CN101461763A - Method for producing cosmetics containing notoginseng polysaccharide and use - Google Patents
Method for producing cosmetics containing notoginseng polysaccharide and use Download PDFInfo
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- CN101461763A CN101461763A CNA2008102337724A CN200810233772A CN101461763A CN 101461763 A CN101461763 A CN 101461763A CN A2008102337724 A CNA2008102337724 A CN A2008102337724A CN 200810233772 A CN200810233772 A CN 200810233772A CN 101461763 A CN101461763 A CN 101461763A
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- radix notoginseng
- cosmetics
- water
- notoginseng polysaccharide
- polysaccharide
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Abstract
The invention relates to a preparation method for cosmetics containing notoginseng polysaccharide and application thereof. Supplementary materials such as a surfactant, an emulsifier, and the like are added into the polysaccharide extract mainly containing notoginseng to produce the cosmetics such as face cleaning emulsion, ionic water, extracted essence, water face mask, face cream, and the like; in addition, the cosmetic has the functions of keeping the skin wet and compensating water. The invention also discloses the preparation method for the cosmetics and the application thereof. The prepared cosmetic has obvious functions of keeping the skin wet and compensating water. The invention provides consumers with a better product.
Description
Technical field:
The invention belongs to the field of Chinese medicines, relate to the Radix Notoginseng polysaccharide purposes and preparation method thereof of the cosmetics that are effective component.
Background technology:
Radix Notoginseng is the root of Araliaceae herbaceos perennial Radix Notoginseng Panax notoginseng (Burk.) F.H.Chen, another name Radix Notoginseng, Radix Notoginseng.Mainly cultivating in Yunnan mountain of papers and Baise of Guangxi area, is the famous valuable ingredient of Chinese medicine of China, has hemostasis, looses effects such as silt, detumescence, pain relieving in recent years, and the research and development of Radix Notoginseng come into one's own day by day.The Radix Notoginseng complex chemical composition was just studied from the thirties, but after the seventies along with the separation of plant glycocide and the development of chemical constitution authenticate technology, significant progress has just been arranged.Result of study shows, contains soap two, flavone, aminoacid, polysaccharide, fatty acid, aliphatic alkynes class and skin compounds etc. in the Radix Notoginseng, is all having important exploitation to be worth aspect pharmaceuticals and the natural health-care products.Wherein, dammarane type Fourth Ring three mushrooms soaps two are considered to one of major physiological active component of Radix Notoginseng.So research in the past mainly concentrates on the arasaponin aspect, to the research of the polysaccharide component of Radix Notoginseng seldom, Radix Notoginseng polysaccharide of the present invention is applied to play in the cosmetics water conservation and mends the application of wet function and do not see that in the prior art report is arranged.
Summary of the invention:
The object of the present invention is to provide a kind of application process of Radix Notoginseng polysaccharide, this Radix Notoginseng polysaccharide can add in the cosmetics, makes the cosmetics of the moisturizing that is used to preserve moisture.
In order to achieve the above object, the present invention has taked following technological means:
Described Radix Notoginseng polysaccharide can prepare according to the following steps:
Get Radix Notoginseng or clip, be ground into 10～60 order granules, add 4～10 times of hot water and boil and carry 3 times, each 2h filters; Filtrate concentrates, and adds equal-volume ethanol, stirs, and leaves standstill 4～12h, filter, and collecting precipitation, drying gets Radix Notoginseng polysaccharide.
The Radix Notoginseng polysaccharide of this method preparation adds adjuvants such as surfactant, emulsifying agent respectively, can be made into cosmetics such as face breast, ionized water, essence, water surface film, facial cream, can play the effect of the moisturizing of preserving moisture.
Below, further specify the present invention with concrete enforcement example:
Embodiment 1: the balance face breast of preserving moisture
A phase: liquid paraffin 6% 16 octadecanol 3% lanoline 1% propylparaben 0.5%
B phase: propylene glycol 8% card ripple 9410.2% purified water 75.28% glycerol 5% Radix Notoginseng polysaccharide 1%
C phase: essence 0.02%
In the oil phase pot, add the A phase, open the jacket steam heating, look material and how much open stirring at low speed or manual stirring, slowly be warming up to 80～85 ℃, make raw material fusing and mix homogeneously.
