CN107157850A - A kind of dendrobium candidum eye skin care item and preparation method thereof - Google Patents
A kind of dendrobium candidum eye skin care item and preparation method thereof Download PDFInfo
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- CN107157850A CN107157850A CN201710482500.7A CN201710482500A CN107157850A CN 107157850 A CN107157850 A CN 107157850A CN 201710482500 A CN201710482500 A CN 201710482500A CN 107157850 A CN107157850 A CN 107157850A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4973—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom
- A61K8/498—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom having 6-membered rings or their condensed derivatives, e.g. coumarin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/678—Tocopherol, i.e. vitamin E
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/005—Preparations for sensitive skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
Abstract
The invention discloses a kind of dendrobium candidum eye skin care item and preparation method thereof.The dendrobium candidum eye skin care item include following raw material：Dendrobium candidum extract, gold engrave prunus mume extract, Prunella vulgaris extract, peach blossom essential oil, include the component of following parts by weight：70 110 parts of Tea Polyphenols, 60 100 parts of trehalose, 30 70 parts of vitamin E, 20 60 parts of olive oil, 10 30 parts of evening primrose oil.The invention also discloses the preparation method of the dendrobium candidum eye skin care item.The dendrobium candidum eye skin care item can effectively remove fat granule removal, livid ring around eye, pouch, and alleviation circumference of eyes skin fatigue is effectively alleviated microgroove, dry line near the eyes, do not stimulated naturally, safe and effective.
Description
Technical field
The invention belongs to cosmetics field, it is related to a kind of eye skin care item, more particularly to a kind of dendrobium candidum eye
Skin care item and preparation method thereof.
Background technology
Dendrobium candidum, is orchid dendrobium candidum Dendrobiumofficinale Kimumet Migo drying stem,
Also known as ribbed hedyotis herb, iron bracketplant.Record in《Chinese Pharmacopoeia》Version in 2015：【Nature and flavor and channel tropism】It is sweet, it is slightly cold.Return stomach, kidney channel.【Work(
Can be with curing mainly】Reinforcing stomach reg fluid, nourishing Yin and clearing heat.For pyreticosis Tianjin wound, dry polydipsia, deficiency of stomach-Yin, deficiency of food is retched, and abnormal heat is not after being ill
Move back, fire excess from yin deficiency, hectic fever due to yin labor heat, mesh is secretly failed to understand, muscles and bones impotence.Dendrobium candidum have " help celestial grass ", " Chinese nine big celestial grass it
The good reputations such as head ", in China, dendrobium candidum is not only traditional rare traditional Chinese medicine, and is special-protection-by-the-State Chinese medicine.Iron sheet
The stem of noble dendrobium be able to can also not only be passed through rich in a variety of nutriments such as polysaccharide, flavonoids, phenols, amino acid by oral absorption
Skin absorbs.Dendrobium officinale polysaccharide has effects that antibacterial, anti-inflammatory, moisturizing and nourishing；Flavones and aldehydes matter are natural antioxygens
Agent, with stronger antioxidation activity in vitro；Amino acid can supplement nutrition and the moisture of skin, make with good moisturizing
With while having the characteristics of being easily absorbed by the skin.
Eye skin is human body most thin skin, while being the most frequent position of activity again.The special feature of eye skin
It is that, almost without sweat gland and sebaceous glands, this part skin is hardly fuel-displaced, does not perspire, due to lacking the natural protection of sebum film,
Eye skin is easily dried, water shortage.Therefore, whatsoever skin quality, eye skin is all desert on the face.And eye most easily occurs
The problem of just because of dry caused by dry line and wrinkle.The skin of eyes surrounding, because sebum secretion is few, the holding of moisture is not
Easily, skin thickness is added again thin, contained collagen, elastin are less, while increasing at the age, easily than other portions
Position, which is tried to be the first, to be occurred drying and wrinkle.Plus the allegro life style of present people and its irregular work and rest custom, eye flesh
Skin is in addition to long wrinkle, the problems such as there is also livid ring around eye, pouch, eye edema, long fat granule.Eye skin care on the market
Product mainly have a glue, eye mask, eye essence, eye cream etc., but eye glue is too fast due to absorbing, and is not suitable for the eye flesh of aging
Skin, is only suitable only for dryness, the young skin of mixed type is used；Eye mask can only keep the skin wet in a short time, be adapted to it is neutral or
Oily skin is used；Eye essence nutrient composition content is too high, is not suitable for youth skin and uses.Eye glue, eye mask, eye essence
Element is all to be only applicable to single skin quality, is restricted Consumer groups to a certain extent.With skin care item " green, it is natural,
It is non-stimulated " idea be gradually rooted in the hearts of the people, the skin care item of natural plant formula are by the concern of more and more researchers and vast
The favor and high praise of consumer.Because the skin of eye is very careful and fragile, especially easily come to harm, therefore, in selection
Eyeware products and solution for lenses and contact lenses, consumer is more likely to that selection is gentle, not stimulated, the eyeware products and solution for lenses and contact lenses of low responsive type.Dendrobium candidum is carried
Thing energy enriching yin moisturizing is taken, skin-nourishing situation is can effectively improve, promotes skin metabolism, recovers skin vitality and elastic force, is increased
Strong skin water lock function.And the present invention is based on this and works out a kind of dendrobium candidum eye skin care item, at present, there is not yet phase
Close report.
