KR102174199B1 - Manufacturing method for fermented oil of houttuynia cordata comprising wood-cultivated ginseng ingredient and fermented oil of houttuynia cordata manufactured by the same - Google Patents

Abstract

The present invention relates to a method for producing fermented Houttuynia cordata oil comprising a wood-cultivated ginseng ingredient, and fermented Houttuynia cordata oil produced thereby. The method for producing fermented Houttuynia cordata oil comprising a wood-cultivated ginseng ingredient, according to the present invention, includes the following steps: preparing and washing a wood-cultivated ginseng, pulverizing the washed wood-cultivated ginseng, heating and steaming the pulverized wood-cultivated ginseng with steam, drying the steamed wood-cultivated ginseng, and extracting the dried wood-cultivated ginseng to produce a wood-cultivated ginseng extract; preparing and washing Houttuynia cordata, steaming the washed Houttuynia cordata with steam, drying the steamed Houttuynia cordata, and heating and roasting the dried and washed Houttuynia cordata and then cooling the same; spraying the wood-cultivated ginseng extract, minerals, and a lactic acid bacteria culture solution, to the cooled Houttuynia cordata and mixing the same; fermenting the Houttuynia cordata mixed with the wood-cultivated ginseng extract, the minerals, and the lactic acid bacteria culture solution; drying the fermented Houttuynia cordata with cold air; extracting the cold-air dried Houttuynia cordata to produce oil; and purifying the oil by a filter to produce refined fermented oil. Due to said feature, the present invention provides fermented oil which includes ingredients of wood-cultivated ginseng and Houttuynia cordata, thereby allowing users to easily intake active ingredients of wood-cultivated ginseng and Houttuynia cordata, and can produce fermented Houttuynia cordata oil which can be effectively used as an additive in cosmetics or health functional foods.

Description

Manufacturing method of fermented Eoseongcho oil containing wild ginseng ingredients, and fermented Eoseongcho oil produced by this method TECHNICAL FIELD OF THE INVENTION

The present invention relates to a method for producing fermented Eoseongcho oil containing wild ginseng components and to a fermented Eoseongcho oil produced thereby, and more particularly, by preparing a fermented oil including wild ginseng and Eoseongcho ingredients, the active ingredients of wild ginseng and Eoseongcho are easily The present invention relates to a method for preparing fermented Eoseongcho oil containing wild ginseng ingredients that can be consumed in a healthy manner and effectively used as additives such as cosmetics or health functional foods, and fermented Eoseongcho oil produced thereby.

Fat, including vegetable oils, is one of the three important nutrients that create energy for humans. However, if fat is not digested, absorbed and discharged smoothly in the human body, it causes disorders in health and body functions and is an important cause of lifestyle changes. This is because oxygen is used to burn and decompose fat during fat metabolism in the body, and energy is generated through this process, but active oxygen is generated. Therefore, it is necessary to improve the antioxidant function of vegetable oils and fats, thereby minimizing the generation or influence of active oxygen during metabolism of vegetable oils.

In order to throw a conventional vegetable oil, it is obtained by roasting seeds or nuts, which are raw vegetable oils, at a high temperature (after roasting) and then milking at a high temperature again. In the production of conventional vegetable oils, vegetable oils are produced through the processes of selecting raw materials, washing and drying, then roasting, cropping, filtration, collecting and filling. In this method, benzopyrene, a carcinogen, is generated due to two high-temperature treatment processes in roasting and collecting, and there are many problems such as rancidity within the shelf life due to transformation of vegetable fat. Therefore, it is necessary to develop vegetable oils that have high antioxidant activity and can lower the likelihood of rancidity.

Meanwhile, fermentation refers to a process in which microorganisms decompose organic matter using their own enzymes. The difference between fermentation reaction and decay reaction is that fermentation is a process in which substances useful in human life, including health and taste, are made, whereas decay is a process by which odors or harmful substances are produced. Since ancient times, humans have frequently used fermentation in the manufacture of food. Kimchi, yogurt, soybean paste, and red pepper paste that are widely used are all foods made using fermentation. In addition to traditional fermented foods, many fermented foods, health foods, medicines, cosmetics, etc., which are intended to increase more beneficial ingredients by fermentation, are being developed.

Domestic registered patent No. 10-1276789 (registered on June 13, 2013) Domestic registered patent No. 10-1080076 (registered on October 31, 2011) Korean Patent Publication No. 10-2019-0029296 (published on March 20, 2019)

The present invention is a fermented oil containing wild ginseng components that can be easily ingested with the active ingredients of wild ginseng and eoseongcho by preparing fermented oil including wild ginseng and eoseongcho components, and can be effectively used as additives such as cosmetics or health functional foods. It is to provide a method of manufacturing and fermented Eoseongcho oil produced thereby.

Various problems to be solved by the present invention are not limited to the problems mentioned above, and other problems that are not mentioned will be clearly understood by those skilled in the art from the following description.

