KR102309548B1 - Functional Face Oil Compostion Containg Aromatic Natural Essential Oil and Seed Oil - Google Patents

Abstract

The present invention includes plum seed, tea seed, citron seed, and camellia seed cold-pressed oil, and Angelica keiskei essential oil, lavender essential oil, rosemary essential oil, geranium essential oil, eoseongcho essential oil, neroli essential oil and jasmine essential oil. The aroma is excellent.

Description

Functional face oil containing aromatic natural essential oil and seed oil and its manufacturing method {Functional Face Oil Composition Containg Aromatic Natural Essential Oil and Seed Oil}

The present invention relates to a face oil composition comprising a seed oil extracted by cold pressing from plum seeds, tea seeds, citron seeds and camellia seeds, and natural essential oils of Angelica serrata, lavender, rosemary, geranium, Eoseongcho, neroli and jasmine, and a method for preparing the same. it's about

Aromatherapy refers to natural therapy that treats various stressful symptoms such as headache, fatigue, insomnia, and skin and respiratory diseases by naturally inhaling the natural fragrance of essential oils in plants.

These essential oils refer to volatile oils with strong fragrances obtained from plant flowers, buds, leaves, stems, roots, and natural resins. Terpene compounds such as aldehydes, ketones and esters. There are more than 1,500 essential oils currently known, and about 100 of them are used as natural and synthetic fragrances. In particular, in the case of natural fragrances, mainly in France, raw materials for high-quality and abundant natural aromatic plants have been secured and refinery production facilities have been developed. Accordingly, natural essential oils used for fragrances are being mass-produced, and the development of functional cosmetics and fragrance products using essential oils extracted from natural resources is on the rise.

On the other hand, more than 90% of edible oil production in Korea is imported from abroad. Before the mid-1990s, almost all cosmetic raw materials were imported from abroad, and recently, about 80% of cosmetic raw materials are imported. As the Nagoya Protocol entered into force in October 2014, it is stipulated that it is obligatory to share the benefits arising from the use of genetic resources with resource providers. The protection of biodiversity, including genetic resources, is an essential element for human survival, and its importance is expected to increase further in the future as much attention is paid to it. Therefore, if most of the cosmetic raw materials are dependent on foreign countries, monetary and non-monetary costs are expected to increase, and it is urgent to secure materials using domestic biological resources.

In the present invention, plum seed, tea seed, citron seed, which are materials that can be mass-produced in Korea, and seed oil obtained by cold-pressing camellia seed cultivated in the southern coastal region of Korea and traditionally used in beauty products, and natural essential oil having aromatherapy effect. We want to develop a face oil using

Republic of Korea Patent Registration No. 10-1943346

The problem to be solved by the present invention is 30 to 50% by weight of seed oil (a), including plum seed oil, tea seed oil, citron seed oil and camellia seed oil, and Angelica keiskei essential oil, lavender essential oil, rosemary essential oil, geranium It is to provide a face oil composition containing 0.1 to 10% by weight of a natural essential oil (b), including essential oil, Eoseongcho essential oil, neroli essential oil and jasmine essential oil.

Another problem of the present invention is 1 to 10% by weight of essential oil of Angelica larvae, 4 to 60% by weight of lavender essential oil, 10 to 30% by weight of rosemary essential oil, 10 to 30% by weight of geranium essential oil, 1 to 10% by weight of Eosongcho essential oil, neroli essential oil 1 to 10% by weight and 1 to 10% by weight of jasmine essential oil to prepare a blended natural essential oil, 5 to 15% by weight of plum seed oil, 15 to 25% by weight of tea seed oil, 25 to 35% by weight of citron seed oil , A method for producing a face oil comprising the steps of preparing a blended seed oil by mixing 35 to 45 wt% of camellia seed oil, and preparing a face oil by mixing the blended natural essential oil and the blended seed oil to provide a way

In order to solve the above problems, the present invention provides 30 to 50% by weight of seed oil (a), including plum seed oil, tea seed oil, citron seed oil and camellia seed oil, and Angelica keiskei essential oil, lavender essential oil in one embodiment. , Rosemary essential oil, geranium essential oil, Eoseongcho essential oil, neroli essential oil and jasmine essential oil, it provides a face oil composition comprising 0.1 to 10% by weight of a natural essential oil (b).

The face oil composition of the present invention contains 30 to 50% by weight of seed oil, including plum seed oil, tea seed oil, citron seed oil and camellia seed oil, and Angelica keiskei essential oil, lavender essential oil, rosemary essential oil, geranium essential oil, eoseongcho essential oil, 0.1 to 10% by weight of natural essential oils, including neroli essential oil and jasmine essential oil.

In the present invention, "plum" is the fruit of the plum tree ( Prunus mume Siebold & Zucc. ). The plum tree is a deciduous small arboreous tree belonging to the Rosaceae family, and its origin is China. It is distributed in Korea, Japan, and China, and the flower is called plum. The plum tree is about 5-10m high, and the bark is yellowish white, and there are greenish white and red colors. Small branches are hairy or not, and the leaves are alternate phyllotaxis, egg-shaped or broad egg-shaped, and the length is 4~10cm. It has sharp saw teeth on the edge, hairs on both sides, and lines on the petiole.

"Plum seed oil" of the present invention is oil obtained by cold-pressing plum seeds, and "plum seeds" in the present invention are plum seeds separated from by-products remaining after distillation of plum fruits, and seeds (seeds) from which the seed coat has not been removed. However, preferably, the seed coat (shell) may be removed. In addition, the plum seeds may be dried after steaming.

In an embodiment of the present invention, the plum fruit was distilled for 13 hours, the plum seeds including the seed coat and seeds were separated from the distillation extraction by-product of the plum fruit, and the plum seeds obtained by removing the seed coat (shell) from the plum seeds were obtained. After steaming, it was dried. The dried plum seeds were cold-pressed at a temperature of 70 to 80° C. to extract plum seed oil.

