KR20120001111A - Perfume composition containing forest and warm temperate zone species of trees and manufacturing method the same - Google Patents

Abstract

PURPOSE: A perfume composition containing natural perfume from forest trees is provided to ensure excellent scent and to ensure eco-friendly natural perfume. CONSTITUTION: A method for manufacturing perfume composition containing natural perfume from forest trees comprises: a step of isolating leaves and stems of Cinnamomum iaponicum or Chamaecyparis obtuse by steam distillation to prepare essential oil; and a step of preparing natural perfume containing one or more selected among the essential oil, Dendropanax morbifera liquid, and absolute of Robinia pseudoacacia or Chamaecyparis obtuse(S100). The perfume composition contains 0.03-0.13 wt% of the natural perfume.

Description

Perfume composition containing forest and warm temperate zone species of trees and manufacturing method the same

The present invention is the absolute oil (Essential oil) extracted from the leaves and stems of the selected tree of the wild tree, edible tree, cypress, vapor, and the sap of the Hwangchil trees, and the flowers of the brier and locust tree by the solvent extraction method (Absolute ) Or the natural fragrance consisting of two or more of the natural fragrance consisting of Absolute extracted by steam distillation and solvent extraction method of the leaves and stems of camphor tree added to the total weight ratio of 0.03 ~ 0.13% by weight, It is a natural fragrance that adds the fragrance of brier and locust tree to the fragrance of camphor tree, sproutwood and cypress and adds the scent of hwangchil tree. It is a tropical and forest species that provides natural fragrance with excellent fragrance and harmless to human body. It relates to a perfume manufacturing method and a perfume composition containing a natural flavor of.

In general, with the development of the economy, as the standard of living improves, the desire to enhance the appearance beautifully increases, and various cosmetics and perfumes have been proposed and marketed as materials that can beautifully shape the appearance.

On the other hand, perfume is a kind of cosmetics, which is made by mixing fragrance substances in proper ratios and dissolving them in alcohol, etc., spraying them on parts of the body and clothes, and mixing them with body temperature or body odor emitted from the skin to give off fragrance. will be.

The use of perfume in the body or clothing like this reduces or blocks bad smells from the body, and makes the other person feel good by the good fragrances emitted from the perfume.

It was established as a kind of arms.

On the other hand, as a main component of the perfume, the fragrance material added and mixed as a natural perfume and chemical synthetic fragrance, the perfume is added to the perfume produced in large quantities, mostly chemical synthetic fragrance is used.

However, perfumes prepared by adding such artificially synthesized chemical synthetic fragrances do not have a natural aroma, easily get tired of using it for a long time, and contain other chemical ingredients to keep the fragrance for a long time. There is a problem of causing an Alergy) reaction, and since the pharmacological function useful to the human body cannot be expected, the interest in perfumes using natural plant essential oils extracted from plants has recently increased.

In addition, recently, consumers have a tendency to expect functional cosmetics that can exhibit a certain care effect on the skin and the human body or eliminate defects when using cosmetics, and thus have a good pharmacological effect when using the cosmetics. Research is actively being conducted on plants containing components that emit scents.

However, as the climate change caused by global warming is expected to expand the tropics in the future, the introduction of ovarian resources, functional lifesaving and development research on them are needed. There was a problem that the fragrance composition having dual directionality using flowers of camphor tree, wild tree, yellow chile and forest tree, cypress, brier, and locust tree, which is a tropical resource, could not be provided.

In order to solve the above problems, the present invention is added to the fragrance composition by adding the fragrance of the brier and locust tree to the scent of cool bark, camphor tree, edible tree, cypress, and added the scent of hwangchil wood to the perfume composition To provide a fragrance composition and its fragrance composition containing natural fragrances of new tropical species and forest species which are excellent in fragrance of natural fragrance extracted from unique tropical species and forest species and provide natural natural fragrance that is harmless to human body. The purpose is.

In order to achieve the above object, the manufacturing method of the present invention, the essential oil (Essential oil) or Hwangchil wood extracted from the leaves and stems of the trees selected from wild tree, edible tree, cypress, steam, stab, and locust tree The step of preparing a natural perfume consisting of two or more of natural flavors consisting of absolute (Absolute) produced by the solvent extraction method or the leaves and stems of camphor tree extracted by steam distillation method and solvent extraction method Wow; The natural fragrance is characterized in that it consists of a step of adding to the whole fragrance composition to be mixed.