The method for preparing fermented oil of Eoseongcho containing wild ginseng according to the present invention comprises preparing wild ginseng and then washing, pulverizing the washed wild ginseng, heating the pulverized wild ginseng with steam to steam, and drying the steamed wild ginseng. , Extracting the dried wild ginseng to prepare a wild ginseng extract, preparing and washing Eoseongcho, steaming the washed Eoseongcho with steam, drying the steamed Eoseongcho, heating the dried Eoseongcho and cooling it And, the sanyangsam extract, mineral, and lactic acid bacteria culture solution are sprayed and mixed in the cooled Eoseongcho, and the Eoseongcho mixed with the sanyangsam extract, mineral and lactic acid bacteria culture solution is fermented, and the fermented Eoseongcho is cold-air dried, and the cold-air dried Eoseongcho is extracted to prepare oil, and the oil is purified with a filter to prepare refined fermented oil, and in the step of drying the steamed wild ginseng, drying of the steamed wild ginseng is 5-10 at a temperature of 50 to 55°C. In the step of steaming the washed Eoseongcho with steam, the steaming is performed by heating the washed Eoseongcho with water vapor at a temperature of 145 to 155°C and a pressure of 4 to 5kgf/cm ² for 20 to 40 minutes, and , In the step of drying the steamed Eoseongcho, the drying is performed by drying the Eoseongcho at a temperature of 18 to 22°C and a humidity of 55 to 60% for 40 to 60 hours, and the sanyangsam extract, minerals and lactic acid bacteria in the cooled Eoseongcho In the step of spraying the culture solution, spraying and mixing in a weight ratio of 3 to 7 parts by weight of the wild ginseng extract, 1 to 3 parts by weight of minerals, and 2 to 6 parts by weight of the lactic acid bacteria culture solution are mixed with respect to 100 parts by weight of the cooled Eoseongcho. In the step of fermenting Eoseongcho mixed with the extract, mineral and lactic acid bacteria culture liquid, the Eoseongcho mixed with the wild ginseng extract, mineral and lactic acid bacteria culture liquid is maintained at a temperature of 40 to 42°C and a humidity of 60 to 62%, and then 5 to 10 Fermented for one day, the fermented fish Cold air drying of the fermented Eoseongcho in the step of cold-air drying the fermented Eoseongcho dry the fermented Eoseongcho for 10 to 20 hours with cold air at a temperature of 3 to 6°C, and maintained at a temperature of 55 to 60°C for 2 to 4 days In the step of producing purified fermented oil by purifying the oil with a filter, the oil is mixed with charcoal activated carbon powder and then stirred for 20 to 40 minutes, and the oil mixed with the charcoal activated carbon powder is filtered through a filter. To prepare a refined Eoseongcho fermented oil, the charcoal activated carbon powder is mixed so as to contain 1 to 5 parts by weight based on the total 100 parts by weight of the oil, and the charcoal activated carbon powder is charcoal activated carbon having a particle size of 10 to 100 mesh A powder is used, and the Eoseongcho fermented oil is contained in a weight ratio of 10 to 20 parts by weight, 5 to 15 parts by weight of sunjit extract, and 3 to 7 parts by weight of inorganic extract, to constitute a shampoo composition, but the sunjit extract is After preparing the mineral, pulverize the pulverized junite mineral to have a particle size in the range of 10 to 300 µm, heat the pulverized pure git by heating at a temperature of 1200 to 1600°C for 1 to 20 minutes, and the heat-treated pure paper The extract was washed with purified water of 30 to 50°C, and mixed in a weight ratio of 200 to 400 parts by weight of Hwangchil tree leaf extract based on 100 parts by weight of the total content of the washed purezit, and then 5 to 10 at a temperature of 60 to 65°C. After storing and aging for a day, separating and removing the sunjit immersed in the Hwangchil tree leaf extract, and centrifuging the Hwangchil tree leaf extract from which the active ingredient of the sunjit is leached, and the lower layer in which the sunjit particles are located , It is prepared through a process of dividing and separating it into a supernatant and a supernatant positioned above the lower layer, and heating the centrifuged supernatant and the supernatant to a temperature of 120 to 130°C, and the hwangchil wood The leaf extract is washed after preparing hwangchil tree leaves, pulverizing the washed hwangchil tree leaves, and the After preparing a mixture by mixing the pulverized Hwangchil tree leaves with a solvent, it is introduced into an ultrasonic extractor to apply ultrasonic waves to the mixture, and is prepared by removing solids contained in the mixture, wherein the solvent is the pulverized It is mixed at a weight ratio of 1000 to 2000 parts by weight based on 100 parts by weight of Hwangchil tree leaves, and as the solvent, any one or more solvents selected from water or alcohols having 1 to 4 carbon atoms (C1 to C4) are used, and 20 to 25°C The ultrasonic wave applied to the mixture at a temperature of and a pressure of 0.1 to 0.5kgf/cm ² is manufactured through a process of extracting using an output of 100 to 200 watts for 30 to 60 minutes at a vibration frequency of 30 to 50 KHz. In addition, the inorganic extract is characterized in that it is included in a weight ratio of 5 to 10 parts by weight of sericite extract, 1 to 5 parts by weight of elvan extract, 3 to 7 parts by weight of ocher extract and 2 to 6 parts by weight of zeolite extract.

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Details of other embodiments are included in the detailed description.

The method for producing fermented Eoseongcho oil containing wild ginseng ingredients according to the present invention is to produce fermented oil including wild ginseng and Eoseongcho ingredients, so that the active ingredients of wild ginseng and Eoseongcho can be easily ingested and used as additives such as cosmetics or health functional foods. Eoseongcho fermented oil that can be effectively used can be prepared.

It will be fully understood that the embodiments of the technical idea of the present invention can provide various effects not specifically mentioned.

Advantages and features of the present invention, and a method of achieving them will become apparent with reference to the embodiments described below in detail. However, the present invention is not limited to the embodiments described herein and may be embodied in other forms. Rather, the embodiments introduced herein are provided so that the disclosed content may be thorough and complete, and the spirit of the present invention may be sufficiently conveyed to those skilled in the art.

The terms used in the present application are only used to describe specific embodiments, and are not intended to limit the present invention. Singular expressions include plural expressions unless the context clearly indicates otherwise.

Unless otherwise defined, all terms including technical or scientific terms used herein have the same meaning as commonly understood by one of ordinary skill in the art to which the present invention belongs. Terms such as those defined in a commonly used dictionary should be interpreted as having a meaning consistent with the meaning of the related technology, and should not be interpreted as an ideal or excessively formal meaning unless explicitly defined in this application. Does not.

Hereinafter, a method for preparing fermented Eoseongcho oil containing wild ginseng components according to the present invention will be described in detail with reference to a preferred embodiment.

First, you can wash after preparing wild ginseng.

The above-mentioned wild ginseng is cultivation by sowing seeds of natural wild ginseng in the mountains, harvesting the roots of natural wild ginseng in the deep mountain and re-transplanting them in a suitable location in the forest, and sowing and cultivating the seeds of cultivated ginseng in the forest. It can be classified as such, and it is also called camphor ginseng.These wild ginsengs contain 10 times more saponin than ginseng and 4 to 5 times more than red ginseng, so they have great efficacy in enhancing immunity. In addition, blood circulation and diabetes It is effective in preventing, improving digestion, relieving stress, and improving energy.

Next, the washed sanyangsam can be pulverized.

The pulverization of the washed wild ginseng in the above step may use a known pulverizer or the like in order to allow the active ingredient to be extracted from the wild ginseng within a short period of time, for example, the pulverization of the wild ginseng may be made in a length of 0.5 to 3 cm. have.

Then, the pulverized wild ginseng can be heated with steam to steam.

In the above step, the pulverized wild ginseng may be steamed by heating with steam at a constant temperature, and the steaming of the wild wild ginseng may be performed by heating the pulverized wild ginseng for 5 to 10 minutes with steam.

Subsequently, the steamed wild ginseng can be dried.

