CN102113987B - Cosmetic containing natural plant extractives and preparation method thereof - Google Patents

Cosmetic containing natural plant extractives and preparation method thereof Download PDF

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Publication number
CN102113987B
CN102113987B CN2011100520873A CN201110052087A CN102113987B CN 102113987 B CN102113987 B CN 102113987B CN 2011100520873 A CN2011100520873 A CN 2011100520873A CN 201110052087 A CN201110052087 A CN 201110052087A CN 102113987 B CN102113987 B CN 102113987B
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extract
cosmetics
broken
natural plant
concentrated
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CN2011100520873A
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CN102113987A (en
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袁珂
林茵
殷明文
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浙江农林大学
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Abstract

The invention relates to a cosmetic containing natural plant extractives and a preparation method thereof, belonging to the technical field of cosmetics. The cosmetic containing natural plant extractives is characterized by being prepared from the following components in percentage by weight: 1.0-2.2 percent of okra fruit extractive, 1.0-2.0 percent of grape seed extractive, 0.5-1.2 percent of sapindus extractive and the balance of aid and carrier. The favorable synergy and excellent efficacy in aspects of improving skin winkles, whitening and beautifying skin, clearing radicals, lightening speckles and decomposing melanin is presented due to simultaneously using the okra fruit extractive, the grape seed extractive and the sapindus extractive, and the favorable antimicrobial preservative action of the sapindus extractive ensures that the microorganism index of the product can accord with the cosmetic production requirements.

Description

Contain cosmetics of natural plant extracts and preparation method thereof

Technical field

The invention belongs to the cosmetics technical field, be specially cosmetics that contain natural plant extracts and preparation method thereof.

Background technology

Cosmetics and skin care item play crucial effects to beautifying with skin protection of the mankind in the world today, and beauty treatment has become one of 21 centurys ten big hot topic industry.In the process of rapid economic development, the cosmetics market of China from small to large, from weak to strong, cosmetic industry is grown up strong and sturdy just like the mushrooms after rain, brand is to emerge in an endless stream, at present the cosmetics market of China has become maximum market, the whole world.

Be accompanied by the domestic consumer to the cognition of daily use chemicals industries such as cosmetics be familiar with; Increasing consumer pays close attention to safety, health, effective care method more; Especially the appearance of plants herb class skin care item has further promoted the fast development of cosmetic industry.China has abundant Chinese herbal medicine resource, and the annual rate of growth of Chinese herbal medicine cosmetics is up to 60%.Therefore the cosmetics of natural plant kind are worth expectation, will have the bigger development potentiality and the market space from now on.

See that from nearly 2 years cosmetics market natural cosmetics will become the trend that people will consume from now on undoubtedly.Natural cosmetics extracts from natural plants, can play effects such as nutrition protection and skin care to the skin of human body, can not cause the functional component of zest damage again to skin.Therefore the vegetalitas article of making up that from plant, extract natural component are methods of science, environmental protection.

Abelmoschus esculentus is the annual herb plant, has another name called coffee Radix seu folium abelmoschi moschati, swordweed, Abelmoschus esculentus, Herba Lysimachiae Clethroids (Radix Seu Herba Lysimachiae Clethroidis) etc.All there is the distribution and cultivation of Abelmoschus esculentus the southern and northern various places of China; The American is referred to as " plant viagra "; The Japanese is referred to as " Green Ginseng ", and it also is decided to be athletic first-selected vegetable by many countries, is a kind of new type of health vegetable with better nutritivity and medical value.Functional components such as rich in proteins, fat, carbohydrate, vitamin, mineral and dietary fiber, flavone, pectin, polysaccharide in the Abelmoschus esculentus; The mucus shape material that particularly is rich in the tender pod of Abelmoschus esculentus; Be the mixture by poly galactose, galactan and ARABINANS and pectin, wherein pectin is a kind of soluble fiber, and it can promote the drainage of organic substance in the body; Reduce accumulation, blood sugar lowering and the content of cholesterol of toxin.Glutinous sliding juice ability facilitating digestion prevents constipation.Have that cancer is anticancer, kidney invigorating and YANG supporting, enhancing immunity, effect such as aid digestion.Water-soluble fibre pectin, polysaccharide in the Abelmoschus esculentus also have good health-care effect to skin, smash the tender fruit of Abelmoschus esculentus to pieces taking juice and are used for that skin protection has unique looks improving and the skin nourishing, increases skin elasticity and slow down aging, dispels moth patch on the skin, makes skin-whitening, delicate effect.