The research of modern natural botanical finds, gold is engraved prunus mume extract and can releived skin, can remove in Skin Cell
Free radical, mitigates injury of the ultraviolet to skin, has obvious inhibitory action to the generation of wrinkle.Prunella vulgaris extract can be balanced
Skin oil, has the obvious effect of releiving to sensitive skin.Peach blossom essential oil can expand blood vessel, and promotion of blood circulation, skin of moistening changes
Kind blood circulation, promotes skin-nourishing and oxygen supply, the lipofuscin element of promotion human senility is accelerated excretion, prevents melanin from existing
Chronic deposition in skin, can effectively prevent and treat dry skin, coarse and wrinkle.Tea Polyphenols has effects that extravasated blood of releiving, Ke Yihuan
Solve eye skin fatigue and eye edema.Trehalose has the excellent characteristic for keeping cell viability and large biological molecule activity,
Can be in cell surface layer one layer of special diaphragm of formation, from film under the environment such as high temperature, high and cold, dry, intensive ultraviolet radiation
The mucus of upper precipitation not only moistens Skin Cell, also with the function of radiateing external heat, so as to protect skin
It will not be damaged.Vitamin E acts on deep skin, effective moisturizing moisturizing, makes skin water around eyes tender, moreover it is possible to anti-oxidant, prevents
Only skin is injured by external environment, smooths eye skin microgroove.Olive oil can eliminate eye microgroove, promote eye skin thin
Greasy, gloss.Evening primrose oil is a kind of essential oil with effect of releiving, rich in leukotrienes and antioxidant, helps to alleviate skin
Skin is dried, and improves livid ring around eye.
The disclosure of background above technology contents is only used for inventive concept and the technical scheme that auxiliary understands the present invention, and it is not
The prior art of present patent application is necessarily belonged to, the applying date of the above in present patent application is being shown without tangible proof
In the case of disclosed, above-mentioned background technology should not be taken to evaluate the novelty and creativeness of the application.
The content of the invention
It is an object of the invention to provide a kind of dendrobium candidum eye skin care item and preparation method thereof, to solve prior art
Present in：Eye skin-protection product using effect is not obvious, and side effect is more, is adapted to single skin quality, and consumer is asked using limited etc.
Topic.
The present invention is prepared by scientific and reasonable using natural plant extracts as raw material, a kind of eye skin care item is made.It is described
Eye skin care item can moisten moisturizing, strengthen skin metabolism, by supplementing moisture and nutritional ingredient needed for eye skin, have
Imitate Vitamin K, eliminate pouch and microgroove, strengthen the self-repairing capability of skin, natural no stimulation is safe and effective.
Technical scheme is as follows：
A kind of dendrobium candidum eye skin care item, including following raw material：It is withered that dendrobium candidum extract, gold engrave prunus mume extract, summer
Careless extract, peach blossom essential oil.
Above-described dendrobium candidum eye skin care item, include the component of following parts by weight：70-110 parts of Tea Polyphenols, sea
60-100 parts of algae sugar, 30-70 parts of vitamin E, 20-60 parts of olive oil, 10-30 parts of evening primrose oil.
Above-described dendrobium candidum eye skin care item, the preparation method of dendrobium candidum extract is：Take new after cleaning
Fresh 160-200 parts plus 5-8 times of dendrobium candidum stem measures water immersion 0.5-1h, heating and refluxing extraction 1-2h, and filtrate decompression is condensed into thick
Paste, produces dendrobium candidum extract.
Above-described dendrobium candidum eye skin care item, gold engraves the preparation method of prunus mume extract and is：Gold is taken to engrave 50-80 parts of plum
Plus 10-15 times measured water immersion 1-2h, heating distillation 2-3h, point distillate is taken, produce gold and engrave prunus mume extract.
Above-described dendrobium candidum eye skin care item, the preparation method of Prunella vulgaris extract is：Take 50-80 parts of selfheal
Plus 10-15 times of 70% ethanol measured, refluxing extraction 1h, extract 2 times, suction filtration, merging filtrate is simultaneously concentrated, and is freeze-dried to obtain selfheal
Extract.
Above-described dendrobium candidum eye skin care item, the preparation method of peach blossom essential oil is：Take 40-60 parts of peach blossom plus 1-2
Amount water immersion 2-3h, is placed in supercritical carbon dioxide extraction apparatus, extracting pressure is 12-15MPa by the peach blossom soaked again, extracts
It is 45-50 DEG C to take temperature, and CO2 flows are 15-20kg/h, and extraction time is 1-2h, and entrainer is made with 80-90% ethanol, is used
Measure as 200-250ml, produce peach blossom essential oil.
Above-described dendrobium candidum eye skin care item, can be prepared into eye cream, eye glue, eye mask, eye essence, optimal excellent
Choosing is prepared into eye cream.
