CN104083300A - Preparation method and product of skin cream - Google Patents
Preparation method and product of skin cream Download PDFInfo
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- CN104083300A CN104083300A CN201410309406.8A CN201410309406A CN104083300A CN 104083300 A CN104083300 A CN 104083300A CN 201410309406 A CN201410309406 A CN 201410309406A CN 104083300 A CN104083300 A CN 104083300A
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Abstract
The invention discloses a preparation method of skin cream. The method comprises the following steps: (1) preparing the following components in parts by weight: 4-5 parts of stearic acid, 2-3 parts of octadecanol, 2-3 parts of hexadecanol, 2-4 parts of white oil, 0.3-0.7 part of Twenn-60, 1-1.5 parts of wool fat, 0.3-0.7 part of olive oil, 1-3 parts of glycyrrhizic acid solution, 1-3 parts of bitter gourd solution, 1-3 parts of water hyacinth solution, 6-7 parts of glycerinum, 0.2-0.4 part of triethanolamine, 0.5-1 part of Chinese angelica extract, 60-80 parts of distilled water, 0.3-0.7 part of essence and 0.1-0.3 part of a preservative; (2) preparing an oil-phase mixture, namely stirring the stearic acid, octadecanol, hexadecanol, white oil, Twenn-60, wool fat and olive oil in an electric heating constant temperature water bath kettle, and forming the oil-phase mixture; (3) preparing an aqueous phase mixture, namely stirring the glycyrrhizic acid solution, glycerinum, triethanolamine, water hyacinth solution, bitter gourd solution, Chinese angelica extract and distilled water in the electric heating constant temperature water bath kettle, preserving the temperature for 10-30 minutes, sterilizing and filtering to obtain the aqueous phase mixture; and (4) mixing, stirring, standing, cooling to obtain the emulsifiable paste shaped skin cream. The invention also discloses skin cream prepared by the method. The skin cream can eliminate skin pigments, and the skin is natural, white and bright in color.
Description
Technical field
The present invention relates to the preparation of face skin care item, be specifically related to a kind of preparation method and goods thereof of protective skin cream.
Background technology
Along with social progress and development, the raising day by day of living standard, cosmetics more and more become an indispensable part in modern's life.Meanwhile, people require also more and more higher for the quality and performance of cosmetics.
Protective skin cream is one of cosmetics the most frequently used in daily life.Current synthetic cosmetics, owing to having more chemical adding ingredient, although it is not perishable, easily cause skin allergy, or bring out various skin problems, and potential side effect is large.
People wish to occur a series of being harmful to human health, and have again skin protection cosmetics prepared by the natural material of beauty and health care functions.Its feature of natural plant kind cosmetics is: in oil water mixture, add the cosmetics of all kinds of extracted form natural plant nutrient substance.Utilize the additive of natural plant extracts as beauty and skin care cosmetics, have the property of medicine stable, effect is lasting, to skin action temperature and, the feature such as zest is little, safe, evident in efficacy.Therefore, using plant extract as natural goods additive application in cosmetics, become gradually the focus of new product development.
Summary of the invention
For the above-mentioned deficiency of prior art, the object of the invention is to, a kind of preparation method and goods thereof of protective skin cream are provided.
The technical scheme that the present invention adopted is for achieving the above object: a kind of preparation method of protective skin cream, it is characterized in that, and it comprises the steps:
1) the following weight ratio ingredient of preparation:
Wherein:
The preparation of Herba Eichhorniae liquid: taking fresh water calabash as raw material, add 95% alcohol solvent, put in thermostat water bath after 60 DEG C of lixiviate 5h, vacuum filtration, carried out centrifugal 10min with 1000r/min, formed Herba Eichhorniae liquid, be loaded on brown bottle and be placed in refrigerator and keep in Dark Place.