In addition, the natural flavor is characterized in that 0.03% by weight to 0.13% by weight relative to the total weight ratio of the perfume composition.

In addition, the steam distillation method of the bark, hawthorn, cypress is characterized in that the stem and leaves of the bark, hawthorn, cypress are cut and heated for 1 hour to extract the rectification.

In addition, the stems and leaves of the bark, hawthorn, cypress are characterized in that the cut to 2cm ~ 3cm.

In addition, the solvent extraction method of the brier and locust tree flowers is filtered by immersing the brier and locust tree flowers at 1 to 1.5 l to 3 l of hexane (n-Hexan 95%) for 12 hours to 24 hours at room temperature. Hexane and fragrance and water in the water is removed using anhydrous sodium sulfate (Na ₂ S0 ₄ ), and the concrete (Concrete) oil hexane is removed with a rotary vacuum condenser dissolved in alcohol and filtered with a filter to extract the absolute It features.

In addition, in the conditions of the rotary vacuum concentrator, the heating is maintained at 20 ℃ ~ 22 ℃ to minimize the loss of the volatile odor component, so as not to exceed 23 ℃ and to maintain the rotational speed of 5 ~ 6, the concrete oil It is characterized in that the alcohol is dissolved at a ratio of 1:10 to 50 and filtered with the filter of 0.45 µm to remove insoluble wax.

In addition, the solvent solution extraction method of the yellow lacquer tree is shaken by mixing 10g of the lactose solution with 20ml of a mixture of hexane: alcohol 5: 5 and then remove the moisture using anhydrous sodium sulfate (Na ₂ S0 ₄ ), rotary vacuum concentrator Separating the extract mixed with the perfume and alcohol from the hexane, characterized in that to remove the insoluble wax by filtering the separated extract with a filter of 0.45㎛.

In addition, the leaves and stems of the camphor tree is the steam distillation method and the solvent extraction method of cutting the stems and leaves of the camphor tree to a size of 2cm ~ 3cm after heating for 1 hour, the material attached to the crystals around the peripheral candle such as a cooler Dissolve in hexane solvent and collect it in one place to remove unnecessary moisture using anhydrous sodium sulfate (Na ₂ S0 ₄ ), and the fragrance dissolved in the solvent was dissolved in alcohol by using a rotary vacuum condenser. It is characterized in that the extraction of the absolute.

Provided is a perfume composition prepared by the perfume manufacturing method.

In addition, the perfume composition is 26.30% by weight of ISO E SUPER, 25.46% by weight of Musk T, 2.80% by weight of GERANOL, and HYDROXY CETRONELLAL 2.70 Wt%, 2.50 wt% of CITRONELLOL, 4.70 wt% of PHENYL ETHYL ALCOHOL, 12.10 wt% of Linalool, 18.40 wt% of D-LIMONENE, It is characterized by consisting of 0.07% by weight of cypress fragrance, 0.07% by weight of apricot blossom, and 4.90% by weight.

In addition, the perfume composition is 39.50% by weight of ISO E SUPER, 25.60% by weight of Musk T, and 3.10% by weight of GERANOL 2.10% by weight of hydroxy cetronellal (HYDROXY CETRONELLAL) 2.50% by weight of CITRONELLOL, 4.70% by weight of phenyl ethyl alcohol (PHENYL ETHYL ALCOHOL), 6.70% by weight of linalool, 10.00% by weight of di-limonene, It is characterized by consisting of 0.10% by weight of wood, 0.10% by weight of brier, 0.10% by weight of redwood flower, and 4.90% by weight.

In addition, the perfume composition is 19.60% by weight of linalool, 24.20% by weight of D-LIMONENE, 25.10% by weight of DIHYDROMYRCENOL, and 17.30% by LINALYL ACETATE. %, 6.70% by weight of musk T, 1.90% by weight of LYSMERAL, 0.13% by weight of wild wood, 0.10% by weight of camphor, 0.04% by weight of brier, 0.03% of redwood flower, 0.03% And 4.90% by weight and the other.

