CN105796407A - Plant extract composition, application of plant extract composition in cosmetics, shampoo composition and preparing method of shampoo composition - Google Patents

Plant extract composition, application of plant extract composition in cosmetics, shampoo composition and preparing method of shampoo composition Download PDF

Info

Publication number
CN105796407A
CN105796407A CN201610151023.1A CN201610151023A CN105796407A CN 105796407 A CN105796407 A CN 105796407A CN 201610151023 A CN201610151023 A CN 201610151023A CN 105796407 A CN105796407 A CN 105796407A
Authority
CN
China
Prior art keywords
weight
extract
content
composition
shampoo composite
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610151023.1A
Other languages
Chinese (zh)
Inventor
李春苗
吕雪梅
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Thousand Mu Mu (beijing) Technology Co Ltd
Original Assignee
Thousand Mu Mu (beijing) Technology Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Thousand Mu Mu (beijing) Technology Co Ltd filed Critical Thousand Mu Mu (beijing) Technology Co Ltd
Priority to CN201610151023.1A priority Critical patent/CN105796407A/en
Publication of CN105796407A publication Critical patent/CN105796407A/en
Pending legal-status Critical Current

Links

Classifications

    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/13Coniferophyta (gymnosperms)
    • A61K36/14Cupressaceae (Cypress family), e.g. juniper or cypress
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/23Apiaceae or Umbelliferae (Carrot family), e.g. dill, chervil, coriander or cumin
    • A61K36/232Angelica
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/25Araliaceae (Ginseng family), e.g. ivy, aralia, schefflera or tetrapanax
    • A61K36/258Panax (ginseng)
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/82Theaceae (Tea family), e.g. camellia
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/88Liliopsida (monocotyledons)
    • A61K36/906Zingiberaceae (Ginger family)
    • A61K36/9068Zingiber, e.g. garden ginger
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/006Antidandruff preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/008Preparations for oily hair
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/02Preparations for cleaning the hair
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q7/00Preparations for affecting hair growth
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/42Colour properties
    • A61K2800/43Pigments; Dyes
    • A61K2800/436Interference pigments, e.g. Iridescent, Pearlescent

Landscapes

  • Health & Medical Sciences (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Biotechnology (AREA)
  • Microbiology (AREA)
  • Epidemiology (AREA)
  • Mycology (AREA)
  • Botany (AREA)
  • Engineering & Computer Science (AREA)
  • Medicinal Chemistry (AREA)
  • Medical Informatics (AREA)
  • Chemical & Material Sciences (AREA)
  • Pharmacology & Pharmacy (AREA)
  • Alternative & Traditional Medicine (AREA)
  • Birds (AREA)
  • Dermatology (AREA)
  • Cosmetics (AREA)

Abstract

The invention relates to the field of cosmetics, in particular to a plant shampoo composition.The plant shampoo composition is prepared from effective ingredients including camellia seed extract, Chinese arborvitae twig extract, ginseng extract, fresh ginger extract and radix angelica sinensis extract.The invention further discloses a preparing method of the plant shampoo composition.The preparing method comprises the step that the effective ingredients and auxiliary materials are mixed.The plant extract composition has the multiple effects of preserving moisture, removing scurf, relieving itching, controlling oil and promoting hair growth; all the components of the plant extract have the synergetic effect, the plant shampoo composition prepared with the plant extract as the effective ingredients can be more easily absorbed by the scalp, can deeply control oil, form a protection film on the surface layer of the scalp and reduce hair loss, has fine foam, and is prepared from natural plant essence which can directly reach the deep part of the scalp more quickly for cleaning and nourishing, grease and dirt are cleared array from the scalp pores thoroughly, and the scalp can be better cared; in addition, the plant shampoo composition is aromatic in smell.