Dendrobium candidum eye skin care item described in more than one are prepared into the preparation method of eye cream, comprise the following steps：
S1. dendrobium candidum extract is prepared：160-200 parts plus 5-8 times of fresh dendrobium candidum stem after cleaning is taken to measure water logging
0.5-1h is steeped, heating and refluxing extraction 1-2h, filtrate decompression is condensed into paste, standby；
S2. prepare gold and engrave prunus mume extract：Take gold to engrave 50-80 parts plus 10-15 times of plum and measure water immersion 1-2h, heating distillation 2-
3h, divides and takes distillate, standby；
S3. Prunella vulgaris extract is prepared：70% ethanol for taking 50-80 parts plus 10-15 times of selfheal to measure, refluxing extraction 1h,
Extract 2 times, suction filtration, merging filtrate is simultaneously concentrated, freeze-drying is standby；
S4. peach blossom essential oil is prepared：40-60 parts plus 1-2 times of peach blossom is taken to measure water immersion 2-3h, the peach blossom soaked is placed in super face
Boundary's carbon dioxide extraction apparatus, extracting pressure is 12-15MPa, and extraction temperature is 45-50 DEG C, and CO2 flows are 15-20kg/h, extraction
It is 1-2h to take the time, makees entrainer with 80-90% ethanol, consumption is 200-250ml, produces peach blossom essential oil, standby；
S5. component is weighed by following parts by weight：70-110 parts of Tea Polyphenols, 60-100 parts of trehalose, 30-70 parts of vitamin E,
20-60 parts of olive oil, 10-30 parts of evening primrose oil；
S6. take Tea Polyphenols, trehalose to add the water cooling leaching 12-24h of equivalent, mix, gold made from addition S2 engraves plum extraction
Liquid, mixes, obtains mixture A；
S7. take dendrobium candidum extract, vitamin E made from step S1 to be heated to 60 DEG C, stir to being completely dissolved, it is quiet
Put, when temperature is down to 45 DEG C, add Prunella vulgaris extract made from step S3, peach blossom essential oil, olive made from step S4
Oil, evening primrose oil, are uniformly mixed, obtain mixture B；
S8. mixture B made from mixture A made from step S6 and step S7 is placed in homogenized milk in homogeneous emulsifying machine
Change, obtain creams, creams sterilizing, embedding produces the dendrobium candidum eye cream.
Further, the temperature of the emulsifying described in step S8 is 30-45 DEG C, and frequency is 100-120Hz, emulsifying
Time is 30-40min.
Compared with prior art, beneficial effects of the present invention are as follows：
1. the present invention eye skin care item using natural plant extracts as raw material, hormone, essence, harmful chemical component,
Sensitization preservative zero is added.Substantial amounts of colloid is rich in dendrobium candidum extract, the moisture and collagen of eye skin can be supplemented
Albumen, repairs elastomer, by supplementing nutritional ingredient and moisture needed for skin, and prevents moisture and nutritional ingredient for a long time
It is lost in, is inherently eliminated eye microgroove, significantly, total effective rate is up to 95%, 98%, 97.5% for effect.
2. the present invention eye skin care item by moisturizing and water lock, be provided simultaneously with improve microgroove, dry line, eliminate fat granule,
The effectiveness such as pouch, livid ring around eye, edema.Tea Polyphenols can alleviate eye skin fatigue and eye edema, and trehalose can decompose eye
The fat granule of portion's skin, vitamin E can effectively smooth eye skin microgroove, and olive oil can eliminate the same of eye microgroove
When, promote eye skin exquisiteness, gloss, evening primrose oil helps to alleviate eye skin drying, improves livid ring around eye.
3. the eye skin care item of the present invention, moist non-greasy, easily absorption, suitable various skin quality and each age level
Consumer.
Embodiment
With reference to specific embodiment, the invention will be further described, but do not limit the scope of the invention and apply
Scope：
First, the preparation of dendrobium candidum eye cream
Embodiment 1
A kind of preparation method of dendrobium candidum eye cream, comprises the following steps：
S1. dendrobium candidum extract is prepared：170 parts plus 6 times amount water immersion 0.6h of fresh dendrobium candidum stem after cleaning are taken,
Heating and refluxing extraction 1.2h, filtrate decompression is condensed into paste, standby；
S2. prepare gold and engrave prunus mume extract：Take gold to engrave 60 parts of plum and add 11 times of amounts water immersion 1.2h, heating distillation 2.5h, divide and take
Distillate, it is standby；
S3. Prunella vulgaris extract is prepared：70% ethanol of 60 parts plus 11 times amounts of selfheal is taken, refluxing extraction 1h extracts 2
Secondary, suction filtration, merging filtrate is simultaneously concentrated, freeze-drying, standby；
S4. peach blossom essential oil is prepared：50 parts plus 1 times amount water immersion 2.2h of peach blossom are taken, the peach blossom soaked are placed in overcritical
Carbon dioxide extraction apparatus, extracting pressure is 13MPa, and extraction temperature is 46 DEG C, and CO2 flows are 16kg/h, and extraction time is
1.2h, entrainer is made with 85% ethanol, and consumption is 210ml, produces peach blossom essential oil, standby；
S5. component is weighed by following parts by weight：80 parts of Tea Polyphenols, 70 parts of trehalose, 40 parts of vitamin E, 30 parts of olive oil,
15 parts of evening primrose oil；
S6. take Tea Polyphenols, trehalose to add the water cooling leaching 18h of equivalent, mix, gold made from addition S2 engraves plum extract solution,
Mix, obtain mixture A；
S7. take dendrobium candidum extract, vitamin E made from step S1 to be heated to 60 DEG C, stir to being completely dissolved, it is quiet
Put, when temperature is down to 45 DEG C, add Prunella vulgaris extract made from step S3, peach blossom essential oil, olive made from step S4
Oil, evening primrose oil, are uniformly mixed, obtain mixture B；
S8. mixture B made from mixture A made from step S6 and step S7 is placed in homogeneous emulsifying machine, setting is equal
The temperature of matter emulsification is 35 DEG C, and frequency is 105Hz, and the emulsifying time is 32min, obtains creams, and creams sterilizing, embedding is produced
The dendrobium candidum eye cream.
