KR101541818B1 - Perfume composition of Chrysanthemum boreale oil - Google Patents

Perfume composition of Chrysanthemum boreale oil Download PDF

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KR101541818B1
KR101541818B1 KR1020130141174A KR20130141174A KR101541818B1 KR 101541818 B1 KR101541818 B1 KR 101541818B1 KR 1020130141174 A KR1020130141174 A KR 1020130141174A KR 20130141174 A KR20130141174 A KR 20130141174A KR 101541818 B1 KR101541818 B1 KR 101541818B1
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perfume composition
oil
present
essential oil
fragrance
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KR20150057612A (en
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조경숙
황인택
윤봉기
최경주
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전라남도
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    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00—Essential oils; Perfumes
    • C11B9/0003—Compounds of unspecified constitution defined by the chemical reaction for their preparation
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/36—Carboxylic acids; Salts or anhydrides thereof
    • A61K8/365—Hydroxycarboxylic acids; Ketocarboxylic acids
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/37—Esters of carboxylic acids
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L9/00—Disinfection, sterilisation or deodorisation of air
    • A61L9/01—Deodorant compositions
    • A61L9/013—Deodorant compositions containing animal or plant extracts, or vegetable material
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q13/00—Formulations or additives for perfume preparations
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q15/00—Anti-perspirants or body deodorants
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00—Essential oils; Perfumes
    • C11B9/0061—Essential oils; Perfumes compounds containing a six-membered aromatic ring not condensed with another ring

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  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
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  • Veterinary Medicine (AREA)
  • Chemical & Material Sciences (AREA)
  • Epidemiology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Birds (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Emergency Medicine (AREA)
  • Engineering & Computer Science (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Botany (AREA)
  • Zoology (AREA)
  • Fats And Perfumes (AREA)
  • Cosmetics (AREA)

Abstract

본 발명은 산국 정유, 꽃향유 정유, 배초향 정유, 로즈제라늄 정유, 쵸코제라늄 정유, 패랭이꽃 정유, 쟈스민 정유, 은방울꽃 정유, 바닐린(Vanillin PGA), 페닐아세트알데히드(Phenylacet aldehyde) 및 페닐에틸이소부티레이트(Phenyl ethyl isobutyrate)로 이루어져 탈취력 및 머스킹 효과가 우수하며, 달콤하고 평안함을 주면서도 시원하고 파우더리한 꽃 향이 나는 향료 조성물을 개시한다.The present invention relates to a process for the production of polyunsaturated fatty acids, which comprises the steps of: (a) mixing the essential oils selected from the group consisting of essential oils selected from the group consisting of essential oils selected from the group consisting of essential oils selected from the group consisting of sunflower oil, ethyl isobutyrate, which is excellent in deodorizing power and musking effect, and has a sweet and powdery floral feel.

Description

산국 정유를 함유하는 향료 조성물{Perfume composition of Chrysanthemum boreale oil}(Perfume composition of Chrysanthemum boreale oil)

본 발명은 산국 정유를 함유하는 것을 특징으로 하는 향료 조성물에 관한 것으로, 보다 구체적으로는 다양한 꽃 향이 어우러진 부케형의 꽃 향료 조성물에 관한 것이다.
The present invention relates to a perfume composition characterized by containing essential oils of a country of origin, and more particularly, to a bouquet-type floral perfume composition blended with various floral compositions.

건강한 피부를 유지하기 위해서는 화장품과 같이 유효성분을 인체 외부에서 공급해야 한다. 이에, 천연에서 추출 분리된 유효성분들이 첨가와 같이 천연소재들의 사용이 급증하고 있다. 특히, 화장품 및 향장품의 제조 특성상 정유나, 허브 추출물이 주로 사용되므로 향료작물 관련 시장은 결코 간과하기 어려운 큰 분야이다. 세계 향료작물 관련 시장 규모는 600억 달러로 추정되며 미국, 유럽 등 선진국을 중심으로 대중화 사업으로 정착되고 지속적으로 확대 성장하고 있다(2004년, 세계향신산업 동향).In order to maintain healthy skin, active ingredients such as cosmetics should be supplied from outside the body. Thus, the use of natural materials is rapidly increasing, such as the addition of active ingredients extracted from natural sources. In particular, cosmetics and fragrance products are mainly used for refining and herbal extracts, so the market for fragrant crops is a large field that is never overlooked. The global spice crop market is estimated at US $ 60 billion, and has been established as a popularization business centered on developed countries such as the US and Europe, and is growing steadily.

한편, 유럽, 특히 프랑스를 중심으로 고품질의 풍부한 방향식물의 원료확보와 정유 생산 설비의 발달로 향장품 향으로 사용되는 정유를 대량생산하고 있으며, 세계적으로 합성향료의 부작용으로 인한 문제점이 발생하면서 천연향료 개발에 대한 연구가 활발히 진행되고 있다. 또한, 최근에는 천연자원에서 추출한 향료를 이용한 기능성 화장품 및 방향성 제품개발이 증가하는 추세이다.On the other hand, Europe, especially in France, has been producing massive amounts of essential oils used as perfume products due to the securing of raw materials of high quality and rich aroma plants and the development of refinery production facilities. As a result of the problems caused by the side effects of synthetic perfumes worldwide, Research on development is actively proceeding. Recently, the development of functional cosmetics and aromatic products using spices extracted from natural resources is increasing.