Description

Composition of plant extracts and application and shampoo composite and preparation method thereof in cosmetics
Technical field
The invention belongs to cosmetic field, relate to a kind of composition of plant extracts and the application that this composition of plant extracts is in cosmetics, further relate to a kind of shampoo composite and preparation method thereof.
Background technology
Along with the raising of people's living standard, the prescription of shampoo is also more and more higher.Originally, as long as shampoo meets the requirement of clean of people, but along with growth in the living standard, it is straight smooth that people require to wash rear hair at leisure, removing scurf and relieving itching etc., nowadays, along with the trend of international naturalization of hair shampoo article, nutrient laden and curative effect, the favor of consumer increasingly it is subject to the composite shampoo of have no side effect, have curative effect and the natural Chinese medicinal herb of Nutrition, plant extraction liquid and natural nutriment.
At present, head on the market is washed, is protected product, of a great variety, but for dandruff, hair is fuel-displaced, scalp itch, and in the treatment of the problem such as alopecia, moisturizing, onset is slow, and periodically strong, side effect is big, DeGrain.
Summary of the invention
It is an object of the invention to overcome disadvantages described above, a kind of generation that can effectively reduce scalp oils and fats and the dandruff is provided, improve scalp itch and withered problem and reduce the composition of plant extracts of alopecia, said composition application in cosmetics, and a kind of shampoo composite and preparation method thereof.
In order to realize object above, first aspect, the invention provides a kind of composition of plant extracts, wherein, this composition of plant extracts contains Camellia extract, Cacumen Platycladi extract, Radix Ginseng extract, Rhizoma Zingiberis Recens extract and Radix Angelicae Sinensis extract.
Second aspect, the invention provides the composition of plant extracts as above application in cosmetics.
The third aspect, present invention also offers a kind of shampoo composite, and wherein, this shampoo composite contains composition of plant extracts as above as effective ingredient, and with the gross weight of described shampoo for benchmark, the content of described effective ingredient is 1-50 weight %.
Preferably, possibly together with guar hydroxypropyltrimonium chloride, EDTA-disodium, lauric acid amide of ethanol, AES ammonium salt, cocamido propyl betaine, emulsified silicone oil, Pearl Concentrate, essence, Methylisothiazolinone, DMDM Hydantoin and sodium sarcosinate in described compositions.
Fourth aspect, the preparation method that present invention also offers a kind of shampoo composite, the method includes: effective ingredient as above and adjuvant as above are mixed.
Preferably, the method includes:
(1) guar hydroxypropyltrimonium chloride and the EDTA-disodium as A1 phase is added to water and mix homogeneously, then add as the lauric acid amide of ethanol of A phase, AES ammonium salt, cocamido propyl betaine mix homogeneously, add described composition of plant extracts, obtain mixture 1;
(2) described mixture 1 is heated to 70-90 DEG C, after insulation 10-60min, be cooled to 30-45 DEG C;
(3) mixture after processing to step (2) adds as the emulsified silicone oil of B phase, Pearl Concentrate, essence, Methylisothiazolinone, DMDM Hydantoin and sodium sarcosinate, mix homogeneously.
Composition of plant extracts provided by the invention takes into account moisturizing, anti-dandruff, antipruritic, control oil, the multiple efficacies such as hair growth promoting, and between each component of described plant extract, also there is collaborative effect, the effect that each component is divided is made to perform to maximum, also it is more easy to it for shampoo composite prepared by effective ingredient and is absorbed by scalp, degree of depth control oil, and protecting film can be formed on scalp top layer, reduce alopecia, its foam is fine and smooth, natural plant essence can faster be gone directly scalp depths, cleaning and nourishing, grease soils is thoroughly cleaned out scalp pore, scalp is allowed better to be takeed good care of;Additionally, the shampoo composite fragrant odour of the present invention, consumers in general are enjoyed to be liked.
Other features and advantages of the present invention will be described in detail in detailed description of the invention part subsequently.
Detailed description of the invention
Hereinafter the specific embodiment of the present invention is described in detail.It should be appreciated that detailed description of the invention described herein is merely to illustrate and explains the present invention, it is not limited to the present invention.
First aspect, the invention provides a kind of composition of plant extracts, wherein, this composition of plant extracts contains Camellia extract, Cacumen Platycladi extract (preferred Australia Cacumen Platycladi extract), Radix Ginseng extract, Rhizoma Zingiberis Recens extract and Radix Angelicae Sinensis extract;Preferably it is made up of Camellia extract, Cacumen Platycladi extract, Radix Ginseng extract, Rhizoma Zingiberis Recens extract and Radix Angelicae Sinensis extract.
Flos Camelliae Japonicae (CamelliaJaponica), call also known as Flos Daturae, sea Punica granatum L., the shallow lake overgrown with wild plants spring, mountain Chinese toon, the resistance to winter, Camellia oil manufacturing process such as can be divided into: by Camellia is shelled, dry, pulverize, oil expression, filter just can obtain Camellia extract (also known as, Camellia oil, Oleum Camelliae, camellia seed oil, Camellia oil).Camellia extract is nutritious, reduce blood pressure, blood fat, prevent and treat heart disease and vessel softening etc. effect.It can pass through to prepare voluntarily, it is also possible to commercially available, for instance, purchased from Perfect (China) Co., Ltd..