Embodiment 2
A kind of preparation method of dendrobium candidum eye cream, comprises the following steps：
S1. dendrobium candidum extract is prepared：180 parts plus 7 times amount water immersion 0.7h of fresh dendrobium candidum stem after cleaning are taken,
Heating and refluxing extraction 1.5h, filtrate decompression is condensed into paste, standby；
S2. prepare gold and engrave prunus mume extract：Take gold to engrave 70 parts of plum and add 12 times of amounts water immersion 1.5h, heating distillation 2.5h, divide and take
Distillate, it is standby；
S3. Prunella vulgaris extract is prepared：70% ethanol of 70 parts plus 12 times amounts of selfheal is taken, refluxing extraction 1h extracts 2
Secondary, suction filtration, merging filtrate is simultaneously concentrated, freeze-drying, standby；
S4. peach blossom essential oil is prepared：55 parts plus 1.5 times amount water immersion 2.5h of peach blossom are taken, the peach blossom soaked is placed in super face
Boundary's carbon dioxide extraction apparatus, extracting pressure is 14MPa, and extraction temperature is 47 DEG C, and CO2 flows are 17kg/h, and extraction time is
1.5h, entrainer is made with 82% ethanol, and consumption is 220ml, produces peach blossom essential oil, standby；
S5. component is weighed by following parts by weight：90 parts of Tea Polyphenols, 80 parts of trehalose, 50 parts of vitamin E, 40 parts of olive oil,
20 parts of evening primrose oil；
S6. take Tea Polyphenols, trehalose to add the water cooling leaching 24h of equivalent, mix, gold made from addition S2 engraves plum extract solution,
Mix, obtain mixture A；
S7. take dendrobium candidum extract, vitamin E made from step S1 to be heated to 60 DEG C, stir to being completely dissolved, it is quiet
Put, when temperature is down to 45 DEG C, add Prunella vulgaris extract made from step S3, peach blossom essential oil, olive made from step S4
Oil, evening primrose oil, are uniformly mixed, obtain mixture B；
S8. mixture B made from mixture A made from step S6 and step S7 is placed in homogeneous emulsifying machine, setting is equal
The temperature of matter emulsification is 38 DEG C, and frequency is 110Hz, and the emulsifying time is 35min, obtains creams, and creams sterilizing, embedding is produced
The dendrobium candidum eye cream.
Embodiment 3
A kind of preparation method of dendrobium candidum eye cream, comprises the following steps：
S1. dendrobium candidum extract is prepared：160 parts plus 5 times amount water immersion 0.5h of fresh dendrobium candidum stem after cleaning are taken,
Heating and refluxing extraction 1h, filtrate decompression is condensed into paste, standby；
S2. prepare gold and engrave prunus mume extract：Take gold to engrave 50 parts of plum plus 10 times of amounts water immersion 1h, heating distillation 2h, point take and to distillate
Liquid, it is standby；
S3. Prunella vulgaris extract is prepared：70% ethanol of 50 parts plus 10 times amounts of selfheal is taken, refluxing extraction 1h extracts 2
Secondary, suction filtration, merging filtrate is simultaneously concentrated, freeze-drying, standby；
S4. peach blossom essential oil is prepared：40 parts plus 1 times amount water immersion 2h of peach blossom are taken, the peach blossom soaked is placed in overcritical two
Carbonoxide extraction equipment, extracting pressure is 12MPa, and extraction temperature is 45 DEG C, and CO2 flows are 15kg/h, and extraction time is 1h, are used
80% ethanol makees entrainer, and consumption is 200ml, produces peach blossom essential oil, standby；
S5. component is weighed by following parts by weight：70 parts of Tea Polyphenols, 60 parts of trehalose, 30 parts of vitamin E, 20 parts of olive oil,
10 parts of evening primrose oil；
S6. take Tea Polyphenols, trehalose to add the water cooling leaching 12h of equivalent, mix, gold made from addition S2 engraves plum extract solution,
Mix, obtain mixture A；
S7. take dendrobium candidum extract, vitamin E made from step S1 to be heated to 60 DEG C, stir to being completely dissolved, it is quiet
Put, when temperature is down to 45 DEG C, add Prunella vulgaris extract made from step S3, peach blossom essential oil, olive made from step S4
Oil, evening primrose oil, are uniformly mixed, obtain mixture B；
S8. mixture B made from mixture A made from step S6 and step S7 is placed in homogeneous emulsifying machine, setting is equal
The temperature of matter emulsification is 30 DEG C, and frequency is 100Hz, and the emulsifying time is 30min, obtains creams, and creams sterilizing, embedding is produced
The dendrobium candidum eye cream.