Contain a large amount of procyanidins in the Semen Vitis viniferae, grape polyphenols is described as strong effect free radical scavenger, is one of efficient antioxidants of plant origin.Show that with in vitro tests the antioxidant effect of Semen Vitis viniferae extract is vitamin C and vitamin E 30~50 times in the body.Has the powerful effect of removing free radical, improving body immunity.Semen Vitis viniferae is natural sunlight overcover, can encroach on skin by shielding of ultraviolet, prevents and improve UV-induced skin pigment to precipitate.Former blue and white pigment in the Semen Vitis viniferae can be repaired injured collagen protein and elastic fiber; Can improve multiple anaphylaxis; Can also reduce melanin pigmentation, particularly can prevent and improve UV-induced skin pigment deposition, can make colour of skin homogeneous transparent, desalination melanin.Semen Vitis viniferae extract has astriction, can tighten up skin, prevents occurring ahead of time of wrinkle of skin, and life-time service can keep the moist of skin, improves and the enhancing skin elasticity, has the effect of looks improving and the skin nourishing.Semen Vitis viniferae has functions such as antiinflammatory, antioxidation, beauty treatment, blood circulation promoting simultaneously, can also reduce melanin deposition and dermatitis and take place through the active free radical of removing of restraint of tyrosinase.Semen Vitis viniferae not only can efficiently be removed the intravital free radical of people, and can promote the metabolism of skin, and the pollution of isolation environment and the injury of cosmetics are desalinated mottle, decomposed melanin, reach the effect of skin whitening.Contain abundant glycoside material in the natural plants Fructus Sapindi Mukouossi, be mainly triterpene saponin, sesquiterpene glycoside.Have very strong anti-bacterial, anti-itching, sterilization and anticorrosion, antiinflammatory, cleaning skin, prevent and treat dermatosis, dispelling speckles and whitening face, effectively take out stains; Foam enriches free from extraneous odour; And 100% degraded can not produce any residue that is harmful to health and hostile environment, belongs to the fully natural green nuisance-free plant.At present existing a large amount of evidences confirm to act on human body skin to have effective cleaning skin, anti-bacterial, anti-itching, beauty treatment and brightens, and removes the speckle acne removing, prevents and treats dermopathic effect such as acne.

Though have report to use Semen Vitis viniferae or Fructus Sapindi Mukouossi to be applied in the cosmetics separately, do not report that as yet containing this three's natural plant extracts of Abelmoschus esculentus fruit, Semen Vitis viniferae and Fructus Sapindi Mukouossi simultaneously is applied in the cosmetics.

Summary of the invention

To the problems referred to above that exist in the prior art situation; The objective of the invention is to design the technical scheme that cosmetics of containing natural plant extracts and preparation method thereof are provided, these cosmetics have the effect of improving wrinkle of skin, increasing skin elasticity, beauty face-whitening-nourishing, speckle dispelling.

The cosmetics that contain natural plant extracts is characterized in that containing the following material of weight percentage: Abelmoschus esculentus fruit extract 1.0~2.2%, and Semen Vitis viniferae extract 1.0~2.0%, Fructus Sapindi Mukouossi extract 0.5~1.2%, surplus is auxiliary agent and carrier;

The method for preparing of said Abelmoschus esculentus fruit extract may further comprise the steps: drying after the crosspiece face section or air-dry, it is in the container of broken extractor of 800~1800 W that exsiccant Abelmoschus esculentus fruit is placed power of motor, adds 20~60% aquiferous ethanol with the tender fruit of Abelmoschus esculentus; Starting switch carries out with the rotating speed of 6000-10000 r/min that room temperature texture is broken to extract 2~3 times, and raw material is broken into 20~100 purpose granularities; If Abelmoschus esculentus fruit dry weight be 1kg then the aquiferous ethanol consumption be 6~8 liters; Extraction time is 1~5 minute, with the extracting solution sucking filtration, discards filtering residue; The extracting solution that obtains is at 50~80 ℃; Vacuum is to adopt Reduced Pressure Concentration Device to carry out flash concentration under 0.090~0.095 Mpa condition, regulates the feed liquor speed of solution to be concentrated, with 150~300 mL min -1Flow be concentrated into 1/5~1/6 of original volume repeatedly, continue that concentrated solution is carried out vacuum drying and become dry powder, with obtaining Abelmoschus esculentus fruit extract dry powder behind the mortar porphyrize;

The method for preparing of said Semen Vitis viniferae extract may further comprise the steps: it is the container of the broken extractor of 800~1800 W that exsiccant Semen Vitis viniferae is placed power of motor, adds 40~80% aquiferous ethanol, starting switch; Rotating speed with 6000-10000 r/min carries out historrhexis's extraction 1~3 time; Raw material is broken into 40~100 purpose granularities, if Semen Vitis viniferae dry weight be 1kg then the aquiferous ethanol consumption be 8~12 liters, each extraction time is 1~5 minute; With the extracting solution sucking filtration; Discard filtering residue, the extracting solution that merging obtains is at 50~80 ℃, and vacuum is to adopt Reduced Pressure Concentration Device to carry out flash concentration under 0.090~0.095 Mpa condition; Regulate the feed liquor speed of solution to be concentrated, with 100~300 mL min -1Flow be concentrated into 1/6~1/10 of original volume repeatedly, continue that concentrated solution is carried out vacuum drying and become dry powder, with obtaining Semen Vitis viniferae extract dry powder behind the mortar porphyrize;

Said Fructus Sapindi Mukouossi preparation method of extract may further comprise the steps: with the fruit of Fructus Sapindi Mukouossi tree through artificial dry in the sun, peeling, the pure peel that then obtains, it is the container of the broken extractor of 800~1800 W that pure peel is placed power of motor; Add 40~100% aquiferous ethanol, starting switch carries out with the rotating speed of 6000-10000 r/min that room temperature texture is broken to extract 1~3 time; Raw material is broken into 40~100 purpose granularities, if the pure peel weight of Fructus Sapindi Mukouossi be 1kg then the aquiferous ethanol consumption be 6~10 liters, each extraction time is 2~5 minutes; With the extracting solution sucking filtration; Discard filtering residue, the extracting solution that merging obtains is at 50~80 ℃, and vacuum is to adopt Reduced Pressure Concentration Device to carry out flash concentration under 0.090~0.095 Mpa condition; Regulate the feed liquor speed of solution to be concentrated, with 100~300 mL min -1Flow be concentrated into 1/5~1/8 of original volume repeatedly, then concentrated solution is proceeded vacuum drying and becomes dry powder, with obtaining Fructus Sapindi Mukouossi extract dry powder behind the mortar porphyrize.

