CN106344442A - Anti-alopecia composition and preparation method thereof - Google Patents
Anti-alopecia composition and preparation method thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/42—Amides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q7/00—Preparations for affecting hair growth
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Abstract
The invention discloses an anti-alopecia composition which comprises the following components in percentage by mass: 20.0-40.0% of ethanol, 1.0-10.0% of cacumen platycladi extract, 1.0-10.0% of angelica sinensis extract, 1.0-10.0% of salvia officinalis extract, 1.0-10.0% of kuh-seng extract, 1.0-10.0% of ginseng extract, 1.0-10.0% of dittany root extract, 1.0-2.0% of melaleuca alternifolia leaf oil, 1.0-2.0% of panthenol and the balance of deionized water. The invention also discloses a preparation method of the anti-alopecia composition. The anti-alopecia composition disclosed by the invention is a pure natural preparation which is free of any toxic or side effect and realizes obvious effects on preventing alopecia and promoting hair growth.
Description
Technical field
The present invention relates to cosmetics of everyday use field, more particularly, to a kind of compositionss with Anti-hair loss effect and its preparation side
Method.
Background technology
Alopecia and because alopecia lead to bald, be a kind of commonplace phenomenon now.General alopecia is divided into two kinds of bases
This type: the permanent alopecia causing because hair follicle is impaired and the temporary alopecia causing because the hair follicle short time is impaired, the former
It is common male bald.The cause of disease academic circles at present of alopecia there is no unified suggestion, but mostly thinks relevant with following factors:
Excessive, the spiritual hypertonicity of inherited genetic factorss, androgen secretion, emotional instability, do not have enough sleep, surfeit high lipid food, chronic
Poisoning, trace element deficiency, stress ability are low, autoimmune endocrine functional disorder, menstruation and postpartum recuperating improper, middle aged
Deficiency of the kidney etc..These factors cause the heads such as scalp nutrition supply is unbalance, blood circulation is not smooth, oils and fatss are excessive, hair follicle blocks ecological
Ecological deterioration, thus hindering root of hair to absorb nutrition, affecting hair growth, leading to alopecia.Additionally, hair dyeing, electricity send out, hair-waving, blowing,
Strong sun exposure, radiation, environment and chemistry hair washing water pollution, air humidity be excessive or too small etc. that external factor will also result in
Or accelerate the formation of alopecia.
The means of hair growth are a lot of at present, mainly have surgical operation therapy, chemotherapys, Chinese herbal treatment etc..
Operative treatment, after itself rear pillow part health hair follicle is separated, cultivates by the method for operation, is uniformly planted in alopecia position, is made
It grows new hair again.Chemotherapys are for example administered orally finasteride (finasteride), topical minoxidil
(minoxidil) etc..But these treatment meanss exist or need the shortcomings of special and professional care operation inconvenience or large side effects.
Content of the invention
In order to overcome the deficiencies in the prior art, it is an object of the invention to provide a kind of Anti-hair loss compositionss, it is pure sky
So preparation, without any side effects, to preventing and treating alopecia, promotes natural on-off cycles of hair growth to have obvious effect.
Another object of the present invention is to improving the preparation method of this Anti-hair loss compositions.
The purpose of the present invention employs the following technical solutions realization:
A kind of Anti-hair loss compositionss, the following component including in parts by weight: ethanol 20.0%～40.0%, Cacumen Platycladi
Extract 1.0%～10.0%, Radix Angelicae Sinensis extract 1.0%～10.0%, medicine sage extract 1.0%～10.0%, Radix Sophorae Flavescentiss
Extract 1.0%～10.0%, Radix Ginseng extract 1.0%～10.0%, shaggy-fruited dittany root extract 1.0%～10.0%, alternate leaf
Cortex Melaleucae leucadendrae leaf oil 1.0%～2.0%, pantothenylol 1.0%～2.0%, balance of deionized water.
Preferably, described Anti-hair loss compositionss include following component in parts by weight: ethanol 20.0%～30.0%,
Cacumen Platycladi extract 3.0%～6.0%, Radix Angelicae Sinensis extract 1.0%～5.0%, medicine sage extract 2.0%～7.0%, hardship
Conopsea extraction 4.0%～8.0%, Radix Ginseng extract 3.0%～10.0%, shaggy-fruited dittany root extract 1.0%～6.0%, alternate leaf
Cortex Melaleucae leucadendrae leaf oil 0.2%～0.8%, pantothenylol 0.2%～1.0%, balance of deionized water.
