CN103550101A - Plant extract with whitening and moisturizing functions and application thereof - Google Patents
Plant extract with whitening and moisturizing functions and application thereof Download PDFInfo
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- CN103550101A CN103550101A CN201310545979.6A CN201310545979A CN103550101A CN 103550101 A CN103550101 A CN 103550101A CN 201310545979 A CN201310545979 A CN 201310545979A CN 103550101 A CN103550101 A CN 103550101A
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- blue berry
- extraction liquid
- plant extraction
- aloe
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Abstract
The invention discloses a plant extract with whitening and moisturizing functions and application thereof. The plant extract is an extract of a mixture of blueberry leaves, blueberry fruits and aloe, and can be applied to the cosmetics. According to a preparation method of the plant extract with the whitening and moisturizing functions, through a lot of experiments and experience of an inventor, an optimal process combination of process parameters is obtained; the activity of substances in the extract prepared by adopting the method is higher, and the plant extract is remarkable in whitening and moisturizing effects in the cosmetics; the raw materials used by the extract are pure plants, the extract is natural, reliable and nontoxic, the utilization rate of blueberry is increased, and the raw materials are prevented from being wasted.
Description
Technical field
The present invention relates to cosmetic field, particularly relate to a kind of plant extraction liquid and application thereof with tender white moisturizing effect.
Background technology
Along with improving constantly of social progress and expanding economy and living standards of the people, people are also more and more higher to the requirement of beauty and skin care cosmetics, more and more to the future development of " naturalization, nutrient laden, curative effect ".But great majority all contain harmful chemical substance in various beauty and skin care cosmetics in the market, as poisonous and harmful substances such as leaded, hydrargyrum, these skin care item easily cause people's skin allergy, and human organ and function are caused to damage.From eighties of last century eighties, skin expert just finds, adds various natural materials in skin care item, skin is had to good nourishing effect, and have no side effect, and particularly from plant, effective component extracting adds to and in skin care item, has good effect.Therefore, developing effective ingredient that a kind of utilization extracts from plant makes the beauty and skin care cosmetics that human body skin is had to nutrition and a protective effect and has very important meaning.
Summary of the invention
Based on this, the invention provides a kind of plant extraction liquid with tender white moisturizing effect.
The concrete technical scheme solving the problems of the technologies described above is as follows:
A plant extraction liquid with tender white moisturizing effect, comprises following component: the extracting solution of the mixture of Blue berry leaf, blue berry and Aloe, described extracting solution preparation method comprises the steps:
(1) extract: by above-mentioned weight ratio, by Blue berry leaf, blue berry and Folium Aloe chopping, homogenate, obtains serosity; Serosity, by weight for 1:9-11 adds in deionized water, is heated to 40-60 ℃, then is that 9-11:1 adds cellulase by the weight ratio of serosity and cellulase, stir, then add ethanol, to the final concentration of ethanol be 43-47%(volume fraction), supersound process, stirs, and obtains feed liquid;
(2) concentrated: feed liquid is filtered, and gained filtrate be-0.08～-0.1Mpa in vacuum, distilling under reduced pressure at 40 ℃-45 ℃ of temperature, steams completely to ethanol, and filtration is centrifugal, obtains the extracting solution of the mixture of Blue berry leaf, blue berry and Aloe.
In some embodiment, in the mixture of described Blue berry leaf, blue berry and Aloe, the weight portion proportioning of Blue berry leaf, blue berry and Aloe is (1-10): (1-10): (1-10) therein.
In some embodiment, in the mixture of described Blue berry leaf, blue berry and Aloe, the weight ratio of certain kind of berries leaf, blue berry and Aloe is 5-7:1.5-2.5:1 therein.
In some embodiment, in the mixture of described Blue berry leaf, blue berry and Aloe, the weight portion proportioning of certain kind of berries leaf, blue berry and Aloe is 6:2:1 therein.
The present invention also provides the application of a kind of above-mentioned plant extraction liquid with tender white moisturizing effect in cosmetics.
In some embodiment, in described cosmetics, contain the plant extraction liquid that mass fraction is the tender white moisturizing effect of having of 1-10% therein.
In some embodiment, in described cosmetics, contain the plant extraction liquid that mass fraction is the tender white moisturizing effect of having of 5-10% therein.
In some embodiment, described cosmetics are protective skin cream, facial cleaning cream, emulsion or astringent therein.