The preparation of Fructus Momordicae charantiae liquid: a) get the raw materials ready: choose fresh Fructus Momordicae charantiae, remove melon capsule, it is pulled an oar, serosity, through centrifugal filtration, is rejected filtrate, and filtering residue is carried out to the extraction of Fructus Momordicae charantiae liquid; B) lixiviate: as extracting solvent, be 1: 3 by the solid-liquid ratio of Fructus Momordicae charantiae filtering residue and 95% ethanol composition with 95% ethanol, at 45 DEG C, pH value is 8.0, carries out lixiviate under the condition that extraction time is 2h, obtains preliminary Fructus Momordicae charantiae liquid after filtration; C) concentrated: under the environment of avoiding irradiate light, to b) the preliminary Fructus Momordicae charantiae liquid employing vacuum-concentrcted of gained of step, thickening temperature is controlled in 50 DEG C; D) petroleum ether extraction: under the environment of avoiding irradiate light, employing petroleum ether and step c) the preliminary Fructus Momordicae charantiae liquid of gained extract in the ratio of 1: 1, to remove phylloxanthin, carotene, obtain Fructus Momordicae charantiae liquid.
The preparation of Radix Glycyrrhizae acid solution: Radix Glycyrrhizae coarse powder is added containing 60% alcohol heating reflux of ammonia 0.5% and extracted, and by ammonia alcoholic solution heating and refluxing extraction, centrifugal, acid is heavy, the acetone Radix Glycyrrhizae extract that refluxes to obtain, acetone is reclaimed in distilling under reduced pressure, obtains Radix Glycyrrhizae acid solution.
The preparation of eumenol: by Radix Angelicae Sinensis porphyrize, with after defat with petroleum ether, dry, the ethanol taking volume fraction as 90% is as extractant, the mass ratio of ethanol and Radix Angelicae Sinensis is 8: 1, leave standstill 10min with moistening material, microwave 450W radiation 5min, filters, add proper amount of active carbon, stir 15min decolouring, filter, filtrate with Rotary Evaporators vacuum concentration to forming eumenol.
2) prepare oil mixture: by stearic acid, octadecanol, hexadecanol, white oil, Twenn-60, lanoline, olive oil be placed in electric-heated thermostatic water bath, be heated with stirring to 80 to 100 DEG C completely fusing be after homogeneous phase, form oil mixture;
3) prepare aqueous mixture: by Radix Glycyrrhizae acid solution, glycerol, triethanolamine, Herba Eichhorniae liquid, Fructus Momordicae charantiae liquid, eumenol, distilled water be placed in electric-heated thermostatic water bath, be heated with stirring to 80 to 100 DEG C completely fusing be after homogeneous phase, insulation 10, to 30min, obtains aqueous mixture after sterilising filtration;
4) keep 80 to 100 DEG C, slowly oil mixture is added in aqueous mixture and stirred, after stirring, continue to stir 0.5 to 1.5 hour; Slow cooling to 60 during to 70 DEG C, adds Aloe extractum, stirs while being cooled to 40 to 50 DEG C, adds essence, antiseptic, continues to stir, and in the time that temperature is down to 30 to 40 DEG C, stops stirring, and leaves standstill, cooling, obtains emulsifiable paste shape protective skin cream.
Described essence is jasmin essence.
Described antiseptic is one or both of Bronopol, propylparaben.Preferably, described antiseptic is mixed by Bronopol and propylparaben, and both mass ratioes are 1: 4.
A kind of protective skin cream of being prepared by described method.
The invention has the advantages that: the present invention utilizes the additive of natural plant extracts as beauty and skin care cosmetics, there is the property of medicine stable, effect is lasting, to skin action temperature and, the feature such as zest is little, safe, evident in efficacy, protective skin cream prepared by the present invention can be eliminated skin pigment, makes skin nature, whitening glossy.
Detailed description of the invention
Embodiment 1
The preparation method of the protective skin cream that the present embodiment provides, it comprises the steps:
1) the following weight ratio ingredient of preparation:
Wherein:
The preparation of Herba Eichhorniae liquid: taking fresh water calabash as raw material, add 95% alcohol solvent, put in thermostat water bath after 60 DEG C of lixiviate 5h, vacuum filtration, carried out centrifugal 10min with 1000r/min, formed Herba Eichhorniae liquid, be loaded on brown bottle and be placed in refrigerator and keep in Dark Place.