B is added in the water pot, and adds the evaporated water of total growth 3%, open stirring at low speed, open the jacket steam heating, slowly be warming up to 80～85 ℃, make the abundant mix homogeneously of material.Open inlet valve, with in the material process filter suction emulsifying still in the oil cauldron, start simultaneously and scrape the limit agitator in the still with flexible pipe, temperature is controlled at 80～85 ℃, treat that material has advanced after, with the material in the kettle with flexible pipe through in the filter suction emulsifying still, it is constant to scrape the limit agitator speed in the still, temperature-resistant.
After biphase mixing, keep temperature and scrape the limit agitator speed constant, open homogenizer, open vacuum valve, observe liquid level by visor and adjust vacuum, 2500 rev/mins of homogenizing of homogenizing speed 4 minutes.Close homogenizing, continue to stir, be incubated 20 minutes.
Be incubated after 20 minutes, feed the chuck cooling water, it is constant to keep scraping the limit agitator speed, makes the system temperature middling speed be cooled to 55～60 ℃, adds C phase materials and mix homogeneously.
After mastic continues to be cooled to 35 ℃ in the emulsifying still, stop to scrape the limit and stir, close cooling water, vacuum breaker is put into clean Plastic Drum, packing with the mode of pressurization discharging with material in the pot.
Embodiment 2 ionized water of preserving moisture
A phase: allantoin 0.08% oily 3% purified water, 86.7% Radix Notoginseng polysaccharide, 2% reed fragrant plant glue 2%
B phase: 1% hyaluronic acid 2%
C phase: essence 0.02% methyl hydroxybenzoate 0.12% propylparaben 0.08% PG 4%
Pure water is dropped in the water pot earlier, and add the evaporated water of total growth 2%, under agitation add the A phase materials, feed the jacket steam heating, stirring at low speed is warming up to 80～85 ℃ and kept 20 minutes, forms system I, cooling;
Be cooled to 60 ℃, add the B phase materials, stir and continued cooling in 10 minutes;
Take by weighing propylene glycol, methyl hydroxybenzoate, propylparaben with a small container, heating in water bath to 60 ℃ stirring and dissolving is complete, lowers the temperature 45 ℃, adds essence and solubilizing agent and forms the C phase;
Feed the chuck cooling water and make system be cooled to 43～45 ℃, add the C phase materials, stir and make abundant mixing, dissolving; Be cooled to 35～40 ℃, through the filter screen discharging; Check.
Embodiment 3: balance moisturizing essence
A phase: transparent HANSHENGJIAO 0.3% glycerol 3% purified water 81% Radix Notoginseng polysaccharide 1% melon pulp element 0.5%
B phase: 1% hyaluronic acid 10%
C phase: PG 4% methyl hydroxybenzoate 0.1% propylparaben 0.1%
Accurately take by weighing hyaluronic acid and a part of purified water, content is controlled at about 1%, starts high speed agitator, makes its mix homogeneously; Accurately take by weighing transparent HANSHENGJIAO and glycerol, transparent HANSHENGJIAO is uniformly dispersed; Accurately take by weighing methyl hydroxybenzoate, propylparaben and propylene glycol, heat slightly, make Metagin, propyl ester dissolving fully.
Accurately take by weighing the A phase, drop in the preparation pot, add the water yield that evaporation consumes (total growth 2%), open and stir 50～55 rev/mins, be warming up to 80～85 ℃, be incubated 20 minutes.
Scattered HANSHENGJIAO under stirring condition, is slowly added in the preparation pot, feed cooling water temperature.
Be cooled to 60 ℃ and add the B phase materials, stir, slowly drip the mixed liquor of Metagin, propyl ester and propylene glycol, continue to stir, continue cooling after making the abundant mix homogeneously of material;
After being cooled to 35～40 ℃, stop to stir, in the washed in advance clean Plastic Drum of under filtercondition, material being packed into, packing, check.
