The content of the invention
It is an object of the invention to provide a kind of facial mask congealed fat containing Dendrobium officinale polysaccharide body and preparation method thereof, Neng Gou
In the case of modification agent need not being added, with softness, good toughness, moisturizing, tender skin, skin care and releive skin the effects such as.
Technical scheme
A kind of facial mask congealed fat containing Dendrobium officinale polysaccharide body, including following weight raw material composition:Dendrobium candidum
Polysaccharide 2,5-8 parts, 2.0-6.5 parts of fibroin, 4 parts of marine algae extract, 2 parts of aloe extract, 1 part of chlorophyll, cuke carry
0.5 part of thing, 0.5 part of Ganodenna Lucidum P.E, 0.5 part of fiddlehead dish root extract, 0.5 part of extractive of olive growing leaves, anise seed is taken to extract
0.5 part of thing, 0.6 part of camellia oil extract, 0.5 part of ginkgo biloba p.e, 0.5 part of poplar flower extract, 3 parts of β-glucan, coconut palm
25 parts of oleoyl isethionic acid ester sodium, 5 parts of shea butter, 5 parts of glycerine, 0.8 part of dendrobium candidum flower essential oil, laruyl alcohol sulfosuccinic acid
4-10 parts of ester disodium, 3-6 parts of lauric alcohol sodium sulfovinate, 8 parts of wheaten starch, 0.5-2.5 parts of paraffin, 0.1-0.3 parts of titanium dioxide,
And appropriate distilled water.
A kind of facial mask congealed fat preparation method containing Dendrobium officinale polysaccharide body, is comprised the steps of:
Step is 1.:Sieving is placed into hot water and extracted 3-6 times after being smashed after dendrobium candidum is freeze-dried by disintegrating machine,
By centrifuging and taking liquid and filtered, then reduced vacuum is concentrated into after the 1/10 of original volume, alcohol precipitation by centrifuging simultaneously
Dendrobium officinale polysaccharide is obtained after frozen drying standby;
Step is 2.:Dendrobium candidum flower raw material freeze-drying is weighed after sieving, filled by disintegrating machine grinding and sieving
Material, then extracts that discrete after essential oil condensation to obtain dendrobium candidum flower essential oil finished product standby by steam distillation;
Step is 3.:Laruyl alcohol sulfosuccinate disodium, lauric alcohol sodium sulfovinate, the wheat that predetermined weight is matched form sediment
Powder, paraffin, glycerine, titanium dioxide and the smart matter emulsification of distilled water feeding homogeneous emulsifying machine, mixing and emulsifying is into semi-finished product for standby;
Step is 4.:Fibroin that predetermined weight is matched, marine algae extract, aloe extract, chlorophyll, cuke carry
Take thing, Ganodenna Lucidum P.E, fiddlehead dish root extract, extractive of olive growing leaves, poplar flower extract, anise seed extract, camellia
The iron sheet of oil extract, ginkgo biloba p.e, beta glucan, cocounut oil acyl isethionic acid ester sodium, shea butter, step 1. middle extraction
After the dendrobium candidum flower essential oil finished product of dendrobium polysaccharide, step 2. middle extraction, the smart matter emulsion reaction obtained in adding step 3.
Semi-finished product, mixing stand after by high-speed stirred and penetrating final molding in a mold after heating tank diameter heating;
Step is 5.:Finished product after ejection formation is prevented to carry out air drying in hothouse.
Further, step 1. in, hot water temperature is 55-100 DEG C, solid-liquid ratio is 1: 15~1: 50, when extracting every time
Between be 2-4 hours, sifting step is after dendrobium candidum is crushed:First 100 mesh sieve coarse filtration, then cross 150 mesh refined filtrations.
Further, step 2. in, dendrobium candidum flower raw material sifting step be:First 50 mesh sieve coarse filtration, then cross 80 mesh
Refined filtration.
Further, step 3. in, the smart matter emulsion reaction time be 12-48 hours.
Further, step 4. in, mixing time is 40-120 minute, and time of repose is 1-4 hour.
Further, step 4. in, during heating stirring, mixing speed is 500-1500 per minute turn, and heating-up temperature is
55-75 DEG C, time control is projected at 1.5-3.5 seconds.
Further, step 5. in, time of air drying is 2-4 days.