Therefore, the plum seeds may be separated from by-products remaining after distilling and extracting plum fruits for 10 to 15 hours. If the plum fruit is distilled and extracted, the seeds or seeds from the by-product can be more easily separated from the plum fruit that has not been distilled, so it is possible to reduce the time and manpower required to separate the plum seeds or seeds, and also to extract the plum fruit It is economical as it is produced using the remaining by-products.

Plum fruits contain toxic cyanide compounds, specifically amygdalin. The amygdalin is a type of cyan glycoside, and is decomposed into hydrogen cyanide (HCN) known as cyanide by β-glucosidase of intestinal bacteria. , can cause convulsions.

In the plum seed of the present invention, the cyan glycosides in the plum seeds are dissolved in water during the distillation extraction process of the plum fruits, or the enzyme is inactivated for a long time heating, so that toxicity does not occur, and the cyan glycosides are separated or decomposed into other components become volatilized

Therefore, the plum seeds separated from the by-products remaining after distilling the plum fruit are not toxic by cyanic glycosides. In addition, since the oil is produced by cold-pressing the plum seeds from which the toxicity has been removed through this process at 70 to 80° C., it is possible to produce a stable and functional oil.

The plum seed oil has aging, wrinkle improvement, dryness, sensitivity, anti-inflammatory, and skin softening effects.

In the present invention, "tea" is Camellia sinensis and belongs to the family Theaceae , and green tea, black tea, oolong tea, etc. are produced from the leaves. The green tea, unlike black tea or oolong tea, does not enter the fermentation process of tea leaves, and is obtained by heat-treating fresh and young tea leaves to inactivate oxidation-related enzymes and stably maintaining polyphenol components.

It is known that 30-40% of polyphenols found in tea are flavonols and catechins, and the main components of green tea catechins are epicatechin, epicatechin-3-gallate, and epigallocatechin. (epigallocatechin) and epigallocatechin-3-gallate (EGCG), and among them, the content of epigallocatechin-3-gallate component is known to be the highest.

The polyphenol component of the tea is known to have various efficacy effects such as antioxidant, anticancer, anti-inflammatory, and antibacterial.

In the present invention, "tea seed oil" is an oil extracted by cold pressing the seeds of a tea tree, and "tea seed" in the present invention is a seed obtained by drying tea fruits harvested from a tea tree and then removing the rind, and the seed coat. It includes seeds (seeds) that have not been removed, but may preferably be those from which the seed coat (husk) has been removed. In addition, the tea seeds may be dried after steaming.

In an embodiment of the present invention, tea seeds were separated by removing the rind and seed coat from the tea fruit, and the tea seeds were steam-treated and dried, and then cold-pressed at 70 to 80° C. to extract tea seed oil.

Accordingly, the tea seed oil of the present invention may be an oil prepared by drying and crushing the tea seeds, followed by cold pressing at 70 to 80° C., followed by extraction and purification.

The tea seed oil has antibacterial and antioxidant effects, and contains catechins to have antibacterial, pore shrinkage, sebum control, and whitening effects.

In the present invention, "citron" is a fruit of a citrus tree (Citrus Junos ), and the citron is well separated from the inside and outside, and as the citron matures, the rind becomes thick and has a bright yellow color. In particular, by using the essential oil component of the fruit skin, the fruit peel is used for beverages and flavorings rather than the flesh. Among essential oil components, limonene has an antibacterial effect, and phenol and flavonoid substances have antioxidant effects, so they are being used as folk remedies for detoxification, cough and cold.

In the present invention, “citron seed oil” is an oil extracted by cold-pressing citron seeds. In the present invention, “citron seed” is a seed separated from a by-product after distillation of citron fruit, and the seed coat (shell) is not removed. Contains unstained seeds (seeds). In addition, the citron seeds may be dried after steaming.

In an embodiment of the present invention, the citron fruit was distilled for 13 hours, and the citron seed including the seed coat and seeds was separated from the distillation extraction by-product of the citron fruit. Citron seeds were difficult to remove because the thickness of the seed coat was thin, so seeds (seeds) from which the seed coat was not removed were used. After the citron seeds were steamed and dried, citron seed oil was extracted by cold pressing at 70 to 80°C.

Therefore, the citron seeds are characterized in that the citron fruit is distilled and extracted for 10 to 15 hours and separated from the remaining by-products. When the citron fruit is distilled and extracted, the seeds or seeds are easily separated from the by-products, thereby reducing the time and manpower required to separate the citron seeds or seeds.

The citron seed is rich in natural flavor and essential oil, and the pulp contains amino acids, free sugars, organic acids, etc., and the citron seed oil has astringent, waste removal, keratin removal, whitening, and skin softening effects.

In the present invention, "camellia" ( Camellia japonica L. ) is an evergreen broad-leaved arboreous tree belonging to the Aceae family, but it often looks like a shrub due to its slow growth rate. It is usually about 7m tall, but some camellia trees grown in an environment suitable for growth are 18m tall and have a circumference of 2.8m at breast height. Seeds are dark brown ellipsoids and mature in late autumn. The oil obtained by pressing the seeds of camellia is extracted, and this oil is used as a hair oil, precision machine oil, and a substitute for olive oil in the pharmaceutical industry, and the refined oil has been used for cooking.

In the present invention, “camellia seed oil” is an oil extracted by cold-pressing camellia seeds. It may include a seed (seed), but preferably, the seed coat (shell) may be removed. In addition, the camellia seeds may be dried after steaming.

In an example of the present invention, camellia seeds were separated by removing the pericarp and seed coat from the camellia fruit, and the camellia seed oil was extracted by cold pressing at 70 to 80° C. after steaming and drying the camellia seeds.

Therefore, the camellia seed oil of the present invention may be an oil prepared by drying and crushing the camellia seeds, extracting and refining them by cold pressing at 70 to 80°C.

The camellia seed oil is used as a massage oil and has moisturizing, soothing, anti-wrinkle and anti-inflammatory effects.

In the present invention, "Cham Angelica gigas " is a herbal name for Angelica (當歸). It is also called Wengui (文歸), Daegeun (大芹), and Geongui (乾歸). Pharmacologically, it promotes blood flow in the coronary arteries and aids in the production of red blood cells.