한편, 국내 향료산업은 3500억으로 추정되며 매년 6%의 신장세를 보이고 있다. 향료 상품별로는 합성향료 14.8%, 천연향료 17.5%, 식품향료 28.5%, 화장품 향료 29.2%를 차지하고 있다. 다만, 향료 원료의 수입이 95% 이상으로 2006년에는 천연향료 수입량이 865톤 이였으며, 매년 8%씩 증가하고 있다고 보고되었다(2006년 통계청). 이에 따라, 국내 자생품종을 중심으로 한 우수 천연향료 개발과 함께 수입대체를 위한 천연향 상품화가 절실한 실정이다.
On the other hand, domestic spice industry is estimated to be 350 billion, showing 6% increase every year. By fragrance products, synthetic fragrance accounts for 14.8%, natural fragrance 17.5%, food fragrance 28.5%, and cosmetics fragrance 29.2%. However, the import of natural spices was 865 tons in 2006, with the import of spice ingredients more than 95%, and it was reported that it increased by 8% every year (2006 National Statistical Office). As a result, it is inevitable to develop natural perfumes, focusing on domestic native varieties, and to commercialize natural flavors for import substitution.

대한민국 공개특허 제10-2012-0001111호(발명의 명칭: 난대수종 및 산림수종의 천연향료를 함유하는 향수 제조방법 및 그 향수 조성물)에는 생달나무, 붓순나무, 편백나무 중 선택된 나무의 잎과 줄기를 수증기증류법으로 추출한 정유 또는 황칠나무의 칠액과, 찔레꽃 및 아까시나무의 꽃 중 선택된 어느 하나를 용매추출법으로 생산한 앱솔루트 또는 녹나무의 잎과 줄기를 수증기증류법 및 용매추출법으로 추출된 앱솔루트로 이루어진 천연향료들 중 둘 이상으로 이루어진 천연향료로 준비되는 단계(S100)와; 상기 천연향료가 전체향수조성물에 첨가되어 혼합되는 단계(S200)로 구성되는 것을 특징으로 하는 난대수종 및 산림수종의 천연향료를 함유하는 향수 제조방법에 대해 개시되어 있다.Korean Patent Laid-Open No. 10-2012-0001111 (the name of the invention: a method for producing fragrance containing natural fragrance of wild species and forest species and a perfume composition thereof) includes leaf and stem of a selected tree, Is extracted with steam distillation method, and the leaves and stems of Absolut or camphor produced by solvent extraction method selected from the oil of oil or yellowtail, flowers of bell pepper and bark of Acacia var. Wood are mixed with natural fragrance of Absolut extracted by steam distillation method and solvent extraction method (S100) which is prepared as a natural fragrance composed of two or more of the fragrances; And a step (S200) of mixing and adding the natural perfume composition to the whole perfume composition. 대한민국 등록특허 제10-0927969호(발명의 명칭: 천연 백합향을 이용하여 백합의 향취를 재현한 향료 조성물)에는 전체 조성물 100중량%에 대해 리나롤(Linalool) 10~15중량%, 게라니올(Geraniol) 15~20중량%, 헤디온(Hedione) 6~10중량%, 페닐에틸알콜(Phenyl ethyl alcohol) 5~10중량%, 벤질아세테이트(Benzyl acetate) 5~10중량% 및 백합향 추출물 3~5중량%를 함유하여 백합 향취를 재현한 향료 조성물에 대해 개시되어 있다.Korean Patent No. 10-0927969 (a perfume composition in which the fragrance of a lily is reproduced using a natural lily flavor) is characterized by containing 10 to 15% by weight of linalool with respect to 100% by weight of the whole composition, 15 to 20% by weight of geraniol, 6 to 10% by weight of Hedione, 5 to 10% by weight of phenyl ethyl alcohol, 5 to 10% by weight of benzyl acetate and 3 to 10% ≪ / RTI > to 5% by weight of the perfume composition.

본 발명은 우리나라의 자생자원과 꽃을 이용한 향수, 방향제 및 탈취제를 개발하여 국민건강에 기여하고 자생자원 활용 증대로 농가 고소득 작물을 육성 및 보급하는데 목적이 있다.The present invention aims at cultivating and distributing high-income farm products by contributing to the public health and utilizing natural resources by developing perfume, fragrance and deodorant using natural resources and flowers of Korea.

또한, 본 발명은 달콤하고 평안함을 주면서도 시원하고 파우더리한 꽃 향이 나는 향료 조성물을 제공하는데 목적이 있다.
It is also an object of the present invention to provide a fragrance composition which is sweet and smooth, but which has a cool and powdery floral scent.