Preferably, described Anti-hair loss compositionss include following component in parts by weight: ethanol 30.0%, Cacumen Platycladi carry
Take thing 6.0%, Radix Angelicae Sinensis extract 3.0%, medicine sage extract 2.0%, Radix Sophorae Flavescentis extract 4.0%, Radix Ginseng extract
4.0%th, shaggy-fruited dittany root extract 3.0%, Melaleuca alternifolia leaf oil 0.7%, pantothenylol 1.0%, balance of deionized water.
The invention also discloses the preparation method of above-mentioned Anti-hair loss compositionss, comprise the steps:
1) add deionized water in container, sequentially add Cacumen Platycladi extract, Radix Angelicae Sinensis extract, the extraction of medicine Salvia japonica Thunb.
Thing, Radix Sophorae Flavescentis extract, Radix Ginseng extract, shaggy-fruited dittany root extract and pantothenylol, stirring, it is heated to 70～80 DEG C and be incubated, to each group
Divide and be completely dissolved；
2), when temperature is down to 45-48 DEG C in container, it is added to container by after ethanol and the mixing of Melaleuca alternifolia leaf oil
In, stir to mix homogeneously, obtain final product after filtration；
Preferably, in step 1) in, the speed of stirring is 150-300 rev/min, is incubated 10～15 minutes.
Preferably, in step 2) in, filtering and discharging when temperature is down to 38 DEG C～40 DEG C in container, obtain described Anti-hair loss group
Compound.
In this programme, described Cacumen Platycladi extract, Radix Angelicae Sinensis extract, medicine sage extract, Radix Sophorae Flavescentis extract, Radix Ginseng carry
Take thing, shaggy-fruited dittany root extract to be to prepare through following steps:
1) add the raw material in supercritical extraction reactor, and the input co toward in supercritical extraction reactor2Fluid, extraction；
2) take out extraction mixture, and be input to separation in supercritical separating still, obtain separator；
3) separator is added to the water, distillation, steam condensation recovery obtains final product.
Preferably, in step 1) in, described raw material is that particle diameter≤80 purpose is unqualified, co2Flow velocity is 10～20kg/h, extraction
Pressure is 25～30mpa, and extraction temperature is 30 DEG C, and extraction time is 3 hours.
Preferably, in step 2) in, separating pressure is 6～8mpa, separation temperature is 35～36 DEG C, and disengaging time is 2～3
Hour.
Preferably, in step 3) in, the ratio of separator and water is 1:10g/l, and distillation time is 3～5 hours.
Compared to existing technology, the beneficial effects of the present invention is:
1. the Anti-hair loss compositionss of the present invention, with the addition of that Cacumen Platycladi extract, Radix Angelicae Sinensis extract etc. are multiple to have anticreep work(
The natural plant extracts of effect, safety non-toxic, have no toxic side effect；Coordinate the ethanol of upper Penetration enhancing effect and Nutrition simultaneously
Pantothenylol, produces the effect of Synergistic between them, promote active component and go deep into cell, activate hair follicle blood microcirculation, support
Anti- scalp is aging, promotes the health of hair follicle, is effectively reduced hair and drops.
2. the plant extract in the present invention is to be extracted using advanced supercritical extraction technique, active component therein
Retain more, impurity is less, effect of product is far superior to traditional steam distillation.
3. the Anti-hair loss compositionss of the present invention, in addition to having obvious anticreep effect, can also increase collagen in scalp
Albumen, the generation of elastin laminin, increase hair follicle to the firm effect of hair it is adaptable to various people.
4. add a certain proportion of ethanol in the Anti-hair loss compositionss of the present invention, not only can prevent product by microorganism
Pollution, also improves the ability that active component infiltrates into hair follicle, improves effect of product.
Specific embodiment
Below, in conjunction with specific embodiment, the present invention is described further:
In implementation below, Melaleuca alternifolia leaf oil is purchased from Australian g.r.davis company, trade name:
australian tea tree oil.
Cacumen Platycladi extract, Radix Angelicae Sinensis extract, medicine sage extract, Radix Sophorae Flavescentis extract, Radix Ginseng extract, dittany root carry
Thing is taken to make through following step:
1) select that high-quality is fresh, complete and pure fresh plant raw material, after being cleaned up with pure water, put into pulverizing
It is unqualified that device is ground into particle diameter≤80 purpose；
2) it is transported to unqualified for raw material in supercritical extraction reactor, into supercritical extraction reactor, then input co2Fluid, co2
Flow velocity be 10～20kg/h, extracting pressure be 25～30mpa, extraction temperature be 30 DEG C under conditions of extract 3 hours；
3) take out extraction mixture from supercritical extraction reactor outlet, then mixture be input in supercritical separating still,
Separating pressure be 6～8mpa, separation temperature be 35～36 DEG C under conditions of separate 2～3 hours, obtain separator；
4) separator obtaining is added to the water for 1:10g/l by solid-liquid ratio, directly fire heating distillation 3～5 hours, steam is cold
Solidifying recovery obtains extract.