The preparation of Fructus Momordicae charantiae liquid: a) get the raw materials ready: choose fresh Fructus Momordicae charantiae, remove melon capsule, it is pulled an oar, serosity, through centrifugal filtration, is rejected filtrate, and filtering residue is carried out to the extraction of Fructus Momordicae charantiae liquid; B) lixiviate: as extracting solvent, be 1: 3 by the solid-liquid ratio of Fructus Momordicae charantiae filtering residue and 95% ethanol composition with 95% ethanol, at 45 DEG C, pH value is 8.0, carries out lixiviate under the condition that extraction time is 2h, obtains preliminary Fructus Momordicae charantiae liquid after filtration; C) concentrated: under the environment of avoiding irradiate light, to b) the preliminary Fructus Momordicae charantiae liquid employing vacuum-concentrcted of gained of step, thickening temperature is controlled in 50 DEG C; D) petroleum ether extraction: under the environment of avoiding irradiate light, employing petroleum ether and step c) the preliminary Fructus Momordicae charantiae liquid of gained extract in the ratio of 1: 1, to remove phylloxanthin, carotene, obtain Fructus Momordicae charantiae liquid.
The preparation of Radix Glycyrrhizae acid solution: Radix Glycyrrhizae coarse powder is added containing 60% alcohol heating reflux of ammonia 0.5% and extracted, and by ammonia alcoholic solution heating and refluxing extraction, centrifugal, acid is heavy, the acetone Radix Glycyrrhizae extract that refluxes to obtain, acetone is reclaimed in distilling under reduced pressure, obtains Radix Glycyrrhizae acid solution.
The preparation of eumenol: by Radix Angelicae Sinensis porphyrize, with after defat with petroleum ether, dry, the ethanol taking volume fraction as 90% is as extractant, the mass ratio of ethanol and Radix Angelicae Sinensis is 8: 1, leave standstill 10min with moistening material, microwave 450W radiation 5min, filters, add proper amount of active carbon, stir 15min decolouring, filter, filtrate with Rotary Evaporators vacuum concentration to forming eumenol.
2) prepare oil mixture: by stearic acid, octadecanol, hexadecanol, white oil, Twenn-60, lanoline, olive oil be placed in electric-heated thermostatic water bath, be heated with stirring to 80 to 100 DEG C completely fusing be after homogeneous phase, form oil mixture;
3) prepare aqueous mixture: by Radix Glycyrrhizae acid solution, glycerol, triethanolamine, Herba Eichhorniae liquid, Fructus Momordicae charantiae liquid, eumenol, distilled water be placed in electric-heated thermostatic water bath, be heated with stirring to 80 to 100 DEG C completely fusing be after homogeneous phase, insulation 10, to 30min, obtains aqueous mixture after sterilising filtration;
4) keep 80 to 100 DEG C, slowly oil mixture is added in aqueous mixture and stirred, after stirring, continue to stir 0.5 to 1.5 hour; Slow cooling to 60 during to 70 DEG C, adds Aloe extractum, stirs while being cooled to 40 to 50 DEG C, adds essence, antiseptic, continues to stir, and in the time that temperature is down to 30 to 40 DEG C, stops stirring, and leaves standstill, cooling, obtains emulsifiable paste shape protective skin cream.
Described essence is jasmin essence.
Described antiseptic is one or both of Bronopol, propylparaben.Preferably, described antiseptic is mixed by Bronopol and propylparaben, and both mass ratioes are 1: 4.
A kind of protective skin cream of being prepared by described method.
Embodiment 2
The preparation method of the protective skin cream that the present embodiment provides and goods, substantially the same manner as Example 1, its difference is, it comprises the steps:
1) the following weight ratio ingredient of preparation:
Wherein:
The preparation of Herba Eichhorniae liquid: taking fresh water calabash as raw material, add 95% alcohol solvent, put in thermostat water bath after 60 DEG C of lixiviate 5h, vacuum filtration, carried out centrifugal 10min with 1000r/min, formed Herba Eichhorniae liquid, be loaded on brown bottle and be placed in refrigerator and keep in Dark Place.
