CN108186519A - cassia seed eye essence and preparation method thereof - Google Patents
cassia seed eye essence and preparation method thereof Download PDFInfo
- Publication number
- CN108186519A CN108186519A CN201810150002.7A CN201810150002A CN108186519A CN 108186519 A CN108186519 A CN 108186519A CN 201810150002 A CN201810150002 A CN 201810150002A CN 108186519 A CN108186519 A CN 108186519A
- Authority
- CN
- China
- Prior art keywords
- extract
- cassia seed
- filtrate
- eye
- pearl powder
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/365—Hydroxycarboxylic acids; Ketocarboxylic acids
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/005—Preparations for sensitive skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/52—Stabilizers
- A61K2800/524—Preservatives
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Dermatology (AREA)
- Gerontology & Geriatric Medicine (AREA)
- Emergency Medicine (AREA)
- Zoology (AREA)
- Engineering & Computer Science (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Cosmetics (AREA)
- Medicines Containing Plant Substances (AREA)
- Non-Alcoholic Beverages (AREA)
Abstract
The invention discloses a kind of cassia seed eye essence, include the raw material of following mass percent：Glycine betaine 0.1%~0.5%, hydrolysis avenin 0.1%~0.5%, cassia seed extract 1%~5%, ginseng extract 0.5%~3%, mulberry-leaf extract 1%~5%, camellia leaf extract 1%~5%, Salvia root P.E 1%~5%, Millettia extract 1%~5%, Herba Dendrobii extract 0.5%~3%, rice spent wash 70%~80%, surplus is water.A kind of preparation method of cassia seed eye essence is provided simultaneously, including：Raw material is weighed, is stirred, adds lotus leaf and wormwood mixed extract, pearl powder and Aloe Vera Gel, then carry out homogenization.The present invention has effects that the advantageous effects such as notable, safe, stability is good.
Description
Technical field
The present invention relates to a kind of Essences.It is more particularly related to a kind of cassia seed eye essence, belongs to shield
Skin product technical field.
Background technology
" years urge people old ", for general women from after 25 years old, skin starts slowly aging.Wherein, eye skin is human body
Most thin in skin, most fragile skin, thus aging is easiest to, go out the problems such as dry, eye is puckery, livid ring around eye of losing face；In addition, modern female
It is needed for a long time in face of computer during sex work, radiation is serious, along with often staying up late, it is easier to cause the old of eye skin
Change, eye is led to problems such as to do, eye is puckery, livid ring around eye.
In order to keep the skin wet to eye skin, improve the symptom that eye is done, eye is puckery, while reduce livid ring around eye, people would generally
Eye skin is nursed using eye cream, eye mask, eye essence etc., slows down the aging of eye skin.However, at present on the market mostly
The effect of various problems such as several eyeware products and solution for lenses and contact lenses is done for eye, eye is puckery, skin water shortage, livid ring around eye, is general, and contains
A large amount of pure chemistry synthetic ingredient is used for a long time there are some potential safety problems, particularly to sensibility skin, in addition, some
Product stability is poor, after use the phase often will appear sedimentation, lamination problem, the effect of so as to influence product.Therefore, for
Above-mentioned the deficiencies in the prior art, development is a kind of to solve the various problems such as eye is done, eye is puckery, skin water shortage, livid ring around eye, and work(
Eyeware products and solution for lenses and contact lenses notable, safe, that stability is good is imitated, slows down female group the aging of eye skin, keep eye
It is so beautiful that it excites men to be of great significance.
Invention content
It is an object of the present invention to provide a kind of cassia seed eye essence, can keep the skin wet to eye skin, grow
Moisten eye skin, improve the symptom that eye is done, eye is puckery, while reduce livid ring around eye, and effect is notable, can effectively slow down eye skin
Aging.
It is a still further object of the present invention to provide a kind of preparation methods of cassia seed eye essence, and it is anti-to reduce chemistry
The dosage of rotten agent, the safety of enhancing Essence when used for a long time, while the dispersion stabilization of Essence can also be enhanced, prevent essence
Magnificent liquid settles in use, influences effect, so as to prepare the eye that a kind of effect is notable, safe, stability is good
Portion's Essence.
In order to realize these purposes and other advantages according to the present invention, a kind of cassia seed eye essence is provided, is wrapped
Include the raw material of following mass percent：Glycine betaine 0.1%~0.5%, hydrolysis avenin 0.1%~0.5%, cassia seed extraction
Object 1%~5%, ginseng extract 0.5%~3%, mulberry-leaf extract 1%~5%, camellia leaf extract 1%~5%, Radix Salviae Miltiorrhizae
Extract 1%~5%, Millettia extract 1%~5%, Herba Dendrobii extract 0.5%~3%, rice spent wash 70%~80%,
Surplus is water.