Described Cacumen Platycladi is dry branch top and the leaf of Cacumen Platycladi (PLatycladusorientalis (L.) Franco), there is cooling blood for hemostasis, preventing phlegm from forming and stopping coughing, effect of growing and blacking hair, cure mainly haematemesis, epistaxis, spitting of blood, have blood in stool, metrostaxis, cough due to lung-heat, heat in blood alopecia, the disease such as early whitening of beard and hair.The preparation method of its extract can be various preparation method well known in the art.Such as specifically may include that filtering after Cacumen Platycladi petroleum ether degreasing, obtain defat Cacumen Platycladi;It is added thereto to alcoholic solution and refluxes, cooled and filtered, extract with isopyknic water-saturated n-butanol after filtrate concentration, take n-butyl alcohol and concentrate mutually, add methanol solution afterwards and dissolve, add acetone and fully vibrate, centrifugation, dry.It can also be commercially available, for instance, purchased from the Cacumen Platycladi extract of Xi'an Jin Lv biotechnology company limited.
Radix Ginseng extract is that Hydrolysis kinetics forms from the root of Araliaceae Radix Ginseng, stem and leaf, and it, rich in 18 kinds of Saponins, is dissolved in the water of 80 DEG C, is easily soluble in ethanol.Be primarily adapted for use in coronary heart diseases and angina pectoris, bradycardia, too fast, ventricular premature contraction, disorder of blood pressure, neurasthenia, climacteric syndrome, overfatigue, after being ill, puerperal, the symptom such as postoperative physical weakness;For a long time clothes can life lengthening, and can physical strength reinforcing, the disease such as the immunologic hypofunction that treatment cancer patient causes because of radiation and chemotherapy;There is cold-and-heat resistent stress.There is the vigor strengthening human body surface cell simultaneously, it is suppressed that the effects such as aging.The preparation method of its extract can be various preparation method well known in the art.Specifically may include that rhizome of Radix Ginseng leaf extract system is with dry Radix Ginseng stem and leaf for raw material, with water for extraction, extracting solution filters, and macroporous resin column is adsorbed, and washes assorted, alcohol-water eluting Radix Ginseng total saponins, reclaims ethanol to without alcohol, drying.It can also be commercially available, for instance, purchased from Chemical Reagent Co., Ltd., Sinopharm Group, article No. is CAS:90045-38-8.
Rhizoma Zingiberis Recens extract is the subterraneous stem of plant Rhizoma Zingiberis Recens (ZingiberofficinaleRosc), or claim rhizomatic extract, have stomach invigorating anti-gastric-ulcer, function of gallbladder promoting, protect the liver, heart tonifying, suppression platelet aggregation, anti-corona, antitumor, CNS inhibition, enhancing immunity, antibacterial, parasite killing, antiinflammatory effect, also there is very strong oxidation resistance.The preparation method of its extract can be various preparation method well known in the art.Specifically can be prepared according to the method disclosed in CN103285348A, it is also possible to by commercially available, for instance, purchased from Xi'an Xu Huang Bioisystech Co., Ltd.
Radix Angelicae Sinensis extract is the extract of the root of Umbelliferae umbelliferae plant Radix Angelicae Sinensis AngelicaSinensis (Oliv.) Diels, has replenishing and activating blood, menstruction regulating and pain relieving, loosening bowel to relieve constipation, blood deficiency and yellow complexion, dizziness cardiopalmus, menoxenia, amenorrhea dysmenorrhea, asthenia cold abdominalgia, dryness of the intestine constipation, rheumatic arthralgia, injury from falling down, the effect such as ulcer sores.The preparation method of its extract can be various preparation method well known in the art.Specifically can be prepared according to the method disclosed in CN104546963A, it is also possible to by commercially available, for instance, purchased from Xi'an Chang Yue plant Chemical Co., Ltd..
Although by each Plant Extracts as above with the use of realizing good synergism, but the inventors found that, with the gross weight of described composition of plant extracts for benchmark, the content of described Camellia extract is 1-95 weight %, the content of described Cacumen Platycladi extract is 1-95 weight %, the content of described Radix Ginseng extract is 1-95 weight %, and the content of described Rhizoma Zingiberis Recens extract is 1-95 weight %, and the content of described Radix Angelicae Sinensis extract is 1-95 weight %;Preferably, with the gross weight of described composition of plant extracts for benchmark, the content of described Camellia extract is 3-70 weight %, the content of described Cacumen Platycladi extract is 10-80 weight %, the content of described Radix Ginseng extract is 5-50 weight %, the content of described Rhizoma Zingiberis Recens extract is 5-50 weight %, and the content of described Radix Angelicae Sinensis extract is 5-60 weight %;Preferred, with the gross weight of described composition of plant extracts for benchmark, the content of described Camellia extract is 15-40 weight %, the content of described Cacumen Platycladi extract is 15-50 weight %, the content of described Radix Ginseng extract is 8-30 weight %, the content of described Rhizoma Zingiberis Recens extract is 10-40 weight %, and the content of described Radix Angelicae Sinensis extract is 15-50 weight %.In so preferred scope, the synergy between each composition of each Plant Extracts can be promoted further.
The inventors found that, although described effective ingredient carries out coordinating according to proportioning as above is namely capable of the purpose of the present invention, but when the weight ratio of Camellia extract, Cacumen Platycladi extract, Radix Ginseng extract, Rhizoma Zingiberis Recens extract and Radix Angelicae Sinensis extract is preferably 1:0.3-8:0.1-5:0.1-4:0.1-8, more preferably 1:(1-5): (0.5-1): (0.5-1): time (0.5-1.5), gained synergy can be promoted further.
Based on the beneficial effect of as above composition of plant extracts, second aspect, present invention also offers the composition of plant extracts as above application in cosmetics.
Wherein, described cosmetics can be the various cosmetics that this area is conventional, for instance, shampoo, shampoo, cream, cosmetic water etc..But it was found by the inventors of the present invention that composition of plant extracts as above is particularly useful for making into shampoo.
Based on this, the third aspect, the invention provides a kind of shampoo composite, wherein, this shampoo composite contains composition of plant extracts as above as effective ingredient, with the gross weight of described shampoo for benchmark, the content of described effective ingredient is 1-30 weight %, it is preferred to 3-15 weight %.