In the above step, by drying the steamed wild ginseng to remove moisture remaining in the wild ginseng, the active ingredients of the wild ginseng can be easily extracted in a later process. Drying of the steamed wild ginseng is performed at a temperature of 50 to 55°C. It can be carried out for 10 days.

Next, the dried wild ginseng can be extracted to prepare a wild ginseng extract.

In the above step, the dried wild ginseng can be extracted using a known extraction method such as a solvent extraction method, a hot water extraction method, or a supercritical extraction method.For example, the preparation of the wild wild ginseng extract is (a) 70 to 1000 to 1200 g of dried wild ginseng. %(v/v) ethanol aqueous solution 10~12ℓ at 85 to 90℃ for 3~4 hours, and then 70%(v/v) ethanol aqueous solution 4~6ℓ at 85 to 90℃ for 2~3 hours Completing the secondary extraction and preparing an extract until the concentration is 1000 to 1200 ml in a vacuum rotary evaporator; (b) Add water to the extract, dilute by 2 to 3 times by volume, centrifuge at 14,000 to 15,000 rpm for 20 to 30 minutes to completely remove polymer fibers and solids, and then to remove the collected supernatant into 1.2 to 1.5 times by volume of chloroform. Extracting twice; And (c) removing the chloroform layer, and extracting the aqueous layer with 1.2 to 1.5 times the volume of ethyl acetate three times.

Next, you can prepare and wash Eoseongcho.

The Eoseongcho (Houttuynia cordata thunb) is an outpost of Yakmomil, a plant of the Saururaceae family, and lives in southeastern Asia and particularly in Japan and Korea. Eoseongcho is also called Sip-Yak because it has ten medicinal effects, and the stem is like a sweet potato leaf, and it is also called Eoseongcho because it originates from the fact that when you touch the raw leaves, fish smells badly. Eoseongcho is also available for medicinal and edible use. It is classified as animals and plants that can only be used in a minimum amount as an auxiliary ingredient in the classification of food raw materials in the food code. Pharmacologically, it is widely known for its strong heart, diuretic, antibacterial, detoxifying, and anticancer effects. Is used as a cosmetic and health functional food that helps detoxification and beauty.

Subsequently, the washed Eoseongcho may be steamed with steam.

In the above step, the steaming may be performed by heating the washed Eoseongcho at a temperature of 145 to 155°C and a pressure of 4 to 5kgf/cm ² with steam for 20 to 40 minutes.

Next, the steamed Eoseongcho may be dried.

In the above step, the drying is performed by drying the Eoseongcho for 40 to 60 hours at a temperature of 18 to 22°C and a humidity of 55 to 60% in order to prevent the chlorophyll of the Eoseongcho from being destroyed and volatilization of useful components during sunlight drying. I can.

Next, the dried Eoseongcho can be heated to cool after roasting. The dried Eoseongcho is first roasted at a temperature of 75 to 80°C for 1 to 5 minutes after adding the dried Eoseongcho to a heating container, The first roasted Eoseongcho may be secondarily roasted at a temperature of 120 to 140°C for 10 to 50 seconds, and the second roasted Eoseongcho may be cooled at a temperature of 35 to 45°C for 1 to 3 hours. .

Subsequently, the sanyangsam extract, minerals, and lactic acid bacteria culture solution may be sprayed onto the cooled Eoseongcho and mixed.

In the above step, spraying at a weight ratio of 3 to 7 parts by weight of the wild ginseng extract, 1 to 3 parts by weight of minerals, and 2 to 6 parts by weight of the lactic acid bacteria culture solution with respect to 100 parts by weight of the cooled Eoseongcho may be mixed. In the process such as fermentation of the Eoseongcho, it is absorbed by the Eoseongcho or Sanyangsam extract and is a mineral that is a relatively small amount of nutrients necessary for human growth, maintenance, and reproduction, and calcium, phosphorus, potassium, magnesium, manganese, iodine, selenium, Any one or more selected from the group consisting of molybdenum and cobalt may be used.

In addition, in the step, the lactic acid bacteria may use a lactic acid strain isolated from kimchi, which is a fermented food, specifically, as the lactic acid strain, Lactobacillus curvatus , Weissella viridescens , Lactobacillus plantarum and Any one or more known lactic acid strains selected from the group consisting of Leuconostoc lactis may be used.

For example, in the above step, in order to prepare a lactic acid bacteria culture solution from kimchi, the pH of the medium is adjusted to 2.8-3.2 using 1.2N HCl, and then the lactic acid strain is separated from the kimchi, and the isolated lactic acid strain is MRS broth (Oxoid , England) at 37~39℃ for 20 to 25 hours, then diluted to 1×1.0 ⁸ to 5×1.0 ⁸ CFU/mL, and then centrifuged at 10,000 to 15,000 rpm for 10 to 15 minutes After separating only (supernatant), filtering the supernatant with a 0.45 μm syringe filter, lactic acid bacteria are diluted by mixing in a weight ratio of 1,000 to 2,000 parts by weight of sterilized distilled water with respect to 100 parts by weight of the filtered supernatant. A culture solution can be prepared.

Next, it is possible to ferment Eoseongcho in which the wild ginseng extract, mineral and lactic acid bacteria culture solution are mixed.

In the above step, the Eoseongcho mixed with the wild ginseng extract, minerals and lactic acid bacteria culture liquid is maintained at a temperature of 40 to 42°C and a humidity of 60 to 62%, and then fermented for 5 to 10 days. When it is performed below the above lower limit range, a problem may occur in that the Eoseongcho is not sufficiently fermented, and when it is performed beyond the above upper limit range, the physical properties of the fermented Eoseongcho may be deteriorated.

Then, the fermented Eoseongcho may be dried with cold air.

Cold air drying of the fermented Eoseongcho in the above step may be performed by drying the fermented Eoseongcho for 10 to 20 hours with cold air at a temperature of 3 to 6°C, and maintaining the fermented Eoseongcho for 2 to 4 days at a temperature of 55 to 60°C. .

Subsequently, the cold air dried Eoseongcho may be extracted to prepare an oil.

As a method of obtaining oil from the cold air dried Eoseongcho in the above step, there are various known methods such as steam distillation method and extraction method, and the method for preparing the oil in the present invention may use various known extraction methods as described above. , For convenience of description and clarity of the technical idea of the present invention, a detailed description of a method of extracting oil from the cold-air dried Eoseongcho will be omitted.

Next, refined fermented oil can be prepared by purifying the oil with a filter.

In the above step, after the charcoal activated carbon powder is mixed with the oil, the oil is stirred for 20 to 40 minutes, and the oil mixed with the charcoal activated carbon powder is filtered through a filter to prepare purified Eoseongcho fermented oil.

