CN103550101B - There is plant extraction liquid and the application thereof of tender white moisturizing effect - Google Patents
There is plant extraction liquid and the application thereof of tender white moisturizing effect Download PDFInfo
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- CN103550101B CN103550101B CN201310545979.6A CN201310545979A CN103550101B CN 103550101 B CN103550101 B CN 103550101B CN 201310545979 A CN201310545979 A CN 201310545979A CN 103550101 B CN103550101 B CN 103550101B
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- blue berry
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Abstract
The invention discloses a kind of plant extraction liquid and the application thereof with tender white moisturizing effect, described plant extraction liquid is the extracting solution of Blue berry leaf, blue berry and aloe mixture; It can be applicable in cosmetics.The technological parameter with the preparation method of the plant extraction liquid of tender white moisturizing effect of the present invention, through a large amount of experiment of inventor and experience, obtain optimum process combination, in the extracting solution obtained by the method, the activity of material is higher, and it is for having significant skin nursing effect in cosmetics; And this extracting solution raw materials used be pure plant, extracting solution is natural reliable, nontoxic, and expands the utilization rate of blue berry, avoids the waste of raw material.
Description
Technical field
The present invention relates to cosmetic field, particularly relate to a kind of plant extraction liquid and the application thereof with tender white moisturizing effect.
Background technology
Along with improving constantly of the progress of society and expanding economy and living standards of the people, the requirement of people to beauty and skin care cosmetics is also more and more higher, more and more to the future development of " naturalization, nutrient laden, curative effect ".But great majority all contain harmful chemical substance in various beauty and skin care cosmetics in the market, as poisonous and harmful substances such as leaded, hydrargyrum, these skin care item easily cause people's skin allergy, cause damage to human organ and function.From eighties of last century eighties, skin expert just finds, adds various natural material, have good nourishing effect, and have no side effect to skin in skin care item, and particularly from plant, effective component extracting adds in skin care item and has good effect.Therefore, develop the beauty and skin care cosmetics that effective ingredient that a kind of utilization extracts from plant makes human body skin has nutrition and a protective effect and have very important meaning.
Summary of the invention
Based on this, the invention provides a kind of plant extraction liquid with tender white moisturizing effect.
The concrete technical scheme solved the problems of the technologies described above is as follows:
There is the plant extraction liquid of tender white moisturizing effect, comprise following component: the extracting solution of the mixture of Blue berry leaf, blue berry and Aloe, described extracting solution preparation method comprises the steps:
(1) extract: Blue berry leaf, blue berry and Folium Aloe are shredded by above-mentioned weight ratio, homogenate, obtains serosity; By serosity by weight adding in deionized water for 1:9-11, being heated to 40-60 DEG C, then being that 9-11:1 adds cellulase by the weight ratio of serosity and cellulase, stir, then add ethanol, the final concentration to ethanol is 43-47%(volume fraction), supersound process, stirs, obtains feed liquid;
(2) concentrated: feed liquid filtered, gained filtrate be-0.08 ~-0.1Mpa in vacuum, and distilling under reduced pressure at temperature 40 DEG C-45 DEG C, steams completely to ethanol, filtration, centrifugal, obtain the extracting solution of mixture of Blue berry leaf, blue berry and Aloe.
Wherein in some embodiments, the weight of Blue berry leaf in the mixture of described Blue berry leaf, blue berry and Aloe, blue berry and Aloe is (1-10): (1-10): (1-10).
Wherein in some embodiments, the weight ratio of certain kind of berries leaf in the mixture of described Blue berry leaf, blue berry and Aloe, blue berry and Aloe is 5-7:1.5-2.5:1.
Wherein in some embodiments, the weight of certain kind of berries leaf in the mixture of described Blue berry leaf, blue berry and Aloe, blue berry and Aloe is 6:2:1.
The present invention also provides a kind of above-mentioned application of plant extraction liquid in cosmetics with tender white moisturizing effect.
