CN109125206A - A kind of extraction preparation method that dendrobium candidum drips liquid Normal juice and the application in cosmetics - Google Patents

A kind of extraction preparation method that dendrobium candidum drips liquid Normal juice and the application in cosmetics Download PDF

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Publication number
CN109125206A
CN109125206A CN201811018814.2A CN201811018814A CN109125206A CN 109125206 A CN109125206 A CN 109125206A CN 201811018814 A CN201811018814 A CN 201811018814A CN 109125206 A CN109125206 A CN 109125206A
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dendrobium candidum
normal juice
drip liquid
liquid normal
stem
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许亚如
何李
应尚芝
周坚宏
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Zhejiang Poly Product Biological Polytron Technologies Inc
Zhi Ran Fang (hangzhou) Health Science & Technology Co Ltd
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Zhejiang Poly Product Biological Polytron Technologies Inc
Zhi Ran Fang (hangzhou) Health Science & Technology Co Ltd
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Priority to CN201811018814.2A priority Critical patent/CN109125206A/en
Publication of CN109125206A publication Critical patent/CN109125206A/en
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9794Liliopsida [monocotyledons]
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    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • A61K8/345Alcohols containing more than one hydroxy group
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/44Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
    • AHUMAN NECESSITIES
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    • A61K8/73Polysaccharides
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    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • A61K8/735Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9706Algae
    • A61K8/9722Chlorophycota or Chlorophyta [green algae], e.g. Chlorella
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9728Fungi, e.g. yeasts
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
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    • A61K8/98Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
    • A61K8/987Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
    • A61K8/988Honey; Royal jelly, Propolis
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
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    • A61K2800/30Characterized by the absence of a particular group of ingredients
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    • A61K2800/31Anhydrous
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    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions
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    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
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Abstract

Have effects that replenishing water and preserving moisture, bullet profit, the extraction preparation method of soft, maintenance dendrobium candidum drip liquid Normal juice and the application in cosmetics the invention discloses a kind of.Fresh dendrobium candidum stem and dendrobium candidum dried flower are scorched by honey infiltration, sealing and fermenting, mudding, drip liquid naturally, has effects that good replenishing water and preserving moisture, bullet profit, soft, maintenance dendrobium candidum drip liquid Normal juice extract to obtain the final product after filtering.The invention has the benefit that the preparation method through the invention, does not add a drop water and any organic solvent, dendrobium candidum drip liquid Normal juice is naturally sealed up for safekeeping.It assists processing by honey, while improving drip liquid recovery rate, synergy extracts dissolubility, permeability, water-retaining property and the hygroscopicity of aglycon.Dendrobium candidum flower/the stem of acquisition drips liquid Normal juice extract, the replenishing water and preserving moisture not only having for cosmetics, bullet profit, soft, maintenance effect, while being also equipped with excellent art value, promotes the intuitional and experiential thinking sense and the artistic treat of consumer of product.