The charcoal activated carbon powder is used for refining or adsorbing odor, and it is possible to prepare a safe and flavorful Eoseongcho fermented oil by removing already and off-flavor that may remain in the oil. Mixing so as to contain 1 to 5 parts by weight based on 100 parts by weight, and the charcoal activated carbon powder may be used charcoal activated carbon powder having a particle size of 10 to 100 mesh (mesh).

In addition, the charcoal activated carbon powder is manufactured using oak trees such as brown oak, oyster oak, water oak, etc., and mixed with oil to prevent the smell of the charcoal from being transmitted to the oil when refining, odorless charcoal activated carbon powder is used. I can.

Hereinafter, examples and comparative examples of a method for producing fermented Eoseongcho oil containing wild ginseng components according to the present invention will be described in more detail.

<Example 1>

First, sanyangsam was prepared, washed, and pulverized.

Next, after steaming the pulverized wild ginseng for 8 minutes with steam, the steamed wild ginseng was dried for 7 days at a temperature of 53 to 54°C, and a wild ginseng extract was prepared using the dried wild ginseng.

Next, after preparing Eoseongcho, it was steamed by heating with water vapor at a temperature of 150 to 151°C and a pressure of 4.5kgf/cm ² for 30 minutes, and the steamed Eoseongcho was 50 at a temperature of 20 to 21℃ and a humidity of 58%. After drying for a period of time, the first roasting is performed at a temperature of 78 to 79°C for 3 minutes, the first roasted Eoseongcho is secondarily roasted at a temperature of 130 to 132°C for 30 seconds, and the second roasted Eoseongcho is 40 to It was cooled at a temperature of 41° C. for 2 hours.

Subsequently, after spraying and mixing at a weight ratio of 5 parts by weight of the sanyangsam extract, 2 parts by weight of minerals and 4 parts by weight of lactic acid bacteria culture solution with respect to 100 parts by weight of the cooled Eoseongcho, the temperature of 41°C and the humidity of 61% were maintained. Fermented for 8 days.

Next, the fermented Eoseongcho was dried with cold air at a temperature of 5°C for 15 hours and maintained at a temperature of 57 to 58°C for 3 days, followed by cold air drying.

Next, the cold-air dried Eoseongcho was extracted to prepare an oil, and the oil was purified by a filter to prepare a refined fermented oil.

<Example 2>

Sprayed and mixed at a weight ratio of 6 parts by weight of wild ginseng extract, 1 part by weight of mineral, and 6 parts by weight of lactic acid bacteria culture solution to 100 parts by weight of cooled Eoseongcho, and fermented for 10 days after maintaining a temperature of 41°C and a humidity of 61%. A fermented oil refined was prepared in the same manner as in Example 1, except for that.

<Comparative Example 1>

First, after preparing Eoseongcho, it was steamed by heating with steam for 30 minutes at a temperature of 150 to 151°C and a pressure of 4.5kgf/cm ² , and the steamed Eoseongcho was heated at a temperature of 20 to 21℃ and a humidity of 58% for 50 hours. After drying, the first roasting is performed at a temperature of 78 to 79°C for 3 minutes, the first roasted Eoseongcho is secondarily roasted at a temperature of 130 to 132°C for 30 seconds, and the second roasted Eoseongcho is 40 to 41°C. It was cooled for 2 hours at a temperature of.

Next, the cooled Eoseongcho was dried with cold air at a temperature of 5° C. for 15 hours and maintained at a temperature of 57 to 58° C. for 3 days, thereby drying with cold air.

Next, the cold-air dried Eoseongcho was extracted to prepare an oil, and the oil was purified by a filter to prepare a refined oil.

<Comparative Example 2>

Sesame oil was manufactured using sesame seeds that were imported and stored in a warehouse for 2 months.In Comparative Example, the sesame seeds were washed, dried, roasted, cropped, filtered, collected, and filled through a conventional oil production process. Was prepared.

<Sensory evaluation>

As described above, sensory evaluation was performed on the flavor, smell, preference, etc. of the fermented oil according to Examples 1 and 2 and the oil or sesame oil according to Comparative Examples 1 and 2, and the results are shown in Table 2 below. The sensory test was conducted on 50 food-related experts and general consumers, and the score and evaluation criteria used a 9-point scoring method, and are shown in [Table 1] below.

score Evaluation standard 9 Very good 7 good 5 usually 3 Bad One Very bad

zest smell Overall preference Example 1 8.7 8.5 8.7 Example 2 8.5 8.3 8.5 Comparative Example 1 6.1 5.9 6.0 Comparative Example 2 7.9 7.8 7.8

Referring to [Table 2], it was found that the fermented oil according to Examples 1 and 2 was superior to the oil according to Comparative Example 1 or the sesame oil according to Comparative Example 2 in flavor, smell, and overall preference.

It is judged that the refined fermented oil according to Examples 1 and 2 was fermented using wild ginseng extract, minerals, and lactic acid bacteria culture solution to enhance the flavor, smell and preference of the oil.

<Measurement of sediment formation>

The oil or sesame oil prepared according to Examples 1 and 2 and Comparative Examples 1 and 2 was placed in a 300 mL container (250 mm long) and left at room temperature for 4 months. The resulting precipitate was measured, and the results are shown in Table 3 below.

Example 1 Example 2 Comparative Example 1 Comparative Example 2 Sediment generation degree (mm) 1.3 1.4 2.1 3.6

Referring to [Table 3], it was confirmed that a large amount of sediment was generated from the oil or sesame oil prepared according to Comparative Examples 1 and 2 than the fermented oil prepared according to Examples 1 and 2.

<Benzopyrene content investigation>

Benzopyrene is a type of polycyclic aromatic hydrocarbon (PAH). When accumulated in the human body, benzopyrene is an environmental hormone that causes various cancers and causes mutations. The production of benzopyrene in food heats food. It may be produced during the process, and when food is cooked or processed at high temperatures, carbohydrates, proteins, fats, etc., which are the main ingredients of food, may be incompletely burned.

The content of benzopyrene was investigated by an experimental method notified by the Ministry of Food and Drug Safety. The experimental equipment was a high-speed liquid chromatography Youngrin (MODEL: SP925S), a fluorescent detector was JASCO FP-2020PLUS, and an autosampler was used. It was extracted with N,N-dimethylformamide-water (9:1) and hexane using 3-methylcollanthrene, and then purified with a solid phase extraction (SPE) cartridge and analyzed by high-speed liquid chromatography/fluorescence detector.