The described cosmetics that contain natural plant extracts, the content that it is characterized in that said Abelmoschus esculentus fruit extract is 1.2~2.0%, preferred 1.5~1.8%.

The described cosmetics that contain natural plant extracts, the content that it is characterized in that said Semen Vitis viniferae extract is 1.2~1.8%, preferred 1.5~1.7%.

The described cosmetics that contain natural plant extracts, the content that it is characterized in that said Fructus Sapindi Mukouossi extract is 0.6~1.0%, preferred 0.7~0.8%.

The described cosmetics that contain natural plant extracts is characterized in that in the method for preparing of said Abelmoschus Esculentus Linn extract: the concentration of aquiferous ethanol is 30~50%, preferred 35~45%; Broken extraction time is 3~4 minutes; The extracting solution flash temperature is 55 ℃~70 ℃, preferred 60 ℃~65 ℃; Power of motor is 1000~1500 W, and rotating speed is 7000-8000 r/min, and the particle size after cracking of raw material is 50~80 orders, and the feed liquor flow is 150~250 mL min -1

The described cosmetics that contain natural plant extracts is characterized in that in the method for preparing of said Semen Vitis viniferae extract: the concentration of aquiferous ethanol is 50~70%, preferred 55~65%; Broken extraction time is 3~4 minutes; The extracting solution flash temperature is 55 ℃~75 ℃, preferred 65 ℃~70 ℃; Power of motor is 1000~1500 W, and rotating speed is 7000-8000 r/min, and the particle size after cracking of raw material is 50~80 orders, and the feed liquor flow is 150~250 mL min -1

The described cosmetics that contain natural plant extracts, it is characterized in that in the said Fructus Sapindi Mukouossi preparation method of extract: the concentration of aquiferous ethanol is 50~90%, preferred 60~80%; Broken extraction time is 3~4 minutes; The extracting solution flash temperature is 55 ℃~70 ℃, preferred 60 ℃~65 ℃; Power of motor is 1000~1500 W, and rotating speed is 7000-8000 r/min, and the particle size after cracking of raw material is 50~80 orders, and the feed liquor flow is 150~250 mL min -1

The described method for preparing that contains the cosmetics of natural plant extracts is characterized in that comprising following processing step: according to Abelmoschus esculentus fruit extract 1.0~2.2%, and Semen Vitis viniferae extract 1.0~2.0%; The weight percent of Fructus Sapindi Mukouossi extract 0.5~1.2% takes by weighing each component, adds auxiliary agent and carrier then and mixes, and is heated to 70 ℃~85 ℃; Under heating, carry out magnetic agitation, mixing, homogeneity and emulsifying, stirred 5~13 minutes, cool the temperature to 50 ℃~60 ℃ then; Continue to mix, homogeneity and emulsifying; Guarantee to add mutually fully dissolving and emulsion depletion of QI and bubble out at present and be as the criterion, stop heated and stirred, be placed to room temperature and obtain finished product.

The described method for preparing that contains the cosmetics of natural plant extracts is characterized in that: heating-up temperature is that mixing time is 8-10 minute to 75~80 ℃.

Described broken extractor can directly be buied from market, and Reduced Pressure Concentration Device (flash concentration device) is design and assembly voluntarily, also can from market, directly buy.

Above-mentioned cosmetics that contain natural plant extracts and preparation method thereof have following beneficial effect: 1. the cosmetic formulations of originating for pure natural plant, environmental protection, safety and Health.Use in the time of Abelmoschus esculentus fruit extract, Semen Vitis viniferae extract and Fructus Sapindi Mukouossi extract and improving wrinkle of skin, increase skin elasticity, beauty face-whitening-nourishing, removing free radical, desalination mottle, decomposing and demonstrate good synergism aspect the melanin and excellent effect is far longer than wherein a kind of effect of independent use.

2. the Fructus Sapindi Mukouossi extract brightens, effectively also has good antisepsis and sterilization effect in cleaning skin, the speckle removing, acne removing effect having beauty treatment concurrently; Be the pure natural antiseptic; Guaranteed that this product need not have the excellent antibiotic antisepsis under the situation of extra interpolation antiseptic, has guaranteed that microbiological indicator meets the Cosmetic Manufacture requirement.Contain a large amount of flavones ingredients in Abelmoschus Esculentus Linn extract and the Semen Vitis viniferae extract, belong to natural antioxidant, therefore need not extra interpolation antioxidant and just can bring into play measured by esr technique.

