KR102562820B1 - Perfume composition with air purifying effect and manufacturing method thereof - Google Patents
Perfume composition with air purifying effect and manufacturing method thereof Download PDFInfo
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- KR102562820B1 KR102562820B1 KR1020230043182A KR20230043182A KR102562820B1 KR 102562820 B1 KR102562820 B1 KR 102562820B1 KR 1020230043182 A KR1020230043182 A KR 1020230043182A KR 20230043182 A KR20230043182 A KR 20230043182A KR 102562820 B1 KR102562820 B1 KR 102562820B1
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Abstract
Description
본 발명은 공기정화 효과를 가진 향수 조성물 및 그 제조방법에 관한 것이다.The present invention relates to a perfume composition having an air purifying effect and a manufacturing method thereof.
일반적으로, 경제의 발달과 더불어 생활수준이 향상됨에 따라 외모를 아름답게 가꾸고자 하는 욕구가 증대되고 있으며, 이와 같은 외모를 아름답게 가꿀 수 있는 재료로서 각종 화장품 및 향수 등이 제안되어 시판되고 있다.In general, with the development of the economy and the improvement of living standards, the desire to beautify the appearance is increasing, and various cosmetics and perfumes are proposed and marketed as materials that can beautify the appearance.
한편, 향수는 화장품의 일종으로서 향을 내는 물질들을 적당한 비율로 배합한 후 알코올 등에 용해시켜 제조하고, 신체의 일부분이나 옷에 뿌려 사용하며, 피부로부터 발산되는 체온 또는 체취와 함께 섞여서 향기를 발산시키는 것이다.On the other hand, perfume is a type of cosmetic product that is prepared by mixing fragrance-producing substances in an appropriate ratio and then dissolving them in alcohol, etc., spraying them on parts of the body or clothes, and mixing them with body temperature or body odor emitted from the skin to emit fragrance. will be.
이와 같이 향수를 신체 또는 의복 등에 사용하면, 신체 또는 의복으로부터 발산되는 나쁜 냄새가 저감 또는 차단되고, 향수로부터 발산되는 좋은 향기에 의하여 타인으로 하여금 호감을 불러일으키기 때문에 남녀를 불문하고 현대인들에게 매우 선호되는 화장품의 일종으로 자리매김하게 되었다.In this way, when perfume is used on the body or clothes, bad odors emitted from the body or clothes are reduced or blocked, and good fragrance emitted from the perfume arouses others' liking, so it is highly preferred by modern people regardless of gender. It has become a type of cosmetic product.
그러나 종래의 향수는 단순히 향을 발산하는 것에 의해 나쁜 냄새를 잡아주는 것으로, 나쁜 냄새의 완전 제거와 동시에 방향성을 지속하는 데는 한계점이 있었다.However, conventional perfumes simply catch bad smells by emitting fragrance, and there is a limit to completely removing bad smells and maintaining aromaticity at the same time.
따라서 신체나 의복의 불쾌한 냄새를 제거할 목적으로 냄새 제거 및 지속력이 우수한 향수가 요구되고 있다.Therefore, for the purpose of removing unpleasant odors from the body or clothes, perfumes with excellent odor removal and longevity are required.
본 발명은 상기와 같은 문제점을 해결하기 위해 안출된 것으로서, 본 발명의 목적은 지속성이 우수한 향수 조성물 및 그 제조방법을 제공하는 것이다.The present invention has been made to solve the above problems, and an object of the present invention is to provide a perfume composition with excellent durability and a manufacturing method thereof.
본 발명의 과제는 이상에서 언급한 과제들로 제한되지 않으며, 언급되지 않은 또 다른 과제들은 아래의 기재로부터 당업자에게 명확하게 이해될 수 있을 것이다.The object of the present invention is not limited to the tasks mentioned above, and other tasks not mentioned will be clearly understood by those skilled in the art from the following description.
상기 목적을 달성하기 위하여 본 발명은In order to achieve the above object, the present invention
지속성이 우수한 향수 조성물을 제공한다.A perfume composition with excellent durability is provided.
또한, 상기 향수 조성물은,In addition, the perfume composition,
구아이악우드 오일 18-22 중량부, 바닐라 오일 18-22 중량부, 만다린 오일 6-10 중량부, 헥실살리실레이트 4-8 중량부, 디옥틸아디페이트 18-22 중량부, 프로필렌글리콜 1-5 중량부, 부틸페닐메칠프로피오날 1-5 중량부 및 에탄올 18-22 중량부를 포함하는 향료원료 18-22 중량부; 및Guaiacwood oil 18-22 parts by weight, vanilla oil 18-22 parts by weight, mandarin oil 6-10 parts by weight, hexyl salicylate 4-8 parts by weight, dioctyl adipate 18-22 parts by weight, propylene glycol 1- 18-22 parts by weight of perfume raw materials including 5 parts by weight, 1-5 parts by weight of butylphenylmethylpropional and 18-22 parts by weight of ethanol; and
편백수 42-46 중량부, 브로콜리수 38-42 중량부, 이소프로필 이소스테아레이트 1-5 중량부 및 파이버솔-2(Fibersol-2) 1-5 중량부를 포함하는 향수원료 78-82 중량부;를 포함한다.78-82 parts by weight of perfume raw materials including 42-46 parts by weight of cypress water, 38-42 parts by weight of broccoli water, 1-5 parts by weight of isopropyl isostearate and 1-5 parts by weight of Fibersol-2 includes;
또한, 상기 향수 조성물은,In addition, the perfume composition,
구아이악우드 오일 18-22 중량부, 바닐라 오일 18-22 중량부, 만다린 오일 6-10 중량부, 헥실살리실레이트 4-8 중량부, 디옥틸아디페이트 18-22 중량부, 프로필렌글리콜 1-5 중량부, 부틸페닐메칠프로피오날 1-5 중량부 및 에탄올 18-22 중량부를 포함하는 향료원료 18-22 중량부;Guaiacwood oil 18-22 parts by weight, vanilla oil 18-22 parts by weight, mandarin oil 6-10 parts by weight, hexyl salicylate 4-8 parts by weight, dioctyl adipate 18-22 parts by weight, propylene glycol 1- 18-22 parts by weight of perfume raw materials including 5 parts by weight, 1-5 parts by weight of butylphenylmethylpropional and 18-22 parts by weight of ethanol;
편백수 42-46 중량부, 브로콜리수 38-42 중량부, 이소프로필 이소스테아레이트 1-5 중량부 및 파이버솔-2(Fibersol-2) 1-5 중량부를 포함하는 향수원료 68-72 중량부; 및68-72 parts by weight of perfume raw materials including 42-46 parts by weight of cypress water, 38-42 parts by weight of broccoli water, 1-5 parts by weight of isopropyl isostearate and 1-5 parts by weight of Fibersol-2 ; and
황련뿌리추출물 4-8 중량부, 후박나무줄기추출물 4-8 중량부, 동애등에 추출물 2-6 중량부, 타임잎오일 2-6 중량부, 박하잎오일 2-6 중량부, 마누카잎오일 2-6 중량부, 부틸렌글라이콜 3-7 중량부, 글리세린 4-8 중량부, 변성알코올 1-5 중량부, 다이프로필렌글라이콜 1-5 중량부, 글리세레스-26 1-5 중량부, 1,2-헥산다이올 0.5-4 중량부, 자일리톨 0.5-4 중량부, 하이드록시아세토페논 0.5-4 중량부, 글리세레스-25피씨에이아이소스테아레이트 0.5-4 중량부, 다이페닐다이메티콘 0.3-3 중량부, 에틸헥실글리세린 0.05-1 중량부, 트라이에틸헥사노인 0.05-1 중량부, 다이소듐이디티에이 0.05-1 중량부, 하이드로제네이티드레시틴 0.05-1 중량부 및 화산석 추출액 39-43 중량부를 포함하는 탈취원료 8-12 중량부;를 포함한다.4-8 parts by weight of barberry root extract, 4-8 parts by weight of Sulfur tree stem extract, 2-6 parts by weight of Dongae extract, 2-6 parts by weight of thyme leaf oil, 2-6 parts by weight of peppermint leaf oil, 2 parts of manuka leaf oil -6 parts by weight, butylene glycol 3-7 parts by weight, glycerin 4-8 parts by weight, denatured alcohol 1-5 parts by weight, dipropylene glycol 1-5 parts by weight, glycereth-26 1-5 parts by weight , 0.5-4 parts by weight of 1,2-hexanediol, 0.5-4 parts by weight of xylitol, 0.5-4 parts by weight of hydroxyacetophenone, 0.5-4 parts by weight of glycereth-25PCA isostearate, diphenyldime Thicon 0.3-3 parts by weight, ethylhexylglycerin 0.05-1 parts by weight, triethylhexanoin 0.05-1 parts by weight, disodium EDTA 0.05-1 parts by weight, hydrogenated lecithin 0.05-1 parts by weight and volcanic stone extract 39 8-12 parts by weight of deodorizing raw materials including -43 parts by weight;
또한, 본 발명은In addition, the present invention
구아이악우드 오일 18-22 중량부, 바닐라 오일 18-22 중량부, 만다린 오일 6-10 중량부, 헥실살리실레이트 4-8 중량부, 디옥틸아디페이트 18-22 중량부, 프로필렌글리콜 1-5 중량부, 부틸페닐메칠프로피오날 1-5 중량부 및 에탄올 18-22 중량부를 혼합하여 향료원료를 제조하는 단계;Guaiacwood oil 18-22 parts by weight, vanilla oil 18-22 parts by weight, mandarin oil 6-10 parts by weight, hexyl salicylate 4-8 parts by weight, dioctyl adipate 18-22 parts by weight, propylene glycol 1- Preparing a perfume raw material by mixing 5 parts by weight, 1-5 parts by weight of butylphenylmethylpropional and 18-22 parts by weight of ethanol;
편백수 42-46 중량부, 브로콜리수 38-42 중량부, 이소프로필 이소스테아레이트 1-5 중량부 및 파이버솔-2(Fibersol-2) 1-5 중량부를 포함하는 향수원료를 제조하는 단계;Preparing a perfume raw material comprising 42-46 parts by weight of cypress water, 38-42 parts by weight of broccoli water, 1-5 parts by weight of isopropyl isostearate and 1-5 parts by weight of Fibersol-2;