Benzopyrene content (ppb) Example 1 Not detected Example 2 Not detected Comparative Example 1 Not detected Comparative Example 2 2.3

Referring to [Table 4], the oils prepared according to Examples 1 and 2 and Comparative Example 1 were found to be 2.0 ppb or less, which is the legal standard value of benzopyrene.

Hereinafter, the shampoo composition using the fermented Eoseongcho oil according to the present invention will be described in more detail.

The shampoo composition according to the present invention includes fermented Eoseongcho oil, sunjit extract, inorganic extract, and cystamine dimaleate as active ingredients.

In addition, the shampoo composition according to the present invention may be included in a weight ratio of 10 to 20 parts by weight of fermented Eoseongcho oil, 5 to 15 parts by weight of sunjit extract, and 3 to 7 parts by weight of inorganic extract.

The fermented Eoseongcho oil may be fermented Eoseongcho oil prepared by the above-described method.

The sunjit extract may be prepared using sunjit, wherein the sungite is a material containing SiO ₂ (silicate) and C ₆₀ (fullerene) as main components, and refers to a material containing natural fullerene. Sunjit containing 90% or more of fullerene is called Elite shungite or Noble Shungite, and sunjit containing less than 60% fullerene is called Normal shungite.

Representative functions of the sunjit include an antioxidant function, an electromagnetic wave blocking function, a purification and decomposition function of contaminants, and a sterilization and antibacterial function. Sunjit is a powerful natural antioxidant that has the function of enhancing human immunity against a number of diseases, purifying water and air by adsorbing pollutants, and decomposing adsorbed pollutants by themselves.

In addition, since the sunjit has antibacterial and bactericidal properties, it has a function of removing 99% or more of only E. coli, Pseudomonas aeruginosa, staphylococcus aureus, and harmful bacteria, blocking harmful electromagnetic waves, and emitting a large amount of far-infrared rays.

In the present invention, the sunjit extract may be used as a sunjit extract prepared as follows.

First, after preparing the sunjit mineral, it can be pulverized using a ball milling device.

In the above step, the pulverization time may be delayed and the pulverization time may be delayed and work due to dust or fine powder when the pulverized purezit mineral has a particle diameter of 10 to 300㎛. A problem of poor performance may occur, and if it exceeds 300 μm, there may be a problem in that active ingredients contained in the pulverized purezit mineral cannot be easily extracted in a later process.

Next, the pulverized pure jit may be heated to perform heat treatment.

In the above step, impurities remaining in the pulverized pure jite may be removed by heating and heat treatment of the pulverized pure jite. The heat treatment of the pulverized pure jite may be performed at a temperature of 1200 to 1600°C for 1 to 20 minutes. I can.

In the above step, when the heat treatment is performed at a temperature of 1200° C. or less than 1 minute, there may be a problem in that impurities remaining in the pulverized pure paper are not sufficiently removed. When the temperature of 1600° C. or more than 20 minutes Problems may arise where it is difficult to expect further increase in effectiveness.

Next, after the heat-treated sunjit is washed to remove combustion residues adhering to the surface of the sunjit, the washed sunjit and the Hwangchil tree leaf extract may be mixed and then aged.

The washing of the heat-treated sunjit in the above step may be performed by washing the surface of the heat-treated sunjit using distilled water or purified water. For example, the heat-treated sunjit is washed with purified water of 30 to 50°C. This can be done by cleaning the surface of the heat-treated sunjit.

In addition, in the above step, after mixing in a weight ratio of 200 to 400 parts by weight of Hwangchil tree leaf extract with respect to 100 parts by weight of the total content of the washed pure jite, it is stored for 5 to 10 days at a temperature of 60 to 65°C and aged. It is possible to sufficiently leach the active ingredients contained in the sunjit.

Subsequently, after separating and removing the sunjit immersed in the Hwangchil tree leaf extract, the Hwangchil tree leaf extract from which the active ingredient of the sunjit is leached may be centrifuged.

In the above step, the Hwangchil tree leaf extract from which the sunjit is removed is leached with the active ingredients of Sunjit, and by centrifuging the Hwangchil tree leaf extract from which the active ingredients of the sunjit are leached, the lower layer where the sunjit particles are located It can be separated by dividing into a liquid, an intermediate liquid and a supernatant located above the lower liquid.

Next, by heating the centrifuged supernatant and the supernatant, it is possible to prepare a sunzit extract.

In the above step, after separating the centrifuged supernatant and the supernatant, it is possible to prepare a gelled sunzit extract formed by leaching the active ingredients of sunzit by heating at a temperature of 120 to 130°C.

The Hwangchil tree leaf extract is prepared by extracting from the leaves of the Hwangchil tree, and the Hwangchil tree (Dendropanax morbifera Lev) is an evergreen broad-leaved arboreous tree of the genus Araliaceae. It is a native tree native to Korea that grows up to 15m or more in height. Young branches are green and glossy, flowers bloom in June, and the 7~19mm long fruit ripens black. It is a temperate plant that grows in areas where the minimum temperature is above -2℃ and the average annual temperature is above 12~15℃.

Hwangchil wood secretes hwangchil, which is generally composed of 66.7% non-volatile components, 10.8% aroma, 8.1% moisture, and 14.4% solids, which are paint components that form a golden coating. It is known to consist of quiterpenes β-cubebene, γ-selinene, and δ-cadinene. The fragrance component contained in Hwangchil not only has the value as a benzoin that makes the mind and body clear and comfortable, but also has a variety of pharmacological effects, so it is highly useful as a perfume, cosmetic, or functional food and beverage.

The hwangchil tree leaf extract may be used as a hwangchil tree leaf extract prepared by the following manufacturing method.

First, in order to prepare a hwangchil tree leaf extract, hwangchil tree leaves may be prepared and washed.

Next, the washed hwangchil tree leaves can be pulverized into a certain particle size.

In the above step, the active ingredients of the hwangchil tree leaves may be sufficiently extracted by pulverizing the leaves of the hwangchil tree to a certain particle size, and the crushing of the leaves of the hwangchil tree may be pulverized so that the particle diameter is in the range of 500 to 2500 μm. . If the particle diameter of the leaves of the Hwangchil tree is pulverized to less than 500 μm in the above step, it takes a long time to crush, and the particles are too small to cause agglomeration between particles in a later process, and when the particle size exceeds 2500 μm There may be a problem in that it is difficult to effectively extract useful ingredients from the leaves of the hwangchil tree.