According to the present invention, possibly together with adjuvant in described shampoo composite, described adjuvant can be various adjuvants commonly used in the art, the not special restriction of the present invention.Such as, described adjuvant can be guar hydroxypropyltrimonium chloride, EDTA-disodium, lauric acid amide of ethanol, AES ammonium salt (dodecyl ether sulfate ammonium), cocamido propyl betaine, emulsified silicone oil, Pearl Concentrate, essence, Methylisothiazolinone, DMDM Hydantoin (C7H12N2O4) and sodium sarcosinate in one or more, it is furthermore preferred that described adjuvant is guar hydroxypropyltrimonium chloride, EDTA-disodium, lauric acid amide of ethanol, AES ammonium salt, cocamido propyl betaine, emulsified silicone oil, Pearl Concentrate, essence, Methylisothiazolinone, DMDM Hydantoin and sodium sarcosinate.When the adjuvant of the present invention is preferably as above each composition, it is possible to improve the performance of described shampoo composite further.
The present invention not special restriction of content to described adjuvant, it is possible to for the content of the adjuvant of this area routine, it is preferred that the content of described adjuvant is 10-70 weight %, more preferably 24-52 weight %.
It is further preferred that with the gross weight of described shampoo composite for benchmark, the content of guar hydroxypropyltrimonium chloride is 0.05-0.5 weight %;The content of EDTA-disodium is 0.05-0.5 weight %;The content of lauric acid amide of ethanol is 1-5 weight %;The content of AES ammonium salt is 10-25 weight %;The content of cocamido propyl betaine is 0.5-8 weight %;The content of emulsified silicone oil is 0.5-8 weight %;The content of Pearl Concentrate is 1-10 weight %;The content of essence is 0.05-1 weight %;The content of Methylisothiazolinone is 0.01-0.5 weight %;The content of DMDM Hydantoin is 0.05-0.8 weight %;The content of sodium sarcosinate is 1-8 weight %;Further preferred, the content of guar hydroxypropyltrimonium chloride is 0.1-0.3 weight %;The content of EDTA-disodium is 0.08-0.3 weight %;The content of lauric acid amide of ethanol is 1.5-3.5 weight %;The content of AES ammonium salt is 15-20 weight %;The content of cocamido propyl betaine is 1-5 weight %;The content of emulsified silicone oil is 1-6 weight %;The content of Pearl Concentrate is 4-8 weight %;The content of essence is 0.1-0.5 weight %;The content of Methylisothiazolinone is 0.05-0.3 weight %;The content of DMDM Hydantoin is 0.1-0.5 weight %;The content of sodium sarcosinate is 2-6 weight %.
According to the present invention, described emulsified silicone oil is big particle diameter emulsified silicone oil and the mixture of little particle diameter emulsified silicone oil, and the ratio of the two is preferably 2.5-3.5:1, it is preferred to 3:1.Wherein, " big particle diameter emulsified silicone oil " can be such as DOW CORNING DC7137, DOW CORNING DC1491 etc.;" little particle diameter emulsified silicone oil " can be such as DOW CORNING DC1785.
Wherein, term " Pearl Concentrate " is a kind of daily use chemicals raw material, it is possible to give the fluid product nacreous lustres such as shampoo.English name: PearlConcentrate, main component: glycol stearate, alkyl ether sulfate and alkanolamide etc..
Wherein, described essence can be various essence commonly used in the art, it can optionally add according to the actual requirements, such as, described essence can be one or more in green cucumber essence, rose essence, osmanthus flower fragrance, peach flavor, Fructus Citri Limoniae essence, flavoring pineapple essence and jasmin essence.
Fourth aspect, the preparation method that present invention also offers a kind of shampoo composite, the method includes: effective ingredient as above and adjuvant as above are mixed.
Although will effective ingredient as above, adjuvant and water mix after just can obtain the shampoo composite of the present invention, but it was found by the inventors of the present invention that preparation by carrying out shampoo according to the steps, the stability of described shampoo accesses further raising.Wherein, with the gross weight of described shampoo composite for benchmark, water surplus, namely with the shampoo composite of 100 weight portions for benchmark, it is 100 weight portions that compositions is supplied by water.
Described step includes:
(1) guar hydroxypropyltrimonium chloride and the EDTA-disodium as A1 phase is added to water and mix homogeneously, then add as the lauric acid amide of ethanol of A phase, AES ammonium salt, cocamido propyl betaine mix homogeneously, add described composition of plant extracts, obtain mixture 1.It is preferred that, guar hydroxypropyltrimonium chloride and EDTA-disodium order are added, guar hydroxypropyltrimonium chloride to be added adds EDTA-disodium after being completely dispersed, and for the not special restriction of interpolation of component each in A phase.
(2) its each component is made to dissolve and form homogeneous system preferably in heating under the mixing speed of 20-30rpm in mixture 1, after being warming up to 70-90 DEG C, stop heating, and constant temperature maintains 10-60min, preferably process with the mixing speed cooling of 45-55 DEG C/h afterwards, make the temperature of system be down to 30-45 DEG C.
(3) mixture after processing to step (2) adds as the emulsified silicone oil of B phase, Pearl Concentrate, essence, Methylisothiazolinone, DMDM Hydantoin and sodium sarcosinate, and mix homogeneously.Wherein, in B phase the addition sequence present invention of each component also without special restriction, it is possible to the selection conventional according to this area adds.Preferably, in order to be further ensured that the performance of final gained shampoo, it is preferable that controlling between 5.5-6.5 by the pH value of mixture obtained for this step, under room temperature, viscosity controls in the scope of 8000-10000cps.Wherein, the acid for regulating pH value can for various acid commonly used in the art, for instance, citric acid, the reagent for regulating viscosity can also for various reagent commonly used in the art, for instance, it is possible to for sodium sarcosinate or sodium chloride.
The method of the present invention still further comprises and is filtered by the shampoo as above obtained, and described filtration makes described shampoo preferably by the aperture of 170-230 order, obtains filtrate, obtains the finished product of the vegetalitas shampoo composite of the present invention.
The specific embodiment of the present invention described in detail below.