The "Essential Oil of Angelica Root" of the present invention is distilled and extracted from the dried root of the Angelica Root.

As a result of analyzing the aroma components of the essential oil of Angelica basil in an embodiment of the present invention, n-Nonane, (1R)-(+)-α-Pinene, 2-Bornene, Isobutyl hexanoate, limonene+β-phellandrene, beta-dihydroagarofuran, 8-epi-.gama.-eudesmol, (-)-α-Gurjunene, β-Eudesmol, (E)-2-tetradecene, Z-9-Pentadecenol, and the content of 8-epi-.gama.-eudesmol The highest was confirmed with 5.9%.

Accordingly, the essential oil of Angelica larvae is n-Nonane, (1R)-(+)-α-Pinene, 2-Bornene, Isobutyl hexanoate, limonene+β-phellandrene, beta-dihydroagarofuran, 8-epi-.gama.-eudesmol, ( -)-α-Gurjunene, β-Eudesmol, (E)-2-tetradecene, Z-9-Pentadecenol.

In the present invention, "lavender" is a plant belonging to the genus Labandula, and is native to the Mediterranean coast. It is 30-60cm tall and can grow up to 90cm if properly cared for in the garden. It has white hairs all over, and the stem is dull and square, and the branches are many at the bottom. Leaves are alternate or opposite, lanceolate, 4cm long and 4-6mm wide. There is no petiole, and there are fine hairs on the leaves. Flowers bloom in June-September in light purple or white, and run sporadically in a stipule at the end of a long flower stalk without leaves. Among the hairs that cover flowers, leaves, and stems, there are oil glands that emit fragrance. It grows well in well-drained sandy soil with a little bit of gravel, and soil that is not too fertile is preferred. Grows well in a sunny, south-facing location.

It is cultivated to collect perfume oil from lavender flowers and plants, and is also planted for ornamental purposes. Perfume oil is used as a raw material for perfumes and cosmetics, as a flavoring for cooking, and is also used to treat headaches and nervous stability.

In the present invention, "lavender essential oil" is a distillation extraction of the lavender flower.

As a result of analyzing the fragrance components of lavender essential oil in an embodiment of the present invention, β-Myrcene, β-pinene, γ-Terpinene, Linalool, Linalyl acetate, (±)-Lavandulyl Acetate, Neryl acetate, β-Caryophyllene, Terpinen-4 -ol, cis-β-Farnesene, and (-)-Caryophyllene oxide were included, and Linalool was found to have the highest content at 7.6%.

Therefore, the lavender essential oil of the present invention is β-Myrcene, β-pinene, γ-Terpinene, Linalool, Linalyl acetate, (±)-Lavandulyl Acetate, Neryl acetate, β-Caryophyllene, Terpinen-4-ol, cis-β-Farnesene, Contains (-)-Caryophyllene oxide.

In the present invention, "rosemary essential oil" is a distillation extraction of the rosemary.

As a result of analyzing the aroma components of rosemary essential oil in an embodiment of the present invention, D-(+)-alpha-pinene, Camphene, p-Cymene, Linalool, (±)-camphor, isoborneol, Cyclohexen, Geraniol, alpha-fenchyl acetate , β-Caryophyllene was included, and it was confirmed that the content of p-Cymene was the highest at 9.5%.

Accordingly, the rosemary essential oil includes D-(+)-alpha-pinene, Camphene, p-Cymene, Linalool, (±)-camphor, isoborneol, Cyclohexen, Geraniol, alpha-fenchyl acetate, and β-Caryophyllene.

In the present invention, "geranium" may be a rose geranium (Pelargonium capitatum) specifically as a perennial herb of the family Lepidoptera. The rose geranium is a small shrub or perennial plant that grows about 1 m in height. Some white hairs grow densely all over. The leaves are 5-10 cm wide, heart-shaped, ovate or kidney-shaped. The edge of the leaf is toothy, and it is bright green, hard, rough, and has a rose scent. Flowers pink and white from summer to autumn. There are 5 petals with a dark reddish-brown pattern in the middle. Scented Geranium (Scented Geranium) is the most well-known species and is known to have antidepressant, tonic, and bactericidal effects. In particular, rose geranium, which has a rose scent, is widely used as a fragrance material for perfumes, cosmetics, and soaps.

In the present invention, "geranium essential oil" is a distillation extraction of the geranium. Specifically, it may be a distillation extraction of rose geranium outpost.

As a result of analyzing the fragrance component of rose geranium essential oil in an embodiment of the present invention, Linalool, Menthone, iso-Menthone, Geraniol, Citronellol, Geranyl formate, ?-Bourbonene, Caryophyllene oxide and Geranyl tiglate are included, and the content of Geraniol is 37.5% was found to be the highest.

Therefore, the rose geranium essential oil includes Linalool, Menthone, iso-Menthone, Geraniol, Citronellol, Geranyl formate, ?-Bourbonene, Caryophyllene oxide and Geranyl tiglate.

In the present invention, “eoseongcho” is a medicinal herb called yakmomil, and it was named eoseongcho because the leaves smell fishy. It grows in shady forests. Underground stems are long, thin, and white. Stems are upright, 20-50cm high, have several vertical lines, and smell. The leaves are alternate phyllotaxis, 3~8cm long, have a sharp tip, have a flat edge, and stipules are attached to the lower part of the petiole. Use the plant before flowering as a diuretic and insect repellent, crush the leaves and apply to boils and poisonous insect bites. In folk medicine, it is used for swelling, suppuration, and hemorrhoids, and in oriental medicine, the plant is used for gonorrhea, enteritis, urinary tract infection, pneumonia, and bronchitis. The leaves are similar to those of buckwheat and are medicinal plants, so it is called Yakmomil.

"Eoseongcho essential oil" in the present invention is a distillation extraction of the eoseongcho outpost.

