CN104490702B - Herbal mask taking plant extract as anticorrosive antibacterial additive - Google Patents
Herbal mask taking plant extract as anticorrosive antibacterial additive Download PDFInfo
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- CN104490702B CN104490702B CN201410819763.9A CN201410819763A CN104490702B CN 104490702 B CN104490702 B CN 104490702B CN 201410819763 A CN201410819763 A CN 201410819763A CN 104490702 B CN104490702 B CN 104490702B
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- 239000011975 tartaric acid Substances 0.000 description 1
- 239000003440 toxic substance Substances 0.000 description 1
- 231100000419 toxicity Toxicity 0.000 description 1
- 230000001988 toxicity Effects 0.000 description 1
- NGSWKAQJJWESNS-ZZXKWVIFSA-N trans-4-coumaric acid Chemical class OC(=O)\C=C\C1=CC=C(O)C=C1 NGSWKAQJJWESNS-ZZXKWVIFSA-N 0.000 description 1
- 230000008736 traumatic injury Effects 0.000 description 1
- 229960003500 triclosan Drugs 0.000 description 1
- 231100000397 ulcer Toxicity 0.000 description 1
- 210000002700 urine Anatomy 0.000 description 1
- 229940096998 ursolic acid Drugs 0.000 description 1
- PLSAJKYPRJGMHO-UHFFFAOYSA-N ursolic acid Natural products CC1CCC2(CCC3(C)C(C=CC4C5(C)CCC(O)C(C)(C)C5CCC34C)C2C1C)C(=O)O PLSAJKYPRJGMHO-UHFFFAOYSA-N 0.000 description 1
- 231100000611 venom Toxicity 0.000 description 1
- VHBFFQKBGNRLFZ-UHFFFAOYSA-N vitamin p Natural products O1C2=CC=CC=C2C(=O)C=C1C1=CC=CC=C1 VHBFFQKBGNRLFZ-UHFFFAOYSA-N 0.000 description 1
- 239000000341 volatile oil Substances 0.000 description 1
- 230000008673 vomiting Effects 0.000 description 1
- 230000002087 whitening effect Effects 0.000 description 1
Landscapes
- Cosmetics (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The invention relates to a herbal mask taking a plant extract as an anticorrosive antibacterial additive and aims at providing a mask with the effect of effectively nursing the facial skin. According to the technical scheme, the herbal mask taking the plant extract as the anticorrosive antibacterial additive comprises the following components: glyceryl polyether-26 and the like. The method for preparing the herbal mask taking the plant extract as the anticorrosive antibacterial additive comprises the following steps: (1) soaking the raw materials in advance until the materials are completely dissolved, heating and sterilizing; (2) heating, totally melting the materials, and uniformly stirring; (3) stirring and mixing the materials treated in the steps (1) and (2) under vacuum conditions, adding kaolin, homogenizing, reducing the temperature, adding essence raw materials, and uniformly mixing; (4) continuously cooling, and filtering the materials by virtue of an 80-mesh sieve; and (5) sampling and checking. The method for preparing the traditional Chinese medicine extract comprises the following steps: (1) mixing the raw materials according to the ratio; (2) obtaining the supernatant and separating out the extract; and (3) performing vacuum drying on the supernatant and the separated extract, thereby obtaining the dried extract.
Description
Technical field
The present invention relates to a kind of facial mask of cosmetic field and preparation method thereof, more particularly to one kind with oldenlandia diffusa,
Sun plant, Chinese actinidia root, Myrica rubra Dongkui root, japanese avens root are the draft facial mask and preparation method of antisepsis and sterilization additive.
Background technology
The mask product sold in the market, its material composition a multitude of names according to species difference on market, according to
Quality can be divided into tear-pull facial mask, blending paste film, creams type facial mask, fresh fruit self-made face pack, face patch type facial mask dividing.
The nutrient contents such as deep-sea mud, various mineral matters, plants essential oil can be typically added in blending cream pack.It can not only be effectively clear
Clean skin, and moisture can be utilized to soften the hardening sebum for being blocked in pore mouth, acne and blackhead is easily pulled out and come.
But in order to preserve the active ingredient of wherein nutriment, more sterilization antiseptic is often added in product.And it is sterilized anti-
Rotten agent is to cause allergic main cause.