Embodiment 4
A kind of preparation method of dendrobium candidum eye cream, comprises the following steps：
S1. dendrobium candidum extract is prepared：Take 190 parts plus 7.5 times amount water immersions of fresh dendrobium candidum stem after cleaning
0.8h, heating and refluxing extraction 1.8h, filtrate decompression is condensed into paste, standby；
S2. prepare gold and engrave prunus mume extract：Take gold to engrave 75 parts of plum and add 13 times of amounts water immersion 1.8h, heating distillation 2.5h, divide and take
Distillate, it is standby；
S3. Prunella vulgaris extract is prepared：70% ethanol of 75 parts plus 14 times amounts of selfheal is taken, refluxing extraction 1h extracts 2
Secondary, suction filtration, merging filtrate is simultaneously concentrated, freeze-drying, standby；
S4. peach blossom essential oil is prepared：45 parts plus 2 times amount water immersion 2.5h of peach blossom are taken, the peach blossom soaked are placed in overcritical
Carbon dioxide extraction apparatus, extracting pressure is 14MPa, and extraction temperature is 48 DEG C, and CO2 flows are 18kg/h, and extraction time is
1.8h, entrainer is made with 86% ethanol, and consumption is 240ml, produces peach blossom essential oil, standby；
S5. component is weighed by following parts by weight：100 parts of Tea Polyphenols, 90 parts of trehalose, 60 parts of vitamin E, olive oil 50
Part, 25 parts of evening primrose oil；
S6. take Tea Polyphenols, trehalose to add the water cooling leaching 24h of equivalent, mix, gold made from addition S2 engraves plum extract solution,
Mix, obtain mixture A；
S7. take dendrobium candidum extract, vitamin E made from step S1 to be heated to 60 DEG C, stir to being completely dissolved, it is quiet
Put, when temperature is down to 45 DEG C, add Prunella vulgaris extract made from step S3, peach blossom essential oil, olive made from step S4
Oil, evening primrose oil, are uniformly mixed, obtain mixture B；
S8. mixture B made from mixture A made from step S6 and step S7 is placed in homogeneous emulsifying machine, setting is equal
The temperature of matter emulsification is 42 DEG C, and frequency is 115Hz, and the emulsifying time is 35min, obtains creams, and creams sterilizing, embedding is produced
The dendrobium candidum eye cream.
Embodiment 5
A kind of preparation method of dendrobium candidum eye cream, comprises the following steps：
S1. dendrobium candidum extract is prepared：200 parts plus 8 times amount water immersion 1h of fresh dendrobium candidum stem after cleaning are taken, plus
Circumfluence distillation 2h, filtrate decompression is condensed into paste, standby；
S2. prepare gold and engrave prunus mume extract：Take gold to engrave 80 parts of plum plus 15 times of amounts water immersion 2h, heating distillation 3h, point take and to distillate
Liquid, it is standby；
S3. Prunella vulgaris extract is prepared：70% ethanol of 80 parts plus 15 times amounts of selfheal is taken, refluxing extraction 1h extracts 2
Secondary, suction filtration, merging filtrate is simultaneously concentrated, freeze-drying, standby；
S4. peach blossom essential oil is prepared：60 parts plus 2 times amount water immersion 3h of peach blossom are taken, the peach blossom soaked is placed in overcritical two
Carbonoxide extraction equipment, extracting pressure is 15MPa, and extraction temperature is 50 DEG C, and CO2 flows are 20kg/h, and extraction time is 2h, are used
90% ethanol makees entrainer, and consumption is 250ml, produces peach blossom essential oil, standby；
S5. component is weighed by following parts by weight：110 parts of Tea Polyphenols, 100 parts of trehalose, 70 parts of vitamin E, olive oil 60
Part, 30 parts of evening primrose oil；
S6. take Tea Polyphenols, trehalose to add the water cooling leaching 24h of equivalent, mix, gold made from addition S2 engraves plum extract solution,
Mix, obtain mixture A；
S7. take dendrobium candidum extract, vitamin E made from step S1 to be heated to 60 DEG C, stir to being completely dissolved, it is quiet
Put, when temperature is down to 45 DEG C, add Prunella vulgaris extract made from step S3, peach blossom essential oil, olive made from step S4
Oil, evening primrose oil, are uniformly mixed, obtain mixture B；
S8. mixture B made from mixture A made from step S6 and step S7 is placed in homogeneous emulsifying machine, setting is equal
The temperature of matter emulsification is 45 DEG C, and frequency is 120Hz, and the emulsifying time is 40min, obtains creams, and creams sterilizing, embedding is produced
The dendrobium candidum eye cream.
2nd, the quality testing of dendrobium candidum eye cream
1. examination criteria
(1) with reference to QB/T1857-2014《People's Republic of China's light industry standard -- moisturizing cream》
(2)《Cosmetics health specification》(2007 editions)
2. organoleptic indicator
It the results are shown in Table 1.
The organoleptic indicator's testing result table of table 1
Testing result shows：The every organoleptic indicator of 1-5 of embodiment of the present invention eye cream meets QB/T1857-2014《In
Magnificent people's republic's light industry standard -- moisturizing cream》Requirement.
3. physical and chemical index
3.1 heat resistant test
1-5 of embodiment of the present invention samples are poured into test tube respectively, make liquid level about 10cm, each embodiment falls 2
Test tube, is stoppered with clean cork, and a test tube is placed in room temperature, and another test tube, which is placed in, to be pre-adjusted to 40 DEG C ± 1
DEG C electro-heating standing-temperature cultivator in, take out, placed to carrying out range estimation ratio with being placed in the sample of test tube in room temperature after room temperature after 24h
Compared with the results are shown in Table 2.
The heat resistant test result table of table 2
Result of the test shows：1-5 of embodiment of the present invention eye cream places 24h under conditions of 40 DEG C ± 1 DEG C, without profit
Segregation phenomenon, shows that eye cream heat endurance of the present invention is good.
3.2 low temperature resistant test
1-5 of embodiment of the present invention samples are poured into test tube respectively, make liquid level about 10cm, each embodiment falls 2
Test tube, is stoppered with clean cork, and a test tube is placed in room temperature, and another test tube to be tested is placed in (- 8 ± 2) DEG C ice
In case, taken out after 24h, place to room temperature the sample progress range estimation with being placed in test tube in room temperature and compared, the results are shown in Table 3.
The low temperature resistant test result table of table 3
Result of the test shows：1-5 of embodiment of the present invention eye cream places 24h under the conditions of (- 8 ± 2) DEG C, without profit point
From phenomenon, show that the cold-resistant stability of eye cream of the present invention is good.