3. Abelmoschus esculentus fruit, Semen Vitis viniferae, Fructus Sapindi Mukouossi are adopted broken the extraction; Cardinal principle is that plant material that is extracted and appropriate solvent are put in the extractor; Utilize the cutter of high speed rotating that the plant fragmentation is trimmed to fine particle; Simultaneously through realizing the combination of high-speed stirred, vibration, mixing, infiltration, dipping, make the effective ingredient of inside plants in the extremely short time, be transferred in the solvent and reach the stripping balance, realize extracting purpose through filtering.Accomplish when this method for distilling has been realized pulverizing and leaching process, the broken extraction once only needs a few minutes, and leaching process need not heating simultaneously, avoids the destructive probability of thermo-labile component, has greatly kept original nutrition and functional component.Show that through experiment this method for distilling has and extracts quick, complete, energy-efficient, easy and simple to handle, environmental, work efficiency than advantages such as height.Adopting this method to extract can extract the most of functional component in the above natural plants fully, has improved the extraction ratio and the content of nutrition and functional component.

4. adopt Reduced Pressure Concentration Device to carry out flash concentration to Abelmoschus esculentus fruit, Semen Vitis viniferae, Fructus Sapindi Mukouossi extracting solution; Its ultimate principle is under reduced pressure; Make and treat that spissated liquid at the uniform velocity gets in the thin film evaporation pipe with thread; Form thin film after in pipe, being heated, make the partial solvent gasification and reach concentrated purpose.Use this device to concentrate to have heating temperature low, extremely short by the concentrated liquid heated time, the concentrated solution temperature of recovery is no more than 80 ℃, effectively protects the thermal sensitivity composition not to be destroyed, the advantage that solvent recovering yield is high.This installed capacity is big, does not receive by the restriction of concentrated solution volume size, and it is concentrated to circulate continuously, volume required up to being concentrated into.The concentrated speed of this method is fast, efficient is high, and simple to operate, easy to use, energy-conserving and environment-protective have kept nutrition and the functional component in the extract simultaneously to greatest extent.

The percentage composition that relates in the present specification unless otherwise indicated all refers to weight percentage.

The specific embodiment

Below in conjunction with specific embodiment the present invention is described further.

Embodiment 1:

These cosmetics can be processed the skin-protecting face nursing emulsion, are made up of the following material of weight percentage: Abelmoschus esculentus fruit extract 1.0%, Semen Vitis viniferae extract 1.0%, Fructus Sapindi Mukouossi extract 1.0%; Sodium lauryl sulphate 1.0%, glyceryl monostearate 2.5%, octadecanol 3.5%, hydroxyethyl-cellulose 2.0%; Dimethicone 4.0%, glycerol 5.0%, propylene glycol 3.0%, ethyl acetate 1.0%; Ethanol 6.0%, spice 0.5% adds water to 100%.

Embodiment 2:

These cosmetics can be processed anti-drawn grain breast, are made up of the following material of weight percentage: Abelmoschus esculentus fruit extract 1.5%, Semen Vitis viniferae extract 2.0%, Fructus Sapindi Mukouossi extract 0.5%; Polysorbate 2.0%, glyceryl monostearate 2.0%, octadecanol 3.0%, hydroxyethyl-cellulose 2.0%; Triethanolamine 4.0%, glycerol 6.0%, propylene glycol 3.5%, Polyethylene Glycol 2.0%; Ethyl acetate 3.0%, hyaluronate sodium 2.0% adds water to 100%.

Embodiment 3:

These cosmetics can be processed whitening and moistening skin and reveal, and are made up of the following material of weight percentage: Abelmoschus esculentus fruit extract 2.0%, Semen Vitis viniferae extract 1.0%, Fructus Sapindi Mukouossi extract 1.0%; Stearic acid 2.0%, polysorbate 2.0%, octadecanol 3.0%, hydroxyethyl-cellulose 2.0%; Dimethicone 4.0%, glycerol 6.0%, fresh milk 5.0%, benzyl benzoate 2.0%; Ethanol 6.0%, spice 0.5% adds water to 100%.

Embodiment 4:

These cosmetics can be processed spot-removing ointment, are made up of the following material of weight percentage: Abelmoschus esculentus fruit extract 1.5%, Semen Vitis viniferae extract 2.0%, Fructus Sapindi Mukouossi extract 0.5%; Octadecanol 5.0%, sodium lauryl sulphate 2.0%, hydroxyethyl-cellulose 3.0%, wax 2.0%; Glycerol 5.0%, propylene glycol 3.0%, cyclodextrin 3.0%, Polyethylene Glycol 2.0%; Ethanol 3.0%, spice 0.5% adds water to 100%.

Embodiment 5:

These cosmetics can be processed the radioprotective sunlight lotion, are made up of the following material of weight percentage: Abelmoschus esculentus fruit extract 1.5%, Semen Vitis viniferae extract 2.0%, Fructus Sapindi Mukouossi extract 0.5%; Hydroxyethyl-cellulose 5.0%, polysorbate 2.0%, hyaluronate sodium 3.0%; Glycerol 5.0%, propylene glycol 2.0%, vegetable oil 3.0%; Benzyl benzoate 1.0%, ethanol 5.0% adds water to 100%.

