KR102562816B1 - Perfume composition with excellent durability and manufacturing method thereof - Google Patents

Abstract

The present invention provides a perfume composition with excellent durability.

Description

Perfume composition with excellent durability and manufacturing method thereof

The present invention relates to a perfume composition with excellent durability and a manufacturing method thereof.

In general, with the development of the economy and the improvement of living standards, the desire to beautify the appearance is increasing, and various cosmetics and perfumes are proposed and marketed as materials that can beautify the appearance.

On the other hand, perfume is a type of cosmetic product that is prepared by mixing fragrance-producing substances in an appropriate ratio and then dissolving them in alcohol, etc., spraying them on parts of the body or clothes, and mixing them with body temperature or body odor emitted from the skin to emit fragrance. will be.

In this way, when perfume is used on the body or clothes, bad odors emitted from the body or clothes are reduced or blocked, and good fragrance emitted from the perfume arouses others' liking, so it is highly preferred by modern people regardless of gender. It has become a type of cosmetic product.

However, conventional perfumes simply catch bad smells by emitting fragrance, and there is a limit to completely removing bad smells and maintaining aromaticity at the same time.

Therefore, for the purpose of removing unpleasant odors from the body or clothes, perfumes with excellent odor removal and longevity are required.

Patent Document 1: Korean Patent Publication No. 10-2012-0001111

The present invention has been made to solve the above problems, and an object of the present invention is to provide a perfume composition with excellent durability and a manufacturing method thereof.

The object of the present invention is not limited to the tasks mentioned above, and other tasks not mentioned will be clearly understood by those skilled in the art from the following description.

In order to achieve the above object, the present invention

A perfume composition with excellent durability is provided.

In addition, the perfume composition,

Guaiacwood oil 18-22 parts by weight, vanilla oil 18-22 parts by weight, mandarin oil 6-10 parts by weight, hexyl salicylate 4-8 parts by weight, dioctyl adipate 18-22 parts by weight, propylene glycol 1- 18-22 parts by weight of perfume raw materials including 5 parts by weight, 1-5 parts by weight of butylphenylmethylpropional and 18-22 parts by weight of ethanol; and

78-82 parts by weight of perfume raw materials including 42-46 parts by weight of cypress water, 38-42 parts by weight of broccoli water, 1-5 parts by weight of isopropyl isostearate and 1-5 parts by weight of Fibersol-2 includes;

In addition, the perfume composition,

Guaiacwood oil 18-22 parts by weight, vanilla oil 18-22 parts by weight, mandarin oil 6-10 parts by weight, hexyl salicylate 4-8 parts by weight, dioctyl adipate 18-22 parts by weight, propylene glycol 1- 18-22 parts by weight of perfume raw materials including 5 parts by weight, 1-5 parts by weight of butylphenylmethylpropional and 18-22 parts by weight of ethanol;

68-72 parts by weight of perfume raw materials including 42-46 parts by weight of cypress water, 38-42 parts by weight of broccoli water, 1-5 parts by weight of isopropyl isostearate and 1-5 parts by weight of Fibersol-2 ; and

4-8 parts by weight of barberry root extract, 4-8 parts by weight of Sulfur tree stem extract, 2-6 parts by weight of Dongae extract, 2-6 parts by weight of thyme leaf oil, 2-6 parts by weight of peppermint leaf oil, 2 parts of manuka leaf oil -6 parts by weight, butylene glycol 3-7 parts by weight, glycerin 4-8 parts by weight, denatured alcohol 1-5 parts by weight, dipropylene glycol 1-5 parts by weight, glycereth-26 1-5 parts by weight , 0.5-4 parts by weight of 1,2-hexanediol, 0.5-4 parts by weight of xylitol, 0.5-4 parts by weight of hydroxyacetophenone, 0.5-4 parts by weight of glycereth-25PCA isostearate, diphenyldime Thicon 0.3-3 parts by weight, ethylhexylglycerin 0.05-1 parts by weight, triethylhexanoin 0.05-1 parts by weight, disodium EDTA 0.05-1 parts by weight, hydrogenated lecithin 0.05-1 parts by weight and volcanic stone extract 39 8-12 parts by weight of deodorizing raw materials including -43 parts by weight;

In addition, the present invention

Guaiacwood oil 18-22 parts by weight, vanilla oil 18-22 parts by weight, mandarin oil 6-10 parts by weight, hexyl salicylate 4-8 parts by weight, dioctyl adipate 18-22 parts by weight, propylene glycol 1- Preparing a perfume raw material by mixing 5 parts by weight, 1-5 parts by weight of butylphenylmethylpropional and 18-22 parts by weight of ethanol;

Preparing a perfume raw material comprising 42-46 parts by weight of cypress water, 38-42 parts by weight of broccoli water, 1-5 parts by weight of isopropyl isostearate and 1-5 parts by weight of Fibersol-2;