The preparation of Fructus Momordicae charantiae liquid: a) get the raw materials ready: choose fresh Fructus Momordicae charantiae, remove melon capsule, it is pulled an oar, serosity, through centrifugal filtration, is rejected filtrate, and filtering residue is carried out to the extraction of Fructus Momordicae charantiae liquid; B) lixiviate: as extracting solvent, be 1: 3 by the solid-liquid ratio of Fructus Momordicae charantiae filtering residue and 95% ethanol composition with 95% ethanol, at 45 DEG C, pH value is 8.0, carries out lixiviate under the condition that extraction time is 2h, obtains preliminary Fructus Momordicae charantiae liquid after filtration; C) concentrated: under the environment of avoiding irradiate light, to b) the preliminary Fructus Momordicae charantiae liquid employing vacuum-concentrcted of gained of step, thickening temperature is controlled in 50 DEG C; D) petroleum ether extraction: under the environment of avoiding irradiate light, employing petroleum ether and step c) the preliminary Fructus Momordicae charantiae liquid of gained extract in the ratio of 1: 1, to remove phylloxanthin, carotene, obtain Fructus Momordicae charantiae liquid.
The preparation of Radix Glycyrrhizae acid solution: Radix Glycyrrhizae coarse powder is added containing 60% alcohol heating reflux of ammonia 0.5% and extracted, and by ammonia alcoholic solution heating and refluxing extraction, centrifugal, acid is heavy, the acetone Radix Glycyrrhizae extract that refluxes to obtain, acetone is reclaimed in distilling under reduced pressure, obtains Radix Glycyrrhizae acid solution.
The preparation of eumenol: by Radix Angelicae Sinensis porphyrize, with after defat with petroleum ether, dry, the ethanol taking volume fraction as 90% is as extractant, the mass ratio of ethanol and Radix Angelicae Sinensis is 8: 1, leave standstill 10min with moistening material, microwave 450W radiation 5min, filters, add proper amount of active carbon, stir 15min decolouring, filter, filtrate with Rotary Evaporators vacuum concentration to forming eumenol.
2) prepare oil mixture: by stearic acid, octadecanol, hexadecanol, white oil, Twenn-60, lanoline, olive oil be placed in electric-heated thermostatic water bath, be heated with stirring to 80 DEG C completely fusing be after homogeneous phase, form oil mixture;
3) prepare aqueous mixture: by Radix Glycyrrhizae acid solution, glycerol, triethanolamine, Herba Eichhorniae liquid, Fructus Momordicae charantiae liquid, eumenol, distilled water be placed in electric-heated thermostatic water bath, be heated with stirring to 80 DEG C completely fusing be after homogeneous phase, insulation 10min, obtains aqueous mixture after sterilising filtration;
4) keep 80 DEG C, slowly oil mixture is added in aqueous mixture and stirred, after stirring, continue to stir 0.5 hour; When slow cooling to 60 DEG C, add Aloe extractum, stir while being cooled to 40 DEG C, add essence, antiseptic, continue to stir, in the time that temperature is down to 30 DEG C, stop stirring, leave standstill, cooling, obtain emulsifiable paste shape protective skin cream.
Described essence is jasmin essence.
Described antiseptic is mixed by Bronopol and propylparaben, and both mass ratioes are 1: 4.
Embodiment 3
The preparation method of the protective skin cream that the present embodiment provides and goods, basic identical with embodiment 1,2, its difference is, it comprises the steps:
1) the following weight ratio ingredient of preparation:
Wherein:
The preparation of Herba Eichhorniae liquid: taking fresh water calabash as raw material, add 95% alcohol solvent, put in thermostat water bath after 60 DEG C of lixiviate 5h, vacuum filtration, carried out centrifugal 10min with 1000r/min, formed Herba Eichhorniae liquid, be loaded on brown bottle and be placed in refrigerator and keep in Dark Place.