In addition, the fragrance composition is 12.4% by weight of alpha-synthetic aldehyde (a-HEXYL CINNAMIC ALDEHYDE), 32.3% by weight of phenyl ethyl alcohol (PHENYL ETHYL ALCOHOL), 13.6% by weight of di-limonene, and LINALOOL, 9.4% by weight, Musk T, 23.7% by weight, Geranol 3.4% by weight, raw barberry, 0.1% by weight, yellow lacquer, 0.1% by weight, Acacia flower flavor 0.1 And by weight 4.9% by weight.

In addition, the perfume composition is 12.0% by weight of a-HEXYL CINNAMIC ALDEHYDE, 29.9% by weight of phenyl ethyl alcohol (PHENYL ETHYL ALCOHOL), 14.6% by weight of di-limonene, and 10.8% by weight of LINALOOL, 23.5% by weight of Musk T, 4.1% by weight of GERANOL, 0.1% by weight of dalberry, 0.1% by weight of yellow lacquer, Acacia flower flavor 0.1 And by weight 4.9% by weight.

In addition, the color of the perfume composition is characterized in that the yellow (Slightly yellow) (Yellow).

The present invention adds the fragrance of the brier and locust tree to the scent of cool wild tree, camphor tree, edible tree, cypress, and adds the scent of the Hwangchil tree to the fragrance composition, and extracted from unique tropical and forest species It is effective in providing natural fragrance which is excellent in fragrance of natural fragrance and harmless to human body and eco-friendly.

In addition, it has the effect of promoting the local people's profits due to the development of specialties in the region where a lot of tropical species and forest species are distributed.

1 is a schematic view according to the present invention.

Hereinafter, the present invention will be described with reference to a preferred embodiment as follows.

It is composed of camphor tree, wild tree, and yellow lacquer tree which are tropical species used in the present invention.

The camphor tree (Chamaecyparis obtusa) is a camphor family distributed in Japan, Taiwan, China, and Vietnam, and grows native to Jeju Island, Ulleungdo, and the South Sea in Korea.

It grows up to 20m in diameter and 2m in diameter, and grows well in both shades and suns.

It grows in moist, deep soil, high fertile red soil, and mid-air humidity. It is weak to pollution and cold resistance, and grows well in warm and humid climate.

It can be used as roadside trees, green trees, garden trees, and environmentally purified water. Wood is dense and coarse.

The raw leaves are boiled with tea and used to float the leaves in the bath water. Medicinal wood, roots, bark, leaves, extracted crystals and fruits are used.

Cinnamomum iaponicum is a camphor tree distributed in China, Taiwan, and Japan. It grows up to 1,100m above sea level in Jeju Island in Korea and grows in coastal and foothills in warm southern island.

It grows to around 15m and reaches 30 ~ 40cm in diameter. When it is young, it can be exposed to strong light when it is negative or tree, and it grows well in the fertile soil with moisture.

Cold and dry resistance is weak, but flame resistance and pollution resistance is strong and growth is relatively fast. The leaves are rich in scent and are used as a substitute for tea or bathing, and the fruit is extracted with confectionery oil.

Wood is a yellowish white or pale yellow brown industrial material that is indistinguishable from sapwood and heartwood, and its structure is dense and is used as building materials or furniture materials. Bark is called cinnamon and fruit is medicinal.

The Hwangchil tree (Dendropanax morbifera) is a native species of the family Elmaceae.

It is distributed on the southern coast and islands and grows up to 15m in height.

Flowers bloom in light yellow-green in June, cultivate and hang on inflorescences. The stalk is 3 ~ 5cm long and the stalk is 5 ~ 10mm long.

When the bark is cut, yellow liquid comes out. This is called Hwangchil, and it has been used as a paint and has been used as a benzoate since ancient times.

In addition, the forest species used in the present invention is composed of cypress, brier, locust tree.

Chamaecyparis obtusa (Chamaecyparis obtusa) is a cypress plant and its origin is Japan. It grows about 40m in height and 2m in diameter, and its branches spread horizontally to form conical water pipes.

Fruits are coniferous, round, 10 ~ 12m in diameter, reddish brown, and composed of about 8 pieces.