Next, the pulverized hwangchil tree leaf extract may be obtained by applying ultrasonic waves in an atmosphere of low temperature and reduced pressure to remove solids.

In the above step, after preparing a mixture by mixing the pulverized Hwangchil tree leaves with a solvent, it is introduced into an ultrasonic extractor to apply ultrasonic waves to the mixture, and the solids contained in the mixture are mixed with a known strainer such as a sieve, etc. Hwangchil tree leaf extract can be prepared by removing it using, and the solvent is mixed in a weight ratio of 1000 to 2000 parts by weight based on 100 parts by weight of the pulverized hwangchil tree leaf, and the solvent is water or carbon number 1 to 4 Any one or more solvents selected from alcohols of (C1 to C4) may be used.

In addition, in the step, the ultrasonic wave applied to the mixture under a temperature of 20 to 25°C and a pressure of 0.1 to 0.5 kgf/cm ² is output of 100 to 200 watts for 30 to 60 minutes at a vibration frequency of 30 to 50 KHz. Hwangchil tree leaf extract can be obtained by extracting using.

The inorganic extract may be an extract prepared using a material having far-infrared radiation, antibacterial effect, and the like, and the inorganic extract may be an inorganic extract consisting of sericite extract, elvan extract, ocher extract and zeolite extract.

In addition, the inorganic extract may be included in a weight ratio of 5 to 10 parts by weight of sericite extract, 1 to 5 parts by weight of elvan extract, 3 to 7 parts by weight of ocher extract, and 2 to 6 parts by weight of zeolite extract, preferably the inorganic extract Silver sericite extract may be included in a weight ratio of 7 parts by weight, elvan extract 3 parts by weight, ocher stone extract 5 parts by weight, and zeolite extract 4 parts by weight.

The sericite extract may be extracted from sericite, which is also called sericite, belongs to monoclinic system, and has a pearlescent luster in white or grayish white color. Originally, it was referred to as the main constituent mineral of crystalline schist, especially sericite schist, but today it refers to the fine muscovite mica in the shape of clay created by the hydrothermal action. Its chemical composition is almost the same as muscovite mica, but in general, potassium (K) is less than muscovite mica and has a little more water H ₂ O. It is the most common constituent mineral of phyllite slate or phyllite that is generated as secondary deterioration such as feldspar, geuncheongseok, and hongjuseok, and has undergone light dynamic metamorphism. The pottery stone (陶石) is caused by the deterioration of the volcanic rock, and is made of quartz (70%) and sericite (30%). Silky mica is used as an admixture of ceramics or refractory bricks, and has various uses, such as paints, electrical insulators, live horse materials, and cosmetics.

The elvan extract may be extracted from elvan, and the elvan is a rock belonging to porphyry, mixed with quartz and feldspar, is made of porous, has strong adsorption, contains about 25,000 kinds of inorganic salts, and has an action of exchanging heavy metals and ions. Because of this, it is known as a rock that can also be used as a harmful metal removal agent.

The elvan stone is composed of 30,000 to 150,000 multi-layered porous masses per 1 cm ³ , and has strong adsorption, so it has the effect of adsorbing and decomposing heavy metal contaminants, and the effect of dissolving minerals, and contains about 25,000 kinds of inorganic salts. It has the effect of controlling water or strong alkaline water into weak alkaline (pH 7.2~7.4) water through ion exchange, and has far-infrared ray emission.

The ocher stone extract can be extracted from ocher stone, where the far-infrared rays from ocher permeate the subcutaneous layer 80 times deeper than normal heat and finely shake cells 2,000 times per minute to make the vital activity of the cell tissue more vigorous. It promotes blood circulation, discharges wastes and heavy metals in the body, prevents stress, adult diseases, and gynecological diseases, and natural ocher stone has excellent moisture control ability because it breathes because of its porosity, and has excellent antibacterial performance. It is cool and warm in winter.

Ocher gemstone is a healthy stone that retains the ancient primitive nature formed by high pressure after being deposited for more than 300 million years. It is not calcined or processed soil. It is a natural loess gemstone that has almost no impurities such as heavy metals. It is good for health due to its excellent far-infrared radiation rate. Excellent deodorizing effect and antibacterial. It has excellent anti-fungal performance, especially since it is a porous sedimentary rock, so it has excellent humidity control ability, and when it sits directly on the floor because it is cold, it invades the cold, but natural ocher stone has the ingredient of loess as it is, so it has the effect of blocking the cold. .

The zeolite extract can be extracted from zeolite, and the zeolite is a silicate mineral, and since the bonds of each atom are loose structurally in the crystal, the skeleton remains intact even if the moisture filling the space between them is released by high heat. Other particulate matter can be adsorbed. In particular, the zeolite is excellent in deodorizing and adsorption effects, and thus harmful components can be adsorbed and removed.

The inorganic extract may be, for example, an inorganic extract prepared by the following method.

First, sericite, elvan, ocher stone and zeolite are prepared, and then the sericite, elvan, ocher stone, and zeolite may be pulverized into a predetermined particle size.

In this step, the sericite, elvan, ocher, and zeolite may be pulverized using a known grinder such as a ball milling device.

Next, the pulverized sericite, elvan, loess, and zeolite may be heated to heat treatment.

In the above step, impurities and residual organic matters contained in the serous mica, elvan stone, ocher stone and zeolite may be removed by heating the pulverized sericite, elvan stone, ocher stone and zeolite. Heating of the pulverized sericite, elvan stone, ocher stone and zeolite May proceed for 50 to 100 minutes at a temperature of 1500 to 1700 °C.

Next, after washing the heated sericite, elvan, ocher stone and zeolite to remove combustion residues generated during heat treatment adhering to the surface of the sericite, elvan, ocher stone and zeolite, the washed serica, elvan, and ocher stone And zeolite may be immersed in purified water to be aged.

In the above step, washing of the sericite, elvan, ocher stone and zeolite may be performed by washing the surfaces of the sericite, elvan, ocher stone and zeolite with purified water of 50 to 60°C, and the aging of the sericite, elvan, ocher stone and zeolite is described above. After mixing 300 to 500 parts by weight of purified water at a temperature of 60 to 65°C with respect to 100 parts by weight of washed sericite, elvan stone, ocher stone and zeolite, it can be carried out by sealing and storing for 3 to 6 days.

Subsequently, after separating and removing sericite, elvanite, ocherite and zeolite from the mixture of the aged sericite, elvanite, ocherite, zeolite and purified water, the purified water may be centrifuged.