Preferably, the cassia seed eye essence includes the raw material of following mass percent：Glycine betaine 0.2%,
Hydrolyze avenin 0.3%, cassia seed extract 3%, ginseng extract 1%, mulberry-leaf extract 3%, camellia leaf extract
2%th, Salvia root P.E 2%, Millettia extract 2%, Herba Dendrobii extract 1%, rice spent wash 75%, water 10.5%.
The purpose of the present invention can also further be realized that this method includes by the method for preparing cassia seed eye essence
Following steps：
Step 1：Cassia seed extract, ginseng extract, mulberry-leaf extract, the extraction of camellia leaf are weighed by mass percentage
Object, Salvia root P.E, Millettia extract, Herba Dendrobii extract, mixing add in the rice spent wash of half quality, stir evenly, then
Add in lotus leaf and wormwood mixed extract, the additive amount of lotus leaf and wormwood mixed extract is 0.6wt%, is stirred evenly, and obtains the
One mixture；Wherein, the preparation method of lotus leaf and wormwood mixed extract includes：According to mass ratio 1:1 weighs lotus leaf and wormwood,
At 80 DEG C after drying for 24 hours, mixing, addition quality is 10 times of weights of lotus leaf and wormwood gross mass, the second that volume fraction is 95%
Alcoholic solution, under nitrogen protection, the infusion 3h under the conditions of 75 DEG C, 0.5MPa filter after cooling, obtain the first filtrate and the first filter
Slag will crush after the first filter residue and drying, sieving, obtains coarse powder, then coarse powder is carried out ultramicro grinding, crosses 300 mesh screens and obtain carefully
Powder, by the ethanol solution in mass ratio 1 that fine powder and volume fraction are 95%:After 8 mixing, freeze for 24 hours, take out at -20 DEG C, in
It thaws at room temperature, then 3h is heated to reflux at 65 DEG C, filtered after cooling, obtain the second filtrate and the second filter residue, the second filter residue is done
The ethanol solution in mass ratio 1 that dry rear and volume fraction is 95%:5 mixing, the ultrasonic wave for being 500MHz with frequency at 55 DEG C
1h is handled, filters, obtains third filtrate and third filter residue, the first filtrate, the second filtrate, third filtrate are mixed, obtain total filtrate, it will
It is 1.24 that total filtrate, which is concentrated into relative density, and it is 1 to add mass ratio:2 gelatin and chitosan compound, gelatin and chitosan
The 6% of quality, stands 2h after the additive amount of mixture is concentrated for total filtrate after stirring evenly, and filters, obtains clarified solution, then 45
DEG C, under the conditions of 30MPa, with supercritical carbon dioxide extraction 100min, obtain lotus leaf and wormwood mixed extract；
Step 2：It is 1 to weigh mass ratio:1 pearl powder and Aloe Vera Gel, first pre-processes pearl powder, then by aloe
Glue is warming up to 55 DEG C, then adds in pretreated pearl powder while stirring, when temperature is down to 40 DEG C, adds remaining half
The rice spent wash of quality, stirs evenly, and obtains the second mixture, then the second mixture is added to the first mixing made from step 1
It in object, stirs evenly, obtains third mixture；Wherein, the total addition level of pearl powder and Aloe Vera Gel be 0.8wt%, pearl powder it is pre-
Processing procedure includes：In molar ratio 1:1 mixes pearl powder and lactic acid, is stirred to react 1h at 65 DEG C, treats that temperature is down to 50 DEG C
When, it adds in disodium ethylene diamine tetraacetate and continues to be stirred to react 1h, be cooled to room temperature, disodium ethylene diamine tetraacetate and pearl powder
Molar ratio is 1:1；
Step 3：Glycine betaine, hydrolysis avenin and water are mixed, 60 DEG C is heated to, stirs evenly, treat that temperature is down to 40
DEG C when, add mass ratio as 2:2:1:1:The mixing of 1 glycerine, Sodium Hyaluronate, polyethylene glycol, vitamin C and vitamin E
Object stirs evenly, and is cooled to room temperature, and obtains the 4th mixture, and third mixture made from step 2 is added to the 4th mixture
In, it stirs evenly, then carry out homogenization to get eye essence；Wherein, glycerine, Sodium Hyaluronate, polyethylene glycol, dimension life
The additive amount of plain C and tocopherol admixture is 1wt%.