Each seed contains two seeds.

Seeds are about 3mm long, have two cysts, have narrow wings, and are made in Japan.

The rose flower (Rose multiflora) is a rose family, distributed in Korea or Japan, and grows about 1 ~ 2m in height.

It grows in foothills or sunny streams and valleys.

The flowers are white or light red in May, the fruits are round, 6-9mm in diameter, ripen in red in September, and contain a lot of aquatic plants of 2-3mm in length.

In oriental medicine, fruit is used as a medicine called Youngsil, which is effective for insomnia, tenderness, decreased sexual function, and edema and is used as a diuretic.

Robinia pseudoacacia is a legume that literally translates the name 'false acacia', which is often used in English-speaking countries.

In Korea, acacia is commonly called acacia, which is a genus of plants belonging to the genus Acacia of Mimosiaideae.

When the tree is grown, it is about 15-25m high and 80cm in diameter.

The flower is white with strong fragrance and is used as a wheat plant and is edible.

Its roots have nitrogen-fixed bacteria that can grow on harsh lands. They grow quickly, hard, and are resistant to corrosion and are used to make fences and boats.

In addition, the combustion time is long and the smoke is low, so it is not affected by fire.

Therefore, extract the above-mentioned tropical species and forest species with natural fragrance to constitute a perfume production method and perfume composition prepared by the method.

Perfume production method containing a natural flavor of tropical and forest species according to the present invention is as follows.

[Example]

[Steps to prepare with natural fragrances] (S100)

Essential oil of any one selected from wild tree, edible tree, and cypress, Absolute selected from the flowers of the yellow and yellow flowers and brier, and Absolute of the camphor tree (Absolute) It consists of.

Absolute or Absolute produced by the extraction of essential oils (Essential oil) or Hwangchil trees, and the flowers of the brier and locust tree by the solvent extraction method The leaves and stems of camphor tree are prepared with a natural fragrance consisting of two or more of natural fragrances made of Absolute extracted by steam distillation and solvent extraction.

Steam distillation method of the bark, hawthorn, cypress is cut the stem and leaves of the bark, hawthorn, cypress to 2cm ~ 3cm and heated for 1 hour to extract the rectification.

In addition, the solvent extraction method of the flower of the brier and the hawthorn tree is filtered by immersing the flower of the brier and the hawthorn in 1.5l to 3l of hexane (n-Hexan 95%) for 12 hours to 24 hours at room temperature and then filtering and extracting The hexane and the fragrance and the moisture in the water is removed using anhydrous sodium sulfate (Na ₂ S0 ₄ ), and the concrete (Concrete) oil hexane is removed with a rotary vacuum condenser dissolved in alcohol and filtered through a filter to extract the absolute .

In addition, in the conditions of the rotary vacuum concentrator, the heating is maintained at 20 ℃ ~ 22 ℃ to minimize the loss of the volatile odor component so as not to exceed 23 ℃ and to maintain the rotation speed of 5-6.

Thus, the concrete oil is dissolved in the ratio of 1:10 to 50 alcohol and filtered by the filter of 0.45㎛ to remove insoluble wax.

In addition, the solvent solution extraction method of the yellow lacquer tree is shaken by mixing 10g of the lactose solution with 20ml of a mixture of hexane: alcohol 5: 5 and then remove the moisture using anhydrous sodium sulfate (Na ₂ S0 ₄ ), rotary vacuum concentrator The extract mixed with flavor and alcohol is separated from the hexane, and the separated extract is filtered with the filter of 0.45 μm to remove insoluble wax.

In addition, the leaves and stems of the camphor tree is the steam distillation method and the solvent extraction method of cutting the stems and leaves of the camphor tree to a size of 2cm ~ 3cm after heating for 1 hour, the material attached to the crystals around the peripheral candle such as a cooler Dissolve in hexane solvent and collect in one place to remove unnecessary water using anhydrous sodium sulfate (Na ₂ SO ₄ ).

In addition, the fragrance dissolved in the solvent is dissolved in ethanol, a concrete (Concrete) oil from which hexane is removed by a rotary vacuum concentrator, and filtered with a filter to extract the absolute.