As a result of analyzing the fragrance component of Eoseongcho essential oil in an embodiment of the present invention, it contains 1-nonanol, Decanal, 2-Undecanone, Geranyl acetate, Dodecanal, Decanoic acid, 3-oxodecanal, Caryophyllene oxide, L-Ascorbic acid and Linoleic Acid. And it was confirmed that the content of Decanoic acid was the highest at 8.2%.

Therefore, the essential oil of Eoseongcho contains 1-nonanol, Decanal, 2-Undecanone, Geranyl acetate, Dodecanal, Decanoic acid, 3-oxodecanal, Caryophyllene oxide, L-Ascorbic acid and Linoleic Acid.

In the present invention, "neroli essential oil" is an essential oil extracted by steam distillation (a method of extracting an aromatic active ingredient of a plant with steam and cooling it with cooling water to condense it) or a solvent extraction method from the flowers of the orange bitter tree, which is a plant of the rutaceae family. It is a pale yellow, low-viscosity liquid, with a rich and intense fragrance, with a soft floral and fresh citrus notes, and belongs to the top and middle notes. The main chemical composition consists of alcohols such as linalool, α-terpineol and nerol, monoterpenes of limonene, and esters of linalyl acetate. have. It promotes positive thinking, improves self-confidence and happiness, reduces anxiety and tension caused by stress by calming and relaxing the mind and body, and is effective in relieving depression and insomnia. It helps relieve diarrhea, colitis, and colic in babies due to nervous tension, relieves varicose veins by helping circulation, and is useful for relieving high blood pressure and heart palpitations due to its sedative action.

As a result of analyzing the fragrance component of neroli essential oil in an embodiment of the present invention, it contains Limonene, (E)-nerolidol, alpha-terpineol, alpha-terpinyl acetate and (E, E)-farnesol, and the content of Limonene was 27.5%. was found to be the highest.

Accordingly, the neroli essential oil includes Limonene, (E)-nerolidol, alpha-terpineol, alpha-terpinyl acetate and (E, E)-farnesol.

In the present invention, “jasmine” is a plant belonging to the genus Youngchunhwa of the genus of the dicotyledonous plant, Gentian, Ash, and is also called jasmine and jasmine. It is called mali (茉莉) in Chinese characters, and is derived from the Sanskrit word mallik?, originally called malihwa (茉莉花).

The main ingredient in the fragrance of jasmine is methyl jasmonate. Although jasmine flowers contain several fragrance components, among them, cis-jasmon, the only fragrance component that exhibits the fragrance of jasmine, has not yet been industrially produced, and there is only a method to extract and refine it from natural flowers. For this reason, cis-jasmon-based spices are very expensive. Rather than that, methyl jasmonic acid-based fragrances with established industrial production methods can be purchased relatively inexpensively, and are generally widely distributed as perfumes and aromatic oils.

In the present invention, “jasmine essential oil” is an essential oil extracted from jasmine flowers by a solvent extraction method, and may be specifically extracted by cooling in jojoba oil. Jasmine oil has aphrodisiac, hormone control, menopausal symptoms relief, relaxation (relaxation), antidepressant, psychological balance and hypnotic effects.

As a result of analyzing the fragrance component of jasmine essential oil in an embodiment of the present invention, it contains Benzyl acetate, Benzyl benzoate, Benzyl alcohol, Linalool, Indole, (-)0Jasmonlactone, (-)Methyljasmonate, (+)-epi-methyljasmonate, and Benzyl It was confirmed that the content of acetate was the highest at 34%.

Accordingly, the jasmine essential oil includes Benzyl acetate, Benzyl benzoate, Benzyl alcohol, Linalool, Indole, (-)Jasmonlactone, (-)Methyljasmonate, and (+)-epi-methyljasmonate.

In an embodiment of the present invention, a blended seed oil was prepared by adding 10 wt% of plum seed oil, 20 wt% of tea seed oil, 30 wt% of citron seed oil, and 40 wt% of camellia seed oil, and 5 wt. %, lavender essential oil 50% by weight, rosemary essential oil 20% by weight, geranium essential oil 10% by weight, eoseongcho essential oil 5% by weight, neroli essential oil 5% by weight, and jasmine essential oil 5% by weight were mixed to prepare a blended natural essential oil. An aroma face oil was prepared by mixing the blended seed oil, blended natural essential oil, base oil, and additives (vitamin E, seabuckson oil) as shown in Table 1.

In order to evaluate the skin efficacy, feel and sensory of the face oil according to the content of the blended seed oil, the content of the blended seed oil is varied from 20 to 60% by weight, and the content of the base oil is adjusted accordingly, and the blended natural essential oil 4 2% by weight of vitamin E and 5% by weight of Sea Buckson oil were added to the weight % to prepare a face oil. In addition, a face oil that does not contain mixed (blended) seed oil and mixed natural essential oil was prepared and comparatively analyzed.

As a result of the skin efficacy, feeling and sensory evaluation of the face oil according to the content of the blended seed oil, when the content of the seed oil was 40% by weight, the fragrance, absorption, soothing effect, and oil adequacy were excellent, and the feeling and sensory evaluation results were excellent. The best was confirmed.

On the other hand, when it was 60% by weight of seed oil (Comparative Example 3), the skin efficacy (melanin, erythema, skin pH, elasticity) was measured to be the lowest, and the face oil without seed oil had the lowest usability and sensory evaluation. Confirmed.

Therefore, the face oil composition of the present invention may contain 30 to 50% by weight of seed oil, specifically 40% by weight.

In addition, the seed oil contains 5 to 15% by weight of plum seed oil, 15 to 25% by weight of tea seed oil, 25 to 35% by weight of citron seed oil, and 35 to 45% by weight of camellia seed oil based on 100% by weight of seed oil. Specifically, it may contain 10% by weight of plum seed oil, 20% by weight of tea seed oil, 30% by weight of citron seed oil, and 40% by weight of camellia seed oil.

The face oil composition of the present invention may contain 0.1 to 10% by weight of natural essential oil, specifically 4% by weight, based on 100% by weight of the total composition.