Further, the weight distribution ratio of the distilled water is 10-50 parts.
Beneficial effect
It is of the invention compared with present technology, with following significant effect:
Dendrobium officinale polysaccharide is polyhydroxyl polymer, and its polar group can form hydrogen bond with hydrone and combine water
Point.Meanwhile, polysaccharide molecule chain, which is also interleaved with each other, to be reticulated, and plays very strong water retention with the Hydrogenbond of water in addition.In addition,
In extracellular matrix, polysaccharide collectively constitutes the extracellular glue containing large quantity of moisture with the other polysaccharide components and celloglobulin in skin
Shape matrix, moisture is provided for skin.On the other hand, it is because polysaccharide good filming performance in itself, can be formed in skin surface
One layer of uniform film, so as to reduce the moisture evaporation of skin surface, preserves itself moisture so that moisture is from substrate microstructure Mass
To cuticula, the further aquation of cuticula is induced, skin itself moisture is preserved, and then complete moisturizing effect.Therefore, the height of polysaccharide
Degree water absorbing properties are ideally combined with good filming performance, and good moistening effect can be provided for skin.
In addition Dendrobium officinale polysaccharide is to belong to polysaccharide body material, when being applied to skin, can produce calmness, moisturizing, tender skin, shield
Effect of skin and skin of releiving, and because dendrobium candidum extract is extracted via biotechnology technology, in addition to quite natural
Also it is quite environmentally friendly, will not more harmful effect be produced to human body skin.
Embodiment
For a better understanding of the present invention, with reference to the embodiment content that the present invention is furture elucidated, but the present invention
Content is not limited solely to the following examples.
The invention discloses a kind of facial mask congealed fat containing Dendrobium officinale polysaccharide body, including following weight raw material group
Into:
2.5-8 parts of Dendrobium officinale polysaccharide,
2.0-6.5 parts of fibroin,
4 parts of marine algae extract,
2 parts of aloe extract,
1 part of chlorophyll,
0.5 part of cuke extract,
0.5 part of Ganodenna Lucidum P.E,
0.5 part of fiddlehead dish root extract,
0.5 part of extractive of olive growing leaves,
0.5 part of anise seed extract,
0.6 part of camellia oil extract,
0.5 part of ginkgo biloba p.e,
0.5 part of poplar flower extract,
3 parts of beta glucan,
25 parts of cocounut oil acyl isethionic acid ester sodium,
5 parts of shea butter,
5 parts of glycerine,
0.8 part of dendrobium candidum flower essential oil,
4-10 parts of laruyl alcohol sulfosuccinate disodium,
3-6 parts of lauric alcohol sodium sulfovinate,
8 parts of wheaten starch,
0.5-2.5 parts of paraffin,
0.1-0.3 parts of titanium dioxide,
10-50 parts of distilled water.
A kind of facial mask congealed fat preparation method containing Dendrobium officinale polysaccharide body, is comprised the steps of:
Step is 1.
Sieving is placed into hot water and extracted 3-6 times after being smashed after dendrobium candidum is freeze-dried by disintegrating machine, solid-liquid ratio
For 1: 15~1: 50;
By centrifuging and taking liquid and filtered, then reduced vacuum be concentrated into after the 1/10 of original volume, alcohol precipitation by from
The heart is separated and that Dendrobium officinale polysaccharide is obtained after frozen drying is standby;
Wherein hot water temperature be 55-100 DEG C, each extraction time be 2-4 hours, dendrobium candidum crush after sifting step
For:First 100 mesh sieve coarse filtration, then cross 150 mesh refined filtrations.
Step is 2.
By dendrobium candidum flower raw material freeze-drying, by disintegrating machine grinding and sieving, (first 50 mesh sieve coarse filtration, then cross 80 mesh
Refined filtration);
Weighed, fed after sieving;
Then extract that discrete after essential oil condensation to obtain dendrobium candidum flower essential oil finished product standby by steam distillation.
Step is 3.
Laruyl alcohol sulfosuccinate disodium that predetermined weight is matched, lauric alcohol sodium sulfovinate, wheaten starch, paraffin,
Glycerine, titanium dioxide and distilled water send into homogeneous emulsifying machine smart matter emulsion reaction 12-48 hours, and mixing and emulsifying is standby into semi-finished product
With.