상기 목적을 달성하기 위하여, 본 발명은 산국 정유, 꽃향유 정유, 배초향 정유, 로즈제라늄 정유, 쵸코제라늄 정유, 패랭이꽃 정유, 쟈스민 정유, 은방울꽃 정유, 바닐린(Vanillin PGA), 페닐아세트알데히드(Phenylacet aldehyde) 및 페닐에틸이소부티레이트(Phenyl ethyl isobutyrate)로 이루어진 것을 특징으로 하는 향료 조성물을 제공한다.In order to achieve the above-mentioned object, the present invention provides a method for producing an oil-in-water emulsion, comprising the steps of: (1) blending a sunflower oil, a floral essence oil, a blossom oil essential oil, And phenyl ethyl isobutyrate. The present invention also provides a perfume composition comprising:

또한, 본 발명은 산국 정유 5~15중량%, 꽃향유 정유 5~10중량%, 배초향 정유 5~10중량%, 로즈제라늄 정유 6~15중량%, 쵸코제라늄 정유 5~15중량%, 패랭이꽃 정유 4~10중량%, 쟈스민 정유 4~10중량%, 은방울꽃 정유 4~10중량%, 바닐린(Vanillin PGA) 5~15중량%, 페닐아세트알데히드(Phenylacet aldehyde) 4~5중량% 및 페닐 에틸 이소부티레이트(Phenyl ethyl isobutyrate) 4~6중량%로 이루어진 향료 조성물을 제공한다.The present invention also relates to a method for producing a crude oil of the present invention comprising 5 to 15% by weight of a country essential oil, 5 to 10% by weight of a floral perfume essential oil, 5 to 10% by weight of a refined essential oil, 6 to 15% by weight of a rose geranium essential oil, 4 to 10 wt% of jasmine essential oil, 4 to 10 wt% of jasmine essential oil, 4 to 10 wt% of lavender essential oil, 5 to 15 wt% of vanillin PGA, 4 to 5 wt% of phenylacetaldehyde, And 4 to 6% by weight of phenyl ethyl isobutyrate.

산국(Chrysanthemum boreale)은 국화과에 속하는 다년생초로 야국(野菊)이라고도 불린다. 산국의 노란색 꽃은 아름답고 향기가 좋으며, 국화주나 국화차로 음용하기도 한다. 한방에서 주로 두통, 제풍열, 청혈해독 등에 주로 사용되어 왔으며, 산국의 성분으로는 정유(essential oil), 리나린(linarin), 루테오린(luteolin)의 배당체, 크리산테민(chrysanthemin), 크리산테막산틴(chrysanthemaxanthin), 다당류, 쿠마린(coumarins), 예유아 락톤(yejuhua lactone)이 함유되어 있고, 정유 중의 주요 성분은 컴펜(comphene), 캄포(camphor), 카본(carvone) 등이 알려져 있다(Planta Med. 64(3):289-290, 한국농화학회지 40(1):85-87). 또한, 산국 꽃의 추출물에 대해서는 중추신경 진정작용이나, 혈압 강하작용, 결핵균과 각종 바이러스에 대한 억제효과 및 폐암과 간암에 대한 효과를 비롯한 다양한 생리활성들이 알려져 있다(서울대학교 생약연구소 업적집 14:69-74, 동양자원 식물학회). Chrysanthemum boreale ) is also known as a perennial grasshopper (wild chrysanthemum) belonging to the Asteraceae family. The yellow flowers of the country are beautiful and fragrant, and they are also used as chrysanthemums or chrysanthemum tea. It has been mainly used for headache, fever, and decolonization in oriental medicine. Ingredients of the country include essential oil, linarin, glycosides of luteolin, chrysanthemin, Chrysanthemaxanthin, polysaccharides, coumarins and yejuhua lactone. Comphene, camphor, carvone, etc. are known to be the main constituents of essential oils. Planta Med. 64 (3): 289-290, Korean Agricultural Science 40 (1): 85-87). In addition, various extracts of Bacillus subtilis are known to have various physiological activities including central nervous sedation, hypotensive action, inhibitory effect on Mycobacterium tuberculosis and various viruses, and effects on lung cancer and liver cancer (Seoul National University, 69-74, Oriental Resources and Botanical Society).

꽃향유(Elshooltzia splendens)는 꿀풀과(Labiatae family)에 속하는 식물로서 아시아와 북동 지역에서 서식하며 한방에서는 감기, 오한, 발열, 두통, 복통, 구토, 설사, 전신 부종, 각기, 종기 등을 치료하는 약용식물로서 사용되고 있다. 또한, 꽃향유는 박하향과 솔향 그리고 다양한 향이 섞여 매우 상쾌향 향을 내는데, 이러한 특유한 향기로 인하여 차로 음용 하거나, 방향제, 비누, 화장품 등에 사용되고 있다.Flower Essence ( Elshooltzia Splendens belong to the Labiatae family. They live in Asia and the northeastern region. They are used as medicinal plants for treating cold, chills, fever, headache, abdominal pain, vomiting, diarrhea, systemic edema, have. In addition, the floral fragrance is a mixture of peppermint, soya and various fragrances, giving a very refreshing fragrance. Due to the peculiar fragrance, it is used for tea drinking, fragrance, soap, and cosmetics.