Preferably, in step 1, after the first filter residue is crushed, net is sieved with 100 mesh sieve, obtains coarse powder.
Preferably, in step 1, the method for total filtrate concentration is vacuum distillation.
Preferably, in step 2, pearl powder is the Nano pearl powder that natural fresh water pearl is processed.
Preferably, in step 3, the average molecular weight of polyethylene glycol is 200.
The present invention includes at least following advantageous effect：
(1) cassia seed eye essence provided by the invention can keep the skin wet to eye skin, moisten eye skin, change
The symptom that kind eye is done, eye is puckery, while reduce livid ring around eye.
(2) cassia seed eye essence provided by the invention includes various plants extract, can solve various eyes
Portion's skin problem has effects that the advantages such as notable, safe, stability is good.
(3) lotus leaf and the mixed extract of wormwood are added in preparation method provided by the invention, is contained in lotus leaf and wormwood
There are many antipathogenic composition, these antipathogenic compositions have stronger antibacterial action, and Nantural non-toxic, can effectively improve eye essence
The antibacterial ability of magnificent liquid so as to reduce the dosage of chemical preservative, improves the safety in utilization of eye essence.
(4) pearl powder and Aloe Vera Gel are added in preparation method provided by the invention, pearl powder passes through lactic acid and ethylenediamine
The active ingredient in Essence, under the synergistic effect of Aloe Vera Gel, pearl powder energy can be adsorbed after tetraacethyl disodium processing well
It is stably dispersed in Essence well, so as to enhance the dispersion stabilization of Essence, prevents Essence from sending out in use
Raw sedimentation, influences effect.
Part is illustrated to embody by further advantage, target and the feature of the present invention by following, and part will also be by this
The research and practice of invention and be understood by the person skilled in the art.
Specific embodiment
With reference to example, the present invention is described in further detail, to enable those skilled in the art with reference to specification text
Word can be implemented according to this.
It should be appreciated that such as " having ", "comprising" and " comprising " term used herein do not allot one or more
The presence or addition of a other element or combinations.
<Embodiment 1>
The preparation method of cassia seed eye essence includes：Cassia seed extract 1% is weighed by mass percentage, ginseng carries
Take object 3%, mulberry-leaf extract 1%, camellia leaf extract 5%, Salvia root P.E 5%, Millettia extract 5%, stem of noble dendrobium extraction
Object 3%, mixing add in the rice spent wash (mass percent of rice spent wash is 70%) of half quality, stir evenly, add
The additive amount of lotus leaf and wormwood mixed extract, lotus leaf and wormwood mixed extract is 0.6wt%, is stirred evenly, and it is mixed to obtain first
Close object；Wherein, the preparation method of lotus leaf and wormwood mixed extract includes：According to mass ratio 1:1 weighs lotus leaf and wormwood, in 80
At DEG C after drying for 24 hours, it is molten to add in the ethyl alcohol that quality is 10 times of weights of lotus leaf and wormwood gross mass, volume fraction is 95% for mixing
Liquid, under nitrogen protection, the infusion 3h under the conditions of 75 DEG C, 0.5MPa filter after cooling, obtain the first filtrate and the first filter residue, will
It is crushed after first filter residue and drying, sieves with 100 mesh sieve net, obtained coarse powder, then coarse powder is subjected to ultramicro grinding, cross 300 mesh screens and obtain
Fine powder, by the ethanol solution in mass ratio 1 that fine powder and volume fraction are 95%:After 8 mixing, freeze for 24 hours, take out at -20 DEG C,
It thaws at room temperature, then 3h is heated to reflux at 65 DEG C, filtered after cooling, obtain the second filtrate and the second filter residue, by the second filter residue
After drying with volume fraction be 95% ethanol solution in mass ratio 1:5 mixing, the ultrasound for being 500MHz with frequency at 55 DEG C
Wave handles 1h, filters, obtains third filtrate and third filter residue, and the first filtrate, the second filtrate, third filtrate are mixed, obtain total filtrate,
It is 1.24 by total filtrate decompression distillation and concentration to relative density, it is 1 to add mass ratio:2 gelatin and chitosan compound, it is bright
The 6% of quality, stands 2h after the additive amount of glue and chitosan compound is concentrated for total filtrate after stirring evenly, and filters, must clarify
Liquid, then under the conditions of 45 DEG C, 30MPa, with supercritical carbon dioxide extraction 100min, obtain lotus leaf and wormwood mixing extraction
Liquid；It is 1 to weigh mass ratio:1 pearl powder and Aloe Vera Gel, first pre-processes pearl powder, then Aloe Vera Gel is warming up to 55 DEG C,
Then pretreated pearl powder is added in while stirring, when temperature is down to 40 DEG C, adds the rice vinasse of remaining half quality
Water stirs evenly, and obtains the second mixture, then the second mixture is added in the first mixture made from step 1, and stirring is equal