Step is 4.
Predetermined weight is matched
Fibroin,
Marine algae extract,
Aloe extract,
Chlorophyll,
Cuke extract,
Ganodenna Lucidum P.E,
Fiddlehead dish root extract,
Extractive of olive growing leaves,
Poplar flower extract,
Anise seed extract,
Camellia oil extract,
Ginkgo biloba p.e,
Beta glucan,
Cocounut oil acyl isethionic acid ester sodium,
Shea butter,
Step 1. the Dendrobium officinale polysaccharide of middle extraction,
The dendrobium candidum flower essential oil finished product of step 2. middle extraction,
Step 3. in semi-finished product after obtained smart matter emulsion reaction,
Above-mentioned raw materials are mixed and stand 1-4 hour.Then 35-75 DEG C is heated to by heat tank diameter, with every point
The rotating speed that clock 500-1500 turns quickly stirs to penetrate after 40-120 minutes to be molded in a mold, projects time control in 1.5-3.5
Second.
Step is 5.:Finished product after ejection formation is prevented to carry out air drying in hothouse, the time of air drying is 2-4
My god.
It is of the invention compared with present technology, with following significant effect:
Dendrobium officinale polysaccharide is polyhydroxyl polymer, and its polar group can form hydrogen bond with hydrone and combine water
Point.Meanwhile, polysaccharide molecule chain, which is also interleaved with each other, to be reticulated, and plays very strong water retention with the Hydrogenbond of water in addition.In addition,
In extracellular matrix, polysaccharide collectively constitutes the extracellular glue containing large quantity of moisture with the other polysaccharide components and celloglobulin in skin
Shape matrix, moisture is provided for skin.
On the other hand, be because polysaccharide good filming performance in itself, can in one layer of uniform broad film of skin surface formation,
So as to reduce the moisture evaporation of skin surface, itself moisture is preserved so that moisture induces angle from substrate microstructure Mass to cuticula
Matter layer further aquation, preservation skin itself moisture, and then complete moisturizing effect.
Therefore, the high moisture absorption performance of polysaccharide is ideally combined with good filming performance, can be provided for skin well
Moistening effect.
In addition Dendrobium officinale polysaccharide is to belong to polysaccharide body material, when being applied to skin, can produce calmness, moisturizing, tender skin, shield
Effect of skin and skin of releiving, and because dendrobium candidum extract is extracted via biotechnology technology, in addition to quite natural
Also it is quite environmentally friendly, will not more harmful effect be produced to human body skin.
Specifically, the present invention carries out following prepare according to above-mentioned preparation method.
First 100 mesh sieve coarse filtration are smashed by disintegrating machine after dendrobium candidum is freeze-dried, 150 mesh refined filtrations are then crossed, it is fixed
Solid-liquid ratio 1: 50, extraction time 2.5h, extraction time are 3 times, and single factor test is done to Dendrobium officinale polysaccharide yield with Extracting temperature
Experiment.Design Extracting temperature be 60,70,80,90,100 DEG C, the results are shown in Table one.
The influence of table one, extraction temperature to Dendrobium officinale polysaccharide yield
Temperature (DEG C) |
60 |
70 |
80 |
90 |
100 |
Yield (%) |
30.4 |
35.6 |
38.9 |
34.1 |
36.3 |
As shown in Table 1, for dendrobium candidum, extracted in the hot water in 60~100 DEG C, with the rise of temperature, yield
Rise, begun to decline after reaching maximum at 80 DEG C;As temperature is further raised, yield has risen again, due to temperature
Rise causes par-tial polysaccharide to be degraded, peak when yield is not less than 70 DEG C in 100 DEG C of maximum temperature, the choosing of optimum extraction temperature
Select more suitable at 80 DEG C or so.
Further, 150 mesh dendrobium candidums are set, fixed solid-liquid ratio 1: 50, Extracting temperature are 80 DEG C, extraction time is equal
For 3 times, design extraction time be 1.0,1.5,2.0,2.5,3.0h, the results are shown in Table two.
The influence of table two, extraction time to Dendrobium officinale polysaccharide yield
Time (h) |
1.0 |
1.5 |
2.0 |
2.5 |
3.0 |
Yield (%) |
26.1 |
28.2 |
31.9 |
28.4 |
29.7 |
As shown in Table 2, for dendrobium candidum, in 1.0~2.0h, with the extension of time, yield is continuously increased,
Have falling at 2.5h, slightly go up afterwards, but yield not less than 2.0h when.Therefore, optimum extraction selection of time 2.0h or so compared with
To be suitable.