황련뿌리추출물 4-8 중량부, 후박나무줄기추출물 4-8 중량부, 동애등에 추출물 2-6 중량부, 타임잎오일 2-6 중량부, 박하잎오일 2-6 중량부, 마누카잎오일 2-6 중량부, 부틸렌글라이콜 3-7 중량부, 글리세린 4-8 중량부, 변성알코올 1-5 중량부, 다이프로필렌글라이콜 1-5 중량부, 글리세레스-26 1-5 중량부, 1,2-헥산다이올 0.5-4 중량부, 자일리톨 0.5-4 중량부, 하이드록시아세토페논 0.5-4 중량부, 글리세레스-25피씨에이아이소스테아레이트 0.5-4 중량부, 다이페닐다이메티콘 0.3-3 중량부, 에틸헥실글리세린 0.05-1 중량부, 트라이에틸헥사노인 0.05-1 중량부, 다이소듐이디티에이 0.05-1 중량부, 하이드로제네이티드레시틴 0.05-1 중량부 및 화산석 추출액 39-43 중량부를 혼합하여 탈취원료를 제조하는 단계; 및4-8 parts by weight of barberry root extract, 4-8 parts by weight of Sulfur tree stem extract, 2-6 parts by weight of Dongae extract, 2-6 parts by weight of thyme leaf oil, 2-6 parts by weight of peppermint leaf oil, 2 parts of manuka leaf oil -6 parts by weight, butylene glycol 3-7 parts by weight, glycerin 4-8 parts by weight, denatured alcohol 1-5 parts by weight, dipropylene glycol 1-5 parts by weight, glycereth-26 1-5 parts by weight , 0.5-4 parts by weight of 1,2-hexanediol, 0.5-4 parts by weight of xylitol, 0.5-4 parts by weight of hydroxyacetophenone, 0.5-4 parts by weight of glycereth-25PCA isostearate, diphenyldime Thicon 0.3-3 parts by weight, ethylhexylglycerin 0.05-1 parts by weight, triethylhexanoin 0.05-1 parts by weight, disodium EDTA 0.05-1 parts by weight, hydrogenated lecithin 0.05-1 parts by weight and volcanic stone extract 39 - preparing a deodorizing raw material by mixing 43 parts by weight; and
상기 향료원료 18-22 중량부, 향수원료 68-72 중량부 및 탈취원료 8-12 중량부를 혼합하는 단계;를 포함하고,Mixing 18-22 parts by weight of the perfume raw material, 68-72 parts by weight of the perfume raw material and 8-12 parts by weight of the deodorizing raw material;
상기 황련뿌리추출물 및 후박나무줄기추출물은,The barberry root extract and silver gourd tree stem extract,
황련뿌리 및 후박나무 줄기를 세척한 후, 분쇄하여 준비하는 단계; 준비된 황련뿌리 및 후박나무 줄기를 1:1의 중량비율로 혼합한 혼합물 90-110 중량부 및 에탄올과 아세톤이 1:1의 부피비율로 혼합된 혼합용매 900-1100 중량부를 혼합한 후, 초음파공정으로 38-42℃의 온도에서 22-26시간 동안 추출액을 제조하는 단계; 및 상기 추출액을 감압농축 및 동결건조하는 단계;를 수행하여 제조되는 것이고,After washing the root and the stem of the yellow chestnut tree, preparing by crushing; After mixing 90-110 parts by weight of a mixture of the prepared rhizomatous rhizomatous root and Sulfur tree trunk in a weight ratio of 1: 1 and 900-1100 parts by weight of a mixed solvent in which ethanol and acetone are mixed in a volume ratio of 1: 1, ultrasonic process Preparing an extract for 22-26 hours at a temperature of 38-42 ℃; And concentrating and freeze-drying the extract under reduced pressure; it is prepared by performing,
상기 타임잎오일, 박하잎오일 및 마누카잎오일은, The thyme leaf oil, peppermint leaf oil and manuka leaf oil are
타임잎, 박하잎 및 마누카잎을 세척하고, 건조시킨 후 분쇄하는 단계; 분쇄된 타임잎, 박하잎 및 마누카잎을 1:1:1의 중량비율로 혼합하여 혼합물을 제조하고, 상기 혼합물을 이용하여 수증기 증류하는 단계; 및 수증기 증류하여 발생하는 혼합증기를 냉각하여 오일층과 물층으로 분리한 후 오일층을 분리하여 여과하는 단계;를 수행하여 제조되는 것을 특징으로 하는 향수 조성물의 제조방법을 제공한다.Washing, drying, and pulverizing thyme leaves, mint leaves, and manuka leaves; preparing a mixture by mixing pulverized thyme leaves, mint leaves, and manuka leaves in a weight ratio of 1:1:1, and steam distilling the mixture; and cooling the mixed steam generated by steam distillation to separate the oil layer and the water layer, and then separating and filtering the oil layer.
본 발명에 따른 향수 조성물은 지속성이 우수하다. 또한, 향수 발향이 우수하고 피부 자극성이 없어 종합적인 기호도가 우수하다.The perfume composition according to the present invention is excellent in durability. In addition, it is excellent in perfume smell and has no skin irritation, so it has excellent overall acceptability.
도 1은 본 발명에 따른 향수 조성물의 제조방법을 순서도로 나타낸 것이다.1 is a flow chart showing a method for producing a perfume composition according to the present invention.
이하에서는 첨부된 도면을 참조하여 다양한 실시예를 보다 상세하게 설명한다. 본 명세서에 기재된 실시예는 다양하게 변형될 수 있다. 특정한 실시예가 도면에서 묘사되고 상세한 설명에서 자세하게 설명될 수 있다. 그러나 첨부된 도면에 개시된 특정한 실시 예는 다양한 실시예를 쉽게 이해하도록 하기 위한 것일 뿐이다. 따라서 첨부된 도면에 개시된 특정 실시예에 의해 기술적 사상이 제한되는 것은 아니며, 발명의 사상 및 기술 범위에 포함되는 모든 균등물 또는 대체물을 포함하는 것으로 이해되어야 한다.Hereinafter, various embodiments will be described in more detail with reference to the accompanying drawings. The embodiments described in this specification may be modified in various ways. Certain embodiments may be depicted in the drawings and described in detail in the detailed description. However, specific embodiments disclosed in the accompanying drawings are only intended to facilitate understanding of various embodiments. Therefore, the technical idea is not limited by the specific embodiments disclosed in the accompanying drawings, and it should be understood to include all equivalents or substitutes included in the spirit and technical scope of the invention.
1차, 2차, 제1, 제2 등과 같이 서수를 포함하는 용어는 다양한 구성요소들을 설명하는데 사용될 수 있지만, 이러한 구성요소들은 상술한 용어에 의해 한정되지는 않는다. 상술한 용어는 하나의 구성요소를 다른 구성요소로부터 구별하는 목적으로만 사용된다.Terms including ordinal numbers such as primary, secondary, first, and second may be used to describe various elements, but these elements are not limited by the above-mentioned terms. The terminology described above is only used for the purpose of distinguishing one component from another.
본 명세서에서, '포함한다' 또는 '가지다' 등의 용어는 명세서상에 기재된 특징, 숫자, 단계, 동작, 구성요소, 부품 또는 이들을 조합한 것이 존재함을 지정하려는 것이지, 하나 또는 그 이상의 다른 특징들이나 숫자, 단계, 동작, 구성요소, 부품 또는 이들을 조합한 것들의 존재 또는 부가 가능성을 미리 배제하지 않는 것으로 이해되어야 한다. 어떤 구성요소가 다른 구성요소에 '연결되어' 있다거나 '접속되어' 있다고 언급된 때에는, 그 다른 구성요소에 직접적으로 연결되어 있거나 또는 접속되어 있을 수도 있지만, 중간에 다른 구성요소가 존재할 수도 있다고 이해되어야 할 것이다. 반면에, 어떤 구성요소가 다른 구성요소에 '직접 연결되어' 있다거나 '직접 접속되어' 있다고 언급된 때에는, 중간에 다른 구성요소가 존재하지 않는 것으로 이해되어야 할 것이다.In this specification, terms such as 'comprise' or 'having' are intended to designate that there is a feature, number, step, operation, component, part, or combination thereof described in the specification, but one or more other features It should be understood that the presence or addition of numbers, steps, operations, components, parts, or combinations thereof is not precluded. It is understood that when a component is referred to as being 'connected' or 'connected' to another component, it may be directly connected or connected to the other component, but other components may exist in the middle. It should be. On the other hand, when a component is referred to as being 'directly connected' or 'directly connected' to another component, it should be understood that no other component exists in the middle.
그 밖에도, 본 발명을 설명함에 있어서, 관련된 공지 기능 혹은 구성에 대한 구체적인 설명이 본 발명의 요지를 불필요하게 흐릴 수 있다고 판단되는 경우, 그에 대한 상세한 설명은 축약하거나 생략한다.In addition, in describing the present invention, if it is determined that a detailed description of a related known function or configuration may unnecessarily obscure the subject matter of the present invention, the detailed description thereof will be abbreviated or omitted.
본 발명은 the present invention
지속성이 우수한 향수 조성물을 제공한다.A perfume composition with excellent durability is provided.
이하, 본 발명에 따른 향수 조성물에 대하여 상세히 설명한다.Hereinafter, the perfume composition according to the present invention will be described in detail.
본 발명에 따른 향수 조성물은 지속성이 우수하다. 또한, 향수 발향이 우수하고 피부 자극성이 없어 종합적인 기호도가 우수하다.The perfume composition according to the present invention is excellent in durability. In addition, it is excellent in perfume smell and has no skin irritation, so it has excellent overall acceptability.
상기 향수 조성물은,The perfume composition,
구아이악우드 오일 18-22 중량부, 바닐라 오일 18-22 중량부, 만다린 오일 6-10 중량부, 헥실살리실레이트 4-8 중량부, 디옥틸아디페이트 18-22 중량부, 프로필렌글리콜 1-5 중량부, 부틸페닐메칠프로피오날 1-5 중량부 및 에탄올 18-22 중량부를 포함하는 향료원료 18-22 중량부; 및Guaiacwood oil 18-22 parts by weight, vanilla oil 18-22 parts by weight, mandarin oil 6-10 parts by weight, hexyl salicylate 4-8 parts by weight, dioctyl adipate 18-22 parts by weight, propylene glycol 1- 18-22 parts by weight of perfume raw materials including 5 parts by weight, 1-5 parts by weight of butylphenylmethylpropional and 18-22 parts by weight of ethanol; and
편백수 42-46 중량부, 브로콜리수 38-42 중량부, 이소프로필 이소스테아레이트 1-5 중량부 및 파이버솔-2(Fibersol-2) 1-5 중량부를 포함하는 향수원료 78-82 중량부;를 포함하는 것이 바람직하다.78-82 parts by weight of perfume raw materials including 42-46 parts by weight of cypress water, 38-42 parts by weight of broccoli water, 1-5 parts by weight of isopropyl isostearate and 1-5 parts by weight of Fibersol-2 It is preferable to include;
상기 향료원료는 19-21 중량부를 포함하는 것이 더욱 바람직하다.It is more preferable that the spice raw material contains 19-21 parts by weight.