배초향(Agastache rugosa)은 곽향이라고도 불리며, 꿀풀과(Labiatae)의 다년생 초본으로서 지상부 및 전초를 건조하여 약으로 쓴다. 배초향은 성숙한 것을 포기 전체로 하여 소화, 건위, 진통, 구토, 복통, 감기 등의 한방약재로 사용된 것이 본초강목에 개시되어 있다. 배초향의 이러한 기능으로 주로 약재로 사용되어 왔으며, 우리나라 남도지방에서는 배초향 잎을 전병이나 추어탕 등 찌개류에 풍미 재료로 사용하기도 한다. 또한, 은은한 솔향기가 나기 때문에 입냄새 제거에 좋다. Agastache rugosa , also called hwaku, is a perennial herb of Lamiaceae (Labiatae), which is dried and topically overgrown. Bamboo shoots are used as herbal medicine such as digestion, dryness, analgesia, vomiting, abdominal pain, cold and so on, which is disclosed in the main herbarium. It has been mainly used as a medicinal herb by this function of bamboo shoot, and it is also used as a flavor ingredient in stink bamboo shoots such as mackerel and chu-tang in South Korea. Also, it is good for eliminating bad breath because it has a soft purifier.

로즈제라늄(Pelargonium capitatum)은 구문초라고도 불리며, 쥐손이풀과 여러해살이풀로 허브종류로 제라늄 품종 중 하나이다. 로즈제라늄은 잎과 줄기에서 장미향이 나며, 로즈제라늄 추출물은 무독성 물질로 인체에 무해하고, 각종 해충을 쫓는데 효과가 있다고 알려져 있다.Rose geranium ( Pelargonium capitatum ), also called fungi, is a herbaceous variety of geranium and perennial plants, one of the geranium varieties. Rose geranium is rosy in leaves and stems. Rose geranium extract is a non-toxic substance harmless to the human body and is said to be effective in chasing various insects.

쵸코제라늄(Choco Geranjum)은 쥐손이풀과 여러해살이풀로 허브종류로 제라늄 품종 중 하나이다. 잎의 중심부에서 외부로 마치 초콜릿을 바른 것과 같은 진갈색의 무늬가 있는 것이 특징이다. 또한, 진한 쑥향과 국화향이 섞인 듯한 향을 내는 것이 특징이다.Choco Geranjum is a herbaceous and perennial herb that is one of the geranium varieties. It is characterized by the same dark brown pattern as the chocolate from the center of the leaf to the outside. In addition, it is characterized by the fragrance of a mixture of dark mugwort and chrysanthemum.

패랭이꽃(Dianthus chinensis L)은 석죽과에 속하는 다년생초본으로 높이가 30 cm에 달하고 잎은 선형 또는 피침형으로 꽃은 6~8월에 피며, 우리나라 산야에는 패랭이꽃(Dianthus sinensis L)과 갯패랭이꽃(Dianthus japonicas), 술패랭이꽃(Dianthus superbus var . longicalicinus)이 널리 자생하고 있다. 패랭이꽃 전초를 과맥이라고 하며, 꽃과 열매가 달린 전체를 그늘에서 말려 통경, 이뇨제 등 약용으로 널리 사용되어왔다. Dianthus chinensis L ) is a perennial herbaceous perennial herbaceous perennial plant. Its height is 30 cm. Leaves are linear or lanceolate. Flowers bloom in June ~ August. Dianthus sinensis L ) and Dianthus japonicas , Dianthus superbus there is . longicalicinus ) is widely grown. It has been widely used for medicines such as diuretics, and the whole plant with flower and fruit is dried in the shade.

쟈스민(Jasminum polyanthum)은 물푸레나무과 상록성 목본성 덩굴식물로 향이 좋아 꽃을 건조시켜 차로 음용 하거나, 디저트의 향료로도 이용되며, 화장품, 향수 등 다양한 향료 제품에 사용된다.Jasmine ( Jasminum polyanthum ) is an ash tree and an evergreen tree-like vine plant. It is used for various fragrance products such as cosmetics, fragrance and so on.

은방울꽃(Convallaria keiskei Miq)은 꽃의 모양이 은방울을 닮아서 은방울꽃이라는 이름을 얻은 식물로서 외떡잎식물 백합목 백합과의 여러해살이풀이며, 한국, 중국, 동시베리아, 일본 등의 산지에서 자란다. 꽃은 은은하고 좋은 향기를 풍겨서 향수화라고도 한다.Lily of the valley ( Convallaria keiskei Miq ) is a plant with the name of a lily of the valley with the shape of a flower resembling a lily of the valley. It is a perennial plant with a monocotyledon lily of the valley and grows in mountainous areas such as Korea, China, East Siberia and Japan. Flowers are called fragrance because they are sweet and have a good fragrance.