Embodiment 6:

These cosmetics can be processed the convergence skin-tendering cream, are made up of the following material of weight percentage: Abelmoschus esculentus fruit extract 2.0%, Semen Vitis viniferae extract 1.5%, Fructus Sapindi Mukouossi extract 1.0%; Octadecanol 4.0%, polysorbate 2.0%, hyaluronate sodium 2.0%; Glycerol 5.0%, propylene glycol 2.0%, vegetable oil 3.0%; Ethyl acetate 1.0%, ethanol 5.0% adds water to 100%.

Plant extract described in the embodiment 1-6 prepares according to following method.

The method for preparing of said Abelmoschus esculentus fruit extract may further comprise the steps: with the tender fruit of Abelmoschus esculentus to dry after the crosspiece face section or air-dry; It is in the container of broken extractor of 840 W that exsiccant Abelmoschus esculentus fruit is placed power of motor; Add 40% aquiferous ethanol; Starting switch carries out with the rotating speed of 10000 r/min that room temperature texture is broken to extract 2 times, and raw material is broken into 60 purpose granularities.If Abelmoschus esculentus fruit dry weight be 1kg then the aquiferous ethanol consumption be 6 liters; Extraction time is 3 minutes, with the extracting solution sucking filtration, discards filtering residue; The extracting solution that obtains is at 60 ℃; Vacuum is to adopt Reduced Pressure Concentration Device to carry out flash concentration under the 0.090 Mpa condition, regulates the feed liquor speed of solution to be concentrated, with 250 mLmin -1Flow be concentrated into 1/5 of original volume repeatedly, continue that concentrated solution is carried out vacuum drying and become dry powder, with obtaining Abelmoschus esculentus fruit extract dry powder behind the mortar porphyrize, Abelmoschus esculentus fruit extract yield reaches 35.7%.In this method for preparing: the power of motor of broken extract can be 1800 W, and rotating speed can be 6000 r/min, and the concentration of aquiferous ethanol can be 20%, 30%, 50%, 60%; Broken number of times is 3 times, and raw material granularity can be broken into 40,80,100 orders; Extraction time is 1,2,4,5 minute; Abelmoschus esculentus fruit dry weight be 1kg then the aquiferous ethanol consumption be 7 liters, 8 liters, extracting solution flash concentration temperature is 50 ℃, 70 ℃, 80 ℃, vacuum is 0.095 Mpa, the feed liquor speed of solution to be concentrated is 150 mLmin -1, 180 mLmin -1, 200 mLmin -1, 230 mLmin -1, 280 mLmin -1, 300 mLmin -1, other method is the same, and Abelmoschus esculentus fruit extract yield can reach 20.8%~41.3%.

The method for preparing of said Semen Vitis viniferae extract may further comprise the steps: exsiccant Semen Vitis viniferae is put in the broken extractor that power of motor is 840 W; Add 60% aquiferous ethanol; Starting switch carries out historrhexis with the rotating speed of 10000 r/min and extracts 2 times, and raw material is broken into 60 purpose granularities.If Semen Vitis viniferae dry weight be 1kg then the aquiferous ethanol consumption be 10 liters; Each extraction time is 2 minutes, with the extracting solution sucking filtration, discards filtering residue; The extracting solution that merging obtains is at 70 ℃; Vacuum is to adopt Reduced Pressure Concentration Device to carry out flash concentration under the 0.095 Mpa condition, regulates the feed liquor speed of solution to be concentrated, with 200 mL min -1Flow be concentrated into 1/8 of original volume repeatedly, continue that concentrated solution is carried out vacuum drying and become dry powder, with obtaining Semen Vitis viniferae extract dry powder behind the mortar porphyrize, the Semen Vitis viniferae extract yield reaches 30.6%.In this method for preparing: the power of motor of broken extract can be 1800 W, and rotating speed can be 6000 r/min, and the concentration of aquiferous ethanol can be 40%, 50%, 70%, 80%; Broken number of times is 1 time, 3 times, and raw material granularity can be broken into 40,80,100 orders; Extraction time is 1,3,4,5 minute; Abelmoschus esculentus fruit dry weight be 1kg then the aquiferous ethanol consumption be 8 liters, 9 liters, 11 liters, 12 liters, extracting solution flash concentration temperature is 50 ℃, 60 ℃, 80 ℃, vacuum is 0.090 Mpa, the feed liquor speed of solution to be concentrated is 100 mLmin -1, 150 mLmin -1, 180 mLmin -1, 210 mLmin -1, 230 mLmin -1, 280 mLmin -1, 300 mLmin -1, other method is the same, and the Semen Vitis viniferae extract yield reaches 23.4%~38.8%.