Description

The extraction preparation method of a kind of dendrobium candidum drip liquid Normal juice and in cosmetics Using
Technical field
The present invention relates to cosmetic technical fields, mainly a kind of to have effects that replenishing water and preserving moisture, bullet moisten, are soft, maintenance The extraction preparation method and the application in cosmetics that dendrobium candidum drips liquid Normal juice.
Background technique
Dendrobium candidum has splendid enriching yin effect as a kind of rare Chinese herbal medicine.2005 editions " pharmacopeia " records, have " impairment of yin body fluid deficiency, dry polydipsia, eat less it is dry macerate, abnormal heat, mesh are secretly unknown after being ill " the effect of, Chinese nine big mesonas are described as by " Taoist Scriptures " First of, it is known as the title of " a thousand pieces of gold grass ", international medicinal plant circle is called " medicine circle giant panda ".It is rich in more in dendrobium candidum Sugar, dendrobine, microelement, amino acid etc., these mucilaginous substances equally play the role of moist nutrition to human skin, can be light Change wrinkle and delaying skin aging, keep skin smooth tender, there is beautifying face and moistering lotion cosmetical efficacy well.China's medicine ancient books and records In beauty case about dendrobium nobile, have a large amount of record.
In recent years, pure natural, non-stimulated, nontoxic as people are to good life quality and physically and mentally healthy pursuit of rationality Property plant origin effect type cosmetics become the leading of domestic and international Cosmetic Market.
However, the preparation method of the dendrobium candidum extract of current document and patent report, is opened around dendrobium polysaccharide mostly Exhibition research.Extracting mode mainly has heating extraction, enzymatic isolation method, ultrasound assisted extraction method, microwave―assisted extraction etc., and all adopts Water is used as solvent, organic solvent is extracted to isolate and purify.With pure natural source, avirulent cosmetic material, it is certain poor to remain Away from.
The extraction and preparation technique of traditional Chinese medicine fresh bamboo sap is not yet used for the extraction of dendrobium candidum at present, does not add a drop water With any organic solvent, dendrobium candidum drip liquid Normal juice is directly sealed up for safekeeping.Honey is sweet in flavor, mild-natured, nontoxic, coats honey at scald position Layer protecting film can be formed, injured skin rehabilitation as early as possible is conducive to.Since honey has stronger permeability, water-retaining property and suction It is moist, it is also widely used in cosmetics in recent years.In addition to as food and natural drug, honey or a kind of heavy The Chinese medicine pharmaceutic adjuvant wanted.Some researches show that, the honey after processing can enhance the solubility of aglycon in certain medicinal materials so as to The substances such as the sugar in absorption, honey have reproducibility and anti-corrosive antibacterial effect, can be to avoid the oxidation of effective component in medicinal material The rotten quality for ensuring drug.
In consideration of it, finding a kind of has effects that replenishing water and preserving moisture, bullet profit, soft, maintenance dendrobium candidum is natural, stingless intensifies Cosmetic raw material has the huge market demand and social value.
Summary of the invention
It is an object of the invention to overcome the shortcomings of the prior art, and providing one kind, there is replenishing water and preserving moisture, bullet to moisten, is tender The extraction preparation method of sliding, maintenance effect dendrobium candidum drip liquid Normal juice and the application in cosmetics.
The object of the present invention is achieved by the following technical solutions.The extraction preparation of this dendrobium candidum drip liquid Normal juice Fresh dendrobium candidum stem and dendrobium candidum dried flower are infiltrated by honey, are sealed by fermentation by method, mudding scorches, drips liquid naturally, warp Have effects that good replenishing water and preserving moisture, bullet profit, soft, maintenance dendrobium candidum drip liquid Normal juice extract after filtering to obtain the final product.
Method of the present invention mainly comprises the following specific steps that:
(1), the fresh dendrobium candidum stem before selection is not bloomed rejects leaf, fibrous root, and is cleaned and drained with clean water, with cutting Knife is by the fresh dendrobium candidum cutting shoots of above-mentioned processing, every section of about 0.5cm.Dendrobium candidum dried flower is selected, integral petal, yarn are selected Cloth package.Neatly it is placed in porcelain altar;
(2), honey is taken to infiltrate, infiltration condition is: according to honey and the fresh stem of dendrobium candidum, dried flower mass ratio 1:3-10, note Enter in altar, infiltrates honey sufficiently with dendrobium candidum;
(3), it is sealed by fermentation, the treatment conditions that mudding scorches are: above-mentioned porcelain altar is sealed by fermentation 12-48 hours.Be buckled in On glass dish, altar is wrapped up in wet cloth sealing, soil, is embedded in underground, high temperature scorches;
(4), the treatment conditions for dripping liquid naturally are: burying porcelain altar for above-mentioned, keep high temperature to drip liquid 12-50 hours, drip naturally Liquid out;
(5), above-mentioned drip liquid drips liquid Normal juice extract after filtering merges up to dendrobium candidum.
The present invention is by experimental results demonstrate protected by the moisturizing that above method dendrobium candidum extract obtained has Wet effect, while also having effects that excellent bullet profit, soft, maintenance.
Preferably, it is above-mentioned do not bloom before fresh dendrobium candidum stem, for sufficient triennial Wild Goose and Reed Marsh Mountains Organic certification iron sheet stone The fresh stem item of dry measure used in former times.Dendrobium candidum dried flower is Wild Goose and Reed Marsh Mountains Organic certification dendrobium candidum dried flower.Without pesticide, without chemical fertilizer, it is natural close wild Growth.
Preferably, according in honey and the fresh stem item of dendrobium candidum, dried flower mass ratio 1:5-6 injection altar, sealing hair It ferment 24 hours, scorches 2 hours, high temperature drips liquid 48 hours.
