CN108113953A - A kind of dendrobium candidum honey composite extract with moisture-keeping efficacy and preparation method thereof and the application in skin care item - Google Patents
A kind of dendrobium candidum honey composite extract with moisture-keeping efficacy and preparation method thereof and the application in skin care item Download PDFInfo
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- CN108113953A CN108113953A CN201810015667.7A CN201810015667A CN108113953A CN 108113953 A CN108113953 A CN 108113953A CN 201810015667 A CN201810015667 A CN 201810015667A CN 108113953 A CN108113953 A CN 108113953A
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- dendrobium candidum
- honey
- moisture
- composite extract
- keeping efficacy
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Classifications
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
- A61K8/988—Honey; Royal jelly, Propolis
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
Abstract
The present invention relates to natural products and skin care field, specifically disclose a kind of dendrobium candidum honey composite extract with moisture-keeping efficacy and preparation method thereof and the application in skin care item, the extract are prepared comprising following method：(1) the fresh dendrobium candidum before selection is not bloomed rejects root, dead leaf and is simultaneously cleaned up and dried with clean water, with cutter by the fresh dendrobium candidum cauline leaf segment of above-mentioned processing, every section of 0.5cm；(2) it is 10 by weight ratio:15 dendrobium candidum section and honey mixing；(3) said mixture is extracted with pure water, extraction conditions are：According to dendrobium candidum and water quality than 1:5 20 carry out 15 extractions, and extraction time is 60 150min every time, and Extracting temperature is 60 100 DEG C；(4), said extracted liquid is concentrated under reduced pressure through 50 90 DEG C, is drying to obtain dendrobium candidum honey composite extract.Beneficial effect of the present invention：The extract has good moisture-keeping efficacy, and safe and non-toxic, effect stability after skin care item is made.
Description
Technical field
The present invention relates to cosmetic technical fields, and in particular to a kind of dendrobium candidum honey with moisture-keeping efficacy is compound to be carried
Take object and preparation method thereof and the application in skin care item.
Background technology
Dendrobium candidum (Dendrobium officinale Kimura et Migo) is grown nonparasitically upon another plant for orchid family Dendrobium is perennial
Herbaceous plant is named due to its epidermis is green in iron, is the superfine product of the stem of noble dendrobium, the U.S. for just having " gold in medicine " since ancient times
Reputation, it is among the people to be called " help celestial grass ".It is mainly distributed on Eastern Part of Zhejiang Province, China, Sichuan, southeastern Yunnan, In Western Fujian Province, Anhui southwest
The areas such as portion, the Guangxi northwestward.Dendrobium candidum has strengthening spleen and nourishing stomach, enriching yin and nourishing kidney, moistening lung life as China's traditional Chinese medicine
Tianjin is promoted longevity and other effects.
It is deep to be liked by consumers in general containing multiple biological activities ingredient in dendrobium candidum, extract have it is antitumor,
Anticoagulation, reducing blood lipid, blood pressure lowering, the raising medical values such as immunity and anti-aging and health-care efficacy.The beauty shield of dendrobium candidum
Skin effect is more common in medicine ancient books and records.《Compendium of Materia Medica》Described in：Dendrobium candidum " strong the moon strengthening the essence, long term usage, thick stomach, mend in never
Foot, flat stomach gas, long muscle, by skin heat symptoms caused by an exopathgen miliaria gas, the cold numbness of foot knee pain is weak, determines intelligence except frightened, macrobiosis of making light of one's life by commiting suicide.”《It does not record》Described in：
" never sufficient in strengthening the essence benefit, flat stomach gas, long muscle, by skin heat symptoms caused by an exopathgen gas, foot knee pain is weak, is good for positive, kidney tonifying product essence." theory of traditional Chinese medical science
Think, dendrobium candidum cold nature, be enriching yin top grade, it is mostly fire excess from yin deficiency caused that skin, which grows dark sore, acne, acne etc., and is answered
It can alleviate more than skin problem with dendrobium candidum.