4-8 parts by weight of barberry root extract, 4-8 parts by weight of Sulfur tree stem extract, 2-6 parts by weight of Dongae extract, 2-6 parts by weight of thyme leaf oil, 2-6 parts by weight of peppermint leaf oil, 2 parts of manuka leaf oil -6 parts by weight, butylene glycol 3-7 parts by weight, glycerin 4-8 parts by weight, denatured alcohol 1-5 parts by weight, dipropylene glycol 1-5 parts by weight, glycereth-26 1-5 parts by weight , 0.5-4 parts by weight of 1,2-hexanediol, 0.5-4 parts by weight of xylitol, 0.5-4 parts by weight of hydroxyacetophenone, 0.5-4 parts by weight of glycereth-25PCA isostearate, diphenyldime Thicon 0.3-3 parts by weight, ethylhexylglycerin 0.05-1 parts by weight, triethylhexanoin 0.05-1 parts by weight, disodium EDTA 0.05-1 parts by weight, hydrogenated lecithin 0.05-1 parts by weight and volcanic stone extract 39 - preparing a deodorizing raw material by mixing 43 parts by weight; and

Mixing 18-22 parts by weight of the perfume raw material, 68-72 parts by weight of the perfume raw material and 8-12 parts by weight of the deodorizing raw material;

The barberry root extract and silver gourd tree stem extract,

After washing the root and the stem of the yellow chestnut tree, preparing by crushing; After mixing 90-110 parts by weight of a mixture of the prepared rhizomatous rhizomatous root and Sulfur tree trunk in a weight ratio of 1: 1 and 900-1100 parts by weight of a mixed solvent in which ethanol and acetone are mixed in a volume ratio of 1: 1, ultrasonic process Preparing an extract for 22-26 hours at a temperature of 38-42 ℃; And concentrating and freeze-drying the extract under reduced pressure; it is prepared by performing,

The thyme leaf oil, peppermint leaf oil and manuka leaf oil are

Washing, drying, and pulverizing thyme leaves, mint leaves, and manuka leaves; preparing a mixture by mixing pulverized thyme leaves, mint leaves, and manuka leaves in a weight ratio of 1:1:1, and steam distilling the mixture; and cooling the mixed steam generated by steam distillation to separate the oil layer and the water layer, and then separating and filtering the oil layer.

The perfume composition according to the present invention is excellent in durability. In addition, it is excellent in perfume smell and has no skin irritation, so it has excellent overall acceptability.

1 is a flow chart showing a method for producing a perfume composition according to the present invention.

Hereinafter, various embodiments will be described in more detail with reference to the accompanying drawings. The embodiments described in this specification may be modified in various ways. Certain embodiments may be depicted in the drawings and described in detail in the detailed description. However, specific embodiments disclosed in the accompanying drawings are only intended to facilitate understanding of various embodiments. Therefore, the technical idea is not limited by the specific embodiments disclosed in the accompanying drawings, and it should be understood to include all equivalents or substitutes included in the spirit and technical scope of the invention.

Terms including ordinal numbers such as primary, secondary, first, and second may be used to describe various elements, but these elements are not limited by the above-mentioned terms. The terminology described above is only used for the purpose of distinguishing one component from another.

In this specification, terms such as 'comprise' or 'having' are intended to designate that there is a feature, number, step, operation, component, part, or combination thereof described in the specification, but one or more other features It should be understood that the presence or addition of numbers, steps, operations, components, parts, or combinations thereof is not precluded. It is understood that when a component is referred to as being 'connected' or 'connected' to another component, it may be directly connected or connected to the other component, but other components may exist in the middle. It should be. On the other hand, when a component is referred to as being 'directly connected' or 'directly connected' to another component, it should be understood that no other component exists in the middle.

In addition, in describing the present invention, if it is determined that a detailed description of a related known function or configuration may unnecessarily obscure the subject matter of the present invention, the detailed description thereof will be abbreviated or omitted.

the present invention

A perfume composition with excellent durability is provided.

Hereinafter, the perfume composition according to the present invention will be described in detail.

The perfume composition according to the present invention is excellent in durability. In addition, it is excellent in perfume smell and has no skin irritation, so it has excellent overall acceptability.

The perfume composition,

Guaiacwood oil 18-22 parts by weight, vanilla oil 18-22 parts by weight, mandarin oil 6-10 parts by weight, hexyl salicylate 4-8 parts by weight, dioctyl adipate 18-22 parts by weight, propylene glycol 1- 18-22 parts by weight of perfume raw materials including 5 parts by weight, 1-5 parts by weight of butylphenylmethylpropional and 18-22 parts by weight of ethanol; and

78-82 parts by weight of perfume raw materials including 42-46 parts by weight of cypress water, 38-42 parts by weight of broccoli water, 1-5 parts by weight of isopropyl isostearate and 1-5 parts by weight of Fibersol-2 It is preferable to include;

It is more preferable that the spice raw material contains 19-21 parts by weight.