Preferably, integral petal merges up to the drip of dendrobium candidum flower/stem after said extracted liquid is filtered, selects extraction Liquid Normal juice extract.
A kind of to extract preparation method using above-mentioned novel dendrobium candidum drip liquid, resulting dendrobium candidum drip liquid Normal juice mentions Take application of the object in cosmetics.
Preferably, the mass fraction in cosmetics of the present invention containing extract of the present invention is 0.1- 30%.
Preferably, the cosmetics can be with paste, creme, lotion, suspension, perfumed soap, foundation emulsion.
The invention has the benefit that the preparation method through the invention, does not add a drop water and any organic solvent, Naturally seal dendrobium candidum drip liquid Normal juice up for safekeeping.It assists processing by honey, while improving drip liquid recovery rate, synergy extracts glycosides Dissolubility, permeability, water-retaining property and the hygroscopicity of member.Dendrobium candidum flower/the stem of acquisition drips liquid Normal juice extract, will extract for the first time Integral petal is sealed in extracting solution afterwards, replenishing water and preserving moisture, the bullet profit, soft, maintenance effect not only having for cosmetics, simultaneously It is also equipped with excellent art value, promotes the intuitional and experiential thinking sense and the artistic treat of consumer of product.During dendrobium candidum is The traditional rare medicinal herbs of China, does not have any toxic side effect using the cosmetics of extract of the present invention and technology of preparing, provides one Kind drips liquid preparing process for the dendrobium candidum in cosmetics, improves dendrobium candidum flower/stem extraction and applies in cosmetics Artistry and appreciation.
Detailed description of the invention
Fig. 1 is the comparison diagram of skin replenishing water and preserving moisture degree at once.
Specific embodiment
Below in conjunction with attached drawing, the present invention will be described in detail:
Embodiment 1: the preparation of dendrobium candidum flower/stem drip liquid extract
(1), Organic certification dendrobium candidum fresh stem item in triennial Wild Goose and Reed Marsh Mountains before selection is not bloomed, sufficient, rejects leaf, fibrous root, And cleaned and drained with clean water, with cutter by the fresh dendrobium candidum cutting shoots of above-mentioned processing, every section of about 0.5cm.Select Wild Goose and Reed Marsh Mountains Organic certification dendrobium candidum dried flower selects integral petal, gauze package.Neatly it is placed in porcelain altar;
(2), honey is taken to infiltrate, infiltration condition is: according to honey and the fresh stem item of dendrobium candidum, dried flower mass ratio 1:5-6, It injects in altar, infiltrates honey sufficiently with dendrobium candidum;
(3), it is sealed by fermentation, the treatment conditions that mudding scorches are: above-mentioned porcelain altar is sealed by fermentation 24 hours.It is buckled in glass On glass ware, altar is wrapped up in wet cloth sealing, soil, is embedded in underground, high temperature scorches 2 hours;
(4), the treatment conditions for dripping liquid naturally are: burying porcelain altar for above-mentioned, keep high temperature to drip liquid 48 hours, natural leachate Body;
(5), above-mentioned drip liquid, after filtering, merge complete extraction after petal up to dendrobium candidum flower/stem drip liquid extract.
Embodiment 2: the preparation that so square suitable stone flower closes the shining energy essence lotion of rule is planted
It is prepared according to the following recipe with technique
Production technology:
1. A phase constituent is added in agitated kettle, 90 DEG C are then heated with stirring to, B is added in agitated kettle, insulated and stirred 10min is uniform to Material, be cooled to 45 DEG C it is spare.
2. C phase constituent is pre-mixed uniformly, then C, D phase constituent is added, and moderate-speed mixer is adjusted to be uniformly mixed.42 DEG C of inspections Qualification is discharged with two layer of 200 mesh filter-cloth filtering, and after the assay was approved, the E phase that preparatory room temperature is uniformly mixed is added when filling, It packs after the assay was approved, finished product warehousing after passing.
A phase: (part) number raw material 1 in formula
B phase: in formula: 2 (parts), 4,5,14, No. 17 raw materials
C phase: (residue), 13, No. 20 raw materials 1 in formula
D phase: in formula: 1 (part), 3,6-9,11,12,15,16,18, No. 19 raw material
E phase: 2 (residues), No. 10 raw materials
Embodiment 3: it plants the suitable stone flower in so side and closes the preparation that rule grows net essence dew
It is prepared according to the following recipe with technique
Production technology:
1. A phase constituent is added in agitated kettle, then it is heated with stirring to 90 ± 2 DEG C of heat preservations and is uniformly dissolved for 10 minutes, it is spare.
2. B phase constituent is added, bubble is controlled, kick-down is uniformly mixed.
3. C phase is pre-mixed uniformly, C, D phase constituent are added, moderate-speed mixer is adjusted to be uniformly mixed.42 ± 1 DEG C of inspections are closed After lattice, is discharged with one layer of 160~200 mesh filter-cloth filtering, will finally be pre-mixed uniform E phase, be added and mix.After the assay was approved Filling, packaging, product inspection warehousing after passing.
A phase: (part), 2,4 (parts), 18, No. 22 raw materials 1 in formula
B phase: (part), No. 19 raw materials 1 in formula
C phase: (residue), 8,9 (parts), 14,16,21,23,24-28 raw material 1 in formula
D phase: in formula: 3,4 (residues), 5,6,7,10-13,15, No. 20 raw materials
E phase: (residue), No. 17 raw materials 9 in formula
Experimental data: Fig. 1 is the comparison diagram of skin replenishing water and preserving moisture degree at once, selects to plant the suitable stone flower in so side and close rule and grows net essence Replenishing water and preserving moisture measure of merit is intended for single use for 20 24-45 years old subjects in Hua Lu.It smears once, skin water humidity mentions at once Rising mean value is 19.2%;100% trier thinks that the water humidity of skin can be promoted at once, and keeps skin feel more smooth, soft It is tender.
It all should belong to this it is understood that equivalent substitutions or changes are made to the technical scheme and inventive concept of the present invention The protection scope of invention the attached claims.