Countries in the world have carried out limiting and have used to traditional preservatives bactericide, and such as Ministry of environment of Denmark was on December 20th, 2010
Announce, will forbid containing p-hydroxybenzoate in the juvenile product of less than 3 years old.2011.5.4 French Lower House votes through one
Forbid the motion of product salt containing o- benzoic acid, p-hydroxybenzoate and the class chemical substance of alkyl phenol three.2014.1 European Union newly advises,
Triclosan is deleted from regulation No1223/2009 annex V, and limits it and used as cosmetics preservative.Also forbid simultaneously
5 kinds of preservatives without security evaluation data such as oxybenzene isobutyl ester.
By stimulating anaphylaxis clinical investigation to preservative, in 2000-2005 Nofer institute of
Occupation Medicine are tested 1937 patients, and to analyze series of standards preservative contact mistake is caused
Quick probability.(thimerosal,EuxylK400,formaldehyde,Kathon CG,Quatemium 15,parabens)
27 kinds of Preservative Technology for Personal Care, wherein 16 kinds can cause a positive reaction with other chemical substances.EuxylK400 is proved to be this
Main anaphylactogen in serial cosmetics, causes the positive reaction of 21 (18.6%) name patients, but while 17.7% patient couple
Thimerosal can produce positive reaction.The anaphylaxis patch test of cosmetics preservative, wherein 43.4% tester, at least one
Item patch test is presented positive.Therefore in recent years market is studied low irritant preservative, and 1 is dosed in cosmetics,
2- alkane diols replace parabens.No added concept is proposed, while also serving as selling point.
For safely, advocate naturally consideration, in recent years, with the progressively enhancing of the health perception of people, made by plant
The report of cosmetics is added gradually to increase for additive, such as ginseng, aloe but be mostly for brightening the work for improving skin
With.
Chinese invention patent CN103110565A inventions are related to the Pure natural mask made as raw material with Chinese medicine, by all kinds of grass
Drug mill powder, it is light pale powder to invent the Pure natural mask for providing, to improving face pigment deposition weight, have acne or acne,
Little papule is effective, but this facial mask uses process inconvenience.CN201410241891 inventions are related to a kind of pure natural nonirritant facial mask
And preparation method thereof, after use, while have skin oxygen supply, whitening, brighten, anti-acne, nti-freckle (except genetic), skin protect
The effects such as wet and convergence pore, superfluous sebum secretion can also be suppressed.However, Chinese herbal medicine used by foregoing invention is all simple
For improving the effect of skin.
In view of this, a kind of safety and environmental protection, good product quality and using plant as anticorrosion and bactericidal agent are developed, for life
The cosmetics of no added excitant preservative are produced, and is industrialized and is just seemed and be even more important, can so be played it and make up
Extensive application in product field, meets the market demand.
The content of the invention
The invention aims to overcome above-mentioned the deficiencies in the prior art, there is provided one kind is killed by anti-corrosion of plant extracts
The draft facial mask of bacteria additive, the facial mask should possess the effect of effectively nursing skin of face, will not health risk, and shelf-life
Limit complies fully with the regulation of national standard.
The present invention provide technical scheme be：With plant extracts as the draft facial mask of antisepsis and sterilization additive, including
Composition and corresponding weight portion are：
The 2.3-2.5 of glycerin polyether -26, glycerine 4.9-5.1, xanthans 0.23-0.27, allantoin 0.09-0.11, Chinese medicine
Medicinal extract 1～10, dipotassium glycyrrhizinate 0.19-0.21,
Caprylic/capric triglyceride 2.95-3.05, dimethyl silicone polymer 1.95-2.05, cetostearyl alcohol 5.1-5.3,
Ceteth -201.9-2.1, ceteareth -20.48-0.52, Butyrospermum parkii fruit fat 1.4-1.6, Dormant oils 2.5-
3.5th, kaolin 5.0-7.0 and distilled water 63.3-65.8.
The Chinese medical concrete is according to 1:0.8-1.2:1.8-2.2:0.8-1.2:1.8-2.2 part by weight mixing it is white
Flower HERBA HEDYOTIS DIFFUSAE, sun plant, Chinese actinidia root, Myrica rubra Dongkui root, japanese avens root extract medicinal extract；It is preferably in a proportion of 1:1:2:1:2.