It is even, obtain third mixture；Wherein, the total addition level of pearl powder and Aloe Vera Gel be 0.8wt%, the preprocessing process packet of pearl powder
It includes：In molar ratio 1:1 Nano pearl powder for processing natural fresh water pearl and lactic acid mixing, are stirred to react at 65 DEG C
1h when temperature is down to 50 DEG C, adds in disodium ethylene diamine tetraacetate and continues to be stirred to react 1h, be cooled to room temperature, ethylenediamine tetraacetic
The molar ratio of acetic acid disodium and pearl powder is 1:1；The water of glycine betaine 0.1%, hydrolysis avenin 0.1% and surplus is mixed,
60 DEG C are heated to, is stirred evenly, when temperature is down to 40 DEG C, it is 2 to add mass ratio:2:1:1:1 glycerine, hyaluronic acid
The mixture of sodium, average molecular weight for 200 polyethylene glycol, vitamin C and vitamin E, stirs evenly, is cooled to room temperature, obtain
Third mixture made from step 2 is added in the 4th mixture, stirs evenly, then carries out at homogeneous by the 4th mixture
Reason is to get eye essence；Wherein, the addition of glycerine, Sodium Hyaluronate, polyethylene glycol, vitamin C and tocopherol admixture
It measures as 1wt%.
<Embodiment 2>
The preparation method of cassia seed eye essence includes：Cassia seed extract 3% is weighed by mass percentage, ginseng carries
Take object 1%, mulberry-leaf extract 3%, camellia leaf extract 2%, Salvia root P.E 2%, Millettia extract 2%, stem of noble dendrobium extraction
Object 1%, mixing add in the rice spent wash (mass percent of rice spent wash is 75%) of half quality, stir evenly, add
The additive amount of lotus leaf and wormwood mixed extract, lotus leaf and wormwood mixed extract is 0.6wt%, is stirred evenly, and it is mixed to obtain first
Close object；Wherein, the preparation method of lotus leaf and wormwood mixed extract includes：According to mass ratio 1:1 weighs lotus leaf and wormwood, in 80
At DEG C after drying for 24 hours, it is molten to add in the ethyl alcohol that quality is 10 times of weights of lotus leaf and wormwood gross mass, volume fraction is 95% for mixing
Liquid, under nitrogen protection, the infusion 3h under the conditions of 75 DEG C, 0.5MPa filter after cooling, obtain the first filtrate and the first filter residue, will
It is crushed after first filter residue and drying, sieves with 100 mesh sieve net, obtained coarse powder, then coarse powder is subjected to ultramicro grinding, cross 300 mesh screens and obtain
Fine powder, by the ethanol solution in mass ratio 1 that fine powder and volume fraction are 95%:After 8 mixing, freeze for 24 hours, take out at -20 DEG C,
It thaws at room temperature, then 3h is heated to reflux at 65 DEG C, filtered after cooling, obtain the second filtrate and the second filter residue, by the second filter residue
After drying with volume fraction be 95% ethanol solution in mass ratio 1:5 mixing, the ultrasound for being 500MHz with frequency at 55 DEG C
Wave handles 1h, filters, obtains third filtrate and third filter residue, and the first filtrate, the second filtrate, third filtrate are mixed, obtain total filtrate,
It is 1.24 by total filtrate decompression distillation and concentration to relative density, it is 1 to add mass ratio:2 gelatin and chitosan compound, it is bright
The 6% of quality, stands 2h after the additive amount of glue and chitosan compound is concentrated for total filtrate after stirring evenly, and filters, must clarify
Liquid, then under the conditions of 45 DEG C, 30MPa, with supercritical carbon dioxide extraction 100min, obtain lotus leaf and wormwood mixing extraction
Liquid；It is 1 to weigh mass ratio:1 pearl powder and Aloe Vera Gel, first pre-processes pearl powder, then Aloe Vera Gel is warming up to 55 DEG C,
Then pretreated pearl powder is added in while stirring, when temperature is down to 40 DEG C, adds the rice vinasse of remaining half quality
Water stirs evenly, and obtains the second mixture, then the second mixture is added in the first mixture made from step 1, and stirring is equal
It is even, obtain third mixture；Wherein, the total addition level of pearl powder and Aloe Vera Gel be 0.8wt%, the preprocessing process packet of pearl powder
It includes：In molar ratio 1:1 Nano pearl powder for processing natural fresh water pearl and lactic acid mixing, are stirred to react at 65 DEG C
1h when temperature is down to 50 DEG C, adds in disodium ethylene diamine tetraacetate and continues to be stirred to react 1h, be cooled to room temperature, ethylenediamine tetraacetic
The molar ratio of acetic acid disodium and pearl powder is 1:1；The water of glycine betaine 0.2%, hydrolysis avenin 0.3% and surplus is mixed,
60 DEG C are heated to, is stirred evenly, when temperature is down to 40 DEG C, it is 2 to add mass ratio:2:1:1:1 glycerine, hyaluronic acid
The mixture of sodium, average molecular weight for 200 polyethylene glycol, vitamin C and vitamin E, stirs evenly, is cooled to room temperature, obtain
Third mixture made from step 2 is added in the 4th mixture, stirs evenly, then carries out at homogeneous by the 4th mixture
Reason is to get eye essence；Wherein, the addition of glycerine, Sodium Hyaluronate, polyethylene glycol, vitamin C and tocopherol admixture
It measures as 1wt%.