Claims (6)

1. a kind of extraction preparation method of dendrobium candidum drip liquid Normal juice, it is characterised in that: by fresh dendrobium candidum stem and iron sheet stone Dry measure used in former times dried flower is infiltrated by honey, is sealed by fermentation, mudding scorches, drips liquid naturally, after filtering up to good replenishing water and preserving moisture, bullet Profit, soft, maintenance effect dendrobium candidum drip liquid Normal juice extract.
2. the extraction preparation method of dendrobium candidum drip liquid Normal juice according to claim 1, it is characterised in that: this method is main It comprises the following specific steps that:
(1), the fresh dendrobium candidum stem before selection is not bloomed rejects leaf, fibrous root, and is cleaned and drained with clean water, will with cutter The fresh dendrobium candidum cutting shoots of above-mentioned processing select dendrobium candidum dried flower, select integral petal, and gauze package is neat to put In porcelain altar;
(2), it takes honey to infiltrate, infiltration condition is: according to honey and the fresh stem of dendrobium candidum, dried flower mass ratio 1:3-10, injecting altar In, infiltrate honey sufficiently with dendrobium candidum;
(3), it is sealed by fermentation, the treatment conditions that mudding scorches are: above-mentioned porcelain altar being sealed by fermentation 12-48 hours, is buckled in glass On ware, altar is wrapped up in wet cloth sealing, soil, is embedded in underground, high temperature scorches;
(4), the treatment conditions for dripping liquid naturally are: burying porcelain altar for above-mentioned, keep high temperature to drip liquid 12-50 hours, natural leachate Body;
(5), above-mentioned drip liquid drips liquid Normal juice extract after filtering merges up to dendrobium candidum.
3. the extraction preparation method of dendrobium candidum according to claim 2 drip liquid Normal juice, it is characterised in that: it is selected not Fresh dendrobium candidum stem before blooming, for the sufficient fresh stem item of triennial Wild Goose and Reed Marsh Mountains Organic certification dendrobium candidum, dendrobium candidum dried flower, For Wild Goose and Reed Marsh Mountains Organic certification dendrobium candidum dried flower.
4. the extraction preparation method of dendrobium candidum according to claim 2 drip liquid Normal juice, it is characterised in that: according to honey with In the fresh stem item of dendrobium candidum, dried flower mass ratio 1:5-6 injection altar, it is sealed by fermentation 24 hours, scorches 2 hours, high temperature drips liquid 48 Hour.
5. the extraction preparation method of the dendrobium candidum drip liquid Normal juice according to claim 2, it is characterised in that: gained Integral petal, which merges, after extracting solution is filtered, selects extraction drips liquid Normal juice extract up to dendrobium candidum flower/stem.
6. a kind of application of dendrobium candidum drip liquid Normal juice extract in cosmetics.
CN201811018814.2A 2018-09-03 2018-09-03 A kind of extraction preparation method that dendrobium candidum drips liquid Normal juice and the application in cosmetics Withdrawn CN109125206A (en)

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CN113425663A (en) * 2021-08-18 2021-09-24 皖西学院 Preparation method of dendrobium flower soybean skin-beautifying mask

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Application publication date: 20190104