In following example and comparative example, Camellia extract namely Camellia oil are purchased from Perfect (China) Co., Ltd., Cacumen Platycladi extract is purchased from Xi'an Jin Lv biotechnology company limited, Radix Ginseng extract is purchased from Chemical Reagent Co., Ltd., Sinopharm Group, Rhizoma Zingiberis Recens extract is purchased from Xi'an Xu Huang Bioisystech Co., Ltd, and Radix Angelicae Sinensis extract is purchased from Xi'an Chang Yue plant Chemical Co., Ltd..
Embodiment 1-5 and comparative example 1-2
For shampoo composite provided by the invention and preparation method thereof is described
(1) D07 in table 1 is joined equipped with in the emulsifying pot of water, stirring 10min makes it be completely dispersed, add E01 afterwards to stir to being completely dispersed, it is sequentially added into each composition (C22, C21, C04) in A phase and plant extract subsequently, heat under 25rpm stirs and be incubated 30min after dissolving and being warming up to 85 DEG C, be cooled to 38 DEG C with 50rpm mixing speed afterwards.
(2) in material processed as above, add each component in B phase, add citric acid after mix homogeneously and the pH value of system is regulated to 6.0, be subsequently adding sodium sarcosinate and viscosity under the room temperature of system is regulated to 9000cps.
(3), after using ethanol to be sterilized by discharging opening, 200 order filter-cloth filtering dischargings are used, it is thus achieved that the shampoo composite of the present invention.
Table 1
Embodiment 6
For shampoo composite that the present invention is described and preparation method thereof
Shampoo composite is prepared according to the method for embodiment 1, the difference is that, each component is mixed directly in (1) by step, does not first heat up and lowers the temperature afterwards, directly mix homogeneously under 38 DEG C of conditions.
Embodiment 7
For shampoo composite that the present invention is described and preparation method thereof
Shampoo composite is prepared according to the method for embodiment 1, the difference is that, in step (1), during cooling, mixing speed is also 25 DEG C/h.
Embodiment 8
For shampoo composite that the present invention is described and preparation method thereof
Shampoo composite is prepared according to the method for embodiment 1, the difference is that, finally do not include the step filtered.
Embodiment 9
For shampoo composite that the present invention is described and preparation method thereof
Shampoo composite is prepared according to the method for embodiment 1, the difference is that, in step (2), its pH value is 7.0.
Comparative example 3
For shampoo composite that reference is described and preparation method thereof
Shampoo composite is prepared according to the method for embodiment 1, the difference is that, it is added without any plant extract.
Test case
(1) estimation of stability
Respectively take the shampoo composite of 10g embodiment 1-9 and comparative example 1-3, and be each placed in incubation at room temperature case, in 55 DEG C of couveuses and in the temperature cycling case of-10-45 DEG C, then its stability carried out the observation of 6 months.Observed result is shown below in 2.
Table 2
(2) irritation test, anaphylaxis are tested
8 backs of white mice cut off hair, smear respectively by the shampoo of preparation in embodiment 1-9 and comparative example 1-3 in cutting plucked position, and no painting position does not compare, and result does not all have zest and anaphylaxis.
(3) whole structure assessment
Choosing the volunteer of 120 25-45 year age brackets as object on probation, men and women half and half, is randomly divided into 12 groups, often organizes 10 people, the shampoo composite prepared with embodiment 1-9 and comparative example 1-3 respectively.The shampoo using the present invention for average 3 days is washed hair once, and not in use by any agent of defending the doctrine after washing, the use time is 1 month.Every result of use total score is 5 points: five be divided into best result, represents better, very satisfied;4 are divided into very well;3 are divided into and can accept;Less than 3 points is bad, it is impossible to accept, and the evaluation time is the 3rd day after volunteer's hair washing and before hair washing next time.Being below every average, result is in Table 3:
Table 3
Project Smoothness Moisture retention The dandruff Skin pruritus Scalp oils and fats
Embodiment 1 5 5 5 5 5
Embodiment 2 5 5 5 5 5
Embodiment 3 5 5 5 5 5
Embodiment 4 5 4 4 4 4
Embodiment 5 4 4 4 4 4
Embodiment 6 4 4 4 4 3
Embodiment 7 5 5 5 5 5
Embodiment 8 5 5 5 5 5
Embodiment 9 5 5 5 5 5
Comparative example 1 3 2 3 3 2
Comparative example 2 3 3 2 2 3
Comparative example 3 2 1 1 1 1
Compared with comparative example 1-3 by embodiment above 1-9, respectively can complementing each other of vegetalitas shampoo composite provided by the invention, makes hair keep smooth, reduces the generation of the dandruff and scalp oils and fats, and can effectively control scalp itch problem, make hair retentiveness higher.It addition, by embodiment 1-3 is compared with embodiment 4-6 it can be seen that adopt the as above performance of shampoo composite that currently preferred formula and preferred preparation method obtain to be further improved.
And by table 2-3 it can be seen that adopt the shampoo composite of the present invention that the method for the present invention is prepared from can take into account stability and smooth, moisturizing, anti-dandruff, control oily and antipruritic effect.
The preferred embodiment of the present invention described in detail above; but, the present invention is not limited to the detail in above-mentioned embodiment, in the technology concept of the present invention; technical scheme can being carried out multiple simple variant, these simple variant belong to protection scope of the present invention.
It is further to note that each the concrete technical characteristic described in above-mentioned detailed description of the invention, in reconcilable situation, it is possible to be combined by any suitable mode.In order to avoid unnecessary repetition, various possible compound modes are no longer illustrated by the present invention separately.
Additionally, can also carry out combination in any between the various different embodiment of the present invention, as long as it is without prejudice to the thought of the present invention, it should be considered as content disclosed in this invention equally.