상기 향료원료는 구아이악우드 오일 19-21 중량부, 바닐라 오일 19-21 중량부, 만다린 오일 7-9 중량부, 헥실살리실레이트 5-7 중량부, 디옥틸아디페이트 19-21 중량부, 프로필렌글리콜 2-4 중량부, 부틸페닐메칠프로피오날 2-4 중량부 및 에탄올 19-21 중량부를 포함하는 것이 더욱 바람직하다.The perfume raw materials include 19-21 parts by weight of guaiac wood oil, 19-21 parts by weight of vanilla oil, 7-9 parts by weight of mandarin oil, 5-7 parts by weight of hexyl salicylate, 19-21 parts by weight of dioctyl adipate, It is more preferable to include 2-4 parts by weight of propylene glycol, 2-4 parts by weight of butylphenylmethylpropional and 19-21 parts by weight of ethanol.
구아이악우드(Bulnesia Sarmienti) 오일은 남미에서 자생하는 열대 교목을 증류해서 얻어지는 정유로 은은한 로즈향이 나는 우디한 향취를 가진다. 의식용 장식물 또는 류마티스나 류마티스성 관절염, 성병의 치료에 이용한다. 항염, 항산화, 항류마티즘, 방부, 이뇨, 발한, 설사유도의 효과를 가진다.Guaiac Wood (Bulnsia Sarmienti) Oil is an essential oil obtained by distilling a tropical tree native to South America and has a woody scent with a subtle rose scent. It is used for ceremonial decorations or for the treatment of rheumatism, rheumatoid arthritis, and sexually transmitted diseases. It has anti-inflammatory, antioxidant, antirheumatic, antiseptic, diuretic, sweating, and diarrhea inducing effects.
바닐라(Vanilla Planifolia)는 열대 아메리카 멕시코가 원산지인 난초과 식물로서 통상적으로 열매 부분을 바닐라빈이라고 부른다. 본 발명에서 바닐라빈은, 바닐라 열매(바닐라빈)를 여러 번 찌고 말리는 가공 과정을 거쳐서 수득된 검은색의 독특한 향기가 있는 바닐라 가공 빈을 포함하는 의미로 사용된다.Vanilla (Vanilla Planifolia) is an orchid plant native to Mexico, tropical America, and the fruit part is commonly called vanilla bean. In the present invention, vanilla bean is used as a meaning including vanilla processing beans having a unique aroma of black color obtained by steaming and drying vanilla fruits (vanilla beans) several times.
만다린(mandarin)은 만다린계오렌지라고도 하며, 비타민P와 아스코르빈산, 카로티노이드, 리모노이드 플라보노이드, 구마린, 나린제닌 계통의 성분 등이 들어있다. 그 중에서 나린제닌 계통의 성분은 만다린의 껍질 안에 있는 성분인데 항산화작용이 뛰어난 성분으로 산소와 닿으면서 생기는 미생물의 번식을 막아주는 중요한 역할을 한다.Mandarin, also known as mandarin orange, contains vitamin P, ascorbic acid, carotenoids, limonoid flavonoids, gumarin, and naringenin-type components. Among them, the component of the naringenin system is a component in the peel of mandarin.
상기 헥실살리실레이트 그린, 플로럴, 스파이시한 향이 나는 무색의 액체로, 플로럴 조합 향료의 특징적인 꽃향기를 만드는데 많이 사용된다.The hexyl salicylate is a colorless liquid with a green, floral, and spicy scent, and is often used to make a characteristic floral scent of a floral combination spice.
본 발명에서는 구아이악우드 오일, 바닐라빈 오일, 만다린 오일 및 헥실살리실레이트를 적용하여 천연원료로서 고급스러운 향을 나타낼 수 있다.In the present invention, guaiac wood oil, vanilla bean oil, mandarin oil and hexyl salicylate can be applied to exhibit a luxurious fragrance as natural raw materials.
상기 디옥틸아디페이트, 프로필렌글리콜, 부틸페닐메칠프로피오날 및 에탄올 등은 용제로 적용되어 향료원료를 안정화하고 용이하게 분산시킨다.The dioctyl adipate, propylene glycol, butylphenylmethylpropional, and ethanol are applied as solvents to stabilize and easily disperse the perfume raw materials.
상기 향수원료는 79-81 중량부를 포함하는 것이 더욱 바람직하다.It is more preferable that the perfume raw material contains 79-81 parts by weight.
상기 향수원료는 편백수 43-45 중량부, 브로콜리수 39-41 중량부, 이소프로필 이소스테아레이트 2-4 중량부 및 파이버솔-2(Fibersol-2) 2-4 중량부를 포함하는 것이 더욱 바람직하다.It is more preferable that the perfume raw material includes 43-45 parts by weight of cypress water, 39-41 parts by weight of broccoli water, 2-4 parts by weight of isopropyl isostearate and 2-4 parts by weight of Fibersol-2 do.
편백수는 면역력강화, 아토피 치료, 아토피 예방, 비염치료, 피부 면역력 강화 등등 여러 분야에서 효능이 뛰어나다.Cypress water is effective in various fields such as strengthening immunity, treating atopy, preventing atopy, treating rhinitis, and strengthening skin immunity.
브로콜리는 항산화작용을 가진 베타-카로틴, 루틴, 아스코르빈산, 셀레늄, 케르세틴, 글루타티온 등이 다량 함유되어 있을 뿐만 아니라 칼슘과 비타민C, 엽산 등의 영양 성분도 함유하고 있어 피부 미용에 쓰인다.Broccoli contains a large amount of beta-carotene, rutin, ascorbic acid, selenium, quercetin, and glutathione, which have antioxidant effects, as well as nutrients such as calcium, vitamin C, and folic acid, so it is used for skin care.
이소프로필 이소스테아레이트를 포함하여 섬유 탈취제의 고온 안정성을 확보할 수 있다.Including isopropyl isostearate, high-temperature stability of the fiber deodorant can be secured.
파이버솔-2(Fibersol-2)는 식이섬유로서 전분의 가열, 효소분해, 분획, 정제, 분말화, 파이버솔 추출 공정을 통해 제조될 수 있다. 수용성 식이섬유인 파이버솔-2를 포함하여 향기성분이 서서히 지속적으로 발산하는 효과를 나타내고, 항균, 항진균 작용에 도움을 준다.Fibersol-2 is a dietary fiber and can be prepared through starch heating, enzymatic degradation, fractionation, purification, powderization, and Fibersol extraction processes. Including Fibersol-2, a water-soluble dietary fiber, it shows the effect of slowly and continuously dissipating fragrance components, and helps with antibacterial and antifungal action.
또한, 상기 향수 조성물은,In addition, the perfume composition,
구아이악우드 오일 18-22 중량부, 바닐라 오일 18-22 중량부, 만다린 오일 6-10 중량부, 헥실살리실레이트 4-8 중량부, 디옥틸아디페이트 18-22 중량부, 프로필렌글리콜 1-5 중량부, 부틸페닐메칠프로피오날 1-5 중량부 및 에탄올 18-22 중량부를 포함하는 향료원료 18-22 중량부;Guaiacwood oil 18-22 parts by weight, vanilla oil 18-22 parts by weight, mandarin oil 6-10 parts by weight, hexyl salicylate 4-8 parts by weight, dioctyl adipate 18-22 parts by weight, propylene glycol 1- 18-22 parts by weight of perfume raw materials including 5 parts by weight, 1-5 parts by weight of butylphenylmethylpropional and 18-22 parts by weight of ethanol;
편백수 42-46 중량부, 브로콜리수 38-42 중량부, 이소프로필 이소스테아레이트 1-5 중량부 및 파이버솔-2(Fibersol-2) 1-5 중량부를 포함하는 향수원료 68-72 중량부; 및68-72 parts by weight of perfume raw materials including 42-46 parts by weight of cypress water, 38-42 parts by weight of broccoli water, 1-5 parts by weight of isopropyl isostearate and 1-5 parts by weight of Fibersol-2 ; and
황련뿌리추출물 4-8 중량부, 후박나무줄기추출물 4-8 중량부, 동애등에 추출물 2-6 중량부, 타임잎오일 2-6 중량부, 박하잎오일 2-6 중량부, 마누카잎오일 2-6 중량부, 부틸렌글라이콜 3-7 중량부, 글리세린 4-8 중량부, 변성알코올 1-5 중량부, 다이프로필렌글라이콜 1-5 중량부, 글리세레스-26 1-5 중량부, 1,2-헥산다이올 0.5-4 중량부, 자일리톨 0.5-4 중량부, 하이드록시아세토페논 0.5-4 중량부, 글리세레스-25피씨에이아이소스테아레이트 0.5-4 중량부, 다이페닐다이메티콘 0.3-3 중량부, 에틸헥실글리세린 0.05-1 중량부, 트라이에틸헥사노인 0.05-1 중량부, 다이소듐이디티에이 0.05-1 중량부, 하이드로제네이티드레시틴 0.05-1 중량부 및 화산석 추출액 39-43 중량부를 포함하는 탈취원료 8-12 중량부;를 포함하는 것이 더욱 바람직하다.4-8 parts by weight of barberry root extract, 4-8 parts by weight of Sulfur tree stem extract, 2-6 parts by weight of Dongae extract, 2-6 parts by weight of thyme leaf oil, 2-6 parts by weight of peppermint leaf oil, 2 parts of manuka leaf oil -6 parts by weight, butylene glycol 3-7 parts by weight, glycerin 4-8 parts by weight, denatured alcohol 1-5 parts by weight, dipropylene glycol 1-5 parts by weight, glycereth-26 1-5 parts by weight , 0.5-4 parts by weight of 1,2-hexanediol, 0.5-4 parts by weight of xylitol, 0.5-4 parts by weight of hydroxyacetophenone, 0.5-4 parts by weight of glycereth-25PCA isostearate, diphenyldime Thicon 0.3-3 parts by weight, ethylhexylglycerin 0.05-1 parts by weight, triethylhexanoin 0.05-1 parts by weight, disodium EDTA 0.05-1 parts by weight, hydrogenated lecithin 0.05-1 parts by weight and volcanic stone extract 39 It is more preferable to include; 8-12 parts by weight of a deodorizing raw material including -43 parts by weight.