The perfume raw materials include 19-21 parts by weight of guaiac wood oil, 19-21 parts by weight of vanilla oil, 7-9 parts by weight of mandarin oil, 5-7 parts by weight of hexyl salicylate, 19-21 parts by weight of dioctyl adipate, It is more preferable to include 2-4 parts by weight of propylene glycol, 2-4 parts by weight of butylphenylmethylpropional and 19-21 parts by weight of ethanol.

Guaiac Wood (Bulnsia Sarmienti) Oil is an essential oil obtained by distilling a tropical tree native to South America and has a woody scent with a subtle rose scent. It is used for ceremonial decorations or for the treatment of rheumatism, rheumatoid arthritis, and sexually transmitted diseases. It has anti-inflammatory, antioxidant, antirheumatic, antiseptic, diuretic, sweating, and diarrhea inducing effects.

Vanilla (Vanilla Planifolia) is an orchid plant native to Mexico, tropical America, and the fruit part is commonly called vanilla bean. In the present invention, vanilla bean is used as a meaning including vanilla processing beans having a unique aroma of black color obtained by steaming and drying vanilla fruits (vanilla beans) several times.

Mandarin, also known as mandarin orange, contains vitamin P, ascorbic acid, carotenoids, limonoid flavonoids, gumarin, and naringenin-type components. Among them, the component of the naringenin system is a component in the peel of mandarin.

The hexyl salicylate is a colorless liquid with a green, floral, and spicy scent, and is often used to make a characteristic floral scent of a floral combination spice.

In the present invention, guaiac wood oil, vanilla bean oil, mandarin oil and hexyl salicylate can be applied to exhibit a luxurious fragrance as natural raw materials.

The dioctyl adipate, propylene glycol, butylphenylmethylpropional, and ethanol are applied as solvents to stabilize and easily disperse the perfume raw materials.

It is more preferable that the perfume raw material contains 79-81 parts by weight.

It is more preferable that the perfume raw material includes 43-45 parts by weight of cypress water, 39-41 parts by weight of broccoli water, 2-4 parts by weight of isopropyl isostearate and 2-4 parts by weight of Fibersol-2 do.

Cypress water is effective in various fields such as strengthening immunity, treating atopy, preventing atopy, treating rhinitis, and strengthening skin immunity.

Broccoli contains a large amount of beta-carotene, rutin, ascorbic acid, selenium, quercetin, and glutathione, which have antioxidant effects, as well as nutrients such as calcium, vitamin C, and folic acid, so it is used for skin care.

Including isopropyl isostearate, high-temperature stability of the fiber deodorant can be secured.

Fibersol-2 is a dietary fiber and can be prepared through starch heating, enzymatic degradation, fractionation, purification, powderization, and Fibersol extraction processes. Including Fibersol-2, a water-soluble dietary fiber, it shows the effect of slowly and continuously dissipating fragrance components, and helps with antibacterial and antifungal action.

In addition, the perfume composition,

Guaiacwood oil 18-22 parts by weight, vanilla oil 18-22 parts by weight, mandarin oil 6-10 parts by weight, hexyl salicylate 4-8 parts by weight, dioctyl adipate 18-22 parts by weight, propylene glycol 1- 18-22 parts by weight of perfume raw materials including 5 parts by weight, 1-5 parts by weight of butylphenylmethylpropional and 18-22 parts by weight of ethanol;

68-72 parts by weight of perfume raw materials including 42-46 parts by weight of cypress water, 38-42 parts by weight of broccoli water, 1-5 parts by weight of isopropyl isostearate and 1-5 parts by weight of Fibersol-2 ; and

4-8 parts by weight of barberry root extract, 4-8 parts by weight of Sulfur tree stem extract, 2-6 parts by weight of Dongae extract, 2-6 parts by weight of thyme leaf oil, 2-6 parts by weight of peppermint leaf oil, 2 parts of manuka leaf oil -6 parts by weight, butylene glycol 3-7 parts by weight, glycerin 4-8 parts by weight, denatured alcohol 1-5 parts by weight, dipropylene glycol 1-5 parts by weight, glycereth-26 1-5 parts by weight , 0.5-4 parts by weight of 1,2-hexanediol, 0.5-4 parts by weight of xylitol, 0.5-4 parts by weight of hydroxyacetophenone, 0.5-4 parts by weight of glycereth-25PCA isostearate, diphenyldime Thicon 0.3-3 parts by weight, ethylhexylglycerin 0.05-1 parts by weight, triethylhexanoin 0.05-1 parts by weight, disodium EDTA 0.05-1 parts by weight, hydrogenated lecithin 0.05-1 parts by weight and volcanic stone extract 39 It is more preferable to include; 8-12 parts by weight of a deodorizing raw material including -43 parts by weight.