4. sanitary index
Testing result is shown in Table 4.
The sanitary index result of table 4 detects table
Testing result shows：Every sanitary index of 1-5 of embodiment of the present invention eye cream meets《Cosmetics health is advised
Model》The regulation of (2007 editions).
3rd, application test
1. eliminate dry line, microgroove near the eyes
1.1 crowds select
Selection has the women 120 of 20-50 one full year of life of microgroove and dry line near the eyes, is randomly divided into two groups, every group of 60 people.
1.2 application method
Test group：Eye skin is cleaned, the eye cream small rice grain size of the embodiment of the present invention 4 is taken, is first existed with nameless finger pulp
Two now side's point scatter, do annular along inner eye corner, upper eyelid, eye tail, lower eyelid and gently massage, generally 4-5 circles left and right.Sooner or later
Respectively once, it is continuous to use 20 days.Trial employment period avoids using excitant cosmetics, it is to avoid the intake of irritable food, it is to avoid endure
Night.
Control group：Using the crease-resistant nursing eye cream of certain commercially available brand, used according to application method, it is continuous to use 20 days.It is on probation
Period avoids using excitant cosmetics, it is to avoid the intake of irritable food, it is to avoid stay up late.
1.3 effects judge
Eliminate：Microgroove, dry line disappear near the eyes, and eye skin water profit is smooth；
It is effective：Microgroove, dry line are reduced or disappeared near the eyes, and eye skin is partially dry；
Effectively：Microgroove, dry line are reduced near the eyes, and eye skin is dried；
It is invalid：It is as good as near the eyes before microgroove, dry line and use, skin before use with being as good as near the eyes.
1.4 result of the test
The results detailed in Table 5.
Table 5 eliminates dry line, microgroove result of the test table near the eyes
| Packet | Number of cases | Eliminate | It is effective | Effectively | It is invalid | Total effective rate (%) |
| Test group | 60 | 31 | 21 | 5 | 3 | 95 |
| Control group | 60 | 20 | 15 | 11 | 14 | 76.7 |
In above process of the test, there is adverse reaction in none in test group patient, and has 3 to occur not in control group
With the red swelling of the skin of degree, the adverse reaction such as itch.
As shown in Table 5, it is 95% that 4 pairs of the embodiment of the present invention, which eliminates dry line, microgroove total effective rate near the eyes, higher than control group,
And not occurring any adverse reaction in process of the test, dry line, microgroove near the eyes can effectively be eliminated by illustrating the eye cream of the present invention, be made
With safe and effective.The following is several typical cases：
Typical case 1：Zhang, female 29 years old, because pseudo-myopia is also not equipped with glasses, sees that the thing habituation of distant place is narrowed
Eye, occurs in that numerous microgrooves in the course of time, around canthus, and eye skin dries, intense darkness without light.Continuously use the embodiment of the present invention
4 eye cream is after 20 days, and canthus microgroove disappears, and eye skin water profit is smooth.
Typical case 2：Mr. Wang, female, 26 years old, because working principle be unable to do without computer and word, the spare time also be unable to do without
Mobile phone and tablet personal computer, add and do not note eye-care usually, cause circumference of eyes to occur in that dry line early.Continuously use this hair
The eye cream of bright embodiment 4 is after 20 days, the dry line of eye disappears, and eye skin water profit is glossy.
2. eliminate livid ring around eye, pouch, eye edema
2.1 crowds select
Selection has livid ring around eye, pouch, the women of 20-50 one full year of life of eye edema 100, is randomly divided into two groups, every group 50
People.
2.2 application method
Test group：Eye skin is cleaned, the eye cream small rice grain size of the embodiment of the present invention 4 is taken, is first existed with nameless finger pulp
Two now side's point scatter, do annular along inner eye corner, upper eyelid, eye tail, lower eyelid and gently massage, generally 4-5 circles left and right.Sooner or later
Respectively once, it is continuous to use 20 days.Trial employment period avoids using excitant cosmetics, it is to avoid the intake of irritable food, is kept away before sleeping
Exempt to drink substantial amounts of water, it is to avoid stay up late.
Control group：It is used for the eye cream for eliminating livid ring around eye, pouch, eye edema using certain commercially available brand, according to application method
Use, it is continuous to use 20 days.Trial employment period avoids using excitant cosmetics, it is to avoid the intake of irritable food, is avoided before sleeping
Drink substantial amounts of water, it is to avoid stay up late.
2.3 effects judge
Eliminate：Livid ring around eye, pouch, eye edema disappear, and eye skin is tender smooth；
It is effective：Livid ring around eye are substantially desalinated, and pouch is obviously reduced, and eye edema is obviously reduced, and eye skin is dark and gloomy without light
It is aobvious to improve；
Effectively：Livid ring around eye are desalinated, and pouch reduces, and eye edema reduces, and eye skin is dark and gloomy unglazed to make moderate progress；
It is invalid：It is as good as before livid ring around eye, pouch, eye edema symptom and use, eye skin before use with being as good as.2.4 examination
Test result
The results detailed in Table 6.
Table 6 eliminates livid ring around eye, pouch, eye oedema assay result table
| Packet | Number of cases | Eliminate | It is effective | Effectively | It is invalid | Total effective rate (%) |
| Test group | 50 | 36 | 9 | 4 | 1 | 98 |
| Control group | 50 | 21 | 10 | 7 | 12 | 76 |
In above process of the test, there is adverse reaction in none in test group patient, and has 1 skin occur in control group
Skin is red and swollen, the adverse reaction such as itch.