Embodiment 1
A kind of Anti-hair loss compositionss, the following component including in parts by weight: ethanol 20.0%, Cacumen Platycladi extract
3.0%th, Radix Angelicae Sinensis extract 5.0%, medicine sage extract 7.0%, Radix Sophorae Flavescentis extract 6.0%, Radix Ginseng extract 10.0%, white
Fresh quench extract 1.0%, Melaleuca alternifolia leaf oil 0.2%, pantothenylol 0.2%, balance of deionized water.
This Anti-hair loss compositions is prepared from through following steps:
1) add deionized water in container, sequentially add Cacumen Platycladi extract, Radix Angelicae Sinensis extract, the extraction of medicine Salvia japonica Thunb.
Thing, Radix Sophorae Flavescentis extract, Radix Ginseng extract, shaggy-fruited dittany root extract and pantothenylol, with 150 revs/min of speed stirring, are heated to 70 DEG C
And it is incubated 10 minutes, it is completely dissolved to each component, then lower the temperature；
2), when in container, temperature is down to 45 DEG C, it is added to after ethanol and the mixing of Melaleuca alternifolia leaf oil in container,
Stir to mix homogeneously, when temperature is down to 38 DEG C, filtering and discharging, obtain final product Anti-hair loss compositionss of the present invention.
Embodiment 2
A kind of Anti-hair loss compositionss, the following component including in parts by weight: ethanol 25.0%, Cacumen Platycladi extract
8.0%th, Radix Angelicae Sinensis extract 5.0%, medicine sage extract 3.0%, Radix Sophorae Flavescentis extract 6.0%, Radix Ginseng extract 3.0%, white
Fresh quench extract 4.0%, Melaleuca alternifolia leaf oil 0.5%, pantothenylol 0.5%, balance of deionized water.
This Anti-hair loss compositions is prepared from through following steps:
1) add deionized water in container, sequentially add Cacumen Platycladi extract, Radix Angelicae Sinensis extract, the extraction of medicine Salvia japonica Thunb.
Thing, Radix Sophorae Flavescentis extract, Radix Ginseng extract, shaggy-fruited dittany root extract and pantothenylol, with 200 revs/min of speed stirring, are heated to 80 DEG C
And it is incubated 15 minutes, it is completely dissolved to each component, then lower the temperature；
2), when in container, temperature is down to 48 DEG C, it is added to after ethanol and the mixing of Melaleuca alternifolia leaf oil in container,
Stir to mix homogeneously, when temperature is down to 40 DEG C, filtering and discharging, obtain final product Anti-hair loss compositionss of the present invention.
Embodiment 3
A kind of Anti-hair loss compositionss, the following component including in parts by weight: ethanol 30.0%, Cacumen Platycladi extract
6.0%th, Radix Angelicae Sinensis extract 3.0%, medicine sage extract 2.0%, Radix Sophorae Flavescentis extract 4.0%, Radix Ginseng extract 4.0%, white
Fresh quench extract 3.0%, Melaleuca alternifolia leaf oil 0.7%, pantothenylol 1.0%, balance of deionized water.
This Anti-hair loss compositions is prepared from through following steps:
1) add deionized water in container, sequentially add Cacumen Platycladi extract, Radix Angelicae Sinensis extract, the extraction of medicine Salvia japonica Thunb.
Thing, Radix Sophorae Flavescentis extract, Radix Ginseng extract, shaggy-fruited dittany root extract and pantothenylol, with 200 revs/min of speed stirring, are heated to 70 DEG C
And it is incubated 12 minutes, it is completely dissolved to each component, then lower the temperature；
2), when in container, temperature is down to 45 DEG C, it is added to after ethanol and the mixing of Melaleuca alternifolia leaf oil in container,
Stir to mix homogeneously, when temperature is down to 38 DEG C, filtering and discharging, obtain final product Anti-hair loss compositionss of the present invention.
