Dendrobium officinale polysaccharide yield
As extraction time increases it can be seen from table three, the extract yield increase of polysaccharide, but extraction time is more than 3 times After, the polysaccharide increase of dissolution is not obvious, and the polysaccharide in possible crude drug illustrates extraction time to polysaccharide close to whole dissolutions Extract yield has an impact.Therefore, optimum extraction selection of times is more suitable at 3 times or so.
Further, influence of the solid-liquid ratio to Dendrobium officinale polysaccharide yield:The dendrobium candidum after 150 mesh fine screens is taken, is carried To take temperature be 80 DEG C, extraction time 2h, extraction time are 3 times, and design solid-liquid ratio is 1: 20,1: 25,1: 30,1: 35,1: 40, it the results are shown in Table four.
The influence of table four, solid-liquid ratio to Dendrobium officinale polysaccharide yield
Solid-liquid ratio 1∶20 1∶25 1∶30 1∶35 1∶40
Yield (%) 27.2 30.1. 32.4 30.2 29.7
As shown in Table 4, the increase of solid-liquid ratio is more obvious to the effect of dendrobium polysaccharide yield.For dendrobium candidum, 1: Between 20~1: 30, polysaccharide yield significantly rises;Fall after rise, risen again at 1: 40 afterwards, rising degree and 1 at 1: 35: 25 is close.Consider cost savings, therefore, optimal solid-liquid ratio selection is more suitable 1: 30 or so.
Further, dendrobium candidum flower raw material freeze-drying by disintegrating machine grinding and sieving (first 50 mesh sieve coarse filtration, so 80 mesh refined filtrations are crossed afterwards), weighed, fed after sieving, then obtain iron by discrete after steam distillation extraction essential oil condensation Skin stem of noble dendrobium flower essential oil finished product weigh leave and take it is standby;
Further, laruyl alcohol sulfosuccinate disodium, lauric alcohol sodium sulfovinate, wheat predetermined weight matched Starch, paraffin, glycerine, titanium dioxide and the smart matter emulsion reaction of distilled water feeding homogeneous emulsifying machine 18 hours, mixing and emulsifying into Semi-finished product for standby;
Fibroin that predetermined weight is matched, marine algae extract, aloe extract, chlorophyll, cuke extract, spirit Sesame extract, fiddlehead dish root extract, extractive of olive growing leaves, poplar flower extract, anise seed extract, camellia oil extract The dendrobium candidum of thing, ginkgo biloba p.e, beta glucan, cocounut oil acyl isethionic acid ester sodium, shea butter, step 1. middle extraction is more After sugar, the dendrobium candidum flower essential oil finished product of step 2. middle extraction, the smart matter emulsion reaction obtained in adding step 3. half into Product, mixing stands 2 hours.Then 50 DEG C are heated to by heat tank diameter, are quickly stirred with 800 turns per minute of rotating speed Penetrate and be molded in a mold after 120 minutes, project time control at 1.5 seconds.
The present embodiment, according to above-mentioned steps, is prepared by the raw material of specific weight proportion, and according to different weight ratio The finished product effect for carrying out multiple embodiments is compared, and following table five is to compare with reference to table.
Table five, compare with reference to table (unit:Part)
Described above, the above embodiments are merely illustrative of the technical solutions of the present invention, rather than its limitations;Although with reference to before Embodiment is stated the present invention is described in detail, it will be understood by those within the art that:It still can be to preceding State the technical scheme described in each embodiment to modify, or equivalent substitution is carried out to which part technical characteristic;And these Modification is replaced, and the essence of appropriate technical solution is departed from the spirit and scope of various embodiments of the present invention technical scheme.

Claims (9)

1. a kind of facial mask congealed fat containing Dendrobium officinale polysaccharide body, it is characterised in that including following weight raw material composition: 2.5-8 parts of Dendrobium officinale polysaccharide, 2.0-6.5 parts of fibroin, 4 parts of marine algae extract, 2 parts of aloe extract, 1 part of chlorophyll, 0.5 part of cuke extract, 0.5 part of Ganodenna Lucidum P.E, 0.5 part of fiddlehead dish root extract, 0.5 part of extractive of olive growing leaves, fennel Fragrant 0.5 part of seed extract, 0.6 part of camellia oil extract, 0.5 part of ginkgo biloba p.e, 0.5 part of poplar flower extract, β-Portugal gather 3 parts of sugar, 25 parts of cocounut oil acyl isethionic acid ester sodium, 5 parts of shea butter, 5 parts of glycerine, 0.8 part of dendrobium candidum flower essential oil, laruyl alcohol sulphur 4-10 parts of base succinate disodium, 3-6 parts of lauric alcohol sodium sulfovinate, 8 parts of wheaten starch, 0.5-2.5 parts of paraffin, titanium dioxide 0.1-0.3 parts and appropriate distilled water.