Of the present invention a kind ofly have the plant extraction liquid of tender white moisturizing effect and application has the following advantages and beneficial effect:
(1) plant extraction liquid with tender white moisturizing effect of the present invention is Blue berry leaf, the mixture extracting solution of blue berry and Aloe, the technological parameter of the preparation method of described extracting solution, through a large amount of experiment and the experiences of inventor, obtain optimum process combination, in the extracting solution making by the method, the activity of material is higher, it has significant skin nursing effect for cosmetics, and draw in research process, with Blue berry leaf, the obtained extracting solution of mixture of blue berry and Aloe, its skin nursing effect is significantly better than first by Blue berry leaf, blue berry and Aloe are extracted separately, the skin nursing effect of the obtained extracting solution of rear mixing.
(2) plant extraction liquid of the present invention is raw materials used is pure plant, and the extracting solution making is natural, nontoxic, and has expanded the utilization rate of blue berry, has avoided the waste of raw material.
The specific embodiment
Below with reference to specific embodiment, the present invention will be further described.
Following embodiment cellulase is purchased from Hangzhou Beiao Bio-Technology Engineering Co., Ltd.;
Blue berry extracting solution and Aloe extraction solution are purchased from Huzhou Jiamei biochemistry Products Co., Ltd.
Embodiment 1 plant extraction liquid and the application in protective skin cream thereof and skin nursing effect
One, experiment purpose
By relative analysis, evaluate the tender white moisturizing effect of the plant extraction liquid making in the present embodiment.
Two, experimental technique
Comparative example 1: commercially available blue berry extracting solution and Aloe extraction solution, by weight preparing mixed extract for 8:1;
Comparative example 2: by Blue berry leaf, blue berry and Folium Aloe chopping, homogenate, obtains serosity; By serosity by weight adding 45% alcoholic solution for 1:10, open and stir, mixing speed is controlled at 15-20 rev/min, stir 30 minutes, filter, gained filtrate is-0.08～-0.1Mpa in vacuum, distilling under reduced pressure at 40 ℃-45 ℃ of temperature, steam completely to ethanol, obtain the extracting solution of Blue berry leaf, blue berry and aloe mixture;
Comparative example 3: by Blue berry leaf, blue berry and Folium Aloe chopping, homogenate, obtains serosity; Serosity, by weight for 1:13 adds in deionized water, is heated to 40-60 ℃, then is that 13:1 adds cellulase by the weight ratio of serosity and cellulase, stir, then add ethanol, to the final concentration of ethanol be 40%(volume fraction), supersound process, stirs, and obtains feed liquid; Feed liquid is filtered, filter, centrifugal, obtain the extracting solution of the mixture of Blue berry leaf, blue berry and Aloe.
Experimental group: the weight ratio of Blue berry leaf, blue berry and Aloe is referring to table 1, and in table, I, II, III and IV are experimental group A, and VI, VII, VIII and IX are experimental group B.
The weight ratio of Blue berry leaf, blue berry and Aloe in table 1 Blue berry leaf, blue berry and aloe mixture
Experimental group A: the preparation method of described extracting solution comprises the steps:
(1) extract: by weight ratio shown in following table 1, by Blue berry leaf, blue berry and Folium Aloe chopping, homogenate, obtains serosity; Serosity, by weight for 1:10 adds in deionized water, is heated to 40-60 ℃, then is that 10:1 adds cellulase by the weight ratio of serosity and cellulase, open and stir, mixing speed is controlled at 15-20 rev/min, stirs 30 minutes; Add ethanol, making concentration of alcohol in system rise to volume fraction is 45% again, the ultrasonic Treatment 5-9 minute that proportion is 20kHZ, then open and stir, mixing speed is controlled at 15-20 rev/min, stirs 30 minutes, obtains feed liquid;
(2) concentrated: feed liquid is filtered, and gained filtrate be-0.08～-0.1Mpa in vacuum, distilling under reduced pressure at 40 ℃-45 ℃ of temperature, steams completely to ethanol, and filtration is centrifugal, obtains the extracting solution of Blue berry leaf, blue berry and aloe mixture.