한편, 본 발명의 향료 조성물에 있어서, 상기 산국 정유, 꽃향유 정유, 배초향 정유, 로즈제라늄 정유, 쵸코제라늄 정유, 패랭이꽃 정유, 쟈스민 정유 및 은방울꽃 정유의 추출방법은 당업계에서 통상적으로 이용하는 방법을 이용하여 정유를 추출할 수 있다. 예를 들어, 압착법을 이용하거나, 대한민국 등록특허 제10-1105539호에 개시된 방법을 이용하여 정유를 추출할 수 있다.Meanwhile, in the perfume composition of the present invention, the extraction method of the above-mentioned essential oils of sunflower oil, flower essence oil, syrup essential oil, rose geranium oil, choco geranium oil, chrysanthemum essential oil, jasmine essential oil and lily of the valley can be performed by a method commonly used in the art So that the essential oil can be extracted. For example, the essential oil can be extracted by using the compression method or by the method disclosed in Korean Patent No. 10-1105539.

한편, 본 발명의 향료 조성물에 있어서, 상기 바닐린(Vanillin PGA)은 향료 조성물에 달콤한 향조를 제공하며, 본 발명의 향료 조성물에 사용되는 바닐린은 식품과 향장에 모두 사용되는 천연 바닐라빈을 식용 알코올로 추출한 천연 정유를 사용하는 것이 좋다.Meanwhile, in the perfume composition of the present invention, the vanillin PGA provides a sweet aroma to the perfume composition, and the vanillin used in the perfume composition of the present invention is a natural vanilla bean It is good to use extracted natural essential oil.

한편, 본 발명의 향료 조성물에 있어서, 상기 페닐아세트알데히드(Phenylacet aldehyde)는 장미꽃, 메밀씨, 초콜릿 등에서 발견되는 향이다. 상기 페닐아세트알데히드를 본 발명의 향료 조성물에 조성하여, 꿀처럼 달콤한 장미향, 신선한 풀향 및 세련된 꽃 향을 표현할 수 있다.On the other hand, in the perfume composition of the present invention, the phenylacetaldehyde is an aroma found in roses, buckwheat, chocolate and the like. The phenylacetaldehyde can be formulated into the perfume composition of the present invention to express honey-like sweet roses, fresh roses, and sophisticated floral aromas.

한편, 본 발명의 향료 조성물에 있어서, 상기 페닐에틸이소부티레이트(Phenyl ethyl isobutyrate)는 식품향료로도 사용되는 향이다. 상기 페닐에틸이소부티레이트를 본 발명의 향료 조성물에 조성하여, 꿀 및 복숭아향과 같은 달콤한 과일 향을 표현할 수 있다.On the other hand, in the perfume composition of the present invention, the phenylethyl isobutyrate is an aroma used as a food fragrance. The phenylethylisobutyrate can be incorporated into the perfume composition of the present invention to express a sweet fruit flavor such as honey and peach flavor.

한편, 본 발명의 향료 조성물은, 바람직하게 향수일 수 있다.On the other hand, the perfume composition of the present invention may preferably be perfume.

또한, 본 발명에 있어서, 상기 향수는 퍼퓸, 오뜨트왈렛, 샤워코롱 등 다양한 형태로 제공될 수 있다.Also, in the present invention, the perfume may be provided in various forms such as perfume, hautet wallet, and shower coron.

한편, 본 발명의 향료 조성물은, 바람직하게 방향제일 수 있다On the other hand, the perfume composition of the present invention may preferably be an aromatic

또한, 본 발명에 있어서, 상기 방향제는 액상형, 젤형 등 다양한 형태로 제공될 수 있다.Further, in the present invention, the perfume can be provided in various forms such as a liquid type and a gel type.

한편, 본 발명의 향료 조성물은, 바람직하게 탈취제일 수 있다.On the other hand, the perfume composition of the present invention may preferably be a deodorant.

한편, 본 발명에 있어서, 상기 향수, 방향제 및 탈취제에 첨가되는 향료 조성물은 당 업계에 통상적인 기술에 따라 적절하게 선택하여 배합될 수 있다.
Meanwhile, in the present invention, the perfume composition to be added to the fragrance, the fragrance, and the deodorant may be appropriately selected and blended in accordance with a conventional technique in the art.

본 발명에 의할 경우, 자생자원에서 추출한 천연향료를 첨가하여 항스트레스성과 같은 아로마테라피 효능을 가지는 향료 조성물을 제공할 수 있다.According to the present invention, a perfume composition having an aromatherapy effect such as antistress property can be provided by adding natural fragrance extracted from native sources.