The draft facial mask also configures that essence 0.045-0.055.
The composition and corresponding weight portion that described draft facial mask includes be：
Glycerin polyether -262.4, glycerine 5.0, xanthans 0.25, allantoin 0.1, Chinese medical concrete 5, dipotassium glycyrrhizinate 0.20,
Caprylic/capric triglyceride 3.0, dimethyl silicone polymer 2.0, cetostearyl alcohol 5.2, ceteth -202.0, spermaceti are hard
Lipidol polyethers -20.5, Butyrospermum parkii fruit fat 1.5, Dormant oils 3.0, kaolin 6.0, essence 0.05 and distilled water 64.7.
With plant extracts as the preparation method of the draft facial mask of antisepsis and sterilization additive, carry out according to the following steps：
1) glycerin polyether -26, glycerine, xanthans, allantoin, Chinese medical concrete, dipotassium glycyrrhizinate and distilled water are shifted to an earlier date
It is heated to being completely dissolved after immersion, is heated to 85 DEG C of sterilizing 25-36 minutes；
2) it is caprylic/capric triglyceride, dimethyl silicone polymer, cetostearyl alcohol, ceteth -20, spermaceti is hard
Lipidol polyethers -2, Butyrospermum parkii fruit fat and Dormant oils are added in pot, are heated to be stirred after 85 ± 2 DEG C of whole thawings, homogeneous
30 ± 5 minutes；
3) by through step 1 under -0.02Mpa vacuum conditions), 2) process material body stirring mix and add kaolin
Afterwards homogenization 10-20 minutes, when being then cooled to 45 DEG C, add flavor of raw material and be well mixed；
4) continue to cool to 40 DEG C；Material body is filtered by 80 mesh；
5) censorship is sampled.
The dimethyl silicone polymer need to be well mixed in advance with cetostearyl alcohol.
The step 3) in homogenization be homogeneous mixer with 2000-3000rpm homogeneous 5-6 minutes, be subsequently added into
Kaolin homogeneous 15 ± 2 minutes, then cools to 50 ± 2 DEG C, continues to stir.
The preparation method of the Chinese medical concrete is：
1) 90-110 mesh will be crushed after oldenlandia diffusa, sun plant, Chinese actinidia root, Myrica rubra Dongkui root, japanese avens root drying
Sieve, by 1:0.8-1.2:1.8-2.2:0.8-1.2:1.8-2.2 part by weight mixing；
2) by 1:The solid-liquid part by weight of 9-11 mixed solvent soaks 5-7 hours, and then refluxing extraction three times merge and extract
Liquid, steams solvent, obtains supernatant and separates out medicinal extract；
3) dry extract is obtained after supernatant and precipitation medicinal extract are vacuum dried.
The mixed solvent presses 1 by 95% ethanol and ethyl acetate:1 volume ratio is mixed.
The invention has the beneficial effects as follows：Flavonoid substances, chlorogenic acid and plant polyphenol etc. due to make use of plant itself
The sterilization of material, bacteriostasis, the antisepsis and sterilization ability and quality guarantee period for not only ensuring facial mask (meets national Specification
Require), and the usage amount of anticorrosion and bactericidal agent in facial mask is instead of, and then significantly reduce anticorrosion and bactericidal agent human body is produced
Side effect, environmental protection is also of great importance.
Specific embodiment
The thinking of the present invention, is that the materials such as the Flavonoid substances, chlorogenic acid and the plant polyphenol that are contained in itself using plant are made
For bactericide, there is provided a kind of draft facial mask of environmental protection contributes to consumer.
The Flavonoid substances, chlorogenic acid and plant polyphenol are harmless to the health, are readily biodegradable, and to golden yellow Portugal
The common causative bacterium such as grape coccus and Escherichia coli has killing action, has obvious inhibitory action to fungi, saccharomycete.With white
Flower tongue grass, sun plant, Myrica rubra Dongkui root, japanese avens root, the facial mask that Chinese actinidia root is antisepsis and sterilization additive, except killing with anti-corrosion
Bacterium acts on, and oldenlandia diffusa, sun plant also have strengthens nospecific immunity effect and antioxidation；To skin furuncle sore
The disease of skin such as ulcer, eczema also have certain curative effect.