Honey is sweet in flavor, mild-natured, nontoxic, is both food and drug, has qi-restoratives middle benefit gas, moistens the lung and relieve the cough, clearing heat and detoxicating, profit
Intestines defaecation and other effects has very high medical value.In addition to edible, honey or cold compress and treatment burn, scald is most simple, most has
One of reagent of effect.Layer protecting film can be formed by applying last layer honey immediately at scald position, can make injured skin health as early as possible
It is multiple.Since honey has stronger permeability, water-retaining property and hygroscopicity, certain answer also has been obtained in cosmetics in recent years
With.In addition to as food and natural drug, honey or a kind of important Chinese medicine pharmaceutic adjuvant.After being processed together with Chinese medicine
Synergistic effect can be played, to enhance curative effect of medication, reduces toxic side effect, this process is referred to as refined honey.More some researches show that big guns
Honey after system can enhance the solubility of aglycon in some medicinal materials in order to absorb, and sugar in honey etc. possesses reproducibility and prevents
Rotten antibacterial action can ensure the quality of drug to avoid the oxidation deterioration of active ingredient in medicinal material.
Skin care item are the great demands of modern people's life, with the development of the society, people make up for chemical synthesis class
The side effect of product has deeper understanding, and then people are more prone to selection safety, the skin care item of natural animal and plant source.Have
Patent once reported the application in skin care item by dendrobium candidum extract,《Herba Dendrobii extract, its preparation method and application》It is (public
The number of opening：CN102274138A) extracts such as the saddle stem of noble dendrobium, HERBA DENDROBII, dendrobium loddigesii Rolfe are applied in skin care item, are respectively obtained
Certain moistening effect.《A kind of dendrobium candidum leaf extract with moisture-keeping efficacy and its application in skin care item are prepared》
(publication number：CN105534831A) dendrobium candidum leaf extract is applied in skin care item, there is good moistening effect.But with
Upper patent only extracts the single raw material of the stem of noble dendrobium, is not directed to extract with the compatibility of other natural materials.The present invention is by iron sheet stone
Dry measure used in former times and honey combine, and seek a kind of natural skin care raw material with moistening effect, and making every effort to open up its social value and market needs
It asks.
The content of the invention
The technical problems to be solved by the invention are in order to overcome the shortcomings of natural moisture preserving ingredient in the prior art, and to carry
Application for a kind of dendrobium candidum honey composite extract with moisture-keeping efficacy and preparation method thereof and in skin care item.
The above-mentioned technical problem to be solved belonging to the present invention is achieved by the following technical programs：
A kind of dendrobium candidum honey composite extract with moisture-keeping efficacy, is prepared as follows to obtain：By fresh iron
After the skin stem of noble dendrobium and honey mixing, by water refluxing extraction, up to the dendrobium candidum with moisture-keeping efficacy after the drying that is concentrated under reduced pressure
Honey composite extract.
Preferably, the dendrobium candidum honey composite extract, is prepared by the method comprised the following steps
It arrives：
S1：The fresh dendrobium candidum before not blooming is selected, root, dead leaf is rejected and is simultaneously cleaned up and dried with clean water, use
Cutter is by the fresh dendrobium candidum cutting shoots of above-mentioned processing, every section of about 0.5cm；
S2：It is 10 by weight ratio:Dendrobium candidum section and the honey mixing of 1-5, obtains mixture；
S3：Said mixture is extracted with pure water, obtains extracting solution, extraction conditions are：According to dendrobium candidum and water quality
Than 1:5-20 carries out 1-5 extraction, and extraction time is each 60-150min, and Extracting temperature is 60-100 DEG C；
S4：Said extracted liquid is concentrated under reduced pressure through 50-90 DEG C, is drying to obtain dendrobium candidum honey composite extract.
As preference, according to dendrobium candidum and honey than 10:1-3 carries out mixing extraction.
As preference, according to dendrobium candidum and water quality than 1:10-15、1:10-15、1:8-12 is extracted three times,
Extraction time is each 70-90min.
As preference, said extracted liquid is concentrated under reduced pressure through 60-80 DEG C, is drying to obtain fresh dendrobium candidum stem-leaf extract.
A kind of preparation method of dendrobium candidum honey composite extract using above-mentioned moisture-keeping efficacy, the iron sheet stone of gained
Application of the dry measure used in former times honey composite extract in skin care item.