Comparative example 1
A kind of Anti-hair loss compositionss, the following component including in parts by weight: ethanol 28.0%, Cacumen Platycladi extract
5.0%th, Radix Angelicae Sinensis extract 6.0%, medicine sage extract 6.0%, Radix Ginseng extract 9.0%, Melaleuca alternifolia leaf oil
0.8%th, pantothenylol 0.8%, balance of deionized water.
This Anti-hair loss compositions is prepared from through following steps:
1) add deionized water in container, sequentially add Cacumen Platycladi extract, Radix Angelicae Sinensis extract, the extraction of medicine Salvia japonica Thunb.
Thing, Radix Ginseng extract and pantothenylol, with 150 revs/min of speed stirring, are heated to 70 DEG C and are incubated 10 minutes, complete to each component
CL, then lowers the temperature；
2), when in container, temperature is down to 45 DEG C, it is added to after ethanol and the mixing of Melaleuca alternifolia leaf oil in container,
Stir to mix homogeneously, when temperature is down to 38 DEG C, filtering and discharging, obtain final product Anti-hair loss compositionss of the present invention.
Experimental example
1. Anti-hair loss test:
Method of testing: select the volunteer 150 with alopecia symptom that the age is 40～50 years old, wherein women 52 people,
Male 98 people, volunteer is randomly divided into 5 groups, and every group of 30 people, respectively using the Anti-hair loss of embodiment-embodiment 3, comparative example 1
Compositionss and commercially available anticreep nourishing liquid, using method is: after hair washing, it is applied at scalp, once a day, 3～5ml every time, holds
Continuous 4 weeks.
Appraisal procedure: by the way of questionnaire survey, understand that experimenter uses rear Anti-hair loss to product using after 4 weeks
The evaluation of improvement situation.Evaluation result is divided into: DeGrain, effect are general, more apparent, clearly.
Test result is as shown in table 1:
Table 1 Anti-hair loss test result
As shown in Table 1:, in the volunteer using the Anti-hair loss compositionss of embodiment 1-3, have 50% respectively,
53.3% and 60% people feels there is obviously anticreep effect, and uses comparative example 1 and the aspiration of commercially available anticreep nourishing liquid
In person, only 20% and 10% volunteer feels there is obviously anticreep effect respectively, the Anti-hair loss of this explanation present invention
Compositionss, anticreep effect is substantially better than comparative example and commercially available anticreep nourishing liquid.
2. safety evaluation
Select experimenter 30 people, wherein male 5 people, female 25 people, 18～40 years old age, sensitivity skin crowd.By experimenter
It is randomly divided into 5 groups, every group of 6 people, respectively every group of experimenter is carried out with speckle examination experiment.
Speckle method for testing: try device from qualified speckle, with closed patch test method, by tested material about 0.02ml～
0.025ml is applied in speckle examination device, and external special adhesive tape is pasted on experimenter's forearm song side, removes tested material, in going after 24 hours
Except tested material speckle tries 30min after device, observe dermoreaction after impression disappears, by " cosmetics health specification " (version in 2007)
Dermoreaction grade scale records its result.
Evaluation of result: record reaction result by table 2 (skin adverse reaction grade scale), acquired results are as shown in table 3.
Table 2 skin adverse reaction grade scale
Table 3 safety evaluation result
The result of table 3 shows: in embodiment 1,2,3, all negative (grading system: 0 of 30 subjects skin
Level).According to " cosmetics health specification " (version in 2007) human body skin class patch test criterion, sample is to human body no skin not
Good reaction.Comparative example 1, commercially available anticreep nourishing liquid occur in that 1 order reaction of 2 and 3 respectively.This shows the Anti-hair loss of the present invention
Compositionss show higher safety, even if using the crowd in sensitive skin, also any abnormal response.
It will be apparent to those skilled in the art that can technical scheme as described above and design, make other various
Corresponding change and deformation, and all these change and deformation all should belong to the protection domain of the claims in the present invention
Within.
Claims (10)
1. a kind of Anti-hair loss compositionss are it is characterised in that include following component in parts by weight: ethanol 20.0%～
40.0%th, Cacumen Platycladi extract 1.0%～10.0%, Radix Angelicae Sinensis extract 1.0%～10.0%, medicine sage extract 1.0%
～10.0%, Radix Sophorae Flavescentis extract 1.0%～10.0%, Radix Ginseng extract 1.0%～10.0%, shaggy-fruited dittany root extract 1.0%～
10.0%th, Melaleuca alternifolia leaf oil 1.0%～2.0%, pantothenylol 1.0%～2.0%, balance of deionized water.