In the above step, active ingredients of sericite, elvan, ocherite, and zeolite are leached in the purified water.By centrifuging the purified water, a lower layer in which fine particles of sericite, elvan, ocher, and zeolite are located, and the upper layer of the lower layer It can be separated by dividing it into positional supernatant and supernatant.

Next, after separating the supernatant and the supernatant of the centrifuged purified water, the supernatant and the supernatant are heated to prepare an inorganic extract consisting of a sericite extract, alum extract, a loess extract and a zeolite extract.

In the above step, after separating the intermediate and supernatant of the centrifuged purified water, the inorganic extract consisting of sericite extract, alum extract, ocherite extract and zeolite extract is prepared by heating with a heat source at a temperature of 150 to 170°C to remove moisture. Can be manufactured.

Hereinafter, examples and comparative examples for the shampoo composition according to the present invention will be described in more detail.

Shampoos were prepared using the shampoo compositions according to Examples 3, 4 and 5 and Comparative Examples 3 and 4 so that the ingredients as shown in the following [Table 5] were included.

Ingredient (parts by weight) Example 3 Example 4 Example 5 Comparative Example 3 Comparative Example 4 Eoseongcho fermented oil 15 19 10 - - Sunjit extract 6 10 14 - 6 Inorganic extract 5 3 7 5 - Red oil 30 30 30 30 30 Jojoba seed oil 10 10 10 10 10 Citric acid 2 2 2 2 2 CDE (Cocamide DEA) 10 12 10 10 10 LES (disodium lauret sulfosuccinate) 50 55 50 50 50 Poly Quarter 8 6 7 8 8 glycerin 10 8 8 8 10 Citric acid 2 2 3 2 2 Xanthan gum One One 2 One 2 Cetyl alcohol 7 7 6 6 8 Allantoin 3 3 2 2 4 Tocopheryl acetate 2 2 3 2 3 Biotin 2 2 3 2 3 Methionine One One One One One Mineral water 30 30 30 30 30

<Stability test>

Stability tests of shampoos prepared according to Examples 3, 4, and 5 were performed.

The observation period was the same for one week, and stability was observed at various temperatures, and the results are shown in [Table 2].

Temperature Example 3 Example 4 Example 5 0℃ Good Good Good 40℃ Good Good Good -20℃ Good Good Good

Referring to [Table 6], it was confirmed that the shampoos prepared according to Examples 3, 4, and 5 had good formulation stability.

<Hair conditioning effect test (sensory evaluation)>

Using the shampoo prepared according to Examples 3, 4, 5 and Comparative Examples 3 and 4, a group consisting of 10 people aged 20 to 40 years used it for one week, and then 5 points (very bad, bad , Average, good, very good) The quality was evaluated through a questionnaire and the results are shown in [Table 7].

Survey item Example Comparative example 3 4 5 3 4 Foamy and soft 4.5 4.6 4.5 3.2 3.4 Clean rinse 4.4 4.2 4.4 3.3 3.4 Easy to comb when semi-dry 4.3 4.3 4.1 3.5 3.2 The hair is soft after drying 4.3 4.1 4.2 3.2 3.1 The hair is moist after drying 4.4 4.4 4.3 3.3 3.3 Glossiness is felt on the hair after drying 4.5 4.4 4.3 2.9 3.0

<Scalp stimulation test>

The stimulation clinical test for the shampoo prepared as in Example 3 was conducted as follows.

First, the clinical trial was conducted on 20 healthy subjects (8 males and 12 females) between the ages of 10 and 50, and it was confirmed that no other products such as steroids or antibiotics were used from 2 weeks before the start of the experiment to the end of the experiment. .

In addition, for all test subjects, the scalp condition was observed 24 hours after shampooing, and a qualitative evaluation was performed through an evaluation table as shown in [Table 8].

Experiment item Subjective score Evaluation results

Degree of stimulation a: The skin turns red and the itching is strong - b: The skin is slightly red and itchy - c: The skin is slightly red and irritated. - d: There is no change in skin condition, but there is a slight irritation. - e: No irritation or change in skin condition 20 people

Referring to [Table 8], it can be seen that the shampoo prepared according to Example 3 can be safely used because there is no scalp irritation or change in skin condition.

<Antibacterial effect>

In order to confirm the antibacterial effect of shampoos according to Examples 3, 4, 5 and Comparative Examples 3 and 4, the microbiology guidelines of The Cosmetic, Toility and Fragrance Association, Inc. (CTFA) The test method of was used.

In addition, the bacteria used to confirm the antibacterial effect include Gram-positive bacteria as Staphylococcus aureus ATCC 6538P, Gram-negative bacteria as Escherichia coli (Escherichia coli ATCC 8739), Pseudomonas aeruginosa ATCC 9027), and yeast as Candida albicans. (Candida albicans ATCC 10231), Aspergillus niger ATCC22343 was used.

In a vial containing 10 g of each hair shampoo, a suspension of 3 bacteria (Ecoli, P aeruginosa, S aureus) and 2 fungi (C albicans, A niger) was added to each 1 × 106 cfu/g, 1 × 105 After inoculation so that it becomes cfu/g, 1g of sample is collected under aseptic operation at intervals of 4 hours, 1 day, 2 days, 3 days, 7 days after storage at 25℃ and diluted appropriately with a diluent. Nutrient agar, Difco), and fungi were spread on potatodextrose agar (Difoc) medium and incubated at 35°C and 25°C for 24 to 72 hours, respectively, and then the D-value was obtained through the number of bacteria.

ingredient Fungus D-value(Hr) Example 3 Germ 5.3 Fungi 5.3 Example 4 Germ 5.2 Fungi 5.3 Example 5 Germ 5.4 Fungi 5.4 Comparative Example 3 Germ 9.7 Fungi 9.9 Comparative Example 4 Germ 9.7 Fungi 9.8

* D-value: Time required for 90% of microorganisms to be killed

Referring to [Table 9], it was confirmed that the shampoos according to Examples 3, 4, and 5 had very excellent antibacterial effects.

<Antioxidant activity test>

Using the shampoos of Examples 3, 4 and 5 as samples, the radical scavenging activity was measured.

The antioxidant activity (electron donation ability, EDA%) of the sample was measured by modifying the Blois method. 2 mL of a 0.2 mM DPPH (1,1-diphenyl-2-picryl hydrazyl) solution was mixed with 2 mL of the sample, left for 30 minutes, and the absorbance was measured at 517 nm.