<Embodiment 3>
The preparation method of cassia seed eye essence includes：Cassia seed extract 5% is weighed by mass percentage, ginseng carries
Object 0.5%, mulberry-leaf extract 5%, camellia leaf extract 1%, Salvia root P.E 1%, Millettia extract 1%, the stem of noble dendrobium is taken to carry
Object 0.5% is taken, is mixed, the rice spent wash (mass percent of rice spent wash is 80%) of half quality is added in, stirs evenly, then
Add in lotus leaf and wormwood mixed extract, the additive amount of lotus leaf and wormwood mixed extract is 0.6wt%, is stirred evenly, and obtains the
One mixture；Wherein, the preparation method of lotus leaf and wormwood mixed extract includes：According to mass ratio 1:1 weighs lotus leaf and wormwood,
At 80 DEG C after drying for 24 hours, mixing, addition quality is 10 times of weights of lotus leaf and wormwood gross mass, the second that volume fraction is 95%
Alcoholic solution, under nitrogen protection, the infusion 3h under the conditions of 75 DEG C, 0.5MPa filter after cooling, obtain the first filtrate and the first filter
Slag will crush after the first filter residue and drying, sieve with 100 mesh sieve net, obtains coarse powder, then coarse powder is carried out ultramicro grinding, crosses 300 mesh sieve
Fine powder is netted to obtain, by the ethanol solution in mass ratio 1 that fine powder and volume fraction are 95%:After 8 mixing, freezed at -20 DEG C for 24 hours,
It takes out, thaws, then 3h is heated to reflux at 65 DEG C, filtered after cooling at room temperature, obtain the second filtrate and the second filter residue, by second
After filter residue and drying with volume fraction be 95% ethanol solution in mass ratio 1:5 mixing, with frequency are 500MHz's at 55 DEG C
Ultrasonication 1h filters, obtains third filtrate and third filter residue, and the first filtrate, the second filtrate, third filtrate are mixed, obtained always
Total filtrate decompression distillation and concentration to relative density is 1.24 by filtrate, and it is 1 to add mass ratio:2 gelatin and chitosan mixing
The 6% of quality, stands 2h after the additive amount of object, gelatin and chitosan compound is concentrated for total filtrate after stirring evenly, and filters, obtains
Clarified solution, then under the conditions of 45 DEG C, 30MPa, with supercritical carbon dioxide extraction 100min, obtain lotus leaf and wormwood mixing carries
Take liquid；It is 1 to weigh mass ratio:1 pearl powder and Aloe Vera Gel, first pre-processes pearl powder, then Aloe Vera Gel is warming up to 55
DEG C, pretreated pearl powder is then added in while stirring, when temperature is down to 40 DEG C, adds the rice wine of remaining half quality
Poor water, stirs evenly, and obtains the second mixture, then the second mixture is added in the first mixture made from step 1, stirring
Uniformly, third mixture is obtained；Wherein, the total addition level of pearl powder and Aloe Vera Gel be 0.8wt%, the preprocessing process packet of pearl powder
It includes：In molar ratio 1:1 Nano pearl powder for processing natural fresh water pearl and lactic acid mixing, are stirred to react at 65 DEG C
1h when temperature is down to 50 DEG C, adds in disodium ethylene diamine tetraacetate and continues to be stirred to react 1h, be cooled to room temperature, ethylenediamine tetraacetic
The molar ratio of acetic acid disodium and pearl powder is 1:1；The water of glycine betaine 0.5%, hydrolysis avenin 0.5% and surplus is mixed,
60 DEG C are heated to, is stirred evenly, when temperature is down to 40 DEG C, it is 2 to add mass ratio:2:1:1:1 glycerine, hyaluronic acid
The mixture of sodium, average molecular weight for 200 polyethylene glycol, vitamin C and vitamin E, stirs evenly, is cooled to room temperature, obtain
Third mixture made from step 2 is added in the 4th mixture, stirs evenly, then carries out at homogeneous by the 4th mixture
Reason is to get eye essence；Wherein, the addition of glycerine, Sodium Hyaluronate, polyethylene glycol, vitamin C and tocopherol admixture
It measures as 1wt%.