Embodiment 4: water surface film
A phase: transparent HANSHENGJIAO 0.1% glycerol 7% purified water 80.4% Radix Notoginseng polysaccharide 2.6% melon pulp element 1.4%
B phase: hyaluronic acid 0.1%
C phase: glycyrrhizic acid dipotassium 0.1%
D phase: methyl hydroxybenzoate 0.12% propylparaben 0.08% propylene glycol 8% magnolia compound 0.1%
Go in the water pot A is congenial, open and stir, be warming up to 80-85 ℃ and kept 20～30 minutes; Feed the chuck cooling water and make system be cooled to 60～70 ℃, under agitation add the B phase, be stirred to the system transparent and homogeneous.
When system is cooled to below 50 ℃, add the C phase materials, stir and make abundant mixing, dissolving;
Take by weighing its mixing of the D mutual-assistance, add in the water pot that stirs, stir and made the system transparent and homogeneous in 20 minutes, through the filter screen discharging; Added a cover ageing 24 hours, check, packing.
Embodiment 5: facial cream
A phase: S2A 2.5% 16 mixes pure 3.5% liquid paraffin, 8% GTCC, 3% lanoline 0.8%
Methyl hydroxybenzoate 0.3%
B phase: glycerol 3% propylene glycol 5% Radix Puerariae flavone 0.2% Radix Notoginseng polysaccharide 1.5% purified water 67.18%
C phase: 1% hyaluronic acid 5%
D phase: essence 0.02%
In the oil phase pot, add the A phase, open the jacket steam heating, look material and how much open stirring at low speed or manual stirring, slowly be warming up to 80～85 ℃, make raw material fusing and mix homogeneously.
B is added in the water pot, and adds the evaporated water of total growth 3%, open stirring at low speed, open the jacket steam heating, slowly be warming up to 80～85 ℃, make the abundant mix homogeneously of material.
Place the regulation pipe valve foreheater temperature of emulsifying still, make it be job state, open emulsifying still vacuum valve then, open inlet valve, material in the oil cauldron is passed through in the filter suction emulsifying still with flexible pipe, start simultaneously and scrape the limit agitator in the still, temperature is controlled at 80～85 ℃, treat that material has advanced after, with the material in the kettle with flexible pipe through in the filter suction emulsifying still, it is constant to scrape the limit agitator speed in the still, temperature-resistant.
After biphase mixing, keep temperature and scrape the limit agitator speed constant, open homogenizer, open vacuum valve, observe liquid level by visor and adjust vacuum, 2500 rev/mins of homogenizing of homogenizing speed 5 minutes.Close homogenizing, continue to stir, be incubated 10 minutes, stir.
Feed the chuck cooling water, it is constant to keep scraping the limit agitator speed, makes the system temperature middling speed be cooled to 55～60 ℃, adds C phase materials and mix homogeneously; After system continues to be cooled to 43～45 ℃, add D phase materials and mix homogeneously successively.
After mastic continues to be cooled to 38～40 ℃ in the emulsifying still, stop to scrape the limit and stir, close cooling water, vacuum breaker is put into clean Plastic Drum with material in the pot, adds a cover ageing 12～24 hours, check, packing.
Embodiment 6:
Select 30-50 years old left and right sides female subjects, skin moisture≤12.Sooner or later use above-mentioned moisture-keeping cosmetics every day, used continuously 30 days, other establishes blank.
Method: measure forehead glabella skin moisture.Under rest state, dip in distilled water and clean tested position, dry back mensuration of carrying out moisture content in 15 minutes with clean cotton balls.Result such as following table:
Find out that from last table result the skin moisture of test group increases after applying some make up making, with use before compared significant difference (P＜0.01), comparing with matched group also has significant difference; The PH index changes not quite before and after using, and illustrates that this product is safer.
Claims (4)
1, a kind of purposes of Radix Notoginseng polysaccharide is characterized in that this Radix Notoginseng polysaccharide can be applicable in the cosmetics.
2, the application of Radix Notoginseng polysaccharide as claimed in claim 1 is characterized in that this Radix Notoginseng polysaccharide makes an addition to the cosmetics that can be made into the moisturizing of preserving moisture in the cosmetics.
3, according to claim 1, this Radix Notoginseng polysaccharide can be made into cosmetics such as face breast, ionized water, essence, water surface film, facial cream.