Wherein in some embodiments, be the plant extraction liquid with tender white moisturizing effect of 1-10% containing mass fraction in described cosmetics.
Wherein in some embodiments, be the plant extraction liquid with tender white moisturizing effect of 5-10% containing mass fraction in described cosmetics.
Wherein in some embodiments, described cosmetics are protective skin cream, facial cleaning cream, emulsion or astringent.
Of the present invention a kind ofly have the plant extraction liquid of tender white moisturizing effect and application has the following advantages and beneficial effect:
(1) plant extraction liquid with tender white moisturizing effect of the present invention is Blue berry leaf, the mixture extracting solution of blue berry and Aloe, the technological parameter of the preparation method of described extracting solution, through a large amount of experiment of inventor and experience, obtain optimum process combination, in the extracting solution obtained by the method, the activity of material is higher, it is for having significant skin nursing effect in cosmetics, and draw in research process, with Blue berry leaf, extracting solution obtained by the mixture of blue berry and Aloe, its skin nursing Be very effective is better than first by Blue berry leaf, blue berry and Aloe are extracted separately, the skin nursing effect of extracting solution obtained by rear mixing.
(2) plant extraction liquid of the present invention is raw materials used is pure plant, and obtained extracting solution is natural, nontoxic, and expands the utilization rate of blue berry, avoids the waste of raw material.
Detailed description of the invention
Below with reference to specific embodiment, the present invention will be further described.
Following embodiment cellulase is purchased from Hangzhou Beiao Bio-Technology Engineering Co., Ltd.;
Blue berry extracting solution and Aloe extraction solution are purchased from Huzhou Jiamei Biochemical Products Co., Ltd..
Embodiment 1 plant extraction liquid and the application in protective skin cream thereof and skin nursing effect
One, experiment purpose
By relative analysis, evaluate the tender white moisturizing effect of plant extraction liquid obtained in the present embodiment.
Two, experimental technique
Comparative example 1: commercially available blue berry extracting solution and Aloe extraction solution, prepares mixed extract by weight for 8:1;
Comparative example 2: Blue berry leaf, blue berry and Folium Aloe are shredded, homogenate, obtains serosity; Serosity is added 45% alcoholic solution by weight for 1:10, open and stir, mixing speed controls at 15-20 rev/min, stir 30 minutes, filter, gained filtrate is-0.08 ~-0.1Mpa in vacuum, distilling under reduced pressure at temperature 40 DEG C-45 DEG C, steam completely to ethanol, obtain the extracting solution of Blue berry leaf, blue berry and aloe mixture;
Comparative example 3: Blue berry leaf, blue berry and Folium Aloe are shredded, homogenate, obtains serosity; By serosity by weight adding in deionized water for 1:13, being heated to 40-60 DEG C, then being that 13:1 adds cellulase by the weight ratio of serosity and cellulase, stir, then add ethanol, the final concentration to ethanol is 40%(volume fraction), supersound process, stirs, obtains feed liquid; Feed liquid is filtered, filters, centrifugal, obtain the extracting solution of mixture of Blue berry leaf, blue berry and Aloe.
Experimental group: the weight ratio of Blue berry leaf, blue berry and Aloe is see table 1, and in table, I, II, III and IV are experimental group A, and VI, VII, VIII and Ⅸ is experimental group B.
The weight ratio of Blue berry leaf in table 1 Blue berry leaf, blue berry and aloe mixture, blue berry and Aloe
Experimental group A: the preparation method of described extracting solution comprises the steps:
(1) extract: by weight ratio shown in following table 1, Blue berry leaf, blue berry and Folium Aloe are shredded, homogenate, obtains serosity; By serosity by weight adding in deionized water for 1:10, being heated to 40-60 DEG C, then being that 10:1 adds cellulase by the weight ratio of serosity and cellulase, open and stir, mixing speed controls at 15-20 rev/min, stirs 30 minutes; Add ethanol again, making the concentration of alcohol in system rise to volume fraction is 45%, and adopt frequency to be the ultrasonic Treatment 5-9 minute of 20kHZ, then open stirring, mixing speed controls at 15-20 rev/min, stirs 30 minutes, obtains feed liquid;
(2) concentrated: feed liquid filtered, gained filtrate is-0.08 ~-0.1Mpa in vacuum, and distilling under reduced pressure at temperature 40 DEG C-45 DEG C, steams completely to ethanol, filter, centrifugal, obtain the extracting solution of Blue berry leaf, blue berry and aloe mixture.