Wherein, the cassia seed extract in raw material, ginseng extract, mulberry-leaf extract, camellia leaf extract, Radix Salviae Miltiorrhizae extraction
Object, Millettia extract, Herba Dendrobii extract be according to《Cosmetics health specification》Carry out the qualified products of production acquisition.
In order to illustrate the effect of the present invention, it is as follows that inventor provides comparative experiments：
<Comparative example 1>
The preparation method of cassia seed eye essence with embodiment 2, the difference lies in：People is not added in composition of raw materials
Ginseng, Radix Salviae Miltiorrhizae and Caulis Spatholobi.
<Comparative example 2>
The preparation method of cassia seed eye essence with embodiment 2, the difference lies in：In the preparation process of Essence
Lotus leaf and the mixed extract of wormwood are not added.
<Comparative example 3>
The preparation method of cassia seed eye essence with embodiment 2, the difference lies in：In the preparation process of Essence
Do not add pearl powder and Aloe Vera Gel.
The assay method of eye essence effect：Age does between 25~50 years old and there are eye, eye is puckery, eye for random selection
The female volunteers 180 of skin water shortage and livid ring around eye problem are randomly divided into 6 groups, and every group of 30 people, the 1st~3 group uses embodiment
1~3 cassia seed eye essence prepared, the 4th~6 group of cassia seed eye essence prepared using comparative example 1~3, experiment
In, suitable cassia seed eye essence is uniformly applied in eye skin after the daily morning and evening face cleaning of volunteer, all aspirations
The usage amount of person, access times are identical, and persistently using after 4 weeks, the use of every group of volunteer is evaluated according to following evaluation criterions
Effect, and count the result of each group.
The evaluation criterion of eye essence effect：
1st, it is effective：The eye skin water of volunteer is tender flexible, and eye is done, the puckery symptom of eye completely disappears, and livid ring around eye significantly subtract
It is few, and volunteer does not occur any skin discomfort；
2nd, effectively：The moisture and elasticity of the eye skin of volunteer increased, and eye is done, the puckery symptom of eye is alleviated, black
Eyelet is reduced, and volunteer does not occur any skin discomfort；
3rd, it is invalid：The moisture and elasticity of the eye skin of volunteer do not increase, and eye is done, the puckery symptom of eye is not alleviated, black eye
Circle is not reduced；Either there is skin discomfort in volunteer.
After measured, the result of eye essence effect such as the following table 1：
[table 1]
Remarks：2 invalid people are in comparative example 2：1 people is using not having any effect after eye essence, and 1 people is that occur
Skin is uncomfortable；1 invalid people is using not having any effect after eye essence in comparative example 3.
From upper table 1, it can be seen that the total effective rate of Examples 1 to 3 is 100%, illustrate prepared by Examples 1 to 3
Eye essence has effects that notable, can keep the skin wet well to eye skin, moistens eye skin, is effectively improved eye
Symptom dry, eye is puckery, while significantly reduce livid ring around eye.Wherein, the obvious effective rate highest of embodiment 2, effect is best, implements to be best
Example.
Compared with Example 2, the preparation method of cassia seed eye essence is identical for comparative example 1, the difference lies in：Raw material
Without addition ginseng, Radix Salviae Miltiorrhizae and Caulis Spatholobi in formula.From upper table 1, it can be seen that although the total effective rate of comparative example 1 is also
100%, but obvious effective rate illustrates that the eye essence prepared by comparative example 1 has and moistens eye flesh significantly lower than embodiment 2
Skin, improvement eye are done, the puckery symptom of eye, reduce black-eyed effect, but effect will be significantly lower than embodiment 2.This is because ginseng,
When Radix Salviae Miltiorrhizae and Caulis Spatholobi are used cooperatively, synergistic effect can be played, enhances the moisturizing moisten effect of Herba Dendrobii extract in raw material, changes
Kind eye is done, the puckery symptom of eye, livid ring around eye is reduced, the effect of so as to enhance eye essence.