4, Radix Notoginseng polysaccharide as claimed in claim 1 is characterized in that preparing as follows:
Get Radix Notoginseng or clip, pulverize, adds 4～10 times of hot water and boil and propose filtration; Filtrate concentrates, and adds equal-volume ethanol, stirs, and leaves standstill 4～12h, filter, and collecting precipitation, drying gets Radix Notoginseng polysaccharide.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNA2008102337724A CN101461763A (en) | 2008-12-30 | 2008-12-30 | Method for producing cosmetics containing notoginseng polysaccharide and use |
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| CNA2008102337724A CN101461763A (en) | 2008-12-30 | 2008-12-30 | Method for producing cosmetics containing notoginseng polysaccharide and use |
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| CN101461763A true CN101461763A (en) | 2009-06-24 |
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| CNA2008102337724A Pending CN101461763A (en) | 2008-12-30 | 2008-12-30 | Method for producing cosmetics containing notoginseng polysaccharide and use |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106309157A (en) * | 2016-08-24 | 2017-01-11 | 刘艺鹏 | Moisture-preserving toner containing panax notoginseng polysaccharides |
| CN106309243A (en) * | 2016-10-06 | 2017-01-11 | 刘艺鹏 | Skin rejuvenation radix notoginseng polysaccharides facial mask |
| CN106361602A (en) * | 2016-08-24 | 2017-02-01 | 登封市科创商务咨询有限公司 | Panax notoginseng polysaccharide balancing and moisturizing lotion |
| CN107286265A (en) * | 2017-06-16 | 2017-10-24 | 云南多糖生物科技有限公司 | The method for extraction and purification and promotion cell propagation pharmacology activity research of a kind of neutral notoginseng polysaccharide and application |
| CN108158950A (en) * | 2018-03-08 | 2018-06-15 | 山东省农业科学院农产品研究所 | A kind of natural plants moisture saver mask stoste and preparation method thereof |
| CN108210369A (en) * | 2016-12-09 | 2018-06-29 | 景金发 | Notoginseng polysaccharide essence |
| CN112691079A (en) * | 2021-01-27 | 2021-04-23 | 吉林医药学院 | Foot bacteriostatic care solution containing traditional Chinese medicine extract and preparation method thereof |
| CN114931531A (en) * | 2022-05-10 | 2022-08-23 | 上海枫萃生物科技有限公司 | Compound stock solution for wrinkle-removing antioxidant cosmetics and preparation method thereof |
-
2008
- 2008-12-30 CN CNA2008102337724A patent/CN101461763A/en active Pending
Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106309157A (en) * | 2016-08-24 | 2017-01-11 | 刘艺鹏 | Moisture-preserving toner containing panax notoginseng polysaccharides |
| CN106361602A (en) * | 2016-08-24 | 2017-02-01 | 登封市科创商务咨询有限公司 | Panax notoginseng polysaccharide balancing and moisturizing lotion |
| CN106309243A (en) * | 2016-10-06 | 2017-01-11 | 刘艺鹏 | Skin rejuvenation radix notoginseng polysaccharides facial mask |
| CN108210369A (en) * | 2016-12-09 | 2018-06-29 | 景金发 | Notoginseng polysaccharide essence |
| CN107286265A (en) * | 2017-06-16 | 2017-10-24 | 云南多糖生物科技有限公司 | The method for extraction and purification and promotion cell propagation pharmacology activity research of a kind of neutral notoginseng polysaccharide and application |
| CN107286265B (en) * | 2017-06-16 | 2018-08-10 | 云南多糖生物科技有限公司 | It is a kind of neutrality notoginseng polysaccharide method for extraction and purification and promote cell Proliferation pharmacology activity research with application |
| CN108158950A (en) * | 2018-03-08 | 2018-06-15 | 山东省农业科学院农产品研究所 | A kind of natural plants moisture saver mask stoste and preparation method thereof |
| CN108158950B (en) * | 2018-03-08 | 2021-03-02 | 山东省农业科学院农产品研究所 | Natural plant moisturizing mask stock solution and preparation method thereof |
| CN112691079A (en) * | 2021-01-27 | 2021-04-23 | 吉林医药学院 | Foot bacteriostatic care solution containing traditional Chinese medicine extract and preparation method thereof |
| CN114931531A (en) * | 2022-05-10 | 2022-08-23 | 上海枫萃生物科技有限公司 | Compound stock solution for wrinkle-removing antioxidant cosmetics and preparation method thereof |
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Open date: 20090624 |