The natural essential oil is 1 to 10% by weight of chamomile essential oil, 4 to 60% by weight of lavender essential oil, 10 to 30% by weight of rosemary essential oil, 10 to 30% by weight of geranium essential oil, 1 to 10% by weight of essential oil of geranium based on 100% by weight of natural essential oil %, 1 to 10% by weight of neroli essential oil, and 1 to 10% by weight of jasmine essential oil.

In addition, the composition of the present invention may further comprise 39 to 59% by weight of the base oil based on 100% by weight of the total composition. The base oil is grapeseed oil (Grapeseed oil), evening primrose oil (Evening primrose oil), rosehip oil (Rosehip oil), macadamia nut oil (Macadamia nut oil), borage oil (Borage oil), safflower oil ( Safflower oil, Sesame oil, St.Jhon's wort oil, Sweet almond oil, Avocado oil, Apricot kernel oil, Olive oil (Olive oil), Wheatgerm oil (Calendula oil), Carrot oil (Carrot oil), Coconut oil (Coconut oil), Hazel nut oil (Hazel nut oil) and Jojoba oil (Jojoba oil) It may include one or more oils selected from the group consisting of.

In the present invention, "grapeseed oil" is an oil extracted from grape seeds, which is very light, has no fragrance, and is easily absorbed into the skin. It contains vitamins and hardly irritates the skin, so it is good for oily skin with a lot of acne. It is often used as a carrier oil because it can stay in that condition for several days.

In the present invention, “evening primrose oil” is colorless or pale yellow when extracted from the seeds of evening primrose. Contains a lot of essential fatty acids and γ-linolenic acid. It helps to balance hormones and is effective for premenstrual syndrome (PMS), menstrual pain, and menopausal symptoms. It is also used to relieve rheumatism and arthritis.

In the present invention, "Rosehip oil" is an oil extracted from the fruit of rosehip, which is a kind of wild rose that grows in large quantities in South America or Europe. It is yellow in color and contains large amounts of linoleic and linolenic acids, which are essential fatty acids.

In the present invention, “Macadamia nut oil” is an oil extracted from the fruit of macadamia nut and is not easily oxidized, so it is widely used from cooking to cosmetics.

In the present invention, "borage oil" is a vegetable oil extracted by pressing the seeds of borage, and helps to relieve premenstrual syndrome and menopausal symptoms. It is commonly used as a carrier oil in aromatherapy.

In the present invention, "Safflower oil" is an oil extracted from safflower and is rich in vitamins and minerals.

In the present invention, "Sesame oil" is an oil extracted from raw sesame, and edible sesame oil has a strong flavor because it is roasted and squeezed sesame, but it has no color and flavor because it is extracted raw. This oil is rich in vitamins and minerals, has high oxidative stability and promotes metabolic function.

In the present invention, "St. John's wort oil" is a leaching oil obtained by brewing St. John's flowers in plant oils such as peanut oil or olive oil. It has a pale red color and has excellent analgesic action.

In the present invention, "Sweet almond oil" is a pale yellow oil extracted from almond seeds and has no odor. It has a lot of nutrients and contains a lot of protein, so it has the effect of softening the skin. It contains vitamins D and E and minerals.

In the present invention, “avocado oil” is an oil extracted from avocado fruit and is rich in nutrients such as essential fatty acids and vitamins that are not synthesized in the body.

In the present invention, "Apricot kernel oil" is an oil extracted from apricot seeds, and is rich in minerals including vitamins.

In the present invention, "olive oil" is the extract from the fruit of an olive tree, and contains vitamins A, D, E.

In the present invention, "wheatgerm oil" is a vegetable oil extracted from wheat germ and is infused or extracted with a solvent because it is difficult to extract by a pure cold pressing method. It is viscous, has a characteristic strong odor, and is yellow to brown in color. Also called wheat germ oil, it is rich in vitamins A and B. Because of the antioxidant properties of vitamin E, adding 5% to other base oils can prevent oxidation. It also has an antibacterial effect.

In the present invention, "Calendula oil" is a leaching oil prepared by putting marigold flowers in sunflower oil and the like.

In the present invention, "Carrot oil" is an orange or red color obtained by brewing and extracting the roots of wild carrots in other plant oils. It is characterized by containing kerotene and vitamins A and C.

In the present invention, "coconut oil" is extracted from the dried flesh of coconut, and it is coagulated indoors and has a buttery texture. It is very light to use and has excellent moisturizing effect on the skin, preventing dryness. In addition, it is widely used for hair care because it supplies adequate oil to the hair. However, if you have sensitive skin, do a patch test before use.

In the present invention, “Hazel nut oil” is an oil obtained by cold-pressing hazel nuts, which penetrates quickly and has a good absorption effect in the skin. Because it has a moisturizing effect, it is often used for skin care and has an effect of removing wastes.

In the present invention, “Jojoba oil” refers to the jojoba oil extracted by pressing the seeds of jojoba in the form of a liquid wax. Because the chemical structure is similar to that of human skin, it penetrates the skin very well and is not sticky, so it feels good to use. It is not oxidized well compared to other base oils, so it can be stored for a long time, and it has sebum control and anti-inflammatory effects.

In an embodiment of the present invention, 15% by weight of Wheatgerm oil, 10% by weight of Evening primrose oil, 25% by weight of Hazel nut oil and 50% by weight of Jojoba oil are mixed. to prepare a base oil.

Therefore, the base oil is specifically, Wheatgerm oil, evening primrose oil, hazel nut oil (Hazel nut oil) and a base oil containing jojoba oil (Jojoba oil) 39 to 59% by weight of the base oil. It may include, more specifically, 15% by weight of Wheatgerm oil, 10% by weight of Evening primrose oil, 25% by weight of Hazel nut oil, and 50% by weight of Jojoba oil can be included as

In order to solve the above problems, the present invention provides 1 to 10% by weight of Angelica keiskei essential oil, 4 to 60% by weight of lavender essential oil, 10 to 30% by weight of rosemary essential oil, 10 to 30% by weight of geranium essential oil, and 1 to 10% by weight, preparing a blended natural essential oil by mixing 1 to 10% by weight of neroli essential oil and 1 to 10% by weight of jasmine essential oil, 5 to 15% by weight of plum seed oil, 15 to 25% by weight of tea seed oil, yuzu A step of preparing a blended seed oil by mixing 25 to 35 wt% of seed oil and 35 to 45 wt% of camellia seed oil, and preparing a face oil by mixing the blended natural essential oil and blended seed oil A method for preparing a face oil is provided.