Said Fructus Sapindi Mukouossi preparation method of extract may further comprise the steps: with the fruit of Fructus Sapindi Mukouossi tree through artificial dry in the sun, peeling; The pure peel that then obtains; It is the broken extractor of 840 W that pure peel is placed power of motor, adds 50% aquiferous ethanol, starting switch; Rotating speed with 10000 r/min carries out the broken extraction of room temperature texture 3 times, and raw material is broken into 40 purpose granularities.If the pure peel weight of Fructus Sapindi Mukouossi be 1kg then the aquiferous ethanol consumption be 8 liters; Each extraction time is 2 minutes, with the extracting solution sucking filtration, discards filtering residue; The extracting solution that merging obtains is at 65 ℃; Vacuum is to adopt Reduced Pressure Concentration Device to carry out flash concentration under the 0.095 Mpa condition, regulates the feed liquor speed of solution to be concentrated, with 200 mLmin -1Flow be concentrated into 1/6 of original volume repeatedly, then concentrated solution is proceeded vacuum drying and becomes dry powder, with obtaining Fructus Sapindi Mukouossi extract dry powder behind the mortar porphyrize.The Fructus Sapindi Mukouossi extract yield reaches 28.4%.In this method for preparing: the power of motor of broken extract can be 1800 W, and rotating speed can be 6000 r/min, and the concentration of aquiferous ethanol can be 40%, 60%, 70%, 80%, 90%, 100%; Broken number of times is 1 time, 2 times, and raw material granularity can be broken into 80,100 orders; Extraction time is 3,4,5 minutes; Abelmoschus esculentus fruit dry weight be 1kg then the aquiferous ethanol consumption be 6 liters, 7 liters, 9 liters, 10 liters, extracting solution flash concentration temperature is 50 ℃, 60 ℃, 80 ℃, vacuum is 0.090 Mpa, the feed liquor speed of solution to be concentrated is 100 mLmin -1, 150 mLmin -1, 180 mLmin -1, 210 mLmin -1, 230 mLmin -1, 280 mLmin -1, 300 mLmin -1, other method is the same, and the Fructus Sapindi Mukouossi extract yield reaches 18.7%~36.6%.

The method for preparing of these cosmetics comprises following processing step: according to Abelmoschus esculentus fruit extract 1.0~2.2%, and Semen Vitis viniferae extract 1.0~2.0%, the weight percent of Fructus Sapindi Mukouossi extract 0.5~1.2% takes by weighing each component; Add auxiliary agent and carrier then and mix, be heated to 70~85 ℃, under heating, carry out magnetic agitation, mixing, homogeneity and emulsifying; Stirred 5~10 minutes; Cool the temperature to 50 ℃~60 ℃ then, continue to mix, homogeneity and emulsifying, guarantee to add mutually fully dissolving and emulsion depletion of QI and bubble out at present and be as the criterion; Stop heated and stirred, be placed to room temperature and obtain finished product.

Above-mentioned cosmetics can make several formulations, like skin-protecting face nursing emulsion, anti-drawn grain breast, whitening and moistening skin dew, spot-removing ointment, radioprotective sunlight lotion, convergence skin-tendering cream etc.And according to common process interpolation cosmetic additive and carrier, concrete consumption is a routine techniques, repeats no more at this.Described cosmetic additive and carrier comprise antiseptic, antioxidant, thickening agent, stabilizing agent, flavouring agent, alcohols and esters solvent, polyol, gel forming agent, oils, polymer, emulsifying agent, water, spice, fresh milk etc.Cosmetic additive and carrier are specially Polyethylene Glycol, polysorbate, stearic acid, triethanolamine, cyclodextrin, glyceryl monostearate, sodium lauryl sulphate, octadecanol, hydroxyethyl-cellulose, ethyl acetate, benzyl benzoate, ethanol, 1; The 3-butanediol, kinds such as propylene glycol, hyaluronate sodium, dimethicone, glycerol, wax, water, spice, fresh milk and various plant oils.Vegetable oil comprises Oleum Arachidis hypogaeae semen, Oleum sesami, Oleum Glycines, salad oil, Semen Ricini wet goods.

Below further this explains beneficial effect of the present invention through corresponding experiment data.

Test 1: improve the effect test of wrinkle of skin, result of the test is seen table 1.

For proving that it improves the effect of wrinkle of skin, use the anti-drawn grain breast of embodiment 2 to make an experiment, the test position is facial; Subjects is 2 groups, and one group is the women at 40~50 years old age, and another group is 51~60 years old women for the age; After each clean, smear for twice sooner or later every day, carry out soft and massage with hands simultaneously in the edge of face and eyes; Adhered to 2 months on probation, and observed the improvement situation of estimating face and eye part skin wrinkle.

The anti-drawn grain breast of table 1 improves the effect test of wrinkle of skin

Tried age and position Experimenter's number The massage time Significant effective Appropriateness effectively Invalid Obvious effective rate Facial wrinkles improves effect (40~50 years old) 10 5 minutes 5 4 1 90% Facial wrinkles improves effect (51~60 years old) 8 5 minutes 2 4 2 75% Eye wrinkle-removing improves effect (40~50 years old) 12 5 minutes 6 4 2 83.3% Eye wrinkle-removing improves effect (51~60 years old) 13 5 minutes 3 5 5 61.5%

2. whitening effect test, result of the test is seen table 2.

For proving its whitening effect to skin, use the whitening and moistening skin dew of embodiment 3 to make an experiment, the test position is facial; Subjects is 2 groups, and one group is the women at 20~30 years old age, and another group is 31~45 years old women for the age; After each clean, smear for twice sooner or later every day, carry out softly with hands simultaneously in entire face; Adhered to 1 month on probation, and observed and estimate facial whitening effect.

Table 2 whitening and moistening skin reveals the whitening effect test

Tried the age Experimenter's number Significant effective Appropriateness effectively Invalid Obvious effective rate 20~30 years old 16 8 6 2 87.5% 31~45 years old 12 6 4 2 83.3%

3. freckle effect test, result of the test is seen table 3.