The perfume composition can prevent the growth of microorganisms such as mold and bacteria and remove odor while being harmless to the human body, including deodorizing raw materials.

More preferably, the perfume composition includes 19-21 parts by weight of perfume raw materials, 69-71 parts by weight of perfume raw materials, and 9-11 parts by weight of deodorizing raw materials.

It is more preferable to include 9-11 parts by weight of the deodorizing raw material.

The deodorizing raw material is 5-7 parts by weight of barberry root extract, 5-7 parts by weight of silver gourd stem extract, 3-5 parts by weight of Dongae extract, 3-5 parts by weight of thyme leaf oil, 3-5 parts by weight of peppermint leaf oil, 3-5 parts by weight of manuka leaf oil, 4-6 parts by weight of butylene glycol, 5-7 parts by weight of glycerin, 2-4 parts by weight of denatured alcohol, 2-4 parts by weight of dipropylene glycol, glycereth-26 2 -4 parts by weight, 1-3 parts by weight of 1,2-hexanediol, 1-3 parts by weight of xylitol, 1-3 parts by weight of hydroxyacetophenone, 1-3 parts by weight of glycereth-25 PCA isostearate, Diphenyldimethicone 0.5-1.5 parts by weight, ethylhexylglycerin 0.3-0.7 parts by weight, triethylhexanoin 0.3-0.7 parts by weight, disodium EDTA 0.3-0.7 parts by weight, hydrogenated lecithin 0.3-0.7 parts by weight and 40-42 parts by weight of a volcanic stone extract.

Barberry root is cultivated in China, Korea, and Japan. It makes the stomach healthy and has sedative, anti-inflammatory, and antibacterial effects, so it was used to treat diarrhea caused by heat accumulation in the intestines or stomach or vomiting caused by gastric fever. The main ingredient, berberine, has a strong inhibitory effect on various bacteria, and has anti-inflammatory, hemostatic, blood pressure lowering and anti-cancer effects.

Magnolia officinalis Rehd et Wils. is a deciduous tree that is native to China and is known to grow below 700m above sea level in the southern islands in Korea and grows up to 5-15m in height. It is reported to be effective for gastric ulcer and duodenal spasm, and also to have blood pressure lowering action and relatively strong antibacterial action. In addition, there are clinical reports that it is effective for acute gastroenteritis or bacterial dysentery. The major components of succulents include honokiol, magnolol, eudesmagnolol, magnoloside A, B, C, and magnocurarine. Honokiol has been reported to have antibacterial, muscle tension, anticancer and antioxidant effects, and magnolol is known to have anticancer activity, anti-inflammatory activity, anti-allergic activity and anti-asthmatic activity. And eudesmagnolol has been shown to be cytotoxic.

Black sodier fly (Hermetia illucens, black sodier fly) is a representative environmental cleaning insect of the family Diptera black sodier fly, also known as American black sodier fly. American blackbird (Hermetia illucens) is an environmental cleaning insect that survives in organic waste (food waste, livestock waste, agricultural by-products, etc.) containing a large amount of bacteria, fungi, and viruses, and quickly decomposes these organic wastes with strong antibacterial substances. has a mechanism for expressing Therefore, it is very excellent as a material for development of natural antibiotics that can replace chemical antibiotics, and it is expected to be used as a natural antibiotic because it has a very fast growth rate compared to other insects and does not require additional feed costs.

Thyme is cultivated throughout the world, although it is mainly grown in central or southern Europe and North Africa, and has a height of 30 cm. A square-shaped stem comes out of the root with many fine roots and goes up, giving many side branches. The leaf stem is very short, and the edge of a long oval leaf with a length of 5 to 9 mm and a width of 3 mm is bent inward and has many fine hairs. It is used for antiseptic, antibacterial, and expectorant effects.

Mint is a perennial plant belonging to the Lamiaceae family. It is effective for wind chill, antipyretic, and detoxification, and is effective for wind fever, headache, sore throat, flatulence, toothache, and skin itching. It contains l-limonene as its main ingredient. (Lee Seung-eun et al., 2005, Lee et al., 2005).

Manuka oil contains a large amount of volatile essential oil components, among which terpenoid components are monoterpenoid components such as alpha-pinene, alpha-terpinol, 1, There are 8-cineole (1,8-cineole), p-cymene, etc., and viridiflorol and isomeric alpha, beta, gamma- Contains eudesmols (isomeric alpha, beta, gamma-eudesmols).