상기 향수 조성물은 탈취원료를 포함하여 인체에 무해하면서, 곰팡이, 세균 등 미생물의 증식을 방지하고 악취를 제거할 수 있다.The perfume composition can prevent the growth of microorganisms such as mold and bacteria and remove odor while being harmless to the human body, including deodorizing raw materials.
상기 향수 조성물은 향료원료 19-21 중량부, 향수원료 69-71 중량부 및 탈취원료 9-11 중량부를 포함하는 것이 더욱 바람직하다.More preferably, the perfume composition includes 19-21 parts by weight of perfume raw materials, 69-71 parts by weight of perfume raw materials, and 9-11 parts by weight of deodorizing raw materials.
상기 탈취원료는 9-11 중량부 포함하는 것이 더욱 바람직하다.It is more preferable to include 9-11 parts by weight of the deodorizing raw material.
상기 탈취원료는 황련뿌리추출물 5-7 중량부, 후박나무줄기추출물 5-7 중량부, 동애등에 추출물 3-5 중량부, 타임잎오일 3-5 중량부, 박하잎오일 3-5 중량부, 마누카잎오일 3-5 중량부, 부틸렌글라이콜 4-6 중량부, 글리세린 5-7 중량부, 변성알코올 2-4 중량부, 다이프로필렌글라이콜 2-4 중량부, 글리세레스-26 2-4 중량부, 1,2-헥산다이올 1-3 중량부, 자일리톨 1-3 중량부, 하이드록시아세토페논 1-3 중량부, 글리세레스-25피씨에이아이소스테아레이트 1-3 중량부, 다이페닐다이메티콘 0.5-1.5 중량부, 에틸헥실글리세린 0.3-0.7 중량부, 트라이에틸헥사노인 0.3-0.7 중량부, 다이소듐이디티에이 0.3-0.7 중량부, 하이드로제네이티드레시틴 0.3-0.7 중량부 및 화산석 추출액 40-42 중량부를 포함하는 것이 더욱 바람직하다.The deodorizing raw material is 5-7 parts by weight of barberry root extract, 5-7 parts by weight of silver gourd stem extract, 3-5 parts by weight of Dongae extract, 3-5 parts by weight of thyme leaf oil, 3-5 parts by weight of peppermint leaf oil, 3-5 parts by weight of manuka leaf oil, 4-6 parts by weight of butylene glycol, 5-7 parts by weight of glycerin, 2-4 parts by weight of denatured alcohol, 2-4 parts by weight of dipropylene glycol, glycereth-26 2 -4 parts by weight, 1-3 parts by weight of 1,2-hexanediol, 1-3 parts by weight of xylitol, 1-3 parts by weight of hydroxyacetophenone, 1-3 parts by weight of glycereth-25 PCA isostearate, Diphenyldimethicone 0.5-1.5 parts by weight, ethylhexylglycerin 0.3-0.7 parts by weight, triethylhexanoin 0.3-0.7 parts by weight, disodium EDTA 0.3-0.7 parts by weight, hydrogenated lecithin 0.3-0.7 parts by weight and 40-42 parts by weight of a volcanic stone extract.
황련뿌리는 중국, 한국, 일본 등지에서 재배된다. 위를 건강하게 하고 진정, 소염, 항균 등의 효능이 있어 장이나 위에 열이 쌓여서 생기는 설사나 위열로 인한 구토 등의 치료에 사용하였다. 주성분인 berberine은 여러 세균에 대한 강한 억제효과가 있으며, 항염, 지혈, 혈압강하 작용 및 항암효과가 있다.Barberry root is cultivated in China, Korea, and Japan. It makes the stomach healthy and has sedative, anti-inflammatory, and antibacterial effects, so it was used to treat diarrhea caused by heat accumulation in the intestines or stomach or vomiting caused by gastric fever. The main ingredient, berberine, has a strong inhibitory effect on various bacteria, and has anti-inflammatory, hemostatic, blood pressure lowering and anti-cancer effects.
후박나무(Magnolia officinalis Rehd et Wils.)는 중국이 원산으로 우리나라에서는 주로 남부 도서 지방의 표고 700m 이하에서 자라는 것으로 알려져 있으며 높이가 5~15미터까지 자라는 낙엽교목이다. 후박의 효능으로는 위궤양, 십이지장 경련에 효과가 있고 또한 혈압 강하 작용 및 비교적 강한 항균 작용을 가지는 것으로 보고되어 있다. 이밖에도 급성장염이나 세균성 이질에 효과가 있다는 임상보고도 있다. 후박의 주요성분으로는 honokiol, magnolol, eudesmagnolol, magnoloside A, B, C, magnocurarine이 있다. honokiol은 항균, 근육긴장완화, 항암, 항산화 효과가 보고되었으며, magnolol은 항암활성, 항염증작용, 항알레르기 활성 및 항천식제 기능을 가지는 것으로 알려졌다. 그리고 eudesmagnolol은 세포 독성이 있는 것으로 나타났다.Magnolia officinalis Rehd et Wils. is a deciduous tree that is native to China and is known to grow below 700m above sea level in the southern islands in Korea and grows up to 5-15m in height. It is reported to be effective for gastric ulcer and duodenal spasm, and also to have blood pressure lowering action and relatively strong antibacterial action. In addition, there are clinical reports that it is effective for acute gastroenteritis or bacterial dysentery. The major components of succulents include honokiol, magnolol, eudesmagnolol, magnoloside A, B, C, and magnocurarine. Honokiol has been reported to have antibacterial, muscle tension, anticancer and antioxidant effects, and magnolol is known to have anticancer activity, anti-inflammatory activity, anti-allergic activity and anti-asthmatic activity. And eudesmagnolol has been shown to be cytotoxic.
동애등에(Hermetiaillucens, black sodier fly)는 아메리카 동애등에라고 알려진 파리목 동애등에과의 대표적인 환경정화 곤충이다. 아메리카 동애등에(Hermetia illucens)는 환경정화 곤충으로서 세균, 곰팡이, 바이러스 등이 다량 포함된 유기성폐기물(음식물쓰레기, 축분폐기물, 농업부산물 등)에 생존하면서 이들 유기성폐기물을 신속하게 분해하기 위하여 강력한 항균물질을 발현하는 기작을 보유하고 있다. 따라서 화학항생제를 대체할 수 있는 천연항생제의 개발 소재로써 매우 우수할 뿐만 아니라 다른 곤충에 비하여 성장속도가 매우 빠르며 별도의 사료비가 들지 않아 천연항생제로서 이용을 기대하고 있다.Black sodier fly (Hermetia illucens, black sodier fly) is a representative environmental cleaning insect of the family Diptera black sodier fly, also known as American black sodier fly. American blackbird (Hermetia illucens) is an environmental cleaning insect that survives in organic waste (food waste, livestock waste, agricultural by-products, etc.) containing a large amount of bacteria, fungi, and viruses, and quickly decomposes these organic wastes with strong antibacterial substances. has a mechanism for expressing Therefore, it is very excellent as a material for development of natural antibiotics that can replace chemical antibiotics, and it is expected to be used as a natural antibiotic because it has a very fast growth rate compared to other insects and does not require additional feed costs.
타임(Thyme)은 유럽의 중부 또는 남부와 북아프리카에서 주로 재배되기는 하지만 전세계에서 고루 재배되고 있으며, 높이는 30㎝이다. 잔뿌리가 많은 뿌리에서 사각 모양의 줄기가 나와 위로 올라가며 곁가지를 많이 친다. 잎줄기는 매우 짧고, 길이 5~9㎜, 너비 3㎜ 정도인 긴 타원형의 잎 가장자리는 안으로 굽고 잔털이 많다. 방부작용, 항균작용, 거담작용 등으로 이용되고 있다.Thyme is cultivated throughout the world, although it is mainly grown in central or southern Europe and North Africa, and has a height of 30 cm. A square-shaped stem comes out of the root with many fine roots and goes up, giving many side branches. The leaf stem is very short, and the edge of a long oval leaf with a length of 5 to 9 mm and a width of 3 mm is bent inward and has many fine hairs. It is used for antiseptic, antibacterial, and expectorant effects.
박하는 꿀풀과(Lamiaceae)에 속하는 다년생 식물로 거풍, 해열, 해독의 효능이 있고 풍열, 두통, 인후종통, 복부고창, 치통, 피부소양에 대해 치료효과가 있으며 주성분으로 l-limonene이 포함되어있다(이승은 등, 2005, Lee et al., 2005).Mint is a perennial plant belonging to the Lamiaceae family. It is effective for wind chill, antipyretic, and detoxification, and is effective for wind fever, headache, sore throat, flatulence, toothache, and skin itching. It contains l-limonene as its main ingredient. (Lee Seung-eun et al., 2005, Lee et al., 2005).
마누카 오일에는 휘발성 정유성분이 다량 함유되어 있으며, 이중 테르베노이드(Terpenoid)계 성분으로는 모노테르페노이드 성분으로 알파-피넨(alpha-pinene), 알파-테르피놀(alpha-terpinol), 1,8-시네올(1,8-cineole), p-사이멘(p-cymene)등이 존재하며, 세스키테르페노이드계 성분으로 비리디플로롤(viridiflorol) 및 이소메릭 알파, 베타, 감마-유데스몰류(isomeric alpha, beta, gamma-eudesmols)를 함유하고 있다.Manuka oil contains a large amount of volatile essential oil components, among which terpenoid components are monoterpenoid components such as alpha-pinene, alpha-terpinol, 1, There are 8-cineole (1,8-cineole), p-cymene, etc., and viridiflorol and isomeric alpha, beta, gamma- Contains eudesmols (isomeric alpha, beta, gamma-eudesmols).
화산석 추출액은 다양한 미네랄 성분들이 복합적으로 함유되어 있으며, 특히 유황을 비롯한 마그네슘, 칼슘, 칼륨, 염소, 나트륨 및 인 등의 필수 미네랄 성분들이 다량으로 함유되어 있어 항균 효과 및 탈취 효과가 매우 우수하다.The volcanic stone extract contains a variety of mineral components in a complex way, and in particular, contains a large amount of essential minerals such as sulfur, magnesium, calcium, potassium, chlorine, sodium and phosphorus, so it has excellent antibacterial and deodorizing effects.