For proving its freckle effect to skin of face, use the spot-removing ointment of embodiment 4 to make an experiment, the test position is facial; Subjects is 2 groups, and one group is the women at 40~49 years old age, and another group is 50~60 years old women for the age; After each clean, smear for twice sooner or later every day, carry out softly with hands simultaneously in entire face; Adhered to 2 months on probation, and observed and estimate facial freckle effect.

The test of table 3 spot-removing ointment freckle effect

Tried the age Experimenter's number Significant effective Appropriateness effectively Invalid Obvious effective rate 40~49 years old (chloasma) 10 3 5 2 80% 50~60 years old (chloasma) 8 2 4 4 75%

4. radioprotective, sun-proof result contrast test, result of the test is seen table 4.

For proving its radioprotective, sun-proof result, use the sunscreen cream of embodiment 5 to make an experiment, the test position is facial; Subjects is 2 groups; One group is the women at 40~49 years old age, and another group is 50~60 years old women for the age, at every turn after clean; Smear sunscreen cream in entire face, carry out softly with hands simultaneously.One-month period on probation, feed back its radioprotective, sun-proof effect by the experimenter, estimate.

The radioprotective of table 4 radioprotective sunscreen cream, sun-proof result test

Tried the age Experimenter's number Significant effective Appropriateness effectively Invalid Obvious effective rate 40~49 years old 8 4 3 1 87.5% 50~60 years old 8 3 4 1 87.5%

5. increase the skin elasticity effect test, result of the test is seen table 5.

For proving that it increases the effect of skin elasticity, use the convergence skin-tendering cream of embodiment 6 to make an experiment, the test position is facial; Subjects is 2 groups, and one group is the women at 45~55 years old age, and another group is 56~65 years old women for the age; After each clean; Smear the convergence skin-tendering cream in entire face, smear for twice every day sooner or later, carries out softly with hands simultaneously.2 months on probation, feed back the effect that it increases skin elasticity by the experimenter.

Table 5 convergence skin-tendering cream increases the effect test of skin elasticity

Tried the age Experimenter's number Significant effective Appropriateness effectively Invalid Obvious effective rate 45~55 years old 12 5 4 3 75% 56~65 years old 10 3 3 4 60%

Claims (9)