The volcanic stone extract contains a variety of mineral components in a complex way, and in particular, contains a large amount of essential minerals such as sulfur, magnesium, calcium, potassium, chlorine, sodium and phosphorus, so it has excellent antibacterial and deodorizing effects.

In addition, the deodorizing raw material more preferably includes a fermented rice bran extract, and the fermented rice bran extract preferably contains 0.3-3 parts by weight, and more preferably 0.5-1.5 parts by weight based on 100 parts by weight of the total deodorizing raw material. desirable. The deodorizing performance can be further improved by including the fermented rice bran extract.

In addition, the present invention

Guaiacwood oil 18-22 parts by weight, vanilla oil 18-22 parts by weight, mandarin oil 6-10 parts by weight, hexyl salicylate 4-8 parts by weight, dioctyl adipate 18-22 parts by weight, propylene glycol 1- Preparing a perfume raw material by mixing 5 parts by weight, 1-5 parts by weight of butylphenylmethylpropional and 18-22 parts by weight of ethanol;

Preparing a perfume raw material comprising 42-46 parts by weight of cypress water, 38-42 parts by weight of broccoli water, 1-5 parts by weight of isopropyl isostearate and 1-5 parts by weight of Fibersol-2;

4-8 parts by weight of barberry root extract, 4-8 parts by weight of Sulfur tree stem extract, 2-6 parts by weight of Dongae extract, 2-6 parts by weight of thyme leaf oil, 2-6 parts by weight of peppermint leaf oil, 2 parts of manuka leaf oil -6 parts by weight, butylene glycol 3-7 parts by weight, glycerin 4-8 parts by weight, denatured alcohol 1-5 parts by weight, dipropylene glycol 1-5 parts by weight, glycereth-26 1-5 parts by weight , 0.5-4 parts by weight of 1,2-hexanediol, 0.5-4 parts by weight of xylitol, 0.5-4 parts by weight of hydroxyacetophenone, 0.5-4 parts by weight of glycereth-25PCA isostearate, diphenyldime Thicon 0.3-3 parts by weight, ethylhexylglycerin 0.05-1 parts by weight, triethylhexanoin 0.05-1 parts by weight, disodium EDTA 0.05-1 parts by weight, hydrogenated lecithin 0.05-1 parts by weight and volcanic stone extract 39 - preparing a deodorizing raw material by mixing 43 parts by weight; and

It provides a method for producing a perfume composition comprising the step of mixing 18-22 parts by weight of the perfume raw material, 68-72 parts by weight of the perfume raw material and 8-12 parts by weight of the deodorizing raw material.

At this time, the manufacturing method of the perfume composition according to the present invention in Figure 1 is shown in a flowchart, hereinafter, with reference to Figure 1, the manufacturing method of the perfume composition according to the present invention will be described in detail for each step.

First, the method for producing a perfume composition according to the present invention includes 18-22 parts by weight of guaiac wood oil, 18-22 parts by weight of vanilla oil, 6-10 parts by weight of mandarin oil, 4-8 parts by weight of hexyl salicylate, dioctyl and preparing a perfume raw material by mixing 18-22 parts by weight of adipate, 1-5 parts by weight of propylene glycol, 1-5 parts by weight of butylphenylmethylpropional, and 18-22 parts by weight of ethanol.

The step of preparing the perfume raw material is preferably performed by stirring at a rotational speed of 250-500 rpm at a temperature of 33-37 ° C., and stirring at a rotational speed of 300-400 rpm at a temperature of 34-36 ° C. it is desirable

The guaiac wood oil is obtained by washing, drying, and pulverizing the guaiac wood; steam distillation using pulverized guaiac wood; and cooling the mixed steam generated by steam distillation to separate the oil layer and the water layer, and then separating and filtering the oil layer.

The vanilla oil, washing the vanilla bean, drying and then pulverizing; Steam distillation using pulverized vanilla beans; and cooling the mixed steam generated by steam distillation to separate the oil layer and the water layer, and then separating and filtering the oil layer.

The mandarin oil may be obtained by washing, drying, and grinding the mandarin; steam distillation using pulverized mandarin; and cooling the mixed steam generated by steam distillation to separate the oil layer and the water layer, and then separating and filtering the oil layer.

Next, the manufacturing method of the perfume composition according to the present invention is 42-46 parts by weight of cypress water, 38-42 parts by weight of broccoli water, 1-5 parts by weight of isopropyl isostearate and Fibersol-2 (Fibersol-2) 1 -Including the step of preparing a perfume raw material containing 5 parts by weight.