Compared with Example 2, the preparation method of cassia seed eye essence is identical for comparative example 2, the difference lies in：In essence
Do not have to add lotus leaf and the mixed extract of wormwood in the preparation process of magnificent liquid.From upper table 1, it can be seen that comparative example 2 always has
Efficiency, obvious effective rate are below embodiment 2, and have also appeared the invalid situation of 2 people, wherein 1 people says to there is skin discomfort
The effect of eye essence prepared by bright comparative example 2, is not only below embodiment 2, but also there are certain irritations.This is
Because the alkaline components such as Nuciferine, N-nornuciferine, reticuline, deoxidation aporheine in lotus leaf have stronger antibacterial work
With in addition, the ingredients such as the flavone compounds such as Quercetin, isoquercitin, lotus leaf essential oil, steroidal also have certain antibacterial work
Property, and the ingredients such as the alpha-terpineol, β in wormwood-folium eucalypti essence, α-absinthol, β-cloves alkene, trans- reed alcohol also have stronger resist
Bacterium acts on, and after the mixed extract of lotus leaf and wormwood is added in Essence, can effectively improve the antibacterial ability of Essence, make
Essence has preferable chemical stability in use, ensures that Essence quality does not change, it is ensured that effect, simultaneously
The dosage of chemical synthesis class preservative is reduced, Essence is reduced to the irritation of skin, improves the safety in utilization of Essence, keep away
Exempt from user and phenomena such as skin is uncomfortable occur.
Compared with Example 2, the preparation method of cassia seed eye essence is identical for comparative example 3, the difference lies in：In essence
Without addition pearl powder and Aloe Vera Gel in the preparation process of magnificent liquid.It is from upper table 1, it can be seen that the total effective rate of comparative example 3, effective
Rate is below embodiment 2, while does not have the situation of any effect after having also appeared 1 people's use, illustrates the eye prepared by comparative example 3
, there is apparent reduction in the effect of portion's Essence compared to embodiment 2.This is because pearl powder passes through lactic acid and ethylenediamine tetra-acetic acid two
It can adsorb active ingredient in Essence after sodium processing well, after pearl powder adsorption of effective component, make in the collaboration of Aloe Vera Gel
It under, and can be stably dispersed in Essence, be dispersed in Essence with finally making stable effective ingredients well, enhance essence
The dispersion stabilization of liquid, prevents Essence from settling in use, influences the quality of Essence, reduces the work(of Essence
Effect.
Although the embodiments of the present invention have been disclosed as above, but its be not restricted in specification and embodiment it is listed
With it can be applied to various suitable the field of the invention completely.It for those skilled in the art, can be easily
Realize other modification, therefore without departing from the general concept defined in the claims and the equivalent scope, it is of the invention and unlimited
In specific details and example shown and described herein.
Claims (7)
1. cassia seed eye essence, which is characterized in that include the raw material of following mass percent：Glycine betaine 0.1%~
0.5%th, avenin 0.1%~0.5%, cassia seed extract 1%~5%, ginseng extract 0.5%~3%, mulberry leaf are hydrolyzed
Extract 1%~5%, camellia leaf extract 1%~5%, Salvia root P.E 1%~5%, Millettia extract 1%~5%,
Herba Dendrobii extract 0.5%~3%, rice spent wash 70%~80%, surplus are water.
2. cassia seed eye essence as described in claim 1, which is characterized in that include the raw material of following mass percent：
Glycine betaine 0.2%, hydrolysis avenin 0.3%, cassia seed extract 3%, ginseng extract 1%, mulberry-leaf extract 3%, mountain
Tea extract 2%, Salvia root P.E 2%, Millettia extract 2%, Herba Dendrobii extract 1%, rice spent wash 75%, water
10.5%.