1. the cosmetics that contain natural plant extracts is characterized in that containing the following material of weight percentage: Abelmoschus esculentus fruit extract 1.0~2.2%, and Semen Vitis viniferae extract 1.0~2.0%, Fructus Sapindi Mukouossi extract 0.5~1.2%, surplus is auxiliary agent and carrier;
The method for preparing of said Abelmoschus esculentus fruit extract may further comprise the steps: drying after the crosspiece face section or air-dry, it is in the container of broken extractor of 800~1800 W that exsiccant Abelmoschus esculentus fruit is placed power of motor, adds 20~60% aquiferous ethanol with the tender fruit of Abelmoschus esculentus; Starting switch carries out with the rotating speed of 6000-10000 r/min that room temperature texture is broken to extract 2~3 times, and raw material is broken into 20~100 purpose granularities; If Abelmoschus esculentus fruit dry weight be 1kg then the aquiferous ethanol consumption be 6~8 liters; Extraction time is 1~5 minute, with the extracting solution sucking filtration, discards filtering residue; The extracting solution that obtains is at 50~80 ℃; Vacuum is to adopt Reduced Pressure Concentration Device to carry out flash concentration under 0.090~0.095 Mpa condition, regulates the feed liquor speed of solution to be concentrated, with 150~300 mLmin -1Flow be concentrated into 1/5~1/6 of original volume repeatedly, continue that concentrated solution is carried out vacuum drying and become dry powder, with obtaining Abelmoschus esculentus fruit extract dry powder behind the mortar porphyrize;
The method for preparing of said Semen Vitis viniferae extract may further comprise the steps: it is the container of the broken extractor of 800~1800 W that exsiccant Semen Vitis viniferae is placed power of motor, adds 40~80% aquiferous ethanol, starting switch; Rotating speed with 6000-10000 r/min carries out historrhexis's extraction 1~3 time; Raw material is broken into 40~100 purpose granularities, if Semen Vitis viniferae dry weight be 1kg then the aquiferous ethanol consumption be 8~12 liters, each extraction time is 1~5 minute; With the extracting solution sucking filtration; Discard filtering residue, the extracting solution that merging obtains is at 50~80 ℃, and vacuum is to adopt Reduced Pressure Concentration Device to carry out flash concentration under 0.090~0.095 Mpa condition; Regulate the feed liquor speed of solution to be concentrated, with 100~300 mLmin -1Flow be concentrated into 1/6~1/10 of original volume repeatedly, continue that concentrated solution is carried out vacuum drying and become dry powder, with obtaining Semen Vitis viniferae extract dry powder behind the mortar porphyrize;
Said Fructus Sapindi Mukouossi preparation method of extract may further comprise the steps: with the fruit of Fructus Sapindi Mukouossi tree through artificial dry in the sun, peeling, the pure peel that then obtains, it is the container of the broken extractor of 800~1800 W that pure peel is placed power of motor; Add 40~100% aquiferous ethanol, starting switch carries out with the rotating speed of 6000-10000 r/min that room temperature texture is broken to extract 1~3 time; Raw material is broken into 40~100 purpose granularities, if the pure peel weight of Fructus Sapindi Mukouossi be 1kg then the aquiferous ethanol consumption be 6~10 liters, each extraction time is 2~5 minutes; With the extracting solution sucking filtration; Discard filtering residue, the extracting solution that merging obtains is at 50~80 ℃, and vacuum is to adopt Reduced Pressure Concentration Device to carry out flash concentration under 0.090~0.095 Mpa condition; Regulate the feed liquor speed of solution to be concentrated, with 100~300 mLmin -1Flow be concentrated into 1/5~1/8 of original volume repeatedly, then concentrated solution is proceeded vacuum drying and becomes dry powder, with obtaining Fructus Sapindi Mukouossi extract dry powder behind the mortar porphyrize.
2. the cosmetics that contain natural plant extracts as claimed in claim 1, the content that it is characterized in that said Abelmoschus esculentus fruit extract is 1.2~2.0%.
3. the cosmetics that contain natural plant extracts as claimed in claim 1, the content that it is characterized in that said Semen Vitis viniferae extract is 1.2~1.8%.
4. the cosmetics that contain natural plant extracts as claimed in claim 1, the content that it is characterized in that said Fructus Sapindi Mukouossi extract is 0.6~1.0%.
5. the cosmetics that contain natural plant extracts as claimed in claim 1 is characterized in that in the method for preparing of said Abelmoschus Esculentus Linn extract: the concentration of aquiferous ethanol is 30~50%; Broken extraction time is 3~4 minutes; The extracting solution flash temperature is 55 ℃~70 ℃; Power of motor is 1000~1500 W, and rotating speed is 7000-8000 r/min, and the particle size after cracking of raw material is 50~80 orders, and the feed liquor flow is 150~250 mLmin -1
6. the cosmetics that contain natural plant extracts as claimed in claim 1 is characterized in that in the method for preparing of said Semen Vitis viniferae extract: the concentration of aquiferous ethanol is 50~70%; Broken extraction time is 3~4 minutes; The extracting solution flash temperature is 55 ℃~75 ℃; Power of motor is 1000~1500 W, and rotating speed is 7000-8000 r/min, and the particle size after cracking of raw material is 50~80 orders, and the feed liquor flow is 150~250 mLmin -1
7. the cosmetics that contain natural plant extracts as claimed in claim 1, it is characterized in that in the said Fructus Sapindi Mukouossi preparation method of extract: the concentration of aquiferous ethanol is 50~90%; Broken extraction time is 3~4 minutes; The extracting solution flash temperature is 55 ℃~70 ℃; Power of motor is 1000~1500 W, and rotating speed is 7000-8000 r/min, and the particle size after cracking of raw material is 50~80 orders, and the feed liquor flow is 150~250 mLmin -1
8. the method for preparing that contains the cosmetics of natural plant extracts as claimed in claim 1 is characterized in that comprising following processing step: according to Abelmoschus esculentus fruit extract 1.0~2.2%, and Semen Vitis viniferae extract 1.0~2.0%; The weight percent of Fructus Sapindi Mukouossi extract 0.5~1.2% takes by weighing each component; Add auxiliary agent and carrier then and mix, be heated to 70 ℃~85 ℃, under heating, carry out magnetic agitation, mixing, homogeneity and emulsifying; Stirred 5~13 minutes; Cool the temperature to 50 ℃~60 ℃ then, continue to mix, homogeneity and emulsifying, guarantee to add mutually fully dissolving and emulsion depletion of QI and bubble out at present and be as the criterion; Stop heated and stirred, be placed to room temperature and obtain finished product.
9. the method for preparing that contains the cosmetics of natural plant extracts as claimed in claim 8 is characterized in that: heating-up temperature is that mixing time is 8-10 minute to 75~80 ℃.
CN2011100520873A 2011-03-04 2011-03-04 Cosmetic containing natural plant extractives and preparation method thereof CN102113987B (en)

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MX369122B (en) * 2012-11-21 2019-10-30 Kbs Res Llc Herbal supplements and methods of use thereof.
CN104337743A (en) * 2013-08-07 2015-02-11 海南春蕾南繁实业发展有限公司 Hibiscus esculentus-pearl deep sea bath salt and preparation method thereof
CN104337752A (en) * 2014-10-28 2015-02-11 广西金昊生物科技有限公司 Okra beauty mask powder and preparation method thereof
CN104367508A (en) * 2014-11-13 2015-02-25 杭州高琦香精化妆品有限公司 Okra facial cream and preparation method thereof
CN104431632A (en) * 2014-12-30 2015-03-25 浙江海洋学院 Feed for black carps
CN104644500B (en) * 2015-01-30 2018-05-11 广州澳医生物科技有限公司 A kind of plant moisturizing composition and preparation method thereof
CN104856910A (en) * 2015-06-02 2015-08-26 白华 Non-surgical artistic cosmetic cream
CN106361639A (en) * 2016-10-06 2017-02-01 刘艺鹏 Natural plant beauty cosmetic
CN107961180A (en) * 2016-10-20 2018-04-27 申扬阳 okra nutrition essence
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