Oldenlandia diffusa：Oldenlandia diffusa is Rubiaceae plants of Hedyotis, and all herbal medicine has heat-clearing, removing toxic substances, promoting blood circulation, profit
Effect of urine.Research in recent years shows that oldenlandia diffusa has strengthens nospecific immunity effect and antioxidation, clinically uses
In various cancers and inflammation is treated, its chemical composition is studied, herb containing asperuloside, asperuloside acid, go acetic acid,
The acid of base asperuloside, all square rafter glucoside, Chinese Fevervine Herb time glucoside, Chinese Fevervine Herb time glucoside methyl esters, the p- hydroxyl cinnamyl Chinese Fevervine Herb time glucosides of 6-O-
The p- methoxyl group cinnamyl Chinese Fevervine Herb time glucoside methyl esters of methyl esters, 6-O-, 6-O- asafoetide acyls Chinese Fevervine Herb time glucoside methyl esters, 2- methyl -3- hydroxyls
Anthraquinone, 2- methyl -3- methoxy anthraquinones, 2- methyl -3- hydroxyl -4- methoxy anthraquinones, ursolic acid, cupreol, hentriacontane,
Stigmasterol, oleanolic acid, cupreol-β-glycoside, p-coumaric acid, iridoid, flavones, anthraquinone, p- coumaric acids, Ah
The compositions such as Wei's acid, oleanolic acid, scopolactone, Quercetin, Kaempferol, daucosterol.
Indication：Dyspnea and cough due to lung-heat；Abscess of throat；Acute appendicitis；Furuncle sore；Venomous snake bite；Puckery pain of heat gonorrhea；Oedema；Dysentery；
Enteritis；Jaundice with damp-heat pathogen；It is good at the various cancerous swellings for the treatment of.
Sculellaria barbata：Portulaca grandilora, is the plant of Portulacaceae Portulaca.Herb (carthamidin) containing carthamin,
Isocarthamidin (iso-carthamidin), high mountain baicalein (scutellarein), high mountain Huang official seal glucoside (scutel-larin),
Cupreol (β-sitosterol), stearic acid (steraricacid), alkaloid polysaccharide etc..According to another report, from aerial part
Isolated wogonin (wogo-nin), rivularin (scutervulin), Sculellaria barbata kind element (rivularin), naringenin
(naringenin), apiolin (apigenin), dinatin (hispedulin), eriodictyol (eriodictyol), sweet-scented osmanthus
Careless element (suteolin), and 5,7,4- trihydroxy -8- methoxy flavanones (5,7,-trihydroxy-6-
Methoxyflavanone) 4- hydroxyls wogonin (4-hydroxywogonin), 7- gate of a lane base -5,8- dimethoxy flavone (7-
Hy-droxy-5,8-dimethoxyflavane), p- great base benzene first Tibet (p-hydroxyben-zaldehyde), the p- gate of a lane
Base benzylacetone (p-hydroxybenzylacetone), p-coumaric acid (p-coumaricaicd), protocatechuic acid
(protocatechuicacid), energy tartaric acid (ut-solicacid) phytosterol (phytosterol), phytosterol β-D- Portugals
Grape glucoside (phy-tosteryl- β-D-glucoside) etc..
Indication：Have clearing heat and detoxicating, promoting blood circulation and removing blood stasis, swelling and pain relieving, the effect of anticancer；Appendicitis curing, hepatitis, stomachache,
Early liver cancer, lung cancer, cervix cancer, mastitis etc.；The diseases such as the treatment of pain furuncle, treating swelling and pain by traumatic injury are controlled in external application.
Chinese actinidia root：The root of Actinidiaceae plant Kiwi berry plant, containing triterpene compound, flavone compound, polysaccharide, perfume (or spice)
Legumin class, (-)-epicatechin and (+)-catechin etc..