The preparation of Fructus Momordicae charantiae liquid: a) get the raw materials ready: choose fresh Fructus Momordicae charantiae, remove melon capsule, it is pulled an oar, serosity, through centrifugal filtration, is rejected filtrate, and filtering residue is carried out to the extraction of Fructus Momordicae charantiae liquid; B) lixiviate: as extracting solvent, be 1: 3 by the solid-liquid ratio of Fructus Momordicae charantiae filtering residue and 95% ethanol composition with 95% ethanol, at 45 DEG C, pH value is 8.0, carries out lixiviate under the condition that extraction time is 2h, obtains preliminary Fructus Momordicae charantiae liquid after filtration; C) concentrated: under the environment of avoiding irradiate light, to b) the preliminary Fructus Momordicae charantiae liquid employing vacuum-concentrcted of gained of step, thickening temperature is controlled in 50 DEG C; D) petroleum ether extraction: under the environment of avoiding irradiate light, employing petroleum ether and step c) the preliminary Fructus Momordicae charantiae liquid of gained extract in the ratio of 1: 1, to remove phylloxanthin, carotene, obtain Fructus Momordicae charantiae liquid.
The preparation of Radix Glycyrrhizae acid solution: Radix Glycyrrhizae coarse powder is added containing 60% alcohol heating reflux of ammonia 0.5% and extracted, and by ammonia alcoholic solution heating and refluxing extraction, centrifugal, acid is heavy, the acetone Radix Glycyrrhizae extract that refluxes to obtain, acetone is reclaimed in distilling under reduced pressure, obtains Radix Glycyrrhizae acid solution.
The preparation of eumenol: by Radix Angelicae Sinensis porphyrize, with after defat with petroleum ether, dry, the ethanol taking volume fraction as 90% is as extractant, the mass ratio of ethanol and Radix Angelicae Sinensis is 8: 1, leave standstill 10min with moistening material, microwave 450W radiation 5min, filters, add proper amount of active carbon, stir 15min decolouring, filter, filtrate with Rotary Evaporators vacuum concentration to forming eumenol.
2) prepare oil mixture: by stearic acid, octadecanol, hexadecanol, white oil, Twenn-60, lanoline, olive oil be placed in electric-heated thermostatic water bath, be heated with stirring to 100 DEG C completely fusing be after homogeneous phase, form oil mixture;
3) prepare aqueous mixture: by Radix Glycyrrhizae acid solution, glycerol, triethanolamine, Herba Eichhorniae liquid, Fructus Momordicae charantiae liquid, eumenol, distilled water be placed in electric-heated thermostatic water bath, be heated with stirring to 100 DEG C completely fusing be after homogeneous phase, insulation 30min, obtains aqueous mixture after sterilising filtration;
4) keep 100 DEG C, slowly oil mixture is added in aqueous mixture and stirred, after stirring, continue to stir 1.5 hours; When slow cooling to 70 DEG C, add Aloe extractum, stir while being cooled to 50 DEG C, add essence, antiseptic, continue to stir, in the time that temperature is down to 40 DEG C, stop stirring, leave standstill, cooling, obtain emulsifiable paste shape protective skin cream.
Described essence is jasmin essence.Described antiseptic is mixed by Bronopol and propylparaben, and both mass ratioes are 1: 4.
Embodiment 4
The preparation method of the protective skin cream that the present embodiment provides and goods, basic identical with embodiment 1,2 or 3, its difference is, it comprises the steps:
1) the following weight ratio ingredient of preparation:
Wherein:
The preparation of Herba Eichhorniae liquid: taking fresh water calabash as raw material, add 95% alcohol solvent, put in thermostat water bath after 60 DEG C of lixiviate 5h, vacuum filtration, carried out centrifugal 10min with 1000r/min, formed Herba Eichhorniae liquid, be loaded on brown bottle and be placed in refrigerator and keep in Dark Place.
The preparation of Fructus Momordicae charantiae liquid: a) get the raw materials ready: choose fresh Fructus Momordicae charantiae, remove melon capsule, it is pulled an oar, serosity, through centrifugal filtration, is rejected filtrate, and filtering residue is carried out to the extraction of Fructus Momordicae charantiae liquid; B) lixiviate: as extracting solvent, be 1: 3 by the solid-liquid ratio of Fructus Momordicae charantiae filtering residue and 95% ethanol composition with 95% ethanol, at 45 DEG C, pH value is 8.0, carries out lixiviate under the condition that extraction time is 2h, obtains preliminary Fructus Momordicae charantiae liquid after filtration; C) concentrated: under the environment of avoiding irradiate light, to b) the preliminary Fructus Momordicae charantiae liquid employing vacuum-concentrcted of gained of step, thickening temperature is controlled in 50 DEG C; D) petroleum ether extraction: under the environment of avoiding irradiate light, employing petroleum ether and step c) the preliminary Fructus Momordicae charantiae liquid of gained extract in the ratio of 1: 1, to remove phylloxanthin, carotene, obtain Fructus Momordicae charantiae liquid.