The method for preparing the face oil of the present invention includes 1 to 10% by weight of chamomile essential oil, 4 to 60% by weight of lavender essential oil, 10 to 30% by weight of rosemary essential oil, 10 to 30% by weight of geranium essential oil, 1 to 10% by weight of essential oil, Preparing a blended natural essential oil by mixing 1 to 10% by weight of neroli essential oil and 1 to 10% by weight of jasmine essential oil, 5 to 15% by weight of plum seed oil, 15 to 25% by weight of tea seed oil, 25 to 25% by weight of citron seed oil 35% by weight and 35 to 45% by weight of camellia seed oil are mixed to prepare a blended seed oil, and the blended natural essential oil and blended seed oil are mixed to prepare a face oil.

In the present invention, "distillation extraction" is a method of extracting essential oil by distilling steam, and includes water distillation, water-steam distillation, and steam distillation.

The water distillation method is a method of separating oil and water after cooling the steam and essential oil generated by heating raw materials for oil extraction in water. Because the raw material is immersed in boiling water, it does not come into direct contact with water vapor.

The water-steam distillation method is a method of depositing raw materials for oil extraction on a grid installed inside the distillation unit and heating water from the bottom to extract the separated volatile essential oil components mixed with the steam as the distilled steam passes through the sample. Since plant raw materials do not come into contact with water, they have the advantage of not being overheated, so they are suitable for some seeds, fruits, pericarp, some flowers, outposts, and leaves that mainly require a medium boiling point.

Steam distillation is the most common method of extracting essential oil by putting raw materials in a distillation kiln and blowing steam from the bottom. It is a distillation method that mainly requires a low boiling point. Since the steam distillation method extracts essential oil with steam (water), it is almost nontoxic and has the advantage of being safe for skin application. However, although the chemical composition of the essential oil may be changed due to the high temperature, if the steam distillation method is used, it is possible to extract the essential oil and obtain a hydrosol having aromatherapy effect at the same time.

In an embodiment of the present invention, essential oil was extracted by chilling jasmine flowers in jojoba oil, nenoli or lavender essential oil was extracted by distilling nenoli flowers or lavender flowers, and dried roots of jasmine angelica were distilled and extracted Extracted, and distillation extraction of eoseongcho, rosemary or rose geranium outpost to prepare essential oil, 5% by weight of the chamomile essential oil, 50% by weight of lavender essential oil, 20% by weight of rosemary, 10% by weight of geranium, 5% by weight of eoseongcho, neroli A blended natural essential oil was prepared by mixing 5% by weight and 5% by weight of jasmine.

Therefore, the step of preparing the blended natural essential oil is 1 to 10% by weight of Angelica larvae essential oil, 4 to 60% by weight of lavender essential oil, 10 to 30% by weight of rosemary essential oil, 10 to 30% by weight of geranium essential oil, and 1 to 10% by weight of essential oil of Eoseongcho. , 1 to 10% by weight of neroli essential oil and 1 to 10% by weight of jasmine essential oil are mixed.

In addition, the chamomile essential oil, lavender essential oil, rosemary essential oil, geranium essential oil, eoseongcho essential oil, or neroli essential oil is steam distillation extraction of chamomile, lavender, rosemary, geranium, eoseongcho or neroli, and the jasmine essential oil chills jasmine with jojoba oil. may be extracted.

In an embodiment of the present invention, plum seeds and citron seeds were separated from the by-product obtained by distillation of plum fruits or citron fruits, and the separated plum seeds or citron seeds were steam-treated, dried, and then cold-pressed at 70 to 80° C. to obtain plum seed oil. Alternatively, citron seed oil was prepared. In addition, the rind was separated from the tea fruit and the camellia fruit, and only the seeds were separated by removing the seed coat. Camellia seed oil was prepared.

A blended seed oil was prepared by adding and mixing 10 wt% of the above-prepared plum seed oil, 20 wt% of tea seed oil, 30 wt% of citron seed oil and 40 wt% of camellia seed oil.

Therefore, the “step of preparing the blended seed oil” is a method of mixing 5 to 15% by weight of plum seed oil, 15 to 25% by weight of tea seed oil, 25 to 35% by weight of citron seed oil, and 35 to 45% by weight of camellia seed oil. Specifically, it may be mixed with 10% by weight of seed oil, 20% by weight of tea seed oil, 30% by weight of citron seed oil and 40% by weight of camellia seed oil.

In addition, the manufacturing method of the present invention includes the steps of extracting plum seed oil by separating plum seeds from a plum fruit distillation by-product, and extracting citron seed oil by separating citron seeds from a citron fruit distillation extraction by-product. Blended seed oil It may be further included before the manufacturing step.

Extracting the seed oil may be extracting the oil by cold pressing at 70 to 80 ℃.

In an example of the present invention, a base oil was prepared by mixing 15% by weight of wheat point oil, 10% by weight of evening primrose oil, 25% by weight of hazelnut oil, and 50% by weight of jojoba oil.

Therefore, the manufacturing method of the present invention may further include mixing a base oil comprising 15% by weight of wheat oil, 10% by weight of evening primrose oil, 25% by weight of hazelnut oil and 50% by weight of jojoba oil. The step of mixing the base oil may be performed after the step of preparing the blended natural essential oil.

The blended seed oil (20 to 60% by weight), the blended natural essential oil (4% by weight), the base oil and the additives (vitamin E, Seabuckson oil) in the above-described embodiment to prepare an aroma face oil, and the blended seeds As a result of evaluating the skin efficacy, feeling of use and sensory of the face oil according to the oil content, it was confirmed that when the content of seed oil was 40% by weight, the fragrance, absorbency, soothing effect, and oil adequacy were excellent, and the feeling and sensory evaluation results were the best. did.