The steam distillation method of the bark, hawthorn, cypress, and the camphor vapor distillation method puts the sample on the body plate and heats water at the bottom so that hot steam is injected into the sample to destroy cells including essential oils in the plant. The essential oil was distilled together. When the fat-soluble essential oil and water vapor were separated by a cooler, only the essential oil was extracted.

As such, the equipment used for the steam distillation method was using EssenLab-plus of Hanil Lab Tech Co., Ltd. Reactor is designed to protect against impact or heat medium using stainless steel, and the distillation part and extraction part are Boroliscicate Glass, which is used for accurate Digitai Micro Process Control. Equipment with the function of was used.

In addition, the solvent extraction method is mainly used when it is difficult to extract the steam distillation in a very small amount of the fragrance.

Compared to the fragrance extracted by the distillation method, the fragrance is good, but there is a disadvantage that wax components such as volatile components can be extracted.

There are various kinds of solvents such as petroleum ether, hexane, methanol, ethanol, etc. Recently, carbon dioxide is used, and copper and vegetable oils are also used.

The operation is performed at room temperature by putting fresh ingredients into an extraction apparatus and adding a solvent to extract the fragrance.

It can be extracted without any big change of oil component by the soft extraction method. The extract is transferred to an evaporator such as a rotary vacuum concentrator and concentrated at low temperature and decompressed to completely remove the solvent, which is called concrete.

This concrete contains some wax, protein, pigment, etc. It was shaken with high concentration alcohol, filtered and cooled again to remove insoluble wax to extract Absolute.

Experimental Example 1

The natural fragrance extraction rate according to the extraction method for the camphor tree, the young tree, the cherry tree, the yellow lacquer tree is shown in Table 1 below.

    division   Extraction site           Perfume extraction rate by weight extraction method (wt%)  Water vapor distillation   Solvent extraction Water vapor distillation, solvent  camphor tree  Leaf, stem      -    0.73     0.80  Birch Tree  Leaf, stem    0.06    0.17     0.13  Brushwood  Leaf, stem    0.03    0.13     0.06  Hwangchil wood  Yellow      -    5.00      -

As shown in Table 1, when extracting the natural flavor by extracting the solvent from the leaves and stems of camphor tree 0.73% by weight, water vapor distillation, solvent extraction mixing method showed 0.80% by weight mixed steam distillation method and solvent extraction In one case, the extraction rate is higher.

When the fragrance was extracted from the leaves and stems of the rhododendron, the vapor extraction was 0.06% by weight, the solvent extraction was 0.17% by weight, and the mixture of water vapor distillation and solvent extraction was 0.13%.

In the leaves and stems, the extracts showed 0.03% by weight of steam distillation, 0.13% by weight of solvent extraction, and 0.06% by weight of steam distillation and solvent extraction.

And Hwangchil wood extracted 5% by weight of the fragrance from the solvent using the solvent extraction.

The leaves and stems of dalberry, oleifera and cypress, which are relatively simple and economical methods of steam distillation as described above, extract essential oil by steam distillation and are difficult to extract steam distillation. The solution of the seven-liquid, brier, and locust tree is solvent extraction, and camphor is extracting fragrance in the form of Absolute form using a steam distillation ㆍ solvent extraction mixture.

Experimental Example 2

Experiments of the fragrance component analysis of natural flavors are shown in Tables 2-8.

The chromatograms of the volatile flavor components of Absolute extracted by solvents from the leaves and stems of camphor tree with water vapor are shown in Table 2.

As a result, various fragrance components were detected, and the main fragrance components were camphor, α-pinene, camphere, β-selinene, and α-copaene.

As shown in Table 3, chromatograms of volatile aroma components of essential oils extracted by steam distillation of the leaves and stems of the shoots are shown.

The major fragrance components were eucalyptol, β-myrcene, α-copaene and α-pinene.

As shown in Table 4, chromatograms of the volatile aromas of the absolute obtained by extracting the lacquer of Hilchi chinensis with the solvent were shown.

The main volatile components were germacrene-D and trans-caryophyllen.

As shown in Table 5, the chromatogram of one of the volatile components of the absolute oil extracted from the steam and distillation of the leaves and stems of the Japanese Cypress, as well as the Absolute, obtained by extracting the flowers of the Black Oak and the Black Oak as a solvent.