In experimental group B: VI, VII and VIII, the preparation method of Blue berry leaf extracting solution, blue berry extracting solution or Aloe extraction solution comprises the steps:
(1) extract: by weight ratio described in table 1, Blue berry leaf, blue berry or Folium Aloe are shredded, homogenate, obtains serosity; By serosity by weight adding in deionized water for 1:10, being heated to 40-60 DEG C, then being that 10:1 adds cellulase by the weight ratio of serosity and cellulase, open and stir, mixing speed controls at 15-20 rev/min, stirs 30 minutes; Add ethanol again, making the concentration of alcohol in system rise to volume fraction is 45%, and adopt frequency to be the ultrasonic Treatment 5-9 minute of 20kHZ, then open stirring, mixing speed controls at 15-20 rev/min, stirs 30 minutes, obtains feed liquid;
(2) concentrated: feed liquid filtered, gained filtrate is-0.08 ~-0.1Mpa in vacuum, and distilling under reduced pressure at temperature 40 DEG C-45 DEG C, steams completely to ethanol, filter, centrifugal, obtain the extracting solution of Blue berry leaf, blue berry and aloe mixture.
The above-mentioned obtained plant extraction liquid with tender white moisturizing effect is applied in protective skin cream.
Wherein, the mass fraction of described plant extraction liquid in protective skin cream is see table 2, and in table, I, II, III and IV are experimental group A, and VI, VII, VIII and Ⅸ is experimental group B.
The formula table of table 2 plant extraction liquid in protective skin cream
Three, test
(1) tested object: each group is 100 women (20-30 year);
(2) test instrunment: VISA digital skin analyser (U.S.), Aomei health moisture of skin tester (domestic)
(3) test zone: inner forearm and face; Use: twice daily, continue use 4 weeks;
(4) test event: whitening, humidity of skin, skin delicacy degree.
The tender white moisturizing effect of table 3 embodiment 1
As known from Table 3, the tender white moisturizing effect that with the addition of the experimental group formula I-IV of plant extraction liquid in protective skin cream is all significantly better than VI-Ⅸ, the tender white moisturizing effect of comparative example 1, comparative example 2 and comparative example 3, and the tender white moisturizing best results of experimental group formula I II, illustrate that the Ingredients Active contained in this plant extraction liquid is higher, and in III group, the active component content of extracting solution is the highest; Though experimental group VI-VIII formula one-component is identical with experimental group III, its tender white moisturizing effect is far worse than the tender white moisturizing effect of experimental group formula I II; The tender white moisturizing effect of experimental group formula Ⅸ is worse than the tender white moisturizing effect of experimental group formula I-IV, and the tender white moisturizing effect of comparative example 1, comparative example 2 and comparative example 3 is slightly worse than the tender white moisturizing effect of experimental group formula I V; Draw thus, through the mixed extract that extracting method described in the present embodiment is obtained, its activity is higher, is applied to moisturizing skin nursing best results in protective skin cream.
Embodiment 2
One, the application of plant extraction liquid in astringent
By weight ratio and preparation method thereof described in the I-IV shown in table 1 in embodiment 1, be applied in astringent by obtained plant extraction liquid, concrete formula is see table 4:
The formula table of table 4 plant extraction liquid in astringent
Two, the test of tender white moisturizing effect
Method of testing refers to embodiment 1, and concrete effect is in table 5:
The tender white moisturizing effect of table 5 embodiment 2
As known from Table 5, the tender white moisturizing Be very effective that with the addition of the experimental group formula I-IV of plant extraction liquid in astringent is better than the tender white moisturizing effect of comparative example V, and namely explanation plant extraction liquid is applied in astringent and has significant tender white moisturizing effect.