Indication：It is clearing heat and detoxicating, clearing heat and promoting diuresis, preventing tumor anticancer, dispelling wind and eliminating dampness, diuresis hemostasis, removing toxicity for detumescence, digestion
Bad, vomiting, arthralgia due to wind-dampness, treating rheumatic ostealgia, Alimentary Tract Cancer, tumor in digestive tract, large carbuncle boil, treating rheumatic ostealgia and jaundice etc.
Disease.
Myrica rubra Dongkui root：The root of Myrica rubra Dongkui, containing flavonoids, chlorogenic acid；Tannin, dissociated anthraquinone
Indication：Eliminating dampness treats sore, relieving diarrhea with astringents, promoting blood circulation and stopping pain etc.
Japanese avens root:For the root of dicotyledon medicine madder wort Astragalus tenuis, containing catechin compounds, black bearberry
Acid, oleanolic acid, p sitosterol and alkaloid, glycoside compounds.
Indication：Relieving superficies by cooling；Promoting blood circulation and detoxication.Main cold, fever；Cough；Parotitis；Abscess of throat；Hepatitis；Rheumatism
Arthralgia；Traumatic bleeding.
Further illustrate below in conjunction with specific embodiment.
Embodiment 1
1) by glycerin polyether -26 2.3, glycerine 5.1, xanthans 0.23, allantoin 0.11, Chinese medical concrete 3, glycyrrhizic acid two
Potassium 0.21 and distilled water 64 add water phase pot after soaking in advance, while being heated to being completely dissolved；It is heated to 85 DEG C to sterilize 30 points
Clock.
2) caprylic/capric triglyceride 3.05, dimethyl silicone polymer 1.95, (the poly dimethyl silicon of cetostearyl alcohol 5.3
Oxygen alkane need to be well mixed in advance with cetostearyl alcohol), cetanol 1.9, ceteareth -20.52, Butyrospermum parkii
(BUTYROSPERMUM PARKII) fruit fat 1.4 and Dormant oils 3.5 are added to oil phase pot, are heated to 85 DEG C, after all melting, stir
Mix uniform, homogeneous 30 minutes.
3) pull-up vacuum, first suction part water mutually expects body in main cooker, then sucks oil phase material body, finally sucks water and mutually expects
Body, pulling vacuum to -0.02Mpa, then homogeneous open to 2500rpm, homogeneous 5 minutes adds kaolin 7.0, homogeneous 15 minutes,
Notice that taking out material body sees whether be uniformly dispersed, and stirs 15 minutes, froth breaking thoroughly, opens cooling water, cools to 50 DEG C, and stirring is equal
It is even, vacuum is maintained, continue to lower the temperature, when 45 DEG C, add essence 0.045；It is well mixed.
4) continue to cool to 40 DEG C；Material body is placed into cleaning charging basket by 80 mesh filters.
5) censorship is sampled.
The extracting method of Chinese medical concrete：
100 mesh sieves will be crushed after oldenlandia diffusa, sun plant, Chinese actinidia root, Myrica rubra Dongkui root, japanese avens root drying, pressed
1:1:2:1:2 part by weight mixing；Then 1 is pressed:10 solid-liquid part by weight mixed solvent (V95% ethanol：VEthyl acetate=50:
50) soak 6 hours, refluxing extraction three times, merge extract, steam solvent, obtain supernatant and separate out medicinal extract；Supernatant and precipitation
Dry extract is obtained after medicinal extract is vacuum dried.
Embodiment 2
1) by glycerin polyether -26 2.4, glycerine 5.0, xanthans 0.25, allantoin 0.10, Chinese medical concrete 5, glycyrrhizic acid two
Potassium 0.20 and distilled water 64.7 add water phase pot after soaking in advance, while being heated to being completely dissolved.It is heated to 85 DEG C of sterilizings 35
Minute.
2) caprylic/capric triglyceride 3.00, the dimethyl silicone polymer 2.00, (poly dimethyl of cetostearyl alcohol 5.20
Siloxanes is well mixed in advance with cetostearyl alcohol), cetanol 2.00, ceteareth -20.50, Butyrospermum parkii fruit fat
1.50 and Dormant oils 3.00 be added to oil phase pot, be heated to 85 DEG C, after all melting, stir, homogeneous 30 minutes.