The chromatograms were as in Table 2, Table 3, Table 4.

Table 6 shows the GC / MS chromatograms of the leaves and stems of the Japanese Cypress by steam distillation.

       Table 7 shows GC / MS chromatograms of brier flowers by solvent extraction.

Table 8 shows the GC / MS chromatograms of the Prunus cava by solvent extraction.

[Natural fragrance is added to the whole fragrance composition and mixed] [S200]

 The natural fragrance is composed of a step of adding to the whole fragrance composition and mixing.

In addition, the natural flavor is added 0.03 ~ 0.13% by weight relative to the total weight ratio of the perfume composition.

As described above, various perfumes can be prepared according to the concentration of perfume by using alcohol in the perfume composition to which the perfume composition is added.

Perfume composition containing natural fragrances of tropical and forest species according to the present invention is the essential oil (Essential oil) or Hwangchilchi extracted from the steam and distillation of the leaves and stems of the tree selected from wild tree, oleander, cypress, Natural fragrance consisting of two or more of natural fragrances made of absolute produced by solvent extraction method or one of the flowers of brier or redwood tree by solvent extraction method It is prepared by adding 0.03 to 0.13% by weight relative to the total weight ratio of the perfume composition.

The perfume composition includes a preservative and a stabilizer.

The preservative consists of suitable ones such as phenoxyethanol, formaldehyde solution, parabens, pendandiol, sorbic acid and kosmetikverordnug (similar to 'cosmetic instructions') and the like.

The stabilizer is made of olive liquid (Olive Riquid), HCO-60 and the like suitable.

Provided is a perfume composition prepared by the perfume manufacturing method.

Fragrance Composition Example 1

 The perfume composition is 26.30% by weight of ISO E SUPER, 25.46% by weight of Musk T, 2.80% by weight of Geranol, and HYDROXY CETRONELLAL 2.70 Wt%, 2.50 wt% of CITRONELLOL, 4.70 wt% of PHENYL ETHYL ALCOHOL, 12.10 wt% of Linalool, 18.40 wt% of D-LIMONENE, It consists of 0.07% by weight of cypress, 0.07% by weight of flowering acifer, and 4.90% by weight of others.

Therefore, the fragrance series of the perfume composition of Example 1 may be referred to as a fresh-green-floral-musk type, and a natural fragrance of a cypress acacia aroma is used.

Fragrance Composition Example 2

The perfume composition is 39.50% by weight of ISO E SUPER, 25.60% by weight of Musk T, 3.10% by weight of GERANOL, 2.70% by weight of HYDROXY CETRONELLAL, 2.50 wt% of CITRONELLOL, 4.70 wt% of PHENYL ETHYL ALCOHOL, 6.70 wt% of Linalool, 10.00 wt% of D-LIMONENE, 0.10% by weight, brier aroma 0.10% by weight, acacia aroma 0.10% by weight, and 4.90% by weight.

Therefore, the fragrance series of the perfume composition of Example 2 may be referred to as a fresh-green-floral-musk type, and natural flavors of yellow lacquer, brier, and acacia flowers were used.

Fragrance Composition Example 3

The perfume composition is 19.60% by weight of linalool, 24.20% by weight of D-LIMONENE, 25.10% by weight of DIHYDROMYRCENOL, and 17.30% by weight of linalyl acetate. 6.70% by weight of musk tea, 1.90% by weight of LYSMERAL, 0.13% by weight of wild berry, 0.10% by weight of camphor, 0.04% by weight of brier, 0.03% by weight of holly And 4.90% by weight.

Therefore, the fragrance series of Example 3 of the fragrance composition can be referred to as a fresh-fruity-green-floral type, and the natural fragrances of camphor, wild tree, brier, and locust flower are used. It became.

Fragrance Composition Example 4

The fragrance composition is 12.4% by weight of a-HEXYL CINNAMIC ALDEHYDE, 32.3% by weight of PHENYL ETHYL ALCOHOL, 13.6% by weight of D-LIMONENE, and linalol ( LINALOOL) 9.4% by weight, 23.7% by weight of Musk T, 3.4% by weight of Geranol, 0.1% by weight of wild tree, 0.1% by weight of yellow lacquer, and 0.1% by weight of Red Oak flower And 4.9% by weight.