또한, 본 발명에 의할 경우, 탈취력이 우수하고, 은은한 꽃향으로 머스킹 효과가 우수한 향료 조성물을 제공할 수 있다.Further, according to the present invention, it is possible to provide a fragrance composition which is excellent in deodorizing power and has a musking effect with a soft floral texture.

또한, 본 발명에 의할 경우, 달콤하고 평안함을 주면서도 시원하고 파우더리한 꽃 향이 나는 향료 조성물을 제공할 수 있다.
In addition, according to the present invention, it is possible to provide a fragrance composition that is sweet and pulpy and gives a cool and powdery floral scent.

이하, 본 발명의 내용을 하기 실시예를 통해 더욱 상세히 설명하고자 한다. 다만, 본 발명의 권리범위가 하기 실시예에만 한정되는 것은 아니고, 그와 등가의 기술적 사상의 변형까지를 포함한다.
Hereinafter, the present invention will be described in more detail with reference to the following examples. However, the scope of the present invention is not limited to the following embodiments, and includes modifications of equivalent technical ideas.

실시예Example 1: 본 발명의 향료 조성물 제조 1: Production of the perfume composition of the present invention

산국 정유 10 ㎖, 꽃향유 정유 7 ㎖, 배초향 정유 7 ㎖, 로즈제라늄 정유 10 ㎖, 쵸코제라늄 정유 10 ㎖, 패랭이꽃 정유 7 ㎖, 쟈스민 정유 7 ㎖, 은방울꽃 정유 7 ㎖, 바닐린(Vanillin PGA) 10 ㎖, 페닐아세트알데히드(Phenylacet aldehyde) 4.5 ㎖ 및 페닐에틸이소부티레이트(Phenyl ethyl isobutyrate) 5 ㎖를 혼합하여 본 발명의 향료 조성물을 제조하였다.
10 ml of vinegar essential oil, 7 ml of vinegar essential oil, 7 ml of vinegar essential oil, 10 ml of rosemary essential oil, 10 ml of choco geranium essential oil, 7 ml of jacinth essential oil, 7 ml of jasmine essential oil, 7 ml of lily of the valley, 10 ml of vanillin PGA , 4.5 ml of phenylacetaldehyde and 5 ml of phenylethyl isobutyrate were mixed to prepare a perfume composition of the present invention.

실험예Experimental Example 1: 본 발명의 향료 조성물의 안정성 검사 1: Stability test of the perfume composition of the present invention

본 실험예에서는 상기 실시예 1에서 제조된 향료 조성물의 안정성을 검사하고자 하였다.In this Experimental Example, the stability of the perfume composition prepared in Example 1 was examined.

95%의 식물성 알코올 90 ㎖에 상기 실시예 1에서 제조된 향료 조성물 10 ㎖를 첨가하여 희석한 후, 50 ㎖ 유리 비커에 10 ㎖씩 담아 3평짜리 밀폐된 공간에 두고 발향을 시켰다. 발향 40분 후, 남자 2명, 여자 2명을 들어가게 한 후, 10분 동안 머물도록 하였다. 그 후, 피부점막 및 안구의 자극도, 두통 정도를 확인함으로써 본 발명의 향료 조성물의 안정성을 검사하였다.
10 ml of the perfume composition prepared in Example 1 was diluted with 90 ml of 95% vegetable alcohol, and 10 ml of the perfume composition was placed in a 50 ml glass beaker. After 40 minutes of smell, 2 men and 2 women were allowed to enter and stayed for 10 minutes. Thereafter, the stability of the perfume composition of the present invention was examined by checking the degree of irritation of the mucous membrane of the skin and eyeball and the degree of headache.

샘플Sample 성별gender 피부자극성Skin irritation 안구적막자극 Ocular sedimentation 두통headache 실시예 1Example 1 남south 없음none 없음none 없음none 여female 없음none 없음none 없음none

실험결과(표 1), 상기 표 1에서 확인되는 바와 같이, 본 발명의 향료 조성물은 피부자극성, 안구 점막 자극, 두통 모두 없는 것으로 나타났다.
As a result of the experiment (Table 1), as shown in Table 1, the perfume composition of the present invention showed no skin irritation, ocular mucous membrane irritation, or headache.

실험예Experimental Example 2: 본 발명의 향료 조성물의 향 테스트 2: flavor test of the perfume composition of the present invention

본 실험예에서는 상기 실시예 1에서 제조된 본 발명의 향료 조성물의 향질, 향강도 및 잔향 지속성 테스트를 하고자 하였다.The perfume compositions of the present invention prepared in Example 1 were tested for perfume quality, fragrance strength and reverberation test.

3 L 용량의 향강도 측정용 특수비닐 봉투에 공기를 가득 채운 후, 무처리구(순수공기), 상기 실시예 1에서 제조된 향료 조성물 5 ㎕를 실리지로 주사한 것을 처리구로 하여 상온(25℃)에서 20분간 방치한 후, 향질 및 향강도를 측정하였다. A special plastic bag for measuring the fragrance strength of 3 L was filled with air and then treated with 5 쨉 l of the perfume composition prepared in Example 1 as a treatment solution at room temperature (25 캜) After standing for 20 minutes, the perfume and fragrance strength were measured.