2. Anti-hair loss compositionss as claimed in claim 1 are it is characterised in that include following component in parts by weight: second
Alcohol 20.0%～30.0%, Cacumen Platycladi extract 3.0%～6.0%, Radix Angelicae Sinensis extract 1.0%～5.0%, medicine Salvia japonica Thunb. extract
Thing 2.0%～7.0%, Radix Sophorae Flavescentis extract 4.0%～8.0%, Radix Ginseng extract 3.0%～10.0%, shaggy-fruited dittany root extract
1.0%～6.0%, Melaleuca alternifolia leaf oil 0.2%～0.8%, pantothenylol 0.2%～1.0%, balance of deionized water.
3. Anti-hair loss compositionss as claimed in claim 1 are it is characterised in that include following component in parts by weight: second
Alcohol 30.0%, Cacumen Platycladi extract 6.0%, Radix Angelicae Sinensis extract 3.0%, medicine sage extract 2.0%, Radix Sophorae Flavescentis extract
4.0%th, Radix Ginseng extract 4.0%, shaggy-fruited dittany root extract 3.0%, Melaleuca alternifolia leaf oil 0.7%, pantothenylol 1.0%, surplus
For deionized water.
4. a kind of preparation method of Anti-hair loss compositionss as claimed in claim 1 is it is characterised in that comprise the steps:
1) in container add deionized water, sequentially add Cacumen Platycladi extract, Radix Angelicae Sinensis extract, medicine sage extract,
Radix Sophorae Flavescentis extract, Radix Ginseng extract, shaggy-fruited dittany root extract and pantothenylol, stirring, it is heated to 70～80 DEG C and be incubated, complete to each component
CL；
2), when temperature is down to 45-48 DEG C in container, it is added to after ethanol and the mixing of Melaleuca alternifolia leaf oil in container, stirs
Mix to mix homogeneously, filter after cooling, obtain final product.
5. the preparation method of Anti-hair loss compositionss as claimed in claim 4 is it is characterised in that in step 1) in, the speed of stirring
Spend for 150-300 rev/min, be incubated 10～15 minutes.
6. the preparation method of Anti-hair loss compositionss as claimed in claim 4 is it is characterised in that in step 2) in, container interior temperature
Filtering and discharging when degree is down to 38 DEG C～40 DEG C, obtains described Anti-hair loss compositionss.
7. Anti-hair loss compositionss as claimed in claim 4 preparation method it is characterised in that described Cacumen Platycladi extract, when
Extract, medicine sage extract, Radix Sophorae Flavescentis extract, Radix Ginseng extract, shaggy-fruited dittany root extract is returned to be through following steps preparation
Obtain:
1) add the raw material in supercritical extraction reactor, and the input co toward in supercritical extraction reactor2Fluid, extraction；
2) take out extraction mixture, and be input to separation in supercritical separating still, obtain separator；
3) separator is added to the water, distillation, steam condensation recovery obtains final product.
8. the preparation method of Anti-hair loss compositionss as claimed in claim 7 is it is characterised in that in step 1) in, described raw material
Unqualified, the co for particle diameter≤80 purpose2Flow velocity is 10～20kg/h, and extracting pressure is 25～30mpa, and extraction temperature is 30 DEG C, extraction
The time is taken to be 3 hours.
9. the preparation method of Anti-hair loss compositionss as claimed in claim 7 is it is characterised in that in step 2) in, separating pressure
It is 35～36 DEG C for 6～8mpa, separation temperature, disengaging time is 2～3 hours.
10. the preparation method of Anti-hair loss compositionss as claimed in claim 7 is it is characterised in that in step 3) in, separator with
The ratio of water is 1:10g/l, and distillation time is 3～5 hours.
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| CN109157474A (en) * | 2018-10-15 | 2019-01-08 | 头皮医生健康管理(中国)有限公司 | Oil-control anti-hair loss composition and preparation method thereof and its application |
| CN109419738A (en) * | 2017-09-05 | 2019-03-05 | 香港明及理国际有限公司 | Hair-growing and hair care composition, preparation method and its application |
| CN113730312A (en) * | 2021-10-14 | 2021-12-03 | 柳锋 | Hair and scalp care composition and shampoo containing same |
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| CN105796407A (en) * | 2016-03-16 | 2016-07-27 | 千草万木（北京）科技有限公司 | Plant extract composition, application of plant extract composition in cosmetics, shampoo composition and preparing method of shampoo composition |
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| CN109157474A (en) * | 2018-10-15 | 2019-01-08 | 头皮医生健康管理(中国)有限公司 | Oil-control anti-hair loss composition and preparation method thereof and its application |
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