The preparation of Radix Glycyrrhizae acid solution: Radix Glycyrrhizae coarse powder is added containing 60% alcohol heating reflux of ammonia 0.5% and extracted, and by ammonia alcoholic solution heating and refluxing extraction, centrifugal, acid is heavy, the acetone Radix Glycyrrhizae extract that refluxes to obtain, acetone is reclaimed in distilling under reduced pressure, obtains Radix Glycyrrhizae acid solution.
The preparation of eumenol: by Radix Angelicae Sinensis porphyrize, with after defat with petroleum ether, dry, the ethanol taking volume fraction as 90% is as extractant, the mass ratio of ethanol and Radix Angelicae Sinensis is 8: 1, leave standstill 10min with moistening material, microwave 450W radiation 5min, filters, add proper amount of active carbon, stir 15min decolouring, filter, filtrate with Rotary Evaporators vacuum concentration to forming eumenol.
2) prepare oil mixture: by stearic acid, octadecanol, hexadecanol, white oil, Twenn-60, lanoline, olive oil be placed in electric-heated thermostatic water bath, be heated with stirring to 80 to 100 DEG C completely fusing be after homogeneous phase, form oil mixture;
3) prepare aqueous mixture: by Radix Glycyrrhizae acid solution, glycerol, triethanolamine, Herba Eichhorniae liquid, Fructus Momordicae charantiae liquid, eumenol, distilled water be placed in electric-heated thermostatic water bath, be heated with stirring to 90 DEG C completely fusing be after homogeneous phase, insulation 20min, obtains aqueous mixture after sterilising filtration;
4) keep 90 DEG C, slowly oil mixture is added in aqueous mixture and stirred, after stirring, continue to stir 1 hour; When slow cooling to 65 DEG C, add Aloe extractum, stir while being cooled to 45 DEG C, add essence, antiseptic, continue to stir, in the time that temperature is down to 35 DEG C, stop stirring, leave standstill, cooling, obtain emulsifiable paste shape protective skin cream.
Described essence is jasmin essence.Described antiseptic is mixed by Bronopol and propylparaben, and both mass ratioes are 1: 4.
The present invention is not limited to above-mentioned embodiment, adopts the step identical or approximate with the above embodiment of the present invention, and the preparation method of other protective skin cream that obtain and goods thereof, all within protection scope of the present invention.
Claims (9)
1. a preparation method for protective skin cream, is characterized in that, it comprises the steps:
1) the following weight ratio ingredient of preparation:
2) prepare oil mixture: by stearic acid, octadecanol, hexadecanol, white oil, Twenn-60, lanoline, olive oil be placed in electric-heated thermostatic water bath, be heated with stirring to 80 to 100 DEG C completely fusing be after homogeneous phase, form oil mixture;
3) prepare aqueous mixture: by Radix Glycyrrhizae acid solution, glycerol, triethanolamine, Herba Eichhorniae liquid, Fructus Momordicae charantiae liquid, eumenol, distilled water be placed in electric-heated thermostatic water bath, be heated with stirring to 80 to 100 DEG C completely fusing be after homogeneous phase, insulation 10, to 30min, obtains aqueous mixture after sterilising filtration;
4) keep 80 to 100 DEG C, slowly oil mixture is added in aqueous mixture and stirred, after stirring, continue to stir O.5 to 1.5 hour; Slow cooling to 60 during to 70 DEG C, adds Aloe extractum, stirs while being cooled to 40 to 50 DEG C, adds essence, antiseptic, continues to stir, and in the time that temperature is down to 30 to 40 DEG C, stops stirring, and leaves standstill, cooling, obtains emulsifiable paste shape protective skin cream.