Claims (10)

1. a composition of plant extracts, it is characterised in that this composition of plant extracts contains Camellia extract, Cacumen Platycladi extract, Radix Ginseng extract, Rhizoma Zingiberis Recens extract and Radix Angelicae Sinensis extract.
2. compositions according to claim 1, wherein, with the gross weight of described compositions for benchmark, the content of described Camellia extract is 1-95 weight %, the content of described Cacumen Platycladi extract is 1-95 weight %, the content of described Radix Ginseng extract is 1-95 weight %, and the content of described Rhizoma Zingiberis Recens extract is 1-95 weight %, and the content of described Radix Angelicae Sinensis extract is 1-95 weight %;
Preferably, the weight ratio of Camellia extract, Cacumen Platycladi extract, Radix Ginseng extract, Rhizoma Zingiberis Recens extract and Radix Angelicae Sinensis extract is 1:0.3-8:0.1-5:0.1-4:0.1-8.
3. the application in cosmetics of the composition of plant extracts described in claim 1 or 2.
4. a shampoo composite, it is characterised in that this shampoo composite contains the composition of plant extracts described in claim 1 or 2 as effective ingredient, and with the gross weight of described shampoo composite for benchmark, the content of described effective ingredient is 1-50 weight %.
5. shampoo composite according to claim 4, wherein, described shampoo composite is possibly together with adjuvant, and described adjuvant is selected from one or more in guar hydroxypropyltrimonium chloride, EDTA-disodium, lauric acid amide of ethanol, AES ammonium salt, cocamido propyl betaine, emulsified silicone oil, Pearl Concentrate, essence, Methylisothiazolinone, DMDM Hydantoin and sodium sarcosinate.
6. the shampoo composite according to claim 4 or 5, wherein, with the gross weight of described shampoo composite for benchmark, the content of described adjuvant is 10-70 weight %.
7. the shampoo composite according to claim 5 or 6, wherein, described adjuvant is guar hydroxypropyltrimonium chloride, EDTA-disodium, lauric acid amide of ethanol, AES ammonium salt, cocamido propyl betaine, emulsified silicone oil, Pearl Concentrate, essence, Methylisothiazolinone, DMDM Hydantoin and sodium sarcosinate;
Wherein, with the gross weight of described shampoo composite for benchmark, the content of guar hydroxypropyltrimonium chloride is 0.05-0.5 weight %;The content of EDTA-disodium is 0.05-0.5 weight %;The content of lauric acid amide of ethanol is 1-5 weight %;The content of AES ammonium salt is 10-25 weight %;The content of cocamido propyl betaine is 0.5-8 weight %;The content of emulsified silicone oil is 0.5-8 weight %;The content of Pearl Concentrate is 1-10 weight %;The content of essence is 0.05-1 weight %;The content of Methylisothiazolinone is 0.01-0.5 weight %;The content of DMDM Hydantoin is 0.05-0.8 weight %;The content of sodium sarcosinate is 1-8 weight %.
8. a preparation method for shampoo composite, the method includes: by the composition of plant extracts described in claim 1 or 2 and in claim 5-7 adjuvant described in any one mix.
9. method according to claim 8, wherein, the method includes:
(1) guar hydroxypropyltrimonium chloride and the EDTA-disodium as A1 phase is added to water and mix homogeneously, then add as the lauric acid amide of ethanol of A phase, AES ammonium salt, cocamido propyl betaine mix homogeneously, add described composition of plant extracts, obtain mixture 1;
(2) described mixture 1 is heated to 70-90 DEG C, after insulation 10-60min, be cooled to 30-45 DEG C;
(3) mixture after processing to step (2) adds as the emulsified silicone oil of B phase, Pearl Concentrate, essence, Methylisothiazolinone, DMDM Hydantoin and sodium sarcosinate, mix homogeneously.
10. method according to claim 9, wherein, the method also includes: filtered by step (3) gained mixture.
CN201610151023.1A 2016-03-16 2016-03-16 Plant extract composition, application of plant extract composition in cosmetics, shampoo composition and preparing method of shampoo composition Pending CN105796407A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610151023.1A CN105796407A (en) 2016-03-16 2016-03-16 Plant extract composition, application of plant extract composition in cosmetics, shampoo composition and preparing method of shampoo composition