The radical scavenging activity was expressed by the rate of decrease in absorbance of the sample-added and non-added groups. The radical scavenging activity was calculated by the following equation, and the results are shown in Table 6 below. BHT (synthetic antioxidant) was used as a control sample.

Radical scavenging activity (%) = (1-absorbance of sample added/absorbance of no added group)×100

division Radical scavenging activity Example 1 57.5 ± 0.5 Example 2 58.3 ± 0.4 Example 3 57.5 ± 0.6 Control 62.5 ± 0.4

Referring to [Table 10], the shampoos prepared according to Examples 3, 4, and 5 were found to have antioxidant activity, and have almost similar effects to the radical scavenging ability of conventional synthetic antioxidants used as controls. Confirmed.

Therefore, the shampoo prepared according to Examples 3, 4, and 5 has excellent antioxidant effects to protect the scalp from free radicals and free radicals, and is expected to greatly enhance the physiological activity of the scalp.

In the above, a preferred embodiment of the present invention has been described, but those of ordinary skill in the art to which the present invention pertains will understand that the present invention can be implemented in other specific forms without changing the technical spirit or essential features. I will be able to. Therefore, it should be understood that the exemplary embodiment described above is illustrative in all respects and is not limiting.

Claims (6)

After preparing wild ginseng, wash it,
Crushing the washed wild ginseng,
The pulverized wild ginseng is heated and steamed with steam,
Dry the steamed wild ginseng,
Extracting the dried wild ginseng to prepare a wild ginseng extract,
Prepare and wash Eoseongcho, and steam the washed Eoseongcho with steam,
Dry the steamed Eoseongcho,
The dried Eoseongcho is heated, dried, and then cooled,
Spraying and mixing the sanyangsam extract, minerals and lactic acid bacteria culture solution on the cooled Eoseongcho,
Fermenting Eoseongcho mixed with the wild ginseng extract, mineral and lactic acid bacteria culture solution,
Cold air drying the fermented Eoseongcho,
Extracting the cold-air dried Eoseongcho to prepare an oil,
Purifying the oil with a filter to prepare a refined fermented oil,
In the step of drying the steamed wild ginseng, drying of the steamed wild ginseng is performed at a temperature of 50 to 55°C for 5 to 10 days,
In the step of steaming the washed Eoseongcho with steam, the steaming is performed by heating the washed Eoseongcho with water vapor at a temperature of 145 to 155°C and a pressure of 4 to 5kgf/cm ² for 20 to 40 minutes,
In the step of drying the steamed Eoseongcho, the drying is performed by drying the Eoseongcho at a temperature of 18 to 22°C and a humidity of 55 to 60% for 40 to 60 hours,
In the step of spraying and mixing the sanyangsam extract, mineral and lactic acid bacteria culture solution on the cooled Eoseongcho, 3 to 7 parts by weight of the sanyangsam extract, 1 to 3 parts by weight of minerals, and 2 to 6 parts by weight of the lactic acid bacteria culture solution based on 100 parts by weight of the cooled Eoseongcho Spray and mix in a weight ratio of parts by weight,
In the step of fermenting Eoseongcho mixed with the wild ginseng extract, mineral and lactic acid bacteria culture solution, the Eoseongcho mixed with the wild ginseng extract, mineral and lactic acid bacteria culture solution is maintained at a temperature of 40 to 42°C and a humidity of 60 to 62%, 5 To ferment for 10 days,
In the cold air drying of the fermented Eoseongcho in the step of cold air drying the fermented Eoseongcho, the fermented Eoseongcho is dried for 10 to 20 hours with cold air at a temperature of 3 to 6°C, and 2 to 4 at a temperature of 55 to 60°C. Progress by holding it for days,
In the step of preparing purified fermented oil by purifying the oil with a filter, the oil is mixed with charcoal activated carbon powder and then stirred for 20 to 40 minutes, and the oil mixed with the charcoal activated carbon powder is filtered through a filter. To prepare a fermented oil, the charcoal activated carbon powder is mixed so as to contain 1 to 5 parts by weight based on the total 100 parts by weight of the oil, and the charcoal activated carbon powder is used with a charcoal activated carbon powder having a particle size of 10 to 100 mesh. ,
The Eoseongcho fermented oil is contained in a weight ratio of 10 to 20 parts by weight, 5 to 15 parts by weight of sunjit extract, and 3 to 7 parts by weight of inorganic extract to constitute a shampoo composition,
The sunzit extract is pulverized to have a particle diameter of the sunzit mineral in the range of 10 to 300 μm after preparing the sunzit mineral, and the pulverized sunzit is heated at a temperature of 1200 to 1600°C for 1 to 20 minutes And heat treatment, washing the heat-treated pure jit with purified water at 30 to 50°C, mixing in a weight ratio of 200 to 400 parts by weight of Hwangchil tree leaf extract based on 100 parts by weight of the total content of the washed pure jit, and then 60 to After storing and aging for 5 to 10 days at a temperature of 65°C, separating and removing sunjit immersed in the Hwangchil tree leaf extract, and centrifuging the Hwangchil tree leaf extract from which the active ingredient of the sunjit is leached, The process of separating and dividing into a lower layer in which the particles are positioned, and a middle layer and a supernatant positioned above the lower layer, and heating the centrifuged middle and supernatant to a temperature of 120 to 130°C Is manufactured through
The Hwangchil tree leaf extract is prepared by washing the Hwangchil tree leaves, pulverizing the washed Hwangchil tree leaves, mixing the crushed Hwangchil tree leaves with a solvent to prepare a mixture, and then introducing the mixture into an ultrasonic extractor. Is prepared through a process of applying ultrasonic waves to the mixture and removing solids contained in the mixture, the solvent is mixed in a weight ratio of 1000 to 2000 parts by weight based on 100 parts by weight of the pulverized hwangchil tree leaves, and the solvent is Any one or more solvents selected from water or alcohols having 1 to 4 carbon atoms (C1 to C4) are used, and ultrasonic waves applied to the mixture under a temperature of 20 to 25°C and a pressure of 0.1 to 0.5 kgf/cm ² are 30 to 50 KHz It is manufactured through the process of extracting using an output of 100 to 200 watts for 30 to 60 minutes at the vibration frequency of,
The inorganic extract is Eoseongcho containing wild ginseng component, characterized in that it is included in a weight ratio of 5 to 10 parts by weight of sericite extract, 1 to 5 parts by weight of elvan extract, 3 to 7 parts by weight of ocher extract and 2 to 6 parts by weight of zeolite extract Method for producing fermented oil. delete delete delete delete delete