또한, 잔향 지속성은 시향지 끝에 본 발명의 항료 조성물을 5 ㎜ 정도 묻혀 25℃의 상온에 방치한 후, 잔향 지속시간을 측정하였다.
In addition, the reverberation persistence was measured by measuring the reverberation time after putting 5 ㎜ of the present invention composition at the end of the warping paper and leaving it at room temperature of 25 캜.

조합향료 타입Combination perfume type 향질 및 향강도(5 ㎕/3 L) Flavor and fragrance intensity (5 [mu] L / 3 L) 잔향 지속성
(시향지 테스트)Reverberation persistence
(Stigmatization test) 향질Flesh 향강도Fragrance strength 이취Odor 무처리(공기)Untreated (air) 2828 728728 없음none 없음none 플로럴베이스Floral base 3939 51465146 없음none 84시간84 hours

실험결과(표 2), 본 발명의 향료 조성물의 향질은 39, 향강도는 5146으로 매우 강한 것으로 나타났다.As a result of the experiment (Table 2), the fragrance composition of the present invention showed a very strong fragrance of 39 and a fragrance intensity of 5146.

또한, 84시간 이상 잔향이 지속되어, 본 발명의 향료 조성물의 잔향 지속력이 우수함을 확인할 수 있었다.
In addition, it was confirmed that the reverberation persisted for more than 84 hours and that the perfume composition of the present invention had excellent reverberation sustainability.

실시예Example 2: 본 발명의 향료 조성물을 함유하는 향수 제조 2: perfume preparation containing the perfume composition of the present invention

알코올에 상기 실시예 1에서 제조된 향료 조성물을 15 ㎖를 첨가한 후, 첨가제와 방부제를 첨가하고, 1시간 동안 혼합하였다. 그 후, 4주의 숙성기간을 거친 다음, -3℃에서 냉각하여 녹지않는 물질을 침전되게 하고, 감압 필터로 여과하여 향수를 제조하였다.
After 15 ml of the perfume composition prepared in Example 1 was added to the alcohol, the additive and the preservative were added and mixed for 1 hour. Thereafter, after aging for 4 weeks, the mixture was cooled at -3 DEG C to precipitate a non-soluble substance and filtered through a reduced pressure filter to produce a perfume.

실시예Example 3: 본 발명의 향료 조성물을 함유하는 방향제 제조 3: Production of fragrance containing the perfume composition of the present invention

실리콘 오일과 실리콘 분말을 90 : 10의 비율로 배합하여 실리콘 배지를 제조한 후, 상기 실시예 1에서 제조된 향료 조성물 15 ㎖를 첨가하여 방향제 100 ㎖를 제조하였다.
Silicone oil and silicon powder were blended in a ratio of 90: 10 to prepare a silicone medium. Then, 15 ml of the perfume composition prepared in Example 1 was added to prepare 100 ml of a perfume.

실시예Example 4: 본 발명의 향료 조성물을 함유하는 탈취제 제조 4: Production of deodorant containing the perfume composition of the present invention

하이드로졸과 순도 95%의 식물성 에탄올을 60 : 40의 비율로 배합하여 수용액을 제조한 후, 계면활성제로 에코 바바수 베타인(Babassuamidopropyl Betain) 5 ㎖와 향료 3 ㎖를 첨가하여 탈취제 100 ㎖를 제조하였다.
Hydrousol and vegetable ethanol having a purity of 95% were blended in a ratio of 60:40 to prepare an aqueous solution. Then, 5 ml of a surfactant, and 3 ml of perfume were added to prepare 100 ml of deodorant. Respectively.

실험예Experimental Example 3: 본 발명의 향료 조성물을 함유하는 탈취제의  3: Deodorant containing the perfume composition of the present invention 탈취력Deodorant power 및  And 머스킹Musking 효과 확인 Check the effect

본 실험예에서는 상기 실시예 4에서 제조된 본 발명의 향료 조성물을 함유하는 탈취제의 탈취력 및 머스킹 효과 확인하고자 하였다.In the present Experimental Example, the effect of deodorant and musking of the deodorant containing the perfume composition of the present invention prepared in Example 4 was examined.

천에 김치 냄새, 불고기 냄새, 쌈장 냄새, 홍어 냄새 및 조기 냄새를 분사한 후, 상기 실시예 4에서 제조된 탈취제를 그 위에 분사한 다음, 냄새를 맡아 탈취력 및 머스킹 효과를 확인하였다.
The deodorant prepared in Example 4 was sprayed on the fabric, and the deodorizing power and musking effect were confirmed by smelling the kimchi odor, roasted meat odor, sesame roast odor, smell of red meat, and early smell.