또한, 상기 탈취원료는 미강 발효추출물을 포함하는 것이 더욱 바람직하고, 상기 미강 발효추출물은 전체 탈취원료 100 중량부에 대하여 0.3-3 중량부 포함하는 것이 바람직하고, 0.5-1.5 중량부 포함하는 것이 더욱 바람직하다. 상기 미강 발효추출물을 포함하여 소취성능을 더욱 높일 수 있다.In addition, the deodorizing raw material more preferably includes a fermented rice bran extract, and the fermented rice bran extract preferably contains 0.3-3 parts by weight, and more preferably 0.5-1.5 parts by weight based on 100 parts by weight of the total deodorizing raw material. desirable. The deodorizing performance can be further improved by including the fermented rice bran extract.
또한, 본 발명은In addition, the present invention
구아이악우드 오일 18-22 중량부, 바닐라 오일 18-22 중량부, 만다린 오일 6-10 중량부, 헥실살리실레이트 4-8 중량부, 디옥틸아디페이트 18-22 중량부, 프로필렌글리콜 1-5 중량부, 부틸페닐메칠프로피오날 1-5 중량부 및 에탄올 18-22 중량부를 혼합하여 향료원료를 제조하는 단계;Guaiacwood oil 18-22 parts by weight, vanilla oil 18-22 parts by weight, mandarin oil 6-10 parts by weight, hexyl salicylate 4-8 parts by weight, dioctyl adipate 18-22 parts by weight, propylene glycol 1- Preparing a perfume raw material by mixing 5 parts by weight, 1-5 parts by weight of butylphenylmethylpropional and 18-22 parts by weight of ethanol;
편백수 42-46 중량부, 브로콜리수 38-42 중량부, 이소프로필 이소스테아레이트 1-5 중량부 및 파이버솔-2(Fibersol-2) 1-5 중량부를 포함하는 향수원료를 제조하는 단계;Preparing a perfume raw material comprising 42-46 parts by weight of cypress water, 38-42 parts by weight of broccoli water, 1-5 parts by weight of isopropyl isostearate and 1-5 parts by weight of Fibersol-2;
황련뿌리추출물 4-8 중량부, 후박나무줄기추출물 4-8 중량부, 동애등에 추출물 2-6 중량부, 타임잎오일 2-6 중량부, 박하잎오일 2-6 중량부, 마누카잎오일 2-6 중량부, 부틸렌글라이콜 3-7 중량부, 글리세린 4-8 중량부, 변성알코올 1-5 중량부, 다이프로필렌글라이콜 1-5 중량부, 글리세레스-26 1-5 중량부, 1,2-헥산다이올 0.5-4 중량부, 자일리톨 0.5-4 중량부, 하이드록시아세토페논 0.5-4 중량부, 글리세레스-25피씨에이아이소스테아레이트 0.5-4 중량부, 다이페닐다이메티콘 0.3-3 중량부, 에틸헥실글리세린 0.05-1 중량부, 트라이에틸헥사노인 0.05-1 중량부, 다이소듐이디티에이 0.05-1 중량부, 하이드로제네이티드레시틴 0.05-1 중량부 및 화산석 추출액 39-43 중량부를 혼합하여 탈취원료를 제조하는 단계; 및4-8 parts by weight of barberry root extract, 4-8 parts by weight of Sulfur tree stem extract, 2-6 parts by weight of Dongae extract, 2-6 parts by weight of thyme leaf oil, 2-6 parts by weight of peppermint leaf oil, 2 parts of manuka leaf oil -6 parts by weight, butylene glycol 3-7 parts by weight, glycerin 4-8 parts by weight, denatured alcohol 1-5 parts by weight, dipropylene glycol 1-5 parts by weight, glycereth-26 1-5 parts by weight , 0.5-4 parts by weight of 1,2-hexanediol, 0.5-4 parts by weight of xylitol, 0.5-4 parts by weight of hydroxyacetophenone, 0.5-4 parts by weight of glycereth-25PCA isostearate, diphenyldime Thicon 0.3-3 parts by weight, ethylhexylglycerin 0.05-1 parts by weight, triethylhexanoin 0.05-1 parts by weight, disodium EDTA 0.05-1 parts by weight, hydrogenated lecithin 0.05-1 parts by weight and volcanic stone extract 39 - preparing a deodorizing raw material by mixing 43 parts by weight; and
상기 향료원료 18-22 중량부, 향수원료 68-72 중량부 및 탈취원료 8-12 중량부를 혼합하는 단계;를 포함하는 향수 조성물의 제조방법을 제공한다.It provides a method for producing a perfume composition comprising the step of mixing 18-22 parts by weight of the perfume raw material, 68-72 parts by weight of the perfume raw material and 8-12 parts by weight of the deodorizing raw material.
이때, 도 1에 본 발명에 따른 향수 조성물의 제조방법을 순서도로 나타내었으며, 이하, 도 1을 참조하여 본 발명에 따른 향수 조성물의 제조방법을 각 단계별로 상세히 설명한다.At this time, the manufacturing method of the perfume composition according to the present invention in Figure 1 is shown in a flowchart, hereinafter, with reference to Figure 1, the manufacturing method of the perfume composition according to the present invention will be described in detail for each step.
먼저, 본 발명에 따른 향수 조성물의 제조방법은 구아이악우드 오일 18-22 중량부, 바닐라 오일 18-22 중량부, 만다린 오일 6-10 중량부, 헥실살리실레이트 4-8 중량부, 디옥틸아디페이트 18-22 중량부, 프로필렌글리콜 1-5 중량부, 부틸페닐메칠프로피오날 1-5 중량부 및 에탄올 18-22 중량부를 혼합하여 향료원료를 제조하는 단계를 포함한다.First, the method for producing a perfume composition according to the present invention includes 18-22 parts by weight of guaiac wood oil, 18-22 parts by weight of vanilla oil, 6-10 parts by weight of mandarin oil, 4-8 parts by weight of hexyl salicylate, dioctyl and preparing a perfume raw material by mixing 18-22 parts by weight of adipate, 1-5 parts by weight of propylene glycol, 1-5 parts by weight of butylphenylmethylpropional, and 18-22 parts by weight of ethanol.
상기 향료원료를 제조하는 단계는 33-37℃의 온도에서 250-500 rpm의 회전속도로 교반하여 수행하는 것이 바람직하고, 34-36℃의 온도에서 300-400 rpm의 회전속도로 교반하여 수행하는 것이 바람직하다.The step of preparing the perfume raw material is preferably performed by stirring at a rotational speed of 250-500 rpm at a temperature of 33-37 ° C., and stirring at a rotational speed of 300-400 rpm at a temperature of 34-36 ° C. it is desirable
상기 구아이악우드 오일은, 구아이악우드를 세척하고, 건조시킨 후 분쇄하는 단계; 분쇄된 구아이악우드를 이용하여 수증기 증류하는 단계; 및 수증기 증류하여 발생하는 혼합증기를 냉각하여 오일층과 물층으로 분리한 후 오일층을 분리하여 여과하는 단계;를 수행하여 제조되는 것이 바람직하다.The guaiac wood oil is obtained by washing, drying, and pulverizing the guaiac wood; steam distillation using pulverized guaiac wood; and cooling the mixed steam generated by steam distillation to separate the oil layer and the water layer, and then separating and filtering the oil layer.
상기 바닐라 오일은, 바닐라빈을 세척하고, 건조시킨 후 분쇄하는 단계; 분쇄된 바닐라빈을 이용하여 수증기 증류하는 단계; 및 수증기 증류하여 발생하는 혼합증기를 냉각하여 오일층과 물층으로 분리한 후 오일층을 분리하여 여과하는 단계;를 수행하여 제조되는 것이 바람직하다.The vanilla oil, washing the vanilla bean, drying and then pulverizing; Steam distillation using pulverized vanilla beans; and cooling the mixed steam generated by steam distillation to separate the oil layer and the water layer, and then separating and filtering the oil layer.
상기 만다린 오일은, 만다린을 세척하고, 건조시킨 후 분쇄하는 단계; 분쇄된 만다린을 이용하여 수증기 증류하는 단계; 및 수증기 증류하여 발생하는 혼합증기를 냉각하여 오일층과 물층으로 분리한 후 오일층을 분리하여 여과하는 단계;를 수행하여 제조되는 것이 바람직하다.The mandarin oil may be obtained by washing, drying, and grinding the mandarin; steam distillation using pulverized mandarin; and cooling the mixed steam generated by steam distillation to separate the oil layer and the water layer, and then separating and filtering the oil layer.
다음으로, 본 발명에 따른 향수 조성물의 제조방법은 편백수 42-46 중량부, 브로콜리수 38-42 중량부, 이소프로필 이소스테아레이트 1-5 중량부 및 파이버솔-2(Fibersol-2) 1-5 중량부를 포함하는 향수원료를 제조하는 단계를 포함한다.Next, the manufacturing method of the perfume composition according to the present invention is 42-46 parts by weight of cypress water, 38-42 parts by weight of broccoli water, 1-5 parts by weight of isopropyl isostearate and Fibersol-2 (Fibersol-2) 1 -Including the step of preparing a perfume raw material containing 5 parts by weight.