Therefore, the fragrance series of Example 4 of the fragrance composition can be referred to as fruity-green-floral type, and natural fragrances of pink, yellow, and hawthorn flowers were used.

Fragrance Composition Example 5

The perfume composition is 12.0% by weight of a-HEXYL CINNAMIC ALDEHYDE, 29.9% by weight of PHENYL ETHYL ALCOHOL, 14.6% by weight of D-LIMONENE, and linalol ( LINALOOL) 10.8% by weight, 23.5% by weight Musk T, 4.1% by weight of Geranol, 0.1% by weight of wild tree, 0.1% by weight of yellow lacquer, and 0.1% by weight of Red Oak flower And 4.9% by weight.

Therefore, the fragrance series of the fragrance composition of Example 5 can be referred to as fruity-watery-green-floral type, and natural fragrances extracted from wild tree and yellow lacquer were used.

In addition, the perfume composition of Examples 1 to 5 of the perfume composition is composed of Slightly yellow to Yellow.

The dalberry, cypress used in Examples 1 to 5 of the perfume composition is extracted with essential oils, camphor, yellow lacquer, brier, locust flower is used in the absolute state.

By using the perfume composition and the alcohol of Examples 1 to 5 to make a perfume according to the concentration of the perfume.

It will be apparent to those skilled in the art that various modifications and variations can be made in the present invention without departing from the spirit or scope of the invention.

Therefore, the technical scope of the present invention should not be limited to the contents described in the embodiments, but should be defined by the claims and their equivalents.

S100: steps to prepare with natural flavor
S200: natural fragrance is added to the whole fragrance composition and mixed

Claims (15)