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610151023.1A CN105796407A (en) 2016-03-16 2016-03-16 Plant extract composition, application of plant extract composition in cosmetics, shampoo composition and preparing method of shampoo composition

Publications (1)

Publication Number Publication Date
CN105796407A true CN105796407A (en) 2016-07-27

Family

ID=56453202

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201610151023.1A Pending CN105796407A (en) 2016-03-16 2016-03-16 Plant extract composition, application of plant extract composition in cosmetics, shampoo composition and preparing method of shampoo composition

Country Status (1)

Country Link
CN (1) CN105796407A (en)

Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106344442A (en) * 2016-11-11 2017-01-25 广州金髓生物科技有限责任公司 Anti-alopecia composition and preparation method thereof
CN106591000A (en) * 2016-11-30 2017-04-26 广缘堂药业有限公司 Preparation method of Chinese herbal shampoo soap for treatment and prevention of alopecia and alopecia regeneration
CN108542820A (en) * 2018-05-28 2018-09-18 广州睿森生物科技有限公司 Skin penetration enhancer, skin matrix and its preparation method and application
CN113081927A (en) * 2021-04-27 2021-07-09 福建俪萃缘生物科技有限公司 Tea polyphenol shampoo and preparation method thereof
CN113633576A (en) * 2021-07-14 2021-11-12 郑小青 Dandruff-removing itching-relieving hair washing composition
CN114469801A (en) * 2022-01-19 2022-05-13 南京上元堂沉香生物科技有限公司 Agilawood shampoo for adjusting scalp microecological balance and preparation method thereof
CN115252519A (en) * 2022-08-03 2022-11-01 浙江熙正霖生物科技有限公司 A hair care essence containing bioactive components and its preparation method
CN115487127A (en) * 2022-07-13 2022-12-20 广东嘉丹婷日用品有限公司 Anti-hair loss oil-control silicone-oil-free shampoo and preparation method thereof

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103356413A (en) * 2012-04-05 2013-10-23 赵艳姝 Pure natural anti-hair loss shampoo
CN104434677A (en) * 2014-12-05 2015-03-25 青岛海芬海洋生物科技有限公司 Plant ingredient added hair tonic
CN104666167A (en) * 2013-11-30 2015-06-03 楚乐然 Botanic anti-hair loss liquid shampoo
CN105193695A (en) * 2014-06-12 2015-12-30 张云凯 Preparation of herbaceous plant hair medicine powder and use method thereof