상기 향수원료를 제조하는 단계는 18-22℃의 온도에서 50-150 rpm의 회전속도로 교반하여 수행하는 것이 바람직하고, 19-21℃의 온도에서 80-120 rpm의 회전속도로 교반하여 수행하는 것이 바람직하다.The step of preparing the perfume raw material is preferably carried out by stirring at a rotational speed of 50-150 rpm at a temperature of 18-22 ° C, stirring at a rotational speed of 80-120 rpm at a temperature of 19-21 ° C. it is desirable
다음으로, 본 발명에 따른 향수 조성물의 제조방법은 황련뿌리추출물 4-8 중량부, 후박나무줄기추출물 4-8 중량부, 동애등에 추출물 2-6 중량부, 타임잎오일 2-6 중량부, 박하잎오일 2-6 중량부, 마누카잎오일 2-6 중량부, 부틸렌글라이콜 3-7 중량부, 글리세린 4-8 중량부, 변성알코올 1-5 중량부, 다이프로필렌글라이콜 1-5 중량부, 글리세레스-26 1-5 중량부, 1,2-헥산다이올 0.5-4 중량부, 자일리톨 0.5-4 중량부, 하이드록시아세토페논 0.5-4 중량부, 글리세레스-25피씨에이아이소스테아레이트 0.5-4 중량부, 다이페닐다이메티콘 0.3-3 중량부, 에틸헥실글리세린 0.05-1 중량부, 트라이에틸헥사노인 0.05-1 중량부, 다이소듐이디티에이 0.05-1 중량부, 하이드로제네이티드레시틴 0.05-1 중량부 및 화산석 추출액 39-43 중량부를 혼합하여 탈취원료를 제조하는 단계를 포함한다.Next, the method for producing a perfume composition according to the present invention includes 4-8 parts by weight of barberry root extract, 4-8 parts by weight of silver gourd stem extract, 2-6 parts by weight of Dongae extract, 2-6 parts by weight of thyme leaf oil, Peppermint leaf oil 2-6 parts by weight, Manuka leaf oil 2-6 parts by weight, Butylene glycol 3-7 parts by weight, Glycerin 4-8 parts by weight, Denatured alcohol 1-5 parts by weight, Dipropylene glycol 1- 5 parts by weight, 1-5 parts by weight of glycereth-26, 0.5-4 parts by weight of 1,2-hexanediol, 0.5-4 parts by weight of xylitol, 0.5-4 parts by weight of hydroxyacetophenone, 0.5-4 parts by weight of glycereth-25 PCAI Sostearate 0.5-4 parts by weight, diphenyldimethicone 0.3-3 parts by weight, ethylhexylglycerin 0.05-1 parts by weight, triethylhexanoin 0.05-1 parts by weight, disodium EDTA 0.05-1 parts by weight, and preparing a deodorizing raw material by mixing 0.05-1 part by weight of hydrogenated lecithin and 39-43 parts by weight of a volcanic stone extract.
상기 탈취원료를 제조하는 단계는 38-42℃의 온도에서 700-900 rpm의 회전속도로 교반하여 수행하는 것이 바람직하고, 39-41℃의 온도에서 750-850 rpm의 회전속도로 교반하여 수행하는 것이 바람직하다.The step of preparing the deodorizing raw material is preferably performed by stirring at a rotational speed of 700-900 rpm at a temperature of 38-42 ° C, and stirring at a rotational speed of 750-850 rpm at a temperature of 39-41 ° C. it is desirable
상기 황련뿌리추출물 및 후박나무줄기추출물은,The barberry root extract and silver gourd tree stem extract,
황련뿌리 및 후박나무 줄기를 세척한 후, 분쇄하여 준비하는 단계; 준비된 황련뿌리 및 후박나무 줄기를 1:1의 중량비율로 혼합한 혼합물 90-110 중량부 및 에탄올과 아세톤이 1:1의 부피비율로 혼합된 혼합용매 900-1100 중량부를 혼합한 후, 초음파공정으로 38-42℃의 온도에서 22-26시간 동안 추출액을 제조하는 단계; 및 상기 추출액을 감압농축 및 동결건조하는 단계;를 수행하여 제조되는 것이 바람직하다.After washing the root and the stem of the yellow chestnut tree, preparing by crushing; After mixing 90-110 parts by weight of a mixture of the prepared rhizomatous rhizomatous root and Sulfur tree trunk in a weight ratio of 1: 1 and 900-1100 parts by weight of a mixed solvent in which ethanol and acetone are mixed in a volume ratio of 1: 1, ultrasonic process Preparing an extract for 22-26 hours at a temperature of 38-42 ℃; It is preferably prepared by performing; and concentrating and freeze-drying the extract under reduced pressure.
상기 동애등에 추출물은, The blackcurrant extract,
살아있는 동애등에를 진공 챔버에 놓고, 감압하여 진공상태로 30-90분 동안 유지시키는 단계; 동애등에를 꺼내어 흐르는 물로 세척한 후, 식초물에 15-45분 동안 침지시키고, 다시 흐르는 물로 세척하는 단계; 세척된 동애등에를 80-100℃의 온도에서 60-120분 동안 1차 열처리하는 단계; 1차 열처리된 동애등에를 260-300℃의 온도에서 10-20분 동안 2차 열처리하는 단계; 2차 열처리된 동애등에를 찌는 단계; 및 찐 동애등에를 분쇄하고, 동결건조하는 단계;를 수행하여 제조되는 것이 바람직하다.Placing live black soldier flies in a vacuum chamber and maintaining the vacuum under reduced pressure for 30-90 minutes; Taking out black soldier flies, washing them with running water, immersing them in vinegar water for 15-45 minutes, and washing them again with running water; Primary heat treatment of the washed black soldier flies at a temperature of 80-100 ° C. for 60-120 minutes; Secondary heat treatment for 10-20 minutes at a temperature of 260-300 ° C.; Steaming the secondary heat treatment of Dongae, etc.; and crushing and freeze-drying the steamed black soldier flies.
상기 타임잎오일, 박하잎오일 및 마누카잎오일은, The thyme leaf oil, peppermint leaf oil and manuka leaf oil are
타임잎, 박하잎 및 마누카잎을 세척하고, 건조시킨 후 분쇄하는 단계; 분쇄된 타임잎, 박하잎 및 마누카잎을 1:1:1의 중량비율로 혼합하여 혼합물을 제조하고, 상기 혼합물을 이용하여 수증기 증류하는 단계; 및 수증기 증류하여 발생하는 혼합증기를 냉각하여 오일층과 물층으로 분리한 후 오일층을 분리하여 여과하는 단계;를 수행하여 제조되는 것이 바람직하다.Washing, drying, and pulverizing thyme leaves, mint leaves, and manuka leaves; preparing a mixture by mixing pulverized thyme leaves, mint leaves, and manuka leaves in a weight ratio of 1:1:1, and steam distilling the mixture; and cooling the mixed steam generated by steam distillation to separate the oil layer and the water layer, and then separating and filtering the oil layer.
또한, 상기 탈취원료는 미강 발효추출물을 포함하는 것이 더욱 바람직하고, 상기 미강 발효추출물은 전체 탈취원료 100 중량부에 대하여 0.3-3 중량부 포함하는 것이 바람직하고, 0.5-1.5 중량부 포함하는 것이 더욱 바람직하다. 상기 미강 발효추출물을 포함하여 소취성능을 더욱 높일 수 있다.In addition, the deodorizing raw material more preferably includes a fermented rice bran extract, and the fermented rice bran extract preferably contains 0.3-3 parts by weight, and more preferably 0.5-1.5 parts by weight based on 100 parts by weight of the total deodorizing raw material. desirable. The deodorizing performance can be further improved by including the fermented rice bran extract.
상기 미강 발효추출물은,The fermented rice bran extract,
미강을 끓인 물로 세척하고, 분쇄하여 미강분말을 준비하는 단계; 미강분말 및 물을 혼합한 혼합물에 효모균으로 사카로미케스 케레비시아이(Saccharomyces cerevisiae)를 첨가한 후 33-37℃의 온도에서 22-26시간 동안 발효시키는 단계; 발효된 혼합물 및 부틸렌글리콜을 혼합하고, 28-32℃의 온도에서 6-8일 동안 교반하여 추출물을 제조하는 단계; 및 상기 추출물을 여과 및 감압농축한 후 동결건조하는 단계;를 수행하여 제조되는 것을 사용한다.preparing rice bran powder by washing rice bran with boiled water and grinding it; Adding Saccharomyces cerevisiae as a yeast to a mixture of rice bran powder and water, followed by fermentation at a temperature of 33-37 ° C. for 22-26 hours; Preparing an extract by mixing the fermented mixture and butylene glycol and stirring at a temperature of 28-32 ° C. for 6-8 days; and lyophilizing the extract after filtering and concentrating under reduced pressure.
다음으로, 본 발명에 따른 향수 조성물의 제조방법은 상기 향료원료 18-22 중량부, 향수원료 68-72 중량부 및 탈취원료 8-12 중량부를 혼합하는 단계를 포함한다.Next, the method for producing a perfume composition according to the present invention includes mixing 18-22 parts by weight of the perfume raw material, 68-72 parts by weight of the perfume raw material, and 8-12 parts by weight of the deodorizing raw material.
상기 혼합하는 단계는 33-37℃의 온도에서 500-700 rpm의 회전속도로 교반하여 수행하는 것이 바람직하고, 34-36℃의 온도에서 550-650 rpm의 회전속도로 교반하여 수행하는 것이 바람직하다.The mixing step is preferably performed by stirring at a rotation speed of 500-700 rpm at a temperature of 33-37 ° C, and preferably performed by stirring at a rotation speed of 550-650 rpm at a temperature of 34-36 ° C. .
이하, 본 발명을 하기의 실시예에 의해 보다 상세하게 설명한다.Hereinafter, the present invention will be described in more detail by the following examples.
단, 하기 실시예는 본 발명의 내용을 예시하는 것일 뿐 발명의 범위가 실시예 및 실험예에 의해 한정되는 것은 아니다.However, the following examples are merely illustrative of the content of the present invention, but the scope of the invention is not limited by the examples and experimental examples.
<제조예 1> 향료원료의 제조<Preparation Example 1> Preparation of perfume raw materials
구아이악우드를 세척하고, 건조시킨 후 분쇄하였다. 분쇄된 구아이악우드를 이용하여 수증기 증류하고, 수증기 증류하여 발생하는 혼합증기를 냉각하여 오일층과 물층으로 분리한 후 오일층을 분리하여 여과하여 구아이악우드 오일을 제조하였다.The guaiac wood was washed, dried and pulverized. Steam distillation was performed using pulverized guaiac wood, and the mixed steam generated by steam distillation was cooled to separate an oil layer and a water layer, and then the oil layer was separated and filtered to prepare guaiac wood oil.
또한, 구아이악우드 오일을 제조하는 것과 동일하게 수행하되 구아이악우드 대신에 바닐라빈 또는 만다린을 이용하여 바닐라 오일 및 만다린 오일을 제조하였다.In addition, vanilla oil and mandarin oil were prepared in the same manner as in the preparation of guaiac wood oil, but using vanilla bean or mandarin instead of guaiac wood.
상기 구아이악우드 오일 20 중량부, 상기 바닐라 오일 20 중량부, 상기 만다린 오일 8 중량부, 헥실살리실레이트 6 중량부, 디옥틸아디페이트 20 중량부, 프로필렌글리콜 3 중량부, 부틸페닐메칠프로피오날 3 중량부 및 에탄올 20 중량부를 혼합한 후, 35℃의 온도에서 350 rpm의 회전속도로 교반하여 향료원료를 제조하였다.20 parts by weight of the guaiac wood oil, 20 parts by weight of the vanilla oil, 8 parts by weight of the mandarin oil, 6 parts by weight of hexyl salicylate, 20 parts by weight of dioctyl adipate, 3 parts by weight of propylene glycol, butylphenylmethylpropional After mixing 3 parts by weight and 20 parts by weight of ethanol, the mixture was stirred at a rotational speed of 350 rpm at a temperature of 35° C. to prepare a perfume raw material.