On the other hand, when it was 60% by weight of seed oil (Comparative Example 3), the skin efficacy (melanin, erythema, skin pH, elasticity) was measured to be the lowest, and the face oil without seed oil had the lowest usability and sensory evaluation. Confirmed.

Therefore, the step of preparing the face oil of the present invention is characterized by mixing the blended natural essential oil and the blended seed oil. Specifically, the blended seed oil is blended with 30 to 50 wt% with respect to 100 wt% of the total face oil composition. It may be to mix 0.1 to 10% by weight of the natural essential oil, and more specifically, 40% by weight of the blended seed oil and 4% by weight of the blended natural essential oil.

The present invention includes plum seed oil, tea seed oil, citron seed oil, and camellia seed cold-pressed oil, and Angelica asiatica essential oil, lavender essential oil, rosemary essential oil, geranium essential oil, eoseongcho essential oil, neroli essential oil and jasmine essential oil, It has excellent soothing effect and aroma.

1 shows the manufacturing process of natural essential oil.
2 is a schematic diagram of the production process of seed oil of citron or plum.
3 shows the separation process of the seeds (seeds) of each fruit from the by-product obtained by distilling the citron fruit or the plum fruit.
4 is a photograph of seeds separated from the distillation extraction by-product of plum fruits.
5 is a photograph of citron seeds separated from citron fruit distillation extraction by-products.
6 is a photograph of the process of separating tea seeds from tea fruit.
7 shows a process for producing seed oil by cold-pressing citron seeds, plum seeds, tea seeds or camellia seeds.
8 is a schematic diagram of a method for producing a face oil of the present invention.

Hereinafter, the configuration and effects of the present invention will be described in more detail through examples. These examples are only for illustrating the present invention, and the scope of the present invention is not limited by these examples.

<Preparation Example 1> Preparation of natural essential oil

Using the aromatic essential oil water vapor distillation apparatus (Korea Patent No. 10-1105539), neroli essential oil, lavender essential oil, chamomile essential oil, eoseongcho essential oil, rosemary essential oil, and geranium essential oil were prepared, respectively.

Neroli essential oil and lavender essential oil were prepared by distilling and extracting flowers, the root of Angelica larvae was used, and the essential oil of Eoseongcho, rosemary and geranium was used from outpost.

On the other hand, for jasmine essential oil, 40 g of jasmine flower natural essential oil was added to 60 ml of jojoba oil and cold-chilled essential oil was performed for 1 week (Fig. 1).

<Preparation Example 2> Preparation of seed oil

Plum fruits (including flesh and seeds) or citron fruits (including flesh and seeds) were distilled for 13 hours. Plum seeds or citron seeds were separated from each distillation by-product separated by distillation extraction (FIGS. 2 and 3).

Plum seeds were obtained by removing the seed coat (shell) from the separated plum seeds, and the plum seeds were used as seeds for oil extraction (FIG. 4). The citron seed had a thin seed coat (shell), so the seed itself was used as a seed for oil extraction (FIG. 5).

Camellia seeds or tea seeds were prepared by removing the rind of the camellia fruit and tea fruit, and then separating the camellia seeds or tea seeds by removing the seed coat (husk) from the camellia seeds or tea seeds, drying them, and crushing them to prepare seeds for oil extraction ( Fig. 6).

The seeds for oil extraction (plum seeds, citron seeds, tea seeds, and camellia seeds) were each steam-treated and then dried and used for oil extraction.

The plum seeds, citron seeds, camellia seeds or tea seeds were cold-pressed at a temperature of 70 to 80 ° C. to extract oil, and then purified to prepare plum seeds, citron seeds, camellia seeds or tea seed oil (FIG. 7) .

<Preparation Example 3> Preparation of face oil

3-1. Manufacture of blended natural essential oil for aromatherapy with functionality

Natural essential oil blended by mixing 5% by weight of essential oil prepared in Preparation Example 1, 50% by weight of lavender essential oil, 20% by weight of rosemary, 10% by weight of geranium, 5% by weight of seaweed, 5% by weight of neroli, and 5% by weight of jasmine was prepared.

3-2. Preparation of blended seed oil

10 wt% of plum seed oil prepared in Preparation Example 2, 20 wt% of tea seed oil, 30 wt% of citron seed oil and 40 wt% of camellia seed oil were added and mixed to prepare a blended seed oil.

3-3. Preparation of blended base oil for skin massage

As a base oil for massage, 15% by weight of wheat point oil, 10% by weight of evening primrose oil, 25% by weight of hazelnut oil, and 50% by weight of jojoba oil were mixed.

3-4. manufacture of face oil

An aroma face oil was prepared by mixing the blended seed oil, blended natural essential oil, base oil, and additives (vitamin E, seabuckson oil) as shown in Table 1 (FIG. 8).

To compare the effect of face oil according to the difference in the content of seed oil, face oil was prepared by varying the content of seed oil in an amount of 20 to 60% by weight of the total composition, and 4% by weight of natural essential oil was mixed. In addition, Comparative Example 1 was prepared so as not to include both natural essential oil and seed oil.

division Comparative Example 1 Comparative Example 2 Example 1 Comparative Example 3 natural
essential oil Aroma natural essential oil composition ratio (%): Angelica basil 5 + Lavender 50 + Rosemary 20 + Geranium 10 + Eoseongcho 5 + Neroli 5 + Jasmine 5 0 4 4 4 strain
oil Blended seed oil composition (%) : Plum 10 + Tea seed 20 + Citron 30 + Camellia 40 0 20 40 60 base oil Blending oil composition (%): Wheat oil 15+ Evening primrose oil 10+ Hazelnut oil 25+ Jojoba oil 50 93 69 49 29 additive vitamin E 2 2 2 2 Sea Buckson Oil 5 5 5 5 Sum(%) 100 100 100 100

<Experimental Example 1> Analysis of fragrance components and content of natural essential oil

GC-MASS was performed to analyze the fragrance component and content of each essential oil.

Table 2 shows the results of analyzing the content of jasmine fragrance components, fragrance characteristics, and uses.