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103356413A (en) * 2012-04-05 2013-10-23 赵艳姝 Pure natural anti-hair loss shampoo
CN104666167A (en) * 2013-11-30 2015-06-03 楚乐然 Botanic anti-hair loss liquid shampoo
CN105193695A (en) * 2014-06-12 2015-12-30 张云凯 Preparation of herbaceous plant hair medicine powder and use method thereof
CN104434677A (en) * 2014-12-05 2015-03-25 青岛海芬海洋生物科技有限公司 Plant ingredient added hair tonic

Cited By (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106344442A (en) * 2016-11-11 2017-01-25 广州金髓生物科技有限责任公司 Anti-alopecia composition and preparation method thereof
CN106591000A (en) * 2016-11-30 2017-04-26 广缘堂药业有限公司 Preparation method of Chinese herbal shampoo soap for treatment and prevention of alopecia and alopecia regeneration
CN108542820A (en) * 2018-05-28 2018-09-18 广州睿森生物科技有限公司 Skin penetration enhancer, skin matrix and its preparation method and application
CN108542820B (en) * 2018-05-28 2020-11-03 广州睿森生物科技有限公司 Transdermal absorption enhancer, skin-care matrix and preparation method and application thereof
CN113081927A (en) * 2021-04-27 2021-07-09 福建俪萃缘生物科技有限公司 Tea polyphenol shampoo and preparation method thereof
CN113633576A (en) * 2021-07-14 2021-11-12 郑小青 Dandruff-removing itching-relieving hair washing composition
CN114469801A (en) * 2022-01-19 2022-05-13 南京上元堂沉香生物科技有限公司 Agilawood shampoo for adjusting scalp microecological balance and preparation method thereof
CN114469801B (en) * 2022-01-19 2023-06-06 南京上元堂沉香生物科技有限公司 Agilawood shampoo for regulating scalp microecological balance and preparation method thereof
CN115487127A (en) * 2022-07-13 2022-12-20 广东嘉丹婷日用品有限公司 Anti-hair loss oil-control silicone-oil-free shampoo and preparation method thereof
CN115252519A (en) * 2022-08-03 2022-11-01 浙江熙正霖生物科技有限公司 A hair care essence containing bioactive components and its preparation method

Similar Documents

Publication Publication Date Title
CN105796407A (en) Plant extract composition, application of plant extract composition in cosmetics, shampoo composition and preparing method of shampoo composition
KR101128299B1 (en) Natural soap by using of ripen and decocted oriental medicine and manufacturing method thereof
CN109288779A (en) Anticreep Haircare composition and shampoo
CN105505635B (en) A kind of skin cleansing composition and preparation method thereof containing lotus active constituent
KR20160069953A (en) Herbal shampoo composition for promoting hair growth
CN106377477A (en) Fructus gleditsiae abnormalis shampoo and preparation method thereof
CN104666141A (en) Traditional Chinese medicine liquid shampoo with effects of preventing alopecia and removing dandruff
CN107007517A (en) A kind of strong hair scalp wash and maintenance liquid of strong root
KR102296279B1 (en) Shampoo composite and manufacturing method therefore
CN105362162A (en) Bath cream
CN104887616A (en) Shampoo, bath and mask three-in-one cleaning care product and preparation method thereof
KR100691791B1 (en) Shampoo and hair tonic containing composite for preventing alopecia and growing hair
CN105816373A (en) Pore refining cleansing water and preparation method thereof
CN101569599A (en) Aromatic essential anti-alopecia hair-reviving composite and preparation method thereof
KR101033307B1 (en) Shampoo composition
CN111012712A (en) Liquid shampoo containing saponin and preparation method and application thereof
KR101683034B1 (en) Method with a hair loss prevention shampoos and skin softening features using a smooth loofah natural fermentation broth
CN101695470B (en) Composite for cosmetics, cosmetic product containing same and preparation method thereof
CN105796409A (en) Bath salt and preparation method thereof
CN105232402A (en) Composition with skin care effect
CN105168041A (en) Anti-dandruff antipruritic shampoo and preparation method thereof
KR101794437B1 (en) shampoo for anti hair loss and hair-restorer
KR101742819B1 (en) Medicinal herb extract for growing or restoring hair and cosmetic composition comprising the same
KR20130036959A (en) Cosmetics composition for reinforcement of hair-roots and cleanness of scalp and its preparation method
KR101243530B1 (en) Hair Cosmetic Composition for Growth Promotion of Hairs Containing Extracted Concentrated Solution From Pine Leaves

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
RJ01 Rejection of invention patent application after publication

Application publication date: 20160727

RJ01 Rejection of invention patent application after publication