3) pull-up vacuum, first suction part water mutually expects body in main cooker, then sucks oil phase material body, finally sucks water and mutually expects
Body, pulling vacuum to -0.02Mpa, then homogeneous open to 2500rpm, homogeneous 5 minutes adds kaolin 6.0, homogeneous 15 minutes,
Notice that taking out material body sees whether be uniformly dispersed, and stirs 15 minutes, froth breaking thoroughly, carries out next-step operation.Cooling water is opened, is cooled to
50 DEG C, stir, maintain vacuum, continue to lower the temperature, when 45 DEG C, add essence 0.05；It is well mixed.
4) continue to cool to 40 DEG C；Material body is placed into cleaning charging basket by 80 mesh filters.
5) censorship is sampled.
The extracting method of Chinese medical concrete：
90 mesh sieves will be crushed after oldenlandia diffusa, sun plant, Chinese actinidia root, Myrica rubra Dongkui root, japanese avens root drying, by 1:
0.8:2.2:0.8:2.2 part by weight mixing；Then 1 is pressed:9 solid-liquid part by weight mixed solvent (V95% ethanol：VEthyl acetate=
50:50) soak 5 hours, refluxing extraction three times, merge extract, steam solvent, obtain supernatant and separate out medicinal extract；Supernatant and
Dry extract is obtained after precipitation medicinal extract is vacuum dried.
Embodiment 3
1) by glycerin polyether -26 2.5, glycerine 4.9, xanthans 0.27, allantoin 0.09, Chinese medical concrete 10, glycyrrhizic acid two
Potassium 0.19 and distilled water 62 add water phase pot after soaking in advance, while being heated to being completely dissolved.It is heated to 85 DEG C to sterilize 40 points
Clock.
2) caprylic/capric triglyceride 2.95, dimethyl silicone polymer 2.05, (the poly dimethyl silicon of cetostearyl alcohol 5.1
Oxygen alkane is well mixed in advance with cetostearyl alcohol), ceteth -202.1, ceteareth -20.48, Butyrospermum parkii
Fruit fat 1.6 and Dormant oils 2.5 are added to oil phase pot, are heated to 84 DEG C, after all melting, stir, homogeneous 30 minutes.
3) pull-up vacuum, first suction part water mutually expects body in main cooker, then sucks oil phase material body, finally sucks water and mutually expects
Body, pulling vacuum to -0.02Mpa, then homogeneous open to 2500rpm, homogeneous 5 minutes adds kaolin 5.0, homogeneous 15 minutes,
Notice that taking out material body sees whether be uniformly dispersed, and stirs 15 minutes, froth breaking thoroughly, carries out next-step operation.Cooling water is opened, is cooled to
50 DEG C, stir, maintain vacuum, continue to lower the temperature, when 45 DEG C, add essence 0.055；It is well mixed.
4) continue to cool to 40 DEG C；Material body is placed into cleaning charging basket by 80 mesh filters.
5) censorship is sampled.
The extracting method of Chinese medical concrete：
110 mesh sieves will be crushed after oldenlandia diffusa, sun plant, Chinese actinidia root, Myrica rubra Dongkui root, japanese avens root drying, pressed
1:1.2:1.8:1.2:1.8 part by weight mixing；Then 1 is pressed:11 solid-liquid part by weight mixed solvent (V95% ethanol：
VEthyl acetate=50:50) soak 7 hours, refluxing extraction three times, merge extract, steam solvent, obtain supernatant and separate out medicinal extract；On
Dry extract is obtained after clear liquid and precipitation medicinal extract are vacuum dried.
Each composition in above example is configured by weight.
Refluxing extraction in the method for the invention, merge extract, steam solvent and vacuum drying is conventional work
Skill.
Comparison test
Cosmetics health specification with Ministry of Health of the People's Republic of China's issue carries out microorganism as guidance standard to facial mask
Inspection.
Three products of comparison test：No. 1 is blank, is not added with Chinese medical concrete and anticorrosion and bactericidal agent；No. 2 are done to add Chinese medical concrete
For the product of the present invention of preservative；No. 3 is mud film formulation, is not added with Chinese medical concrete, the mineral mud for plus 5%, plus 0.2% oxybenzene first
Ester, 0.1% Nipasol.