Experimental group B: in VI, VII and VIII, the preparation method of Blue berry leaf extracting solution, blue berry extracting solution or Aloe extraction solution comprises the steps:
(1) extract: press weight ratio described in table 1, Blue berry leaf, blue berry or Folium Aloe are shredded, homogenate, obtains serosity; Serosity, by weight for 1:10 adds in deionized water, is heated to 40-60 ℃, then is that 10:1 adds cellulase by the weight ratio of serosity and cellulase, open and stir, mixing speed is controlled at 15-20 rev/min, stirs 30 minutes; Add ethanol, making concentration of alcohol in system rise to volume fraction is 45% again, the ultrasonic Treatment 5-9 minute that proportion is 20kHZ, then open and stir, mixing speed is controlled at 15-20 rev/min, stirs 30 minutes, obtains feed liquid;
(2) concentrated: feed liquid is filtered, and gained filtrate be-0.08～-0.1Mpa in vacuum, distilling under reduced pressure at 40 ℃-45 ℃ of temperature, steams completely to ethanol, and filtration is centrifugal, obtains the extracting solution of Blue berry leaf, blue berry and aloe mixture.
The above-mentioned plant extraction liquid with tender white moisturizing effect making is applied in protective skin cream.
Wherein, the mass fraction of described plant extraction liquid in protective skin cream is referring to table 2, and in table, I, II, III and IV are experimental group A, and VI, VII, VIII and IX are experimental group B.
The formula table of table 2 plant extraction liquid in protective skin cream
Three, test
(1) tested object: each group is 100 women (20-30 year);
(2) test instrunment: VISA numeral skin analyzer (U.S.), Aomei health moisture of skin tester (domestic)
(3) test zone: forearm inner side and face; Use: every day twice, continue to use 4 weeks;
(4) test event: whitening, humidity of skin, skin delicacy degree.
The tender white moisturizing effect of table 3 embodiment 1
As known from Table 3, the tender white moisturizing effect of having added the experimental group formula I-IV of plant extraction liquid in protective skin cream is all significantly better than the tender white moisturizing effect of VI-IX, comparative example 1, comparative example 2 and comparative example 3, and the tender white moisturizing best results of experimental group formula I II, illustrate that the composition activity containing in this plant extraction liquid is higher, and in III group, the active component content of extracting solution is the highest; Though experimental group VI-VIII formula one-component is identical with experimental group III, its tender white moisturizing effect is far worse than the tender white moisturizing effect of experimental group formula I II; The tender white moisturizing effect of experimental group formula IX is worse than the tender white moisturizing effect of experimental group formula I-IV, and the tender white moisturizing effect of comparative example 1, comparative example 2 and comparative example 3 is slightly worse than the tender white moisturizing effect of experimental group formula I V; Draw thus, the mixed extract making through extracting method described in the present embodiment, its activity is higher, is applied to moisturizing skin nursing best results in protective skin cream.
Embodiment 2
One, the application of plant extraction liquid in astringent
Press in embodiment 1 weight ratio and preparation method thereof described in the I-IV shown in table 1, the plant extraction liquid making is applied in astringent, concrete formula is referring to table 4:
The formula table of table 4 plant extraction liquid in astringent
Two, the test of tender white moisturizing effect
Method of testing refers to embodiment 1, and concrete effect is in Table 5:
The tender white moisturizing effect of table 5 embodiment 2
As known from Table 5, the tender white moisturizing effect of having added the experimental group formula I-IV of plant extraction liquid in astringent is significantly better than the tender white moisturizing effect of comparative example V, illustrates that plant extraction liquid is applied to have in astringent significant tender white moisturizing effect.
The above embodiment has only expressed several embodiment of the present invention, and it describes comparatively concrete and detailed, but can not therefore be interpreted as the restriction to the scope of the claims of the present invention.It should be pointed out that for the person of ordinary skill of the art, without departing from the inventive concept of the premise, can also make some distortion and improvement, these all belong to protection scope of the present invention.Therefore, the protection domain of patent of the present invention should be as the criterion with claims.
Claims (7)
1. a plant extraction liquid with tender white moisturizing effect, is characterized in that, described plant extraction liquid is the extracting solution of the mixture of Blue berry leaf, blue berry and Aloe; The preparation method of described extracting solution comprises the steps:
(1) extract: by Blue berry leaf, blue berry and Folium Aloe chopping, homogenate, obtains serosity; By the weight ratio of serosity and deionized water, be that 1:9-11 adds deionized water, be heated to 40-60 ℃, then be that 9-11:1 adds cellulase by the weight ratio of serosity and cellulase, stir, add ethanol, to the final concentration of ethanol be 43-47%, supersound process, stirs, and obtains feed liquid;
(2) concentrated: feed liquid is filtered, and gained filtrate be-0.08～-0.1Mpa in vacuum, distilling under reduced pressure at 40 ℃-45 ℃ of temperature, steams completely to ethanol, and filtration is centrifugal, obtains the extracting solution of Blue berry leaf, blue berry and aloe mixture.