샘플 Sample 김치 냄새Kimchi odor 불고기 냄새Roasted meat smell 쌈장 냄새Ssamjang odor 홍어 냄새Smell of skate 조기 냄새Early smell 머스킹 효과Musking effect 실시예 4Example 4 미약weak 약함weakness 무취Odorless 무취Odorless 무취Odorless 우수Great 미약weak 약함weakness 무취Odorless 무취Odorless 무취Odorless 우수Great 미약weak 약함weakness 무취Odorless 무치Immature 무취Odorless 우수Great

실험결과(표 3), 김치 냄새는 미약하게 남아 있으나, 쌈장, 홍어 및 조기 냄새는 무취 상태로 되었고, 약간의 산국 및 꽃 향 등이 머스킹되어 탈취 또는 머스킹 효과가 “좋음”으로 평가되었다.The results of the experiment (Table 3) indicate that the smell of kimchi remained weak, but the odor of seaweed, sponges and early smell became odorless, and some acidity and flower fragrance were musked and the deodorization or musking effect was evaluated as "good" .

Claims (5)

산국 정유, 꽃향유 정유, 배초향 정유, 로즈제라늄 정유, 쵸코제라늄 정유, 패랭이꽃 정유, 쟈스민 정유, 은방울꽃 정유, 바닐린(Vanillin PGA), 페닐아세트알데히드(Phenylacet aldehyde) 및 페닐에틸이소부티레이트(Phenyl ethyl isobutyrate)로 이루어진 것을 특징으로 하는 향료 조성물.
Phenylacetaldehyde and Phenyl ethyl isobutyrate are used as essential oils in sunflower oil, sunflower oil, flower essence oil, chrysanthemum essential oil, rose geranium oil, choco geranium oil, jelly essential oil, jasmine essential oil, lily of the valley oil, vanillin PGA, ≪ / RTI >
제1항에 있어서,
상기 향료 조성물은,
본 발명은 산국 정유 5~15중량%, 꽃향유 정유 5~10중량%, 배초향 정유 5~10중량%, 로즈제라늄 정유 6~15중량%, 쵸코제라늄 정유 5~15중량%, 패랭이꽃 정유 4~10중량%, 쟈스민 정유 4~10중량%, 은방울꽃 정유 4~10중량%, 바닐린(Vanillin PGA) 5~15중량%, 페닐아세트알데히드(Phenylacet aldehyde) 4~5중량% 및 페닐에틸이소부티레이트(Phenyl ethyl isobutyrate) 4~6중량%로 이루어진 것을 특징으로 하는 향료 조성물.
The method according to claim 1,
The perfume composition may contain,
The present invention relates to a process for producing a crude oil of the present invention comprising 5 to 15% by weight of a country essential oil, 5 to 10% by weight of a flowering essential oil, 5 to 10% by weight of a flowering essential oil, 6 to 15% by weight of a rose geranium essential oil, 10 to 15 wt% of vanillin PGA, 4 to 5 wt% of phenylacetaldehyde, 4 to 10 wt% of jasmine essential oil, 4 to 10 wt% ethyl isobutyrate in an amount of 4 to 6% by weight.
제1항에 있어서,
상기 향료 조성물은,
향수인 것을 특징으로 하는 향료 조성물.
The method according to claim 1,
The perfume composition may contain,
Perfume composition.
제1항에 있어서,
상기 향료 조성물은,
방향제인 것을 특징으로 하는 향료 조성물.
The method according to claim 1,
The perfume composition may contain,
Wherein the perfume composition is a perfume composition.
제1항에 있어서,
상기 향료 조성물은,
탈취제인 것을 특징으로 하는 향료 조성물.The method according to claim 1,
The perfume composition may contain,
Wherein the perfume composition is a deodorant.
KR1020130141174A 2013-11-20 2013-11-20 Perfume composition of Chrysanthemum boreale oil KR101541818B1 (en)

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Publication number Priority date Publication date Assignee Title
KR20210091574A (en) * 2020-01-14 2021-07-22 이상기 disinfection and deodorant composition and manufacturing method of it
KR20230173355A (en) 2022-06-17 2023-12-27 전라남도 Fragrance composition comprising Agastache rugosa oil extract as an active ingredient

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KR101962892B1 (en) * 2017-09-05 2019-03-27 서울대학교산학협력단 Natural Compositions Having Mind and Body Stability
CN110279616A (en) * 2019-06-28 2019-09-27 南京林业大学 It is a kind of while there is anti-oxidant and moisture-keeping efficacy rose pelargonium essential oil facial mask and preparation method thereof
CN112608791A (en) * 2020-11-26 2021-04-06 北京农业生物技术研究中心 'Xiangjin' essential oil and application thereof

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20210091574A (en) * 2020-01-14 2021-07-22 이상기 disinfection and deodorant composition and manufacturing method of it
KR102314874B1 (en) * 2020-01-14 2021-10-21 이상기 manufacturing method of disinfection and deodorant composition
KR20230173355A (en) 2022-06-17 2023-12-27 전라남도 Fragrance composition comprising Agastache rugosa oil extract as an active ingredient

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