The step of preparing the perfume raw material is preferably carried out by stirring at a rotational speed of 50-150 rpm at a temperature of 18-22 ° C, stirring at a rotational speed of 80-120 rpm at a temperature of 19-21 ° C. it is desirable

Next, the method for producing a perfume composition according to the present invention includes 4-8 parts by weight of barberry root extract, 4-8 parts by weight of silver gourd stem extract, 2-6 parts by weight of Dongae extract, 2-6 parts by weight of thyme leaf oil, Peppermint leaf oil 2-6 parts by weight, Manuka leaf oil 2-6 parts by weight, Butylene glycol 3-7 parts by weight, Glycerin 4-8 parts by weight, Denatured alcohol 1-5 parts by weight, Dipropylene glycol 1- 5 parts by weight, 1-5 parts by weight of glycereth-26, 0.5-4 parts by weight of 1,2-hexanediol, 0.5-4 parts by weight of xylitol, 0.5-4 parts by weight of hydroxyacetophenone, 0.5-4 parts by weight of glycereth-25 PCAI Sostearate 0.5-4 parts by weight, diphenyldimethicone 0.3-3 parts by weight, ethylhexylglycerin 0.05-1 parts by weight, triethylhexanoin 0.05-1 parts by weight, disodium EDTA 0.05-1 parts by weight, and preparing a deodorizing raw material by mixing 0.05-1 part by weight of hydrogenated lecithin and 39-43 parts by weight of a volcanic stone extract.

The step of preparing the deodorizing raw material is preferably performed by stirring at a rotational speed of 700-900 rpm at a temperature of 38-42 ° C, and stirring at a rotational speed of 750-850 rpm at a temperature of 39-41 ° C. it is desirable

The barberry root extract and silver gourd tree stem extract,

After washing the root and the stem of the yellow chestnut tree, preparing by crushing; After mixing 90-110 parts by weight of a mixture of the prepared rhizomatous rhizomatous root and Sulfur tree trunk in a weight ratio of 1: 1 and 900-1100 parts by weight of a mixed solvent in which ethanol and acetone are mixed in a volume ratio of 1: 1, ultrasonic process Preparing an extract for 22-26 hours at a temperature of 38-42 ℃; It is preferably prepared by performing; and concentrating and freeze-drying the extract under reduced pressure.

The blackcurrant extract,

Placing live black soldier flies in a vacuum chamber and maintaining the vacuum under reduced pressure for 30-90 minutes; Taking out black soldier flies, washing them with running water, immersing them in vinegar water for 15-45 minutes, and washing them again with running water; Primary heat treatment of the washed black soldier flies at a temperature of 80-100 ° C. for 60-120 minutes; Secondary heat treatment for 10-20 minutes at a temperature of 260-300 ° C.; Steaming the secondary heat treatment of Dongae, etc.; and crushing and freeze-drying the steamed black soldier flies.

The thyme leaf oil, peppermint leaf oil and manuka leaf oil are

Washing, drying, and pulverizing thyme leaves, mint leaves, and manuka leaves; preparing a mixture by mixing pulverized thyme leaves, mint leaves, and manuka leaves in a weight ratio of 1:1:1, and steam distilling the mixture; and cooling the mixed steam generated by steam distillation to separate the oil layer and the water layer, and then separating and filtering the oil layer.

In addition, the deodorizing raw material more preferably includes a fermented rice bran extract, and the fermented rice bran extract preferably contains 0.3-3 parts by weight, and more preferably 0.5-1.5 parts by weight based on 100 parts by weight of the total deodorizing raw material. desirable. The deodorizing performance can be further improved by including the fermented rice bran extract.

The fermented rice bran extract,

preparing rice bran powder by washing rice bran with boiled water and grinding it; Adding Saccharomyces cerevisiae as a yeast to a mixture of rice bran powder and water, followed by fermentation at a temperature of 33-37 ° C. for 22-26 hours; Preparing an extract by mixing the fermented mixture and butylene glycol and stirring at a temperature of 28-32 ° C. for 6-8 days; and lyophilizing the extract after filtering and concentrating under reduced pressure.

Next, the method for producing a perfume composition according to the present invention includes mixing 18-22 parts by weight of the perfume raw material, 68-72 parts by weight of the perfume raw material, and 8-12 parts by weight of the deodorizing raw material.

The mixing step is preferably performed by stirring at a rotation speed of 500-700 rpm at a temperature of 33-37 ° C, and preferably performed by stirring at a rotation speed of 550-650 rpm at a temperature of 34-36 ° C. .

Hereinafter, the present invention will be described in more detail by the following examples.

However, the following examples are merely illustrative of the content of the present invention, but the scope of the invention is not limited by the examples and experimental examples.

<Preparation Example 1> Preparation of perfume raw materials

The guaiac wood was washed, dried and pulverized. Steam distillation was performed using pulverized guaiac wood, and the mixed steam generated by steam distillation was cooled to separate an oil layer and a water layer, and then the oil layer was separated and filtered to prepare guaiac wood oil.