As shown in Table 6, the embodiment of the present invention 4 is offseted except livid ring around eye, pouch, eye edema total effective rate are 98%, is higher than
Control group, and do not occur any adverse reaction in process of the test, livid ring around eye, eye can effectively be eliminated by illustrating the eye cream of the present invention
Bag, eye edema, using safe and effective.The following is several typical cases：
Typical case 1：Luo, female, 29 years old, because operating pressure is too big, overtime work of often staying up late occurred in that serious black eye
Circle, eye part skin is dark and gloomy unglazed.The continuous eye cream using the embodiment of the present invention 4 is after 20 days, and livid ring around eye disappear, and eye skin is tender
It is smooth.
Typical case 2：Gold certain, female, 43 years old, Yin Laodun, sleep it is not good enough, occur in that serious pouch, eye part skin is dark and gloomy
It is unglazed.The continuous eye cream using the embodiment of the present invention 4 is after 20 days, and pouch disappears, and eye skin water profit is smooth.
Typical case 3：It is blue certain, female, 35 years old, long periods of wear contact lenses caused eye edema often occur.Continuously use
The eye cream of the embodiment of the present invention 4 is after 20 days, and eye edema disappears.
3. eliminate eye fat granule
3.1 crowds select
The women 80 of the 20-50 one full year of life of eye with fat granule is selected, two groups, every group of 40 people are randomly divided into.
3.2 application method
Test group：Eye skin is cleaned, the eye cream small rice grain size of the embodiment of the present invention 4 is taken, is first existed with nameless finger pulp
Two now side's point scatter, do annular along inner eye corner, upper eyelid, eye tail, lower eyelid and gently massage, generally 4-5 circles left and right.Sooner or later
Respectively once, it is continuous to use 7 days.Trial employment period avoids using excitant cosmetics, it is to avoid use the shield that nutrient composition content is too high
Skin product.
Control group：It is used for the eye mask for eliminating eye fat granule using certain commercially available brand, uses, continuously make according to application method
With 7 days.Trial employment period avoids using excitant cosmetics, it is to avoid use the skin care item that nutrient composition content is too high.
3.3 effects judge
Eliminate：Eye fat granule is wholly absent, and eye skin water profit is smooth；
It is effective：Eye fat granule is significantly reduced, and eye is coarse dark and gloomy to be obviously improved；
Effectively：Eye fat granule is reduced, and eye skin is coarse dark and gloomy to make moderate progress；
It is invalid：Eye fat granule before use with being as good as, and eye skin before use with being as good as.
3.4 result of the test
The results detailed in Table 7.
Table 7 eliminates eye fat granule result of the test table
| Packet | Number of cases | Eliminate | It is effective | Effectively | It is invalid | Total effective rate (%) |
| Test group | 40 | 30 | 6 | 3 | 1 | 97.5 |
| Control group | 40 | 18 | 5 | 8 | 9 | 77.5 |
In above process of the test, there is adverse reaction in none in test group patient, and has 2 to occur not in control group
With the red swelling of the skin of degree, the adverse reaction such as itch.
As shown in Table 7, it is 97.5% that 4 pairs of the embodiment of the present invention, which eliminates eye fat granule total effective rate, higher than control group, and
And not occurring any adverse reaction in process of the test, eye fat granule can effectively be eliminated by illustrating the eye cream of the present invention, use peace
It is complete effective.The following is several typical cases：
Typical case 1：Week certain, female 27 years old, because the too high eye skin care item of nutrient composition content are commonly used, causes eye
All skin nutritions are superfluous, grown numerous fat granules, circumference of eyes skin is coarse dark and gloomy.Use the eye cream 7 of the embodiment of the present invention 4
After it, fat granule all disappears, and eye skin water profit is smooth.
Typical case 2：Lee, female 33 years old, likes the eye make-up that picture is dense, removes ornaments and formal dress not complete enough, cause clogging of pores, from
And induce short grained near the eyes produce.After the eye cream 7 days of the embodiment of the present invention 4, little particle is significantly reduced near the eyes, is reused
7 days, little particle all disappearances near the eyes, eye skin water profit was smooth.
The specific implementation of the invention is not to be limited to these illustrations for above content, is led for technology belonging to the present invention
For the those of ordinary skill in domain, without departing from the inventive concept of the premise, some simple deduction or replace can also be made,
The scope of patent protection that the present invention is determined by the claims submitted should be all considered as belonging to.
Claims (10)
1. a kind of dendrobium candidum eye skin care item, it is characterised in that including following raw material：Dendrobium candidum extract, gold are engraved plum and carried
Take thing, Prunella vulgaris extract, peach blossom essential oil.
2. dendrobium candidum eye skin care item according to claim 1, it is characterised in that also include the group of following parts by weight
Point：70-110 parts of Tea Polyphenols, 60-100 parts of trehalose, 30-70 parts of vitamin E, 20-60 parts of olive oil, evening primrose oil 10-30
Part.
3. dendrobium candidum eye skin care item according to claim 1, it is characterised in that the system of the dendrobium candidum extract
Preparation Method is：160-200 parts plus 5-8 times of fresh dendrobium candidum stem after cleaning is taken to measure water immersion 0.5-1h, heating and refluxing extraction
1-2h, filtrate decompression is condensed into paste, produces dendrobium candidum extract.
4. dendrobium candidum eye skin care item according to claim 1, it is characterised in that the gold engraves the preparation of prunus mume extract
Method is：Take gold to engrave 50-80 parts plus 10-15 times of plum and measure water immersion 1-2h, heating distillation 2-3h, divide and take distillate, produce gold and engrave
Prunus mume extract.