The product experimental result just produced is：
| Sequence number | Cosmetics total plate count | Go out excrement colibacillus group | Pseudomonas aeruginosa | Staphylococcus aureus | Yeast and mold sum |
| 1 | 3 | 0 | 0 | 0 | 0 |
| 2 | 2 | 0 | 0 | 0 | 0 |
| 3 | 0 | 0 | 0 | 0 | 0 |
Test result is after 1 year：
| Sequence number | Cosmetics total plate count | Go out excrement colibacillus group | Pseudomonas aeruginosa | Staphylococcus aureus | Yeast and mold sum |
| 1 | Cannot count (bacterium is more) | 0 | 0 | 0 | Cannot count |
| 2 | 0 | 0 | 0 | 0 | 0 |
| 3 | 0 | 0 | 0 | 0 | 0 |
Test result of the production after 2 years be：
Test result of the production after 3 years be：
| Sequence number | Cosmetics total plate count | Go out excrement colibacillus group | Pseudomonas aeruginosa | Staphylococcus aureus | Yeast and mold sum |
| 1 | Cannot count (bacterium is more) | 0 | 0 | 0 | Cannot count |
| 2 | 0 | 0 | 0 | 0 | 0 |
| 3 | 0 | 0 | 0 | 0 | 0 |
Claims (3)
1., with plant extracts as the preparation method of the draft facial mask of antisepsis and sterilization additive, carry out according to the following steps：
1) by glycerin polyether -26 2.3, glycerine 5.1, xanthans 0.23, allantoin 0.11, Chinese medical concrete 3, dipotassium glycyrrhizinate
0.21 and distilled water 64 soak in advance after add water phase pot, while being heated to being completely dissolved；It is heated to 85 DEG C to sterilize 30 minutes；
2) caprylic/capric triglyceride 3.05, dimethyl silicone polymer 1.95, cetostearyl alcohol 5.3, cetanol 1.9, spermaceti
Stereth -2 0.52, Butyrospermum parkii (BUTYROSPERMUM PARKII) fruit fat 1.4 and Dormant oils 3.5 are added to oil phase
Pot, is heated to 85 DEG C, after all melting, stirs, homogeneous 30 minutes；Wherein dimethyl silicone polymer is needed with cetostearyl alcohol
It is well mixed in advance；
3) pull-up vacuum, first suction part water mutually expects body in main cooker, then sucks oil phase material body, finally sucks water and mutually expects body, draws
Vacuum to -0.02Mpa, then homogeneous are opened to 2500rpm, homogeneous 5 minutes, add kaolin 7.0, homogeneous 15 minutes to note
Take out material body and see whether be uniformly dispersed, stir 15 minutes, froth breaking thoroughly, opens cooling water, cools to 50 DEG C, stirs, and ties up
Vacuum is held, continues to lower the temperature, when 45 DEG C, add essence 0.045；It is well mixed；
4) continue to cool to 40 DEG C；Material body is placed into cleaning charging basket by 80 mesh filters；
5) censorship is sampled；
The above each composition is configured by weight；
The extracting method of Chinese medical concrete：
100 mesh sieves will be crushed after oldenlandia diffusa, sun plant, Chinese actinidia root, Myrica rubra Dongkui root, japanese avens root drying, by 1:1:
2:1:2 part by weight mixing；Then 1 is pressed:10 solid-liquid part by weight is soaked 6 hours with mixed solvent, refluxing extraction three times, is closed
And extract, solvent is steamed, obtain supernatant and separate out medicinal extract；Dry extract is obtained after supernatant and precipitation medicinal extract are vacuum dried；
The mixed solvent is 50:50 V95% ethanolWith VEthyl acetate。
2., with plant extracts as the preparation method of the draft facial mask of antisepsis and sterilization additive, carry out according to the following steps：
1) by glycerin polyether -26 2.4, glycerine 5.0, xanthans 0.25, allantoin 0.10, Chinese medical concrete 5, dipotassium glycyrrhizinate
0.20 and distilled water 64.7 soak in advance after add water phase pot, while be heated to being completely dissolved, be heated to 85 DEG C and sterilize 35 points
Clock；
2) caprylic/capric triglyceride 3.00, dimethyl silicone polymer 2.00, cetostearyl alcohol 5.20, cetanol 2.00, whale
Wax stereth -2 0.50, Butyrospermum parkii fruit fat 1.50 and Dormant oils 3.00 are added to oil phase pot, are heated to 85 DEG C, all