2. a kind of facial mask congealed fat preparation method containing Dendrobium officinale polysaccharide body, it is characterised in that comprise the steps of:
Step is 1.:Sieving is placed into hot water and extracted 3-6 times after being smashed after dendrobium candidum is freeze-dried by disintegrating machine, passes through Centrifuging and taking liquid is simultaneously filtered, and then reduced vacuum is concentrated into after the 1/10 of original volume, alcohol precipitation by centrifuging and through low It is standby that Dendrobium officinale polysaccharide is obtained after temperature freeze-drying;
Step is 2.:Dendrobium candidum flower raw material freeze-drying is weighed after sieving, fed, so by disintegrating machine grinding and sieving Extract that discrete after essential oil condensation to obtain dendrobium candidum flower essential oil finished product standby by steam distillation afterwards;
Step is 3.:Laruyl alcohol sulfosuccinate disodium, lauric alcohol sodium sulfovinate, wheaten starch, the stone that predetermined weight is matched Wax, glycerine, titanium dioxide and the smart matter emulsification of distilled water feeding homogeneous emulsifying machine, mixing and emulsifying is into semi-finished product for standby;
Step is 4.:Fibroin that predetermined weight is matched, marine algae extract, aloe extract, chlorophyll, cuke are extracted Thing, Ganodenna Lucidum P.E, fiddlehead dish root extract, extractive of olive growing leaves, poplar flower extract, anise seed extract, camellia oil The iron sheet stone of extract, ginkgo biloba p.e, beta glucan, cocounut oil acyl isethionic acid ester sodium, shea butter, step 1. middle extraction After the dendrobium candidum flower essential oil finished product of dry measure used in former times polysaccharide, step 2. middle extraction, the smart matter emulsion reaction obtained in adding step 3. Semi-finished product, high-speed stirred and final molding in a mold is penetrated after mixing is stood after heating by heating tank diameter;
Step is 5.:Finished product after ejection formation is prevented to carry out air drying in hothouse.
3. a kind of facial mask congealed fat preparation method containing Dendrobium officinale polysaccharide body according to claim 2, it is characterised in that Step 1. in, hot water temperature is 55-100 DEG C, solid-liquid ratio is 1: 15~1: 50, and each extraction time is 2-4 hours, iron sheet stone Dry measure used in former times grinding and sieving step is:First 100 mesh sieve coarse filtration, then cross 150 mesh refined filtrations.
4. a kind of facial mask congealed fat preparation method containing Dendrobium officinale polysaccharide body according to claim 2, it is characterised in that Step 2. in, dendrobium candidum flower raw material sifting step be:50 mesh sieve coarse filtration are crossed, 80 mesh refined filtrations are then crossed.
5. a kind of facial mask congealed fat preparation method containing Dendrobium officinale polysaccharide body according to claim 3, it is characterised in that Step 3. in, the smart matter emulsion reaction time be 12-48 hours.
6. a kind of facial mask congealed fat preparation method containing Dendrobium officinale polysaccharide body according to claim 2, it is characterised in that Step 4. in, mixing time is 40-120 minute, and time of repose is 1-4 hour.
7. a kind of facial mask congealed fat preparation method containing Dendrobium officinale polysaccharide body according to claim 2, it is characterised in that Step 4. in, heating stirring when, mixing speed be 500-1500 per minute turn, heating-up temperature be 55-75 DEG C, injection time control At 1.5-3.5 seconds.
8. a kind of facial mask congealed fat preparation method containing Dendrobium officinale polysaccharide body according to claim 2, it is characterised in that Step 5. in, time of air drying is 2-4 days.
9. a kind of facial mask congealed fat preparation method containing Dendrobium officinale polysaccharide body according to claim 1, it is characterised in that The weight distribution ratio of the distilled water is 10-50 parts.
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