Further, the dendrobium candidum after 150 mesh fine screens, fixed solid-liquid ratio 1: 40,2 hours extraction times, extraction are chosen
Temperature is 80 DEG C, and design extraction time is 1,2,3,4,5, the results are shown in Table three.
The influence of table three, extraction time to Dendrobium officinale polysaccharide yield
As extraction time increases it can be seen from table three, the extract yield increase of polysaccharide, but extraction time is more than 3 times
After, the polysaccharide increase of dissolution is not obvious, and the polysaccharide in possible crude drug illustrates extraction time to polysaccharide close to whole dissolutions
Extract yield has an impact.Therefore, optimum extraction selection of times is more suitable at 3 times or so.
Further, influence of the solid-liquid ratio to Dendrobium officinale polysaccharide yield:The dendrobium candidum after 150 mesh fine screens is taken, is carried
To take temperature be 80 DEG C, extraction time 2h, extraction time are 3 times, and design solid-liquid ratio is 1: 20,1: 25,1: 30,1: 35,1:
40, it the results are shown in Table four.
The influence of table four, solid-liquid ratio to Dendrobium officinale polysaccharide yield
Solid-liquid ratio |
1∶20 |
1∶25 |
1∶30 |
1∶35 |
1∶40 |
Yield (%) |
27.2 |
30.1. |
32.4 |
30.2 |
29.7 |
As shown in Table 4, the increase of solid-liquid ratio is more obvious to the effect of dendrobium polysaccharide yield.For dendrobium candidum, 1:
Between 20~1: 30, polysaccharide yield significantly rises;Fall after rise, risen again at 1: 40 afterwards, rising degree and 1 at 1: 35:
25 is close.Consider cost savings, therefore, optimal solid-liquid ratio selection is more suitable 1: 30 or so.
Further, dendrobium candidum flower raw material freeze-drying by disintegrating machine grinding and sieving (first 50 mesh sieve coarse filtration, so
80 mesh refined filtrations are crossed afterwards), weighed, fed after sieving, then obtain iron by discrete after steam distillation extraction essential oil condensation
Skin stem of noble dendrobium flower essential oil finished product weigh leave and take it is standby;
Further, laruyl alcohol sulfosuccinate disodium, lauric alcohol sodium sulfovinate, wheat predetermined weight matched
Starch, paraffin, glycerine, titanium dioxide and the smart matter emulsion reaction of distilled water feeding homogeneous emulsifying machine 18 hours, mixing and emulsifying into
Semi-finished product for standby;
Fibroin that predetermined weight is matched, marine algae extract, aloe extract, chlorophyll, cuke extract, spirit
Sesame extract, fiddlehead dish root extract, extractive of olive growing leaves, poplar flower extract, anise seed extract, camellia oil extract
The dendrobium candidum of thing, ginkgo biloba p.e, beta glucan, cocounut oil acyl isethionic acid ester sodium, shea butter, step 1. middle extraction is more
After sugar, the dendrobium candidum flower essential oil finished product of step 2. middle extraction, the smart matter emulsion reaction obtained in adding step 3. half into
Product, mixing stands 2 hours.Then 50 DEG C are heated to by heat tank diameter, are quickly stirred with 800 turns per minute of rotating speed
Penetrate and be molded in a mold after 120 minutes, project time control at 1.5 seconds.
The present embodiment, according to above-mentioned steps, is prepared by the raw material of specific weight proportion, and according to different weight ratio
The finished product effect for carrying out multiple embodiments is compared, and following table five is to compare with reference to table.
Table five, compare with reference to table (unit:Part)
Described above, the above embodiments are merely illustrative of the technical solutions of the present invention, rather than its limitations;Although with reference to before
Embodiment is stated the present invention is described in detail, it will be understood by those within the art that:It still can be to preceding
State the technical scheme described in each embodiment to modify, or equivalent substitution is carried out to which part technical characteristic;And these
Modification is replaced, and the essence of appropriate technical solution is departed from the spirit and scope of various embodiments of the present invention technical scheme.