As preference, the mass fraction containing composite extract of the present invention is in skin care item of the present invention
0.1-20%.
As preference, the skin care item are creme, paste, lotion, suspension, gel, oil, foundation emulsion or spray.
Beneficial effects of the present invention are：The dendrobium candidum honey composite extract obtained by preparation method of the present invention
It has no toxic side effect, has good moistening effect after skin care item are added in, this also moisture of skin testing experiment in specific example 7
It is proved.As traditional medicinal material and raw material, the skin care item using extract of the present invention and technology do not have for dendrobium candidum, honey
Any toxic side effect, and a kind of dendrobium candidum development and utilization measure is provided, dendrobium candidum and honey have been increased newly in cosmetics
Application process in formula.
Description of the drawings
Fig. 1 skin moisture content variation diagrams.
Specific embodiment
The present invention is explained further below in conjunction with specific embodiment, but embodiment does not do any type of limit to the present invention
It is fixed.
Embodiment 1：The preparation of dendrobium candidum honey composite extract
S1：Uncivilized preceding fresh dendrobium candidum is selected, root, dead leaf is rejected and is simultaneously cleaned up and dried with clean water, use
Cutter is by the fresh dendrobium candidum cauline leaf segment of above-mentioned processing, every section of about 0.5cm；
S2：It is 10 by weight ratio:1 dendrobium candidum section and honey mixing；
S3：Said mixture is extracted with pure water, extraction conditions are：According to dendrobium candidum and water quality than 1:15、1:15
With 1:10 are extracted three times, and extraction time is each for 90min, and Extracting temperature is 75 DEG C；
S4：Said extracted liquid is through being concentrated under reduced pressure, being drying to obtain dendrobium candidum honey composite extract.
Embodiment 2：The preparation of dendrobium candidum honey composite extract
S1：Uncivilized preceding fresh dendrobium candidum is selected, root, dead leaf is rejected and is simultaneously cleaned up and dried with clean water, use
Cutter is by the fresh dendrobium candidum cauline leaf segment of above-mentioned processing, every section of about 0.5cm；
S2：It is 5 by weight ratio:1 dendrobium candidum section and honey mixing；
S3：Said mixture is extracted with pure water, extraction conditions are：According to dendrobium candidum and water quality than 1:15、1:15
With 1:10 are extracted three times, and extraction time is each for 90min, and Extracting temperature is 75 DEG C；
S4：Said extracted liquid is through being concentrated under reduced pressure, being drying to obtain dendrobium candidum honey composite extract.
Embodiment 3：The preparation of dendrobium candidum honey composite extract
S1：Uncivilized preceding fresh dendrobium candidum is selected, root, dead leaf is rejected and is simultaneously cleaned up and dried with clean water, use
Cutter is by the fresh dendrobium candidum cauline leaf segment of above-mentioned processing, every section of about 0.5cm；
S2：It is 10 by weight ratio:3 dendrobium candidum section and honey mixing；
S3：Said mixture is extracted with pure water, extraction conditions are：According to dendrobium candidum and water quality than 1:15、1:15
With 1:10 are extracted three times, and extraction time is each for 90min, and Extracting temperature is 75 DEG C；
S4：Said extracted liquid is through being concentrated under reduced pressure, being drying to obtain dendrobium candidum honey composite extract.
Embodiment 4：The preparation of moisturiser
1.75 parts of dendrobium candidum honey composite extract (wherein 1 part of dendrobium candidum ingredient, the bee that embodiment 1 is prepared
Sweet 0.75 part of ingredient), 3 parts of monoglyceride, 3 parts of vaseline, 3 parts of dimethicone, mixed 5 parts of alcohol, 8 parts of white oil, 1,3 butylene glycol 22
Part, Preservative qs, remaining be deionized water.
Preparation method：First with 1,3-BDO and portions of de-ionized water dissolving dendrobium candidum honey composite extract, filtering
For use；White oil, vaseline, monoglyceride, mixed alcohol, dimethicone are blended at 75 DEG C -80 DEG C and stir evenly；Remaining deionization
Water, preservative are blended at 75 DEG C -80 DEG C and stir evenly；Both the above mixture is successively pumped into emulsification pot, homogeneous 5min is stirred
It mixes and is cooled to 40 DEG C, add in filtered dendrobium candidum honey composite extract, stir, be cooled to room temperature.