2. the preparation method of protective skin cream according to claim 1, is characterized in that, described step 1) further comprising the steps of:
The preparation of Herba Eichhorniae liquid: taking fresh water calabash as raw material, add 95% alcohol solvent, put in thermostat water bath after 60 DEG C of lixiviate 5h, vacuum filtration, carried out centrifugal 10min with 1000r/min, formed Herba Eichhorniae liquid, be loaded on brown bottle and be placed in refrigerator and keep in Dark Place.
3. the preparation method of protective skin cream according to claim 1, is characterized in that, states step 1) further comprising the steps of:
The preparation of Fructus Momordicae charantiae liquid:
A) get the raw materials ready: choose fresh Fructus Momordicae charantiae, remove melon capsule, it is pulled an oar, serosity, through centrifugal filtration, is rejected filtrate, and filtering residue is carried out to the extraction of Fructus Momordicae charantiae liquid;
B) lixiviate: as extracting solvent, be 1: 3 by the solid-liquid ratio of Fructus Momordicae charantiae filtering residue and 95% ethanol composition with 95% ethanol, at 45 DEG C, p H-number is 8.0, carries out lixiviate under the condition that extraction time is 2h, obtains preliminary Fructus Momordicae charantiae liquid after filtration;
C) concentrated: under the environment of avoiding irradiate light, to b) the preliminary Fructus Momordicae charantiae liquid employing vacuum-concentrcted of gained of step, thickening temperature is controlled in 50 DEG C;
D) petroleum ether extraction: under the environment of avoiding irradiate light, employing petroleum ether and step c) the preliminary Fructus Momordicae charantiae liquid of gained extract in the ratio of 1: 1, to remove phylloxanthin, carotene, obtain Fructus Momordicae charantiae liquid.
4. the preparation method of protective skin cream according to claim 1, is characterized in that, states step 1) further comprising the steps of:
The preparation of Radix Glycyrrhizae acid solution: Radix Glycyrrhizae coarse powder is added containing 60% alcohol heating reflux of ammonia 0.5% and extracted, and by ammonia alcoholic solution heating and refluxing extraction, centrifugal, acid is heavy, the acetone Radix Glycyrrhizae extract that refluxes to obtain, acetone is reclaimed in distilling under reduced pressure, obtains Radix Glycyrrhizae acid solution.
5. the preparation method of protective skin cream according to claim 1, is characterized in that, states step 1) further comprising the steps of:
The preparation of eumenol: by Radix Angelicae Sinensis porphyrize, with after defat with petroleum ether, dry, the ethanol taking volume fraction as 90% is as extractant, the mass ratio of ethanol and Radix Angelicae Sinensis is 8: 1, leave standstill 10min with moistening material, microwave 450W radiation 5min, filters, add proper amount of active carbon, stir 15min decolouring, filter, filtrate with Rotary Evaporators vacuum concentration to forming eumenol.
6. the preparation method of protective skin cream according to claim 1, is characterized in that, described essence is jasmin essence.
7. the preparation method of protective skin cream according to claim 1, is characterized in that, described antiseptic is one or both of Bronopol, propylparaben.
8. the preparation method of protective skin cream according to claim 1, is characterized in that, described antiseptic is mixed by Bronopol and propylparaben, and both mass ratioes are 1: 4.
9. a protective skin cream of being prepared by the described method of one of claim 1 to 8.
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| CN104490686A (en) * | 2014-12-12 | 2015-04-08 | 柳州市京阳节能科技研发有限公司 | Biological beautiful facial cleanser |
| CN104606096A (en) * | 2015-01-07 | 2015-05-13 | 浙江泰康生物科技有限公司 | Skin-beautifying aloe skin cream and preparation method thereof |
| CN104873437A (en) * | 2015-06-04 | 2015-09-02 | 贵阳医学院 | Fructus-rosae-laevigatae skin cream and preparation method thereof |
| CN107174551A (en) * | 2017-06-22 | 2017-09-19 | 西北大学 | Anti-oxidant face cream of Chinese gooseberry seed polyphenol and preparation method thereof |
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