The above embodiment only have expressed several embodiment of the present invention, and it describes comparatively concrete and detailed, but therefore can not be interpreted as the restriction to the scope of the claims of the present invention.It should be pointed out that for the person of ordinary skill of the art, without departing from the inventive concept of the premise, can also make some distortion and improvement, these all belong to protection scope of the present invention.Therefore, the protection domain of patent of the present invention should be as the criterion with claims.
Claims (6)
1. have the plant extraction liquid of tender white moisturizing effect, it is characterized in that, described plant extraction liquid is the extracting solution of mixture of Blue berry leaf, blue berry and Aloe; The weight ratio of Blue berry leaf in the mixture of described Blue berry leaf, blue berry and Aloe, blue berry and Aloe is 1-10:1-10:1-10; The preparation method of described extracting solution comprises the steps:
(1) extract: Blue berry leaf, blue berry and Folium Aloe are shredded, homogenate, obtains serosity; Be that 1:9-11 adds deionized water by the weight ratio of serosity and deionized water, be heated to 40-60 DEG C, then be that 9-11:1 adds cellulase by the weight ratio of serosity and cellulase, stir, add ethanol, the final concentration to ethanol is 43-47%, supersound process, stirs, obtains feed liquid;
(2) concentrated: feed liquid filtered, gained filtrate is-0.08 ~-0.1MPa in vacuum, and distilling under reduced pressure at temperature 40 DEG C-45 DEG C, steams completely to ethanol, filter, centrifugal, obtain the extracting solution of Blue berry leaf, blue berry and aloe mixture.
2. the plant extraction liquid with tender white moisturizing effect according to claim 1, is characterized in that, the weight ratio of Blue berry leaf in the mixture of described Blue berry leaf, blue berry and Aloe, blue berry and Aloe is 5-7:1.5-2.5:1.
3. the plant extraction liquid with tender white moisturizing effect described in any one of claim 1-2 is preparing the application in cosmetics.
4. the plant extraction liquid with tender white moisturizing effect according to claim 3 is preparing the application in cosmetics, it is characterized in that, is the plant extraction liquid with tender white moisturizing effect of 1-10% in described cosmetics containing mass fraction.
5. the plant extraction liquid with tender white moisturizing effect according to claim 3 is preparing the application in cosmetics, it is characterized in that, is the plant extraction liquid with tender white moisturizing effect of 5-10% in described cosmetics containing mass fraction.
6. the plant extraction liquid with replenishing water and preserving moisture effect according to claim 5 is preparing the application in cosmetics, and it is characterized in that, described cosmetics are protective skin cream, facial cleaning cream, emulsion or astringent.
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CN104367512B (en) * | 2014-11-12 | 2017-08-25 | 中国检验检疫科学研究院 | A kind of blueberry leaf flavones Essence and preparation method and application |
CN108309873B (en) * | 2018-05-07 | 2021-04-13 | 深圳润邦之家生物科技有限公司 | Activation-balanced conditioning essence |
CN108653099A (en) * | 2018-07-17 | 2018-10-16 | 襄阳佰蒂生物科技股份有限公司 | A kind of blueberry extract cleanser manufacturing process |
CN108553400A (en) * | 2018-07-17 | 2018-09-21 | 襄阳佰蒂生物科技股份有限公司 | A kind of water profit whitening blueberry facial mask manufacturing process |
CN112220692A (en) * | 2020-10-30 | 2021-01-15 | 深圳市洛奇机电科技有限公司 | Preparation method of facial cell repair gel |
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CN101547615A (en) * | 2006-10-13 | 2009-09-30 | 热尔韦·达诺尼公司 | New composition for improving skin quality and a process for preparing the same |
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