Embodiment 5：The preparation of moisturiser
2.5 parts of dendrobium candidum honey composite extract (wherein 1 part of dendrobium candidum ingredient, the honey that embodiment 2 is prepared
1.5 parts of ingredient), 3 parts of monoglyceride, 3 parts of vaseline, 3 parts of dimethicone, mixed 5 parts of alcohol, 8 parts of white oil, 22 parts of 1,3 butylene glycol,
Preservative qs, remaining be deionized water.
Preparation method：First with 1,3-BDO and portions of de-ionized water dissolving dendrobium candidum honey composite extract, filtering
For use；White oil, vaseline, monoglyceride, mixed alcohol, dimethicone are blended at 75 DEG C -80 DEG C and stir evenly；Remaining deionization
Water, preservative are blended at 75 DEG C -80 DEG C and stir evenly；Both the above mixture is successively pumped into emulsification pot, homogeneous 5min is stirred
It mixes and is cooled to 40 DEG C, add in filtered dendrobium candidum honey composite extract, stir, be cooled to room temperature.
Embodiment 6：The preparation of moisturiser
3.25 parts of dendrobium candidum honey composite extract (wherein 1 part of dendrobium candidum ingredient, the bee that embodiment 3 is prepared
Sweet 2.25 parts of ingredient), 3 parts of monoglyceride, 3 parts of vaseline, 3 parts of dimethicone, mixed 5 parts of alcohol, 8 parts of white oil, 1,3 butylene glycol 22
Part, Preservative qs, remaining be deionized water.
Preparation method：First with 1,3-BDO and portions of de-ionized water dissolving dendrobium candidum honey composite extract, filtering
For use；White oil, vaseline, monoglyceride, mixed alcohol, dimethicone are blended at 75 DEG C -80 DEG C and stir evenly；Remaining deionization
Water, preservative are blended at 75 DEG C -80 DEG C and stir evenly；Both the above mixture is successively pumped into emulsification pot, homogeneous 5min is stirred
It mixes and is cooled to 40 DEG C, add in filtered dendrobium candidum honey composite extract, stir, be cooled to room temperature.
Embodiment 7：Moistening effect is tested
200 healthy womens are selected, are randomly divided into 4 groups, experimental group 1, experimental group 2, experimental group 3 and control group, clear area
Domain statistics is blank group, it is desirable that the age between 16-65 Sui, the basic value of forearm test zone capacitance method moisture of skin analyzer
Between 15-45；Without serious systemic disease, without immune deficiency or autoimmune disease person；No active anaphylactia person；
Previously to skin-care cosmetics without severe allergy history person；Hormone medicine and immunosuppressor person are not used in nearly 1 month；Not
Participate in other clinical test persons；Trial drug carries out blind processing with unified packed without mark.Experimental group 1 is made with embodiment 4
Moisturiser apply 3 × 3cm regions on the inside of left forearm outside, right forearm is check plot；The moisturiser made from embodiment 5 of experimental group 2
3 × 3cm regions on the inside of outer painting left forearm, right forearm is check plot；The moisturiser made from embodiment 6 of experimental group 3 applies left front outside
3 × 3cm regions on the inside of arm, right forearm is check plot；Removing iron sheet stem of noble dendrobium honey compound collecting of the control group described in embodiment 4
The matrix of beyond the region of objective existence applies 3 × 3cm regions on the inside of left forearm, and right forearm is check plot.
Any product cannot be used within 2-3 days before tester's recipient site, tester needs to clean in both hands forearm before experiment
It surveys, and measured zone mark is carried out in both hands inner forearm, sit quietly at least 30min in standard compliant room, it is impossible to it drinks water,
Forearm exposes, and is placed in test mode, keeps loosening.In test, using latex finger cot will test moisturiser by 2.0mg ±
0.1mg/cm2Dosage be spread evenly across in trial zone.After smearing, when measuring 1h, 2h and 4h respectively, Experimental Area and check plot
The moisture content of skin in domain.Test environment conditions：Environment temperature is 24 DEG C ± 1 DEG C, and humidity is 55% ± 5%, and is carried out real-time
Dynamic monitoring.Test equipment is the skin moisture tester CM825 of CK companies of Germany.The result is shown in Figure 1.