After thawing, stir, homogeneous 30 minutes；Wherein dimethyl silicone polymer need to be well mixed in advance with cetostearyl alcohol；
3) pull-up vacuum, first suction part water mutually expects body in main cooker, then sucks oil phase material body, finally sucks water and mutually expects body, draws
Vacuum to -0.02Mpa, then homogeneous are opened to 2500rpm, homogeneous 5 minutes, add kaolin 6.0, homogeneous 15 minutes to note
Take out material body and see whether be uniformly dispersed, stir 15 minutes, froth breaking thoroughly, carries out next-step operation；Cooling water is opened, 50 are cooled to
DEG C, stir, vacuum is maintained, continue to lower the temperature, when 45 DEG C, add essence 0.05；It is well mixed；
4) continue to cool to 40 DEG C；Material body is placed into cleaning charging basket by 80 mesh filters；
5) censorship is sampled；
The above each composition is configured by weight；
The extracting method of Chinese medical concrete：
90 mesh sieves will be crushed after oldenlandia diffusa, sun plant, Chinese actinidia root, Myrica rubra Dongkui root, japanese avens root drying, by 1:0.8:
2.2:0.8:2.2 part by weight mixing；Then 1 is pressed:9 solid-liquid part by weight is soaked 5 hours with mixed solvent, refluxing extraction three
It is secondary, merge extract, solvent is steamed, obtain supernatant and separate out medicinal extract；Must do after supernatant and precipitation medicinal extract are vacuum dried
Medicinal extract；The mixed solvent is 50:50 V95% ethanolWith VEthyl acetate。
3., with plant extracts as the preparation method of the draft facial mask of antisepsis and sterilization additive, carry out according to the following steps：
1) by glycerin polyether -26 2.5, glycerine 4.9, xanthans 0.27, allantoin 0.09, Chinese medical concrete 10, dipotassium glycyrrhizinate
0.19 and distilled water 62 soak in advance after add water phase pot, while being heated to being completely dissolved；It is heated to 85 DEG C to sterilize 40 minutes；
2) caprylic/capric triglyceride 2.95, dimethyl silicone polymer 2.05, cetostearyl alcohol 5.1, ceteth -20
2.1st, ceteareth -2 0.48, Butyrospermum parkii fruit fat 1.6 and Dormant oils 2.5 are added to oil phase pot, are heated to 84 DEG C,
After all melting, stir, homogeneous 30 minutes；Wherein dimethyl silicone polymer need to be well mixed in advance with cetostearyl alcohol；
3) pull-up vacuum, first suction part water mutually expects body in main cooker, then sucks oil phase material body, finally sucks water and mutually expects body, draws
Vacuum to -0.02Mpa, then homogeneous are opened to 2500rpm, homogeneous 5 minutes, add kaolin 5.0, homogeneous 15 minutes to note
Take out material body and see whether be uniformly dispersed, stir 15 minutes, froth breaking thoroughly, carries out next-step operation；Cooling water is opened, 50 are cooled to
DEG C, stir, vacuum is maintained, continue to lower the temperature, when 45 DEG C, add essence 0.055；It is well mixed；
4) continue to cool to 40 DEG C；Material body is placed into cleaning charging basket by 80 mesh filters；
5) censorship is sampled；
The above each composition is configured by weight；
The extracting method of Chinese medical concrete：
110 mesh sieves will be crushed after oldenlandia diffusa, sun plant, Chinese actinidia root, Myrica rubra Dongkui root, japanese avens root drying, by 1:
1.2:1.8:1.2:1.8 part by weight mixing；Then 1 is pressed:11 solid-liquid part by weight is soaked 7 hours with mixed solvent, backflow
Extract three times, merge extract, steam solvent, obtain supernatant and separate out medicinal extract；Supernatant and precipitation medicinal extract are vacuum dried
Dry extract is obtained afterwards；The mixed solvent is 50:50 V95% ethanolWith VEthyl acetate。
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