Absolute produced any one selected from essential oils extracted from steam or distillation method from the leaves and stems of the trees selected from wild tree, safflower tree and cypress, and the flowers of the yellowtail and the flowers of the brier and locust tree by the solvent extraction method (S100) or the leaves and stems of camphor tree are prepared with natural fragrances consisting of two or more of natural fragrances made of absolute (Absolute) extracted by steam distillation and solvent extraction;
The natural fragrance is added to the whole fragrance composition mixing step (S200) characterized in that the fragrance production method containing natural fragrances of tropical species and forest species. The method of claim 1,
The natural fragrance is a perfume manufacturing method containing natural fragrances of tropical and forest species, characterized in that 0.03% by weight to 0.13% by weight relative to the total weight ratio of the perfume composition. The method of claim 1,
The steam distillation method of the bark, hawthorn, cypress is natural fragrance of ovarian species and forest species, characterized in that the stem and leaves of the bark, hawthorn, cypress are cut and heated for 1 hour to extract rectification. Perfume manufacturing method containing a. The method of claim 3, wherein
Stem and leaves of the bark, hawthorn, cypress, perfume production method containing natural fragrances of tropical species and forest species characterized in that the cut to 2cm ~ 3cm. The method of claim 1,
In the solvent extraction method of the brier and Acacia flowers, 1 kg of the brier and Acacia flowers are immersed in 1.5l to 3l of hexane (n-Hexan 95%) for 12 hours to 24 hours at room temperature and filtered, and the filtered hexane and The moisture in the fragrance and moisture is removed using anhydrous sodium sulfate (Na ₂ S0 ₄ ), and the concrete (Concrete) oil from which hexane is removed with a rotary vacuum condenser is dissolved in alcohol and filtered with a filter to extract the absolute. Perfume production method containing natural flavors of the tropical and forest species. 6. The method of claim 5,
In the conditions of the rotary vacuum concentrator, the warming is maintained at 20 ° C. to 22 ° C. to minimize loss of volatile aromatic components, but not to exceed 23 ° C., and the rotation speed is maintained at 5 to 6, and the concrete oil is the alcohol 1 A perfume manufacturing method containing natural fragrances of tropical and forest species, characterized by dissolving at a ratio of 10 to 50 and filtering with a filter of 0.45 µm to remove insoluble wax. The method of claim 1,
The lactose solvent extraction method of the hwangchil wood is shaken by mixing 10g of the lactose solution with 20ml of a mixture of hexane: alcohol 5: 5 and then remove the water using anhydrous sodium sulfate (Na ₂ S0 ₄ ), hexane with a rotary vacuum concentrator Perfume and alcohol from the extract is mixed, and the separated extract is filtered with the filter of 0.45㎛ the insoluble wax, characterized in that to remove the insoluble wax and forest species natural fragrance containing perfume. The method of claim 1,
The leaves and stems of the camphor tree are the vapor distillation method and the solvent extraction method. The stems and leaves of the camphor tree are cut to a size of 2 cm to 3 cm and heated for 1 hour. Dissolve with water and collect it in one place to remove unnecessary moisture using anhydrous sodium sulfate (Na ₂ S0 ₄ ), and then remove the fragrance dissolved in the solvent in concrete to remove hexane with a rotary vacuum condenser in alcohol and filter it with an absolute filter. Perfume manufacturing method containing a natural flavor of tropical and forest species, characterized in that the extraction. Perfume composition containing natural flavors of tropical and forest species produced by the method of any one of claims 1 to 8. The method of claim 9,
The perfume composition is 26.30% by weight of ISO E SUPER, 25.46% by weight of Musk T, 2.80% by weight of GERANOL, 2.70% by weight of HYDROXY CETRONELLAL. And 2.50 wt% of CITRONELLOL, 4.70 wt% of PHENYL ETHYL ALCOHOL, 12.10 wt% of Linalool, 18.40 wt% of D-LIMONENE, Perfume composition containing natural fragrances of tropical and forest species, characterized by consisting of 0.07% by weight of tree, 0.07% by weight of Akushi flower, and 4.90% by weight. The method of claim 9,
The perfume composition is 39.50% by weight of ISO E SUPER, 25.60% by weight of Musk T, 3.10% by weight of GERANOL, 2.70% by weight of HYDROXY CETRONELLAL, 2.50 wt% of CITRONELLOL, 4.70 wt% of PHENYL ETHYL ALCOHOL, 6.70 wt% of Linalool, 10.00 wt% of D-LIMONENE, Perfume composition containing natural fragrances of tropical and forest species, characterized by consisting of 0.10% by weight, brier fragrance 0.10% by weight, acacia fragrance 0.10% by weight, and 4.90% by weight. The method of claim 9,
The perfume composition is 19.60% by weight of Linalool, 24.20% by weight of D-LIMONENE, 25.10% by weight of DIHYDROMYRCENOL, and 17.30% by weight of Linalyl Acetate. 6.70% by weight of musk tea, 1.90% by weight of LYSMERAL, 0.13% by weight of wild berry, 0.10% by weight of camphor, 0.04% by weight of brier, 0.03% by weight of holly And other fragrance composition containing natural fragrances of tropical and forest species, characterized by consisting of 4.90% by weight. The method of claim 9,
The fragrance composition is 12.4% by weight of a-HEXYL CINNAMIC ALDEHYDE, 32.3% by weight of PHENYL ETHYL ALCOHOL, 13.6% by weight of D-LIMONENE, and linalol ( LINALOOL) 9.4% by weight, 23.7% by weight of Musk T, 3.4% by weight of Geranol, 0.1% by weight of wild tree, 0.1% by weight of yellow lacquer, and 0.1% by weight of Red Oak flower And, fragrance composition containing natural fragrances of tropical and forest species, characterized in that 4.9% by weight. The method of claim 9,
The perfume composition is 12.0% by weight of a-HEXYL CINNAMIC ALDEHYDE, 29.9% by weight of PHENYL ETHYL ALCOHOL, 14.6% by weight of D-LIMONENE, and linalol ( LINALOOL) 10.8% by weight, 23.5% by weight Musk T, 4.1% by weight of Geranol, 0.1% by weight of wild tree, 0.1% by weight of yellow lacquer, and 0.1% by weight of Red Oak flower And, fragrance composition containing natural fragrances of tropical and forest species, characterized in that 4.9% by weight. The method according to any one of claims 10 to 14,
The perfume composition is a fragrance composition containing natural fragrances of tropical and forest species, characterized in that the color from Yellow to Yellow (Slightly yellow).

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