<제조예 2> 향수원료의 제조<Preparation Example 2> Preparation of perfume raw materials
편백수 44 중량부, 브로콜리수 40 중량부, 이소프로필 이소스테아레이트 3 중량부 및 파이버솔-2(Fibersol-2) 3 중량부를 혼합한 후, 20℃의 온도에서 100 rpm의 회전속도로 교반하여 향수원료를 제조하였다.After mixing 44 parts by weight of cypress water, 40 parts by weight of broccoli water, 3 parts by weight of isopropyl isostearate and 3 parts by weight of Fibersol-2, stirring at a rotational speed of 100 rpm at a temperature of 20 ° C. Perfume raw materials were prepared.
<제조예 3> 탈취원료의 제조-1<Preparation Example 3> Preparation of deodorizing raw material-1
황련뿌리 및 후박나무 줄기를 세척한 후, 분쇄하여 준비하고, 준비된 황련뿌리 및 후박나무 줄기를 1:1의 중량비율로 혼합한 혼합물 100 중량부 및 에탄올과 아세톤이 1:1의 부피비율로 혼합된 혼합용매 1000 중량부를 혼합한 후, 초음파공정으로 40℃의 온도에서 24시간 동안 추출액을 제조하였다. 이후, 상기 추출액을 감압농축 및 동결건조하여 황련뿌리추출물 및 후박나무줄기추출물을 제조하였다.After washing the root of the yellow lotus and the stem of the blackberry tree, preparing by grinding, 100 parts by weight of a mixture of the prepared root of the yellow lotus and the stem of the silver leaf tree in a weight ratio of 1: 1, and ethanol and acetone are mixed in a volume ratio of 1: 1. After mixing 1000 parts by weight of the mixed solvent, an extract was prepared at a temperature of 40 ° C. for 24 hours by ultrasonic process. Thereafter, the extract was concentrated under reduced pressure and freeze-dried to prepare a root extract and an extract from the stem of Sulfur japonica.
살아있는 동애등에를 진공 챔버에 놓고, 감압하여 진공상태로 60분 동안 유지시킨다. 이후, 동애등에를 꺼내어 흐르는 물로 세척한 후, 식초물에 30분 동안 침지시키고, 다시 흐르는 물로 세척하였다. 세척된 동애등에를 90℃의 온도에서 90분 동안 1차 열처리하고, 1차 열처리된 동애등에를 280℃의 온도에서 15분 동안 2차 열처리하였다. 이후, 2차 열처리된 동애등에를 찜기에 넣어 찌고 찐 동애등에를 분쇄하고, 동결건조하여 동애등에 추출물을 제조하였다.Live black soldier flies are placed in a vacuum chamber, and the vacuum is maintained for 60 minutes under reduced pressure. Thereafter, black soldier flies were taken out, washed with running water, immersed in vinegar water for 30 minutes, and washed again with running water. The washed black soldier flies were subjected to a first heat treatment at a temperature of 90 ° C. for 90 minutes, and a second heat treatment was performed for the first heat treatment of the black soldier flies at a temperature of 280 ° C. for 15 minutes. Thereafter, the secondly heat-treated black soldier flies was put in a steamer and steamed, and the steamed black soldier flies were pulverized and freeze-dried to prepare an extract of black soldier flies.
타임잎, 박하잎 및 마누카잎을 세척하고, 건조시킨 후 분쇄하였다. 분쇄된 타임잎, 박하잎 및 마누카잎을 1:1:1의 중량비율로 혼합하여 혼합물을 제조하고, 상기 혼합물을 이용하여 수증기 증류하하고, 수증기 증류하여 발생하는 혼합증기를 냉각하여 오일층과 물층으로 분리한 후 오일층을 분리하여 여과하여 타임잎오일, 박하잎오일 및 마누카잎오일을 제조하였다.The thyme leaves, mint leaves and manuka leaves were washed, dried and ground. A mixture was prepared by mixing pulverized thyme leaves, mint leaves, and manuka leaves in a weight ratio of 1:1:1, steam distilled using the mixture, and mixed steam generated by steam distillation was cooled to form an oil layer and After separating into the water layer, the oil layer was separated and filtered to prepare thyme leaf oil, peppermint leaf oil and manuka leaf oil.
상기 황련뿌리추출물 및 후박나무줄기추출물 12 중량부, 상기 동애등에 추출물 4 중량부, 상기 타임잎오일, 박하잎오일 및 마누카잎오일 12 중량부, 부틸렌글라이콜 5 중량부, 글리세린 6 중량부, 변성알코올 3 중량부, 다이프로필렌글라이콜 3 중량부, 글리세레스-26 3 중량부, 1,2-헥산다이올 2 중량부, 자일리톨 2 중량부, 하이드록시아세토페논 2 중량부, 글리세레스-25피씨에이아이소스테아레이트 2 중량부, 다이페닐다이메티콘 1 중량부, 에틸헥실글리세린 0.5 중량부, 트라이에틸헥사노인 0.5 중량부, 다이소듐이디티에이 0.5 중량부, 하이드로제네이티드레시틴 0.5 중량부 및 화산석 추출액 41 중량부를 혼합한 후, 40℃의 온도에서 800 rpm의 회전속도로 교반하여 탈취원료를 제조하였다.12 parts by weight of the rhododendron root extract and Sulfur tree stem extract, 4 parts by weight of the Dongae extract, 12 parts by weight of the thyme leaf oil, peppermint leaf oil and manuka leaf oil, 5 parts by weight of butylene glycol, 6 parts by weight of glycerin, Denatured alcohol 3 parts by weight, dipropylene glycol 3 parts by weight, glycereth-26 3 parts by weight, 1,2-hexanediol 2 parts by weight, xylitol 2 parts by weight, hydroxyacetophenone 2 parts by weight, glycereth- 2 parts by weight of 25 PCA isostearate, 1 part by weight of diphenyldimethicone, 0.5 parts by weight of ethylhexylglycerin, 0.5 parts by weight of triethylhexanoin, 0.5 parts by weight of disodium EDTA, 0.5 parts by weight of hydrogenated lecithin After mixing and 41 parts by weight of the volcanic stone extract, the mixture was stirred at a rotational speed of 800 rpm at a temperature of 40° C. to prepare a deodorizing raw material.
<제조예 4> 탈취원료의 제조-2<Preparation Example 4> Preparation of deodorizing raw material-2
상기 제조예 3과 동일하게 탈취원료를 제조하되, 상기 제조예 3에서 제조된 탈취원료 100 중량부에 대하여 미강 발효추출물을 1 중량부 포함하여 탈취원료를 제조하였다. A deodorizing raw material was prepared in the same manner as in Preparation Example 3, but the deodorizing raw material was prepared by including 1 part by weight of rice bran fermented extract with respect to 100 parts by weight of the deodorizing raw material prepared in Preparation Example 3.
상기 미강 발효추출물은, 미강을 끓인 물로 3회 세척하고, 분쇄하여 미강분말을 준비하였다. 미강분말 10 g 및 물 300 g을 혼합하여 혼합물을 제조하고, 혼합물에 효모균으로 사카로미케스 케레비시아이(Saccharomyces cerevisiae)를 0.3 g 첨가한 후 35℃의 온도에서 24시간 동안 발효시켰다. 발효된 혼합물에 부틸렌글리콜 300 g을 혼합하고, 30℃의 온도에서 7일 동안 교반하여 추출물을 제조하였다. 상기 추출물을 여과 및 감압농축한 후 동결건조하여 미강 발효추출물을 제조하여 사용하였다.The fermented rice bran extract was prepared by washing rice bran three times with boiled water and pulverizing the rice bran powder. A mixture was prepared by mixing 10 g of rice bran powder and 300 g of water, and after adding 0.3 g of Saccharomyces cerevisiae as a yeast to the mixture, the mixture was fermented at 35° C. for 24 hours. An extract was prepared by mixing 300 g of butylene glycol with the fermented mixture and stirring at a temperature of 30° C. for 7 days. After filtering and concentrating the extract under reduced pressure, the extract was freeze-dried to prepare and use a fermented rice bran extract.
<실시예 1> 향수 조성물의 제조-1<Example 1> Preparation of perfume composition-1
상기 제조예 1에서 제조된 향료원료 20 중량부 및 상기 제조예 2에서 제조된 향수원료 80 중량부를 혼합한 후, 35℃의 온도에서 600 rpm의 회전속도로 교반하여 향수 조성물을 제조하였다.20 parts by weight of the perfume raw material prepared in Preparation Example 1 and 80 parts by weight of the perfume raw material prepared in Preparation Example 2 were mixed, and stirred at a rotational speed of 600 rpm at a temperature of 35 ° C to prepare a perfume composition.
<실시예 2> 향수 조성물의 제조-2<Example 2> Preparation of perfume composition-2
상기 제조예 1에서 제조된 향료원료 20 중량부, 상기 제조예 2에서 제조된 향수원료 70 중량부 및 상기 제조예 3에서 제조된 탈취원료 10 중량부를 혼합한 후, 35℃의 온도에서 600 rpm의 회전속도로 교반하여 향수 조성물을 제조하였다.After mixing 20 parts by weight of the perfume raw material prepared in Preparation Example 1, 70 parts by weight of the perfume raw material prepared in Preparation Example 2, and 10 parts by weight of the deodorizing raw material prepared in Preparation Example 3, 600 rpm at a temperature of 35 ° C. A perfume composition was prepared by stirring at a rotational speed.
<실시예 3> 향수 조성물의 제조-3<Example 3> Preparation of perfume composition-3
상기 제조예 1에서 제조된 향료원료 20 중량부, 상기 제조예 2에서 제조된 향수원료 70 중량부 및 상기 제조예 4에서 제조된 탈취원료 10 중량부를 혼합한 후, 35℃의 온도에서 600 rpm의 회전속도로 교반하여 향수 조성물을 제조하였다.After mixing 20 parts by weight of the perfume raw material prepared in Preparation Example 1, 70 parts by weight of the perfume raw material prepared in Preparation Example 2, and 10 parts by weight of the deodorizing raw material prepared in Preparation Example 4, 600 rpm at a temperature of 35 ° C. A perfume composition was prepared by stirring at a rotational speed.