5. dendrobium candidum eye skin care item according to claim 1, it is characterised in that the preparation of the Prunella vulgaris extract
Method is：70% ethanol for taking 50-80 parts plus 10-15 times of selfheal to measure, refluxing extraction 1h is extracted 2 times, suction filtration, merging filtrate
And concentrate, it is freeze-dried to obtain Prunella vulgaris extract.
6. dendrobium candidum eye skin care item according to claim 1, it is characterised in that the preparation method of the peach blossom essential oil
For：Take 40-60 parts plus 1-2 times of peach blossom to measure water immersion 2-3h, the peach blossom soaked be placed in supercritical carbon dioxide extraction apparatus,
Extracting pressure is 12-15MPa, and extraction temperature is 45-50 DEG C, and CO2 flows are 15-20kg/h, and extraction time is 1-2h, uses 80-
90% ethanol makees entrainer, and consumption is 200-250ml, produces peach blossom essential oil.
7. dendrobium candidum eye skin care item according to claim 1 or 2, it is characterised in that prepared by the eye skin care item
Into eye cream, eye glue, eye mask, eye essence.
8. dendrobium candidum eye skin care item according to claim 1 or 2, it is characterised in that prepared by the eye skin care item
Into eye cream.
9. a kind of dendrobium candidum eye skin care item according to claim 8 are prepared into the preparation method of eye cream, its feature exists
In comprising the following steps：
S1. dendrobium candidum extract is prepared：160-200 parts plus 5-8 times of fresh dendrobium candidum stem after cleaning is taken to measure water immersion
0.5-1h, heating and refluxing extraction 1-2h, filtrate decompression is condensed into paste, standby；
S2. prepare gold and engrave prunus mume extract：Take gold to engrave 50-80 parts plus 10-15 times of plum and measure water immersion 1-2h, heating distillation 2-3h, point
Distillate is taken, it is standby；
S3. Prunella vulgaris extract is prepared：70% ethanol for taking 50-80 parts plus 10-15 times of selfheal to measure, refluxing extraction 1h extracts 2
Secondary, suction filtration, merging filtrate is simultaneously concentrated, freeze-drying, standby；
S4. peach blossom essential oil is prepared：Take 40-60 parts plus 1-2 times of peach blossom to measure water immersion 2-3h, the peach blossom soaked is placed in overcritical
Carbon dioxide extraction apparatus, extracting pressure is 12-15MPa, and extraction temperature is 45-50 DEG C, and CO2 flows are 15-20kg/h, extraction
Time is 1-2h, and entrainer is made with 80-90% ethanol, and consumption is 200-250ml, produces peach blossom essential oil, standby；
S5. component is weighed by following parts by weight：70-110 parts of Tea Polyphenols, 60-100 parts of trehalose, 30-70 parts of vitamin E, olive
Oily 20-60 parts, 10-30 parts of evening primrose oil；
S6. take Tea Polyphenols, trehalose to add the water cooling leaching 12-24h of equivalent, mix, gold made from addition S2 engraves plum extract solution, mixes
It is even, obtain mixture A；
S7. dendrobium candidum extract, vitamin E made from step S1 is taken to be heated to 60 DEG C, stirring stands, treated to being completely dissolved
When temperature is down to 45 DEG C, Prunella vulgaris extract made from step S3, peach blossom essential oil made from step S4, olive oil, the moon are added
See careless oil, be uniformly mixed, obtain mixture B；
S8. mixture B made from mixture A made from step S6 and step S7 is placed in emulsifying in homogeneous emulsifying machine, obtained
Creams, creams sterilizing, embedding produces the dendrobium candidum eye cream.
10. dendrobium candidum eye skin care item according to claim 9 are prepared into the preparation method of eye cream, it is characterised in that
The temperature of emulsifying described in step S8 is 30-45 DEG C, and frequency is 100-120Hz, and the emulsifying time is 30-40min.
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| CN108379203A (en) * | 2018-05-31 | 2018-08-10 | 南京财经大学 | A kind of natural oat bran antiallergy toner and preparation method thereof |
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| CN108113953A (en) * | 2018-01-08 | 2018-06-05 | 植然方适（杭州）健康科技有限公司 | A kind of dendrobium candidum honey composite extract with moisture-keeping efficacy and preparation method thereof and the application in skin care item |
| CN108186519A (en) * | 2018-02-13 | 2018-06-22 | 卢玉香 | cassia seed eye essence and preparation method thereof |
| CN108379169A (en) * | 2018-05-04 | 2018-08-10 | 无限极（中国）有限公司 | A kind of composition and its application in preparing the cosmetics for releiving fatigue |
| CN108379203A (en) * | 2018-05-31 | 2018-08-10 | 南京财经大学 | A kind of natural oat bran antiallergy toner and preparation method thereof |
| CN109394647A (en) * | 2018-12-17 | 2019-03-01 | 海南诗博丽生物科技有限公司 | A kind of dendrobium nobile repairs eye cream and preparation method thereof |
| CN109394647B (en) * | 2018-12-17 | 2021-10-15 | 海南诗博丽生物科技有限公司 | Dendrobium restoration eye cream and preparation method thereof |
| CN109875933A (en) * | 2019-03-28 | 2019-06-14 | 广州市富宝日用化工有限公司 | Compact eye cream cosmetics of a kind of U.S. pupil and preparation method thereof |
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Application publication date: 20170915 |