Table 3 shows the results of analyzing the content of fragrance components, fragrance characteristics, and uses of nenoli essential oil.

Table 4 shows the results of analyzing the content, fragrance characteristics, and uses of fragrance components of lavender flower essential oil.

Table 5 shows the results of analyzing the content of aroma components, aroma characteristics, and uses of the essential oil of Angelica basilica.

Table 6 shows the results of analyzing the content, fragrance characteristics, and uses of fragrance components of Eoseongcho essential oil.

Table 7 is the result of analyzing the content of the fragrance component of the essential oil of rosemary essential oil, the fragrance characteristic, and the use.

Table 8 shows the results of analyzing the main fragrance components and content of rose geranium essential oil.

<Experimental Example 2> Measurement of skin efficacy of aroma face oil according to the mixing ratio of seed oil

In order to compare the skin effects of aroma face oil according to the blending ratio of seed oil, immediately after washing with soap was used as a control group, and each face oil was taken on the forearm of the experimenter with a cotton swab in a size of 0.5 cm. After 1 hour, 3 hours Skin reactions (melanin, erythema, skin pH and elasticity) over time were analyzed after and after 5 hours.

As a result of the analysis, when the oil of Comparative Example 1 containing only the base oil and additives was applied, the deviation values of melanin, erythema, skin pH and elasticity were measured to be the highest immediately after soap washing and after face oil application, so melanin, erythema, and skin pH And it was confirmed that the effect of improving elasticity was good, and as the content of seed oil increased, the effect on melanin, erythema, skin pH and elasticity was slightly decreased, but skin efficacy (melanin, erythema, skin pH and elasticity) was maintained. It was confirmed that Comparative Example 3 had the lowest deviation value compared with after washing, confirming that melanin, erythema, skin pH and elasticity effects were weak.

<Experimental Example 3> Skin feeling and sensory evaluation of aroma face oil according to the mixing ratio of seed oil

From the above results, it was confirmed that the face oils of Comparative Example 1, Comparative Example 2 and Example 1 had excellent skin efficacy. Next, it was confirmed that the content of seed oil did not affect appearance confirmation (the degree of mixing of oil), skin irritation, and flexibility as a result of feeling and sensory evaluation according to the mixing ratio of seed oil. On the other hand, the odor was measured to be the lowest in Comparative Example 1, and the highest score was obtained in Example 2 containing 40% by weight of seed oil.

Skin rolling effect, elasticity, absorption, soothing effect, oil adequacy and transparency were excellent as the content of seed oil increased. That is, it was confirmed that the face oil having a seed oil content of 40% by weight or more had excellent skin rolling effect, elasticity, absorbency, soothing effect, oil adequacy and transparency.

In the case of Comparative Examples 1 and 2, the skin efficacy (whitening, erythema, skin pH and elasticity) was excellent, but the feeling of use and sensuality were low, so it was not suitable as a face oil, and in the case of Comparative Example 3, the skin efficacy was weak. .

When the skin efficacy, feeling of use and sensory evaluation of the face oil were comprehensively considered, when the content of seed oil was 40% by weight, it was confirmed that the effect of the face oil was excellent due to the excellent skin effect, odor, absorption, soothing effect, and oil compatibility. .

Claims (9)

A face oil composition comprising seed oil, natural essential oil and base oil,
The seed oil contains 5 to 15% by weight of plum seed oil, 15 to 25% by weight of tea seed oil, 25 to 35% by weight of citron seed oil, and 35 to 45% by weight of camellia seed oil based on 100% by weight of seed oil,
The natural essential oil is 1 to 10% by weight of chamomile essential oil, 4 to 60% by weight of lavender essential oil, 10 to 30% by weight of rosemary essential oil, 10 to 30% by weight of geranium essential oil, 1 to 10% by weight of essential oil of geranium based on 100% by weight of natural essential oil %, 1 to 10% by weight of neroli essential oil, and 1 to 10% by weight of jasmine essential oil.
In claim 1,
A face oil composition comprising 30 to 50% by weight of the seed oil and 0.1 to 10% by weight of the natural essential oil based on the total weight% of the composition.
delete delete In claim 1,
The base oil is a face oil composition comprising 15% by weight of wheat point oil, 10% by weight of evening primrose oil, 25% by weight of hazelnut oil and 50% by weight of jojoba oil based on 100% by weight of the base oil. 6. In any one of claims 1, 2 and 5,
The plum seed oil is manufactured by cold pressing using plum seeds separated from the by-products remaining after distilling and extracting plum fruits, and the citron seed oil is cooled using citron seeds separated from the remaining by-products after distilling and extracting citron fruits. manufactured by pressing,
face oil composition.
1 to 10% by weight of Angelica larvae essential oil, 4 to 60% by weight of lavender essential oil, 10 to 30% by weight of rosemary essential oil, 10 to 30% by weight of geranium essential oil, 1 to 10% by weight of essential oil of Eoseongcho, 1 to 10% by weight of neroli essential oil, and jasmine Preparing a blended natural essential oil by mixing 1 to 10% by weight of the essential oil;
Preparing a blended seed oil by mixing 5 to 15% by weight of plum seed oil, 15 to 25% by weight of tea seed oil, 25 to 35% by weight of citron seed oil, and 35 to 45% by weight of camellia seed oil; and
Mixing the blended natural essential oil and the blended seed oil with a base oil to prepare a face oil,
Method for manufacturing face oil.
In claim 7,
The chamomile essential oil, lavender essential oil, rosemary essential oil, geranium essential oil, eoseongcho essential oil, or neroli essential oil is steam distillation extraction of chamomile, lavender, rosemary, geranium, eoseongcho or neroli,
The jasmine essential oil is extracted by cooling jasmine with jojoba oil,
Method for manufacturing face oil. In claim 7,
In the step of preparing the face oil, 30 to 50 wt% of the blended seed oil and 0.1 to 10 wt% of the blended natural essential oil are mixed with respect to 100 wt% of the total face oil composition,
Method for manufacturing face oil.

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