<실험예 1> 향수 조성물의 지속성 및 선호도 분석<Experimental Example 1> Persistence and preference analysis of perfume composition
상기 실시예 1-3에서 제조한 향수 조성물에 대한 선호도 평가를 아래와 같이 수행하였다.Evaluation of preference for the perfume composition prepared in Examples 1-3 was performed as follows.
성인 30명(남자: 10명, 여자: 20명)이 향수 조성물을 스프레이 타입으로 피부에 뿌려 사용한 후, 향수의 발향 정도, 피부 자극성(땡김, 발진, 홍반, 가려움 등 발생 여부) 및 종합적인 선호도를 평가하여 향수 선호도를 실험하였다. 평가는 9점 척도법으로 수행하였으며, 평가 결과는 30명의 평가 총 합에 대한 평균값을 구하였으며, 그 결과를 하기 표 1에 나타내었다.After 30 adults (male: 10, female: 20) sprayed the perfume composition on the skin and used it, the degree of fragrance of the perfume, skin irritation (whether it occurs or not) and overall preference was evaluated to test perfume preference. The evaluation was performed using a 9-point scale method, and the evaluation result was the average value for the total evaluation of 30 people, and the results are shown in Table 1 below.
(9점: 매우 좋음, 7점: 좋음, 5점: 보통, 3점: 나쁨, 1점: 매우 나쁨)(9 points: very good, 7 points: good, 5 points: average, 3 points: poor, 1 point: very bad)
또한, 향수 지속력에 대해서는 8시간이 경과된 시점에서 향수의 발향 정도가 유지되어 있는지 9점 척도법으로 평가하였다.In addition, the persistence of the perfume was evaluated by a 9-point scale method to determine whether the degree of fragrance of the perfume was maintained after 8 hours had elapsed.
(9점: 지속력이 매우 높음, 7점: 지속력 높음, 5점: 보통, 3점: 지속력 나쁨, 1점: 지속력 매우 나쁨)(9 points: very high durability, 7 points: high durability, 5 points: average, 3 points: poor durability, 1 point: very poor durability)
상기 표 1에 나타낸 바와 같이, 본 발명에 따른 향수 조성물은 기호성이 우수하고 향수 지속력이 뛰어난 것을 확인할 수 있었다.As shown in Table 1, it was confirmed that the perfume composition according to the present invention had excellent palatability and excellent perfume durability.
Claims (2)
편백수 42-46 중량부, 브로콜리수 38-42 중량부, 이소프로필 이소스테아레이트 1-5 중량부 및 파이버솔-2(Fibersol-2) 1-5 중량부를 포함하는 향수원료를 제조하는 단계;
황련뿌리추출물 4-8 중량부, 후박나무줄기추출물 4-8 중량부, 동애등에 추출물 2-6 중량부, 타임잎오일 2-6 중량부, 박하잎오일 2-6 중량부, 마누카잎오일 2-6 중량부, 미강 발효추출물 0.3-3 중량부, 부틸렌글라이콜 3-7 중량부, 글리세린 4-8 중량부, 변성알코올 1-5 중량부, 다이프로필렌글라이콜 1-5 중량부, 글리세레스-26 1-5 중량부, 1,2-헥산다이올 0.5-4 중량부, 자일리톨 0.5-4 중량부, 하이드록시아세토페논 0.5-4 중량부, 글리세레스-25피씨에이아이소스테아레이트 0.5-4 중량부, 다이페닐다이메티콘 0.3-3 중량부, 에틸헥실글리세린 0.05-1 중량부, 트라이에틸헥사노인 0.05-1 중량부, 다이소듐이디티에이 0.05-1 중량부, 하이드로제네이티드레시틴 0.05-1 중량부 및 화산석 추출액 39-43 중량부를 혼합하여 탈취원료를 제조하는 단계; 및
상기 향료원료 18-22 중량부, 향수원료 68-72 중량부 및 탈취원료 8-12 중량부를 혼합하는 단계;를 포함하고,
상기 황련뿌리추출물 및 후박나무줄기추출물은,
황련뿌리 및 후박나무 줄기를 세척한 후, 분쇄하여 준비하는 단계; 준비된 황련뿌리 및 후박나무 줄기를 1:1의 중량비율로 혼합한 혼합물 90-110 중량부 및 에탄올과 아세톤이 1:1의 부피비율로 혼합된 혼합용매 900-1100 중량부를 혼합한 후, 초음파공정으로 38-42℃의 온도에서 22-26시간 동안 추출액을 제조하는 단계; 및 상기 추출액을 감압농축 및 동결건조하는 단계;를 수행하여 제조되는 것이고,
상기 타임잎오일, 박하잎오일 및 마누카잎오일은,
타임잎, 박하잎 및 마누카잎을 세척하고, 건조시킨 후 분쇄하는 단계; 분쇄된 타임잎, 박하잎 및 마누카잎을 1:1:1의 중량비율로 혼합하여 혼합물을 제조하고, 상기 혼합물을 이용하여 수증기 증류하는 단계; 및 수증기 증류하여 발생하는 혼합증기를 냉각하여 오일층과 물층으로 분리한 후 오일층을 분리하여 여과하는 단계;를 수행하여 제조되는 것이고,
상기 미강 발효추출물은,
미강을 끓인 물로 세척하고, 분쇄하여 미강분말을 준비하는 단계; 미강분말 및 물을 혼합한 혼합물에 효모균으로 사카로미케스 케레비시아이(Saccharomyces cerevisiae)를 첨가한 후 33-37℃의 온도에서 22-26시간 동안 발효시키는 단계; 발효된 혼합물 및 부틸렌글리콜을 혼합하고, 28-32℃의 온도에서 6-8일 동안 교반하여 추출물을 제조하는 단계; 및 상기 추출물을 여과 및 감압농축한 후 동결건조하는 단계;를 수행하여 제조되는 것을 특징으로 하는 향수 조성물의 제조방법.Guaiacwood oil 18-22 parts by weight, vanilla oil 18-22 parts by weight, mandarin oil 6-10 parts by weight, hexyl salicylate 4-8 parts by weight, dioctyl adipate 18-22 parts by weight, propylene glycol 1- Preparing a perfume raw material by mixing 5 parts by weight, 1-5 parts by weight of butylphenylmethylpropional and 18-22 parts by weight of ethanol;
Preparing a perfume raw material comprising 42-46 parts by weight of cypress water, 38-42 parts by weight of broccoli water, 1-5 parts by weight of isopropyl isostearate and 1-5 parts by weight of Fibersol-2;
4-8 parts by weight of barberry root extract, 4-8 parts by weight of Sulfur tree stem extract, 2-6 parts by weight of Dongae extract, 2-6 parts by weight of thyme leaf oil, 2-6 parts by weight of peppermint leaf oil, 2 parts of manuka leaf oil -6 parts by weight, rice bran fermented extract 0.3-3 parts by weight, butylene glycol 3-7 parts by weight, glycerin 4-8 parts by weight, denatured alcohol 1-5 parts by weight, dipropylene glycol 1-5 parts by weight, 1-5 parts by weight of glycereth-26, 0.5-4 parts by weight of 1,2-hexanediol, 0.5-4 parts by weight of xylitol, 0.5-4 parts by weight of hydroxyacetophenone, 0.5 parts by weight of glycereth-25 PCA isostearate -4 parts by weight, diphenyldimethicone 0.3-3 parts by weight, ethylhexylglycerin 0.05-1 parts by weight, triethylhexanoin 0.05-1 parts by weight, disodium EDTA 0.05-1 parts by weight, hydrogenated lecithin Preparing a deodorizing raw material by mixing 0.05-1 part by weight and 39-43 parts by weight of a volcanic stone extract; and
Mixing 18-22 parts by weight of the perfume raw material, 68-72 parts by weight of the perfume raw material and 8-12 parts by weight of the deodorizing raw material;
The barberry root extract and silver gourd tree stem extract,
After washing the root and the stem of the yellow chestnut tree, preparing by crushing; After mixing 90-110 parts by weight of a mixture of the prepared rhizomatous rhizomatous root and Sulfur tree trunk in a weight ratio of 1: 1 and 900-1100 parts by weight of a mixed solvent in which ethanol and acetone are mixed in a volume ratio of 1: 1, ultrasonic process Preparing an extract for 22-26 hours at a temperature of 38-42 ℃; And concentrating and freeze-drying the extract under reduced pressure; it is prepared by performing,
The thyme leaf oil, peppermint leaf oil and manuka leaf oil are
Washing, drying, and pulverizing thyme leaves, mint leaves, and manuka leaves; preparing a mixture by mixing pulverized thyme leaves, mint leaves, and manuka leaves in a weight ratio of 1:1:1, and steam distilling the mixture; And cooling the mixed steam generated by steam distillation to separate the oil layer and the water layer, and then separating and filtering the oil layer;
The rice bran fermented extract,
preparing rice bran powder by washing rice bran with boiled water and grinding it; Adding Saccharomyces cerevisiae as a yeast to a mixture of rice bran powder and water, followed by fermentation at a temperature of 33-37 ° C. for 22-26 hours; Preparing an extract by mixing the fermented mixture and butylene glycol and stirring at a temperature of 28-32 ° C. for 6-8 days; And filtering and concentrating the extract under reduced pressure, followed by freeze-drying; A method for producing a perfume composition, characterized in that produced by performing.
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| KR20050089452A (en) * | 2004-03-05 | 2005-09-08 | 경상북도농업기술원생물자원연구소 | Perfume using essential oil of tymus quinquecostatus var.japonica hara and manufacturing process of the same |
| KR20120001111A (en) | 2010-06-29 | 2012-01-04 | 전라남도 | Perfume composition containing forest and warm temperate zone species of trees and manufacturing method the same |
| JP2018510941A (en) * | 2015-03-16 | 2018-04-19 | ジボダン エス エー | Improvements in or related to organic compounds |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| KR20050089452A (en) * | 2004-03-05 | 2005-09-08 | 경상북도농업기술원생물자원연구소 | Perfume using essential oil of tymus quinquecostatus var.japonica hara and manufacturing process of the same |
| KR20120001111A (en) | 2010-06-29 | 2012-01-04 | 전라남도 | Perfume composition containing forest and warm temperate zone species of trees and manufacturing method the same |
| JP2018510941A (en) * | 2015-03-16 | 2018-04-19 | ジボダン エス エー | Improvements in or related to organic compounds |
| JP2021102767A (en) * | 2015-03-16 | 2021-07-15 | ジボダン エス エー | Improvements in or relating to organic compounds |
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