It can be seen from the data of Fig. 1 as time increases, blank group and the tested region water content of control group are without bright
Aobvious variation, the moisture of the two is more slightly larger than before smearing moisturiser, this is because skin surface maintains itself water balance to cause
's.The tester of experimental group 1, experimental group 2 and experimental group 3 is being prepared respectively using embodiment 4, embodiment 5 and embodiment 6
Moisturiser after 1h, 2h compare and significantly improve with control group with 4h, and with the increase of honey component in composite extract, moisture
Content also has a degree of increase.It can be seen that using the conspicuousness of SPSS software analysis data differences and smearing moisturiser
Before, the moisture indifference of skin, after the moisturiser of dendrobium candidum honey composite extract for smearing different ratio, skin
There are significant differences for moisture.As it can be seen that adding dendrobium candidum honey composite extract in the formula of moisturiser, can increase
The moisture of skin, and increase with the increase of honey component in composite extract, difference is more significant.
In terms of the correction data of experimental group 1, experimental group 2 and experimental group 3, using in moisturiser 1h, 2h, 4h, experimental group 2
Moisture with experimental group 3 is at least than experimental group 1 high 11% and 14%, it is seen that the guarantor that embodiment 5 and embodiment 6 are prepared
The moistening effect of wet frost is more preferable than the moisturiser effect that embodiment 4 is prepared.Moisture of the experimental group 3 in same time
Also above experimental group 2, but in 2h and 4h, the moisture of the two relatively, the iron sheet from cost consideration, experimental group 2
The stem of noble dendrobium and honey 5:1 proportioning extraction scheme is also a more excellent scheme.
Claims (6)
1. a kind of dendrobium candidum honey composite extract with moisture-keeping efficacy, it is characterised in that：Using dendrobium candidum, honey to carry
After raw material is taken to mix, by water refluxing extraction, answered after the drying that is concentrated under reduced pressure up to the dendrobium candidum honey with moisture-keeping efficacy
Close extract.
2. a kind of preparation method of the dendrobium candidum honey composite extract with moisture-keeping efficacy, it is characterised in that：This method master
It comprises the following specific steps that：
S1：The fresh dendrobium candidum before not blooming is selected, root, dead leaf is rejected and is simultaneously cleaned up and dried with clean water, use cutter
By the fresh dendrobium candidum cutting shoots of above-mentioned processing, every section of 0.5cm；；
S2：It is 10 by weight ratio:Dendrobium candidum section and the honey mixing of 1-5, obtains mixture；
S3：Said mixture is extracted with pure water, obtains extracting solution, extraction conditions are：According to dendrobium candidum and water quality than 1:
5-20 carries out 1-5 extraction, and extraction time is each 60-150min, and Extracting temperature is 60-100 DEG C；
S4：Said extracted liquid is concentrated under reduced pressure through 50-90 DEG C, is drying to obtain dendrobium candidum honey composite extract.
3. the preparation method of the dendrobium candidum honey composite extract according to claim 2 with moisture-keeping efficacy, special
Sign is：According to dendrobium candidum and honey than 10:1-3 carries out mixing extraction.
4. the preparation method of the dendrobium candidum honey composite extract according to claim 2 with moisture-keeping efficacy, special
Sign is：According to dendrobium candidum and water quality than 1:10-15、1:10-15、1:8-12 is extracted three times, and extraction time is every
Secondary 70-90min.
5. the preparation method of the dendrobium candidum honey composite extract according to claim 2 with moisture-keeping efficacy, special
Sign is：Said extracted liquid is concentrated under reduced pressure through 60-80 DEG C, is drying to obtain dendrobium candidum honey composite extract.
6. a kind of application of the dendrobium candidum honey composite extract in skin care item with moisture-keeping efficacy.
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| CN110526997A (en) * | 2019-07-25 | 2019-12-03 | 爱思开百朗德生物科技（海门）有限公司 | A kind of preparation method and application of dendrobium candidum honey toast polysaccharide body |
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