In addition, vanilla oil and mandarin oil were prepared in the same manner as in the preparation of guaiac wood oil, but using vanilla bean or mandarin instead of guaiac wood.

20 parts by weight of the guaiac wood oil, 20 parts by weight of the vanilla oil, 8 parts by weight of the mandarin oil, 6 parts by weight of hexyl salicylate, 20 parts by weight of dioctyl adipate, 3 parts by weight of propylene glycol, butylphenylmethylpropional After mixing 3 parts by weight and 20 parts by weight of ethanol, the mixture was stirred at a rotational speed of 350 rpm at a temperature of 35° C. to prepare a perfume raw material.

<Preparation Example 2> Preparation of perfume raw materials

After mixing 44 parts by weight of cypress water, 40 parts by weight of broccoli water, 3 parts by weight of isopropyl isostearate and 3 parts by weight of Fibersol-2, stirring at a rotational speed of 100 rpm at a temperature of 20 ° C. Perfume raw materials were prepared.

<Preparation Example 3> Preparation of deodorizing raw material-1

After washing the root of the yellow lotus and the stem of the blackberry tree, preparing by grinding, 100 parts by weight of a mixture of the prepared root of the yellow lotus and the stem of the silver leaf tree in a weight ratio of 1: 1, and ethanol and acetone are mixed in a volume ratio of 1: 1. After mixing 1000 parts by weight of the mixed solvent, an extract was prepared at a temperature of 40 ° C. for 24 hours by ultrasonic process. Thereafter, the extract was concentrated under reduced pressure and freeze-dried to prepare a root extract and an extract from the stem of Sulfur japonica.

Live black soldier flies are placed in a vacuum chamber, and the vacuum is maintained for 60 minutes under reduced pressure. Thereafter, black soldier flies were taken out, washed with running water, immersed in vinegar water for 30 minutes, and washed again with running water. The washed black soldier flies were subjected to a first heat treatment at a temperature of 90 ° C. for 90 minutes, and a second heat treatment was performed for the first heat treatment of the black soldier flies at a temperature of 280 ° C. for 15 minutes. Thereafter, the secondly heat-treated black soldier flies was put in a steamer and steamed, and the steamed black soldier flies were pulverized and freeze-dried to prepare an extract of black soldier flies.

The thyme leaves, mint leaves and manuka leaves were washed, dried and ground. A mixture was prepared by mixing pulverized thyme leaves, mint leaves, and manuka leaves in a weight ratio of 1:1:1, steam distilled using the mixture, and mixed steam generated by steam distillation was cooled to form an oil layer and After separating into the water layer, the oil layer was separated and filtered to prepare thyme leaf oil, peppermint leaf oil and manuka leaf oil.

12 parts by weight of the rhododendron root extract and Sulfur tree stem extract, 4 parts by weight of the Dongae extract, 12 parts by weight of the thyme leaf oil, peppermint leaf oil and manuka leaf oil, 5 parts by weight of butylene glycol, 6 parts by weight of glycerin, Denatured alcohol 3 parts by weight, dipropylene glycol 3 parts by weight, glycereth-26 3 parts by weight, 1,2-hexanediol 2 parts by weight, xylitol 2 parts by weight, hydroxyacetophenone 2 parts by weight, glycereth- 2 parts by weight of 25 PCA isostearate, 1 part by weight of diphenyldimethicone, 0.5 parts by weight of ethylhexylglycerin, 0.5 parts by weight of triethylhexanoin, 0.5 parts by weight of disodium EDTA, 0.5 parts by weight of hydrogenated lecithin After mixing and 41 parts by weight of the volcanic stone extract, the mixture was stirred at a rotational speed of 800 rpm at a temperature of 40° C. to prepare a deodorizing raw material.

<Preparation Example 4> Preparation of deodorizing raw material-2

A deodorizing raw material was prepared in the same manner as in Preparation Example 3, but the deodorizing raw material was prepared by including 1 part by weight of rice bran fermented extract with respect to 100 parts by weight of the deodorizing raw material prepared in Preparation Example 3.

The fermented rice bran extract was prepared by washing rice bran three times with boiled water and pulverizing the rice bran powder. A mixture was prepared by mixing 10 g of rice bran powder and 300 g of water, and 0.3 g of Saccharomyces cerevisiae as a yeast was added to the mixture, followed by fermentation at 35° C. for 24 hours. An extract was prepared by mixing 300 g of butylene glycol with the fermented mixture and stirring at a temperature of 30° C. for 7 days. After filtering and concentrating the extract under reduced pressure, the extract was freeze-dried to prepare and use a fermented rice bran extract.