2. the plant extraction liquid with tender white moisturizing effect according to claim 1, is characterized in that, in the mixture of described Blue berry leaf, blue berry and Aloe, the weight ratio of Blue berry leaf, blue berry and Aloe is 1-10:1-10:1-10.
3. the plant extraction liquid with tender white moisturizing effect according to claim 1, is characterized in that, in the mixture of described Blue berry leaf, blue berry and Aloe, the weight ratio of Blue berry leaf, blue berry and Aloe is 5-7:1.5-2.5:1.
4. the application of the plant extraction liquid with tender white moisturizing effect described in claim 1-3 any one in cosmetics.
5. the application of the plant extraction liquid with tender white moisturizing effect according to claim 4 in cosmetics, is characterized in that, contains the plant extraction liquid with tender white moisturizing effect described in the claim 1-3 that mass fraction is 1-10% in described cosmetics.
6. the application of the plant extraction liquid with tender white moisturizing effect according to claim 4 in cosmetics, is characterized in that, contains the plant extraction liquid with tender white moisturizing effect described in the claim 1-3 that mass fraction is 5-10% in described cosmetics.
7. the application of the plant extraction liquid with replenishing water and preserving moisture effect according to claim 6 in cosmetics, is characterized in that, described cosmetics are protective skin cream, facial cleaning cream, emulsion or astringent.
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104367512A (en) * | 2014-11-12 | 2015-02-25 | 中国检验检疫科学研究院 | Blueberry leaf flavone essential liquid as well as preparation method and application thereof |
| CN108309873A (en) * | 2018-05-07 | 2018-07-24 | 深圳润邦之家生物科技有限公司 | Assign balanced conditioning Essence living |
| CN108553400A (en) * | 2018-07-17 | 2018-09-21 | 襄阳佰蒂生物科技股份有限公司 | A kind of water profit whitening blueberry facial mask manufacturing process |
| CN108653099A (en) * | 2018-07-17 | 2018-10-16 | 襄阳佰蒂生物科技股份有限公司 | A kind of blueberry extract cleanser manufacturing process |
| CN112220692A (en) * | 2020-10-30 | 2021-01-15 | 深圳市洛奇机电科技有限公司 | Preparation method of facial cell repair gel |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101547615A (en) * | 2006-10-13 | 2009-09-30 | 热尔韦·达诺尼公司 | New composition for improving skin quality and a process for preparing the same |
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2013
- 2013-11-06 CN CN201310545979.6A patent/CN103550101B/en not_active Expired - Fee Related
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101547615A (en) * | 2006-10-13 | 2009-09-30 | 热尔韦·达诺尼公司 | New composition for improving skin quality and a process for preparing the same |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104367512A (en) * | 2014-11-12 | 2015-02-25 | 中国检验检疫科学研究院 | Blueberry leaf flavone essential liquid as well as preparation method and application thereof |
| CN104367512B (en) * | 2014-11-12 | 2017-08-25 | 中国检验检疫科学研究院 | A kind of blueberry leaf flavones Essence and preparation method and application |
| CN108309873A (en) * | 2018-05-07 | 2018-07-24 | 深圳润邦之家生物科技有限公司 | Assign balanced conditioning Essence living |
| CN108309873B (en) * | 2018-05-07 | 2021-04-13 | 深圳润邦之家生物科技有限公司 | Activation-balanced conditioning essence |
| CN108553400A (en) * | 2018-07-17 | 2018-09-21 | 襄阳佰蒂生物科技股份有限公司 | A kind of water profit whitening blueberry facial mask manufacturing process |
| CN108653099A (en) * | 2018-07-17 | 2018-10-16 | 襄阳佰蒂生物科技股份有限公司 | A kind of blueberry extract cleanser manufacturing process |
| CN112220692A (en) * | 2020-10-30 | 2021-01-15 | 深圳市洛奇机电科技有限公司 | Preparation method of facial cell repair gel |
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