<Example 1> Preparation of perfume composition-1

20 parts by weight of the perfume raw material prepared in Preparation Example 1 and 80 parts by weight of the perfume raw material prepared in Preparation Example 2 were mixed, and stirred at a rotational speed of 600 rpm at a temperature of 35 ° C to prepare a perfume composition.

<Example 2> Preparation of perfume composition-2

After mixing 20 parts by weight of the perfume raw material prepared in Preparation Example 1, 70 parts by weight of the perfume raw material prepared in Preparation Example 2, and 10 parts by weight of the deodorizing raw material prepared in Preparation Example 3, 600 rpm at a temperature of 35 ° C. A perfume composition was prepared by stirring at a rotational speed.

<Example 3> Preparation of perfume composition-3

After mixing 20 parts by weight of the perfume raw material prepared in Preparation Example 1, 70 parts by weight of the perfume raw material prepared in Preparation Example 2, and 10 parts by weight of the deodorizing raw material prepared in Preparation Example 4, 600 rpm at a temperature of 35 ° C. A perfume composition was prepared by stirring at a rotational speed.

<Experimental Example 1> Persistence and preference analysis of perfume composition

Evaluation of preference for the perfume composition prepared in Examples 1-3 was performed as follows.

After 30 adults (male: 10, female: 20) sprayed the perfume composition on the skin and used it, the degree of fragrance of the perfume, skin irritation (whether it occurs or not) and overall preference was evaluated to test perfume preference. The evaluation was performed using a 9-point scale method, and the evaluation result was the average value for the total evaluation of 30 people, and the results are shown in Table 1 below.

(9 points: very good, 7 points: good, 5 points: average, 3 points: poor, 1 point: very bad)

In addition, the persistence of the perfume was evaluated by a 9-point scale method to determine whether the degree of fragrance of the perfume was maintained after 8 hours had elapsed.

(9 points: very high durability, 7 points: high durability, 5 points: average, 3 points: poor durability, 1 point: very poor durability)

level of perfume skin irritation Perfume persistence Comprehensive Symbol Example 1 8.0 8.2 8.2 8.1 Example 2 8.3 8.4 8.4 8.4 Example 3 8.4 8.5 8.5 8.5

As shown in Table 1, it was confirmed that the perfume composition according to the present invention had excellent palatability and excellent perfume durability.

Claims (5)

Guaiacwood oil 18-22 parts by weight, vanilla oil 18-22 parts by weight, mandarin oil 6-10 parts by weight, hexyl salicylate 4-8 parts by weight, dioctyl adipate 18-22 parts by weight, propylene glycol 1- 18-22 parts by weight of perfume raw materials including 5 parts by weight, 1-5 parts by weight of butylphenylmethylpropional and 18-22 parts by weight of ethanol; and
78-82 parts by weight of perfume raw materials including 42-46 parts by weight of cypress water, 38-42 parts by weight of broccoli water, 1-5 parts by weight of isopropyl isostearate and 1-5 parts by weight of Fibersol-2 Perfume composition containing; delete According to claim 1,
The perfume composition,
Guaiacwood oil 18-22 parts by weight, vanilla oil 18-22 parts by weight, mandarin oil 6-10 parts by weight, hexyl salicylate 4-8 parts by weight, dioctyl adipate 18-22 parts by weight, propylene glycol 1- 18-22 parts by weight of perfume raw materials including 5 parts by weight, 1-5 parts by weight of butylphenylmethylpropional and 18-22 parts by weight of ethanol;
68-72 parts by weight of perfume raw materials including 42-46 parts by weight of cypress water, 38-42 parts by weight of broccoli water, 1-5 parts by weight of isopropyl isostearate and 1-5 parts by weight of Fibersol-2 ; and
4-8 parts by weight of barberry root extract, 4-8 parts by weight of Sulfur tree stem extract, 2-6 parts by weight of Dongae extract, 2-6 parts by weight of thyme leaf oil, 2-6 parts by weight of peppermint leaf oil, 2 parts of manuka leaf oil -6 parts by weight, butylene glycol 3-7 parts by weight, glycerin 4-8 parts by weight, denatured alcohol 1-5 parts by weight, dipropylene glycol 1-5 parts by weight, glycereth-26 1-5 parts by weight , 0.5-4 parts by weight of 1,2-hexanediol, 0.5-4 parts by weight of xylitol, 0.5-4 parts by weight of hydroxyacetophenone, 0.5-4 parts by weight of glycereth-25PCA isostearate, diphenyldime Thicon 0.3-3 parts by weight, ethylhexylglycerin 0.05-1 parts by weight, triethylhexanoin 0.05-1 parts by weight, disodium EDTA 0.05-1 parts by weight, hydrogenated lecithin 0.05-1 parts by weight and volcanic stone extract 39 A perfume composition containing 8-12 parts by weight of deodorizing raw materials including -43 parts by weight. delete delete