3. the preparation method of cassia seed eye essence as described in claim 1, which is characterized in that include the following steps：
Step 1：Cassia seed extract, ginseng extract, mulberry-leaf extract, camellia leaf extract, pellet are weighed by mass percentage
Conopsea extraction, Millettia extract, Herba Dendrobii extract, mixing add in the rice spent wash of half quality, stir evenly, add
The additive amount of lotus leaf and wormwood mixed extract, lotus leaf and wormwood mixed extract is 0.6wt%, is stirred evenly, and it is mixed to obtain first
Close object；Wherein, the preparation method of lotus leaf and wormwood mixed extract includes：According to mass ratio 1:1 weighs lotus leaf and wormwood, in 80
At DEG C after drying for 24 hours, it is molten to add in the ethyl alcohol that quality is 10 times of weights of lotus leaf and wormwood gross mass, volume fraction is 95% for mixing
Liquid, under nitrogen protection, the infusion 3h under the conditions of 75 DEG C, 0.5MPa filter after cooling, obtain the first filtrate and the first filter residue, will
It crushes, is sieved after first filter residue and drying, obtain coarse powder, then coarse powder is subjected to ultramicro grinding, cross 300 mesh screens and obtain fine powder, it will
Fine powder and the ethanol solution in mass ratio 1 that volume fraction is 95%:After 8 mixing, freeze for 24 hours, take out, in room temperature at -20 DEG C
Lower defrosting, then 3h is heated to reflux at 65 DEG C, it is filtered after cooling, obtains the second filtrate and the second filter residue, after the second filter residue and drying
With the ethanol solution in mass ratio 1 that volume fraction is 95%:5 mixing, the ultrasonication for being 500MHz with frequency at 55 DEG C
1h filters, obtains third filtrate and third filter residue, and the first filtrate, the second filtrate, third filtrate are mixed, total filtrate is obtained, will always filter
It is 1.24 that liquid, which is concentrated into relative density, and it is 1 to add mass ratio:2 gelatin and chitosan compound, gelatin and chitosan mixing
The additive amount of object for quality after the concentration of total filtrate 6%, 2h is stood after stirring evenly, filters, obtains clarified solution, then 45 DEG C,
Under the conditions of 30MPa, with supercritical carbon dioxide extraction 100min, lotus leaf and wormwood mixed extract are obtained；
Step 2：It is 1 to weigh mass ratio:1 pearl powder and Aloe Vera Gel, first pre-processes pearl powder, then by Aloe Vera Gel liter
Then temperature adds in pretreated pearl powder while stirring to 55 DEG C, when temperature is down to 40 DEG C, add remaining half quality
Rice spent wash, stir evenly, obtain the second mixture, then the second mixture is added to the first mixture made from step 1
In, it stirs evenly, obtains third mixture；Wherein, the total addition level of pearl powder and Aloe Vera Gel be 0.8wt%, the pre- place of pearl powder
Reason process includes：In molar ratio 1:1 mixes pearl powder and lactic acid, and 1h is stirred to react at 65 DEG C, when temperature is down to 50 DEG C,
It adds in disodium ethylene diamine tetraacetate to continue to be stirred to react 1h, is cooled to room temperature, disodium ethylene diamine tetraacetate and pearl powder rub
You are than being 1:1；
Step 3：Glycine betaine, hydrolysis avenin and water are mixed, 60 DEG C is heated to, stirs evenly, treat that temperature is down to 40 DEG C
When, it is 2 to add mass ratio:2:1:1:The mixing of 1 glycerine, Sodium Hyaluronate, polyethylene glycol, vitamin C and vitamin E
Object stirs evenly, and is cooled to room temperature, and obtains the 4th mixture, and third mixture made from step 2 is added to the 4th mixture
In, it stirs evenly, then carry out homogenization to get eye essence；Wherein, glycerine, Sodium Hyaluronate, polyethylene glycol, dimension life
The additive amount of plain C and tocopherol admixture is 1wt%.
4. the preparation method of cassia seed eye essence as claimed in claim 3, which is characterized in that in step 1, by
After one filter residue crushes, net is sieved with 100 mesh sieve, obtains coarse powder.
5. the preparation method of cassia seed eye essence as claimed in claim 3, which is characterized in that total to filter in step 1
The method of liquid concentration is vacuum distillation.
6. the preparation method of cassia seed eye essence as claimed in claim 3, which is characterized in that in step 2, pearl
Powder is the Nano pearl powder that natural fresh water pearl is processed.
7. the preparation method of cassia seed eye essence as claimed in claim 3, which is characterized in that in step 3, poly- second
The average molecular weight of glycol is 200.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810150002.7A CN108186519B (en) | 2018-02-13 | 2018-02-13 | Cassia seed eye essence and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810150002.7A CN108186519B (en) | 2018-02-13 | 2018-02-13 | Cassia seed eye essence and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN108186519A true CN108186519A (en) | 2018-06-22 |
| CN108186519B CN108186519B (en) | 2021-01-05 |
Family
ID=62593493
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810150002.7A Active CN108186519B (en) | 2018-02-13 | 2018-02-13 | Cassia seed eye essence and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN108186519B (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN117547498A (en) * | 2024-01-11 | 2024-02-13 | 珠海远大美业生物科技有限公司 | Distilled grain skin beautifying liquid and preparation method and application thereof |
Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1364468A (en) * | 2001-01-19 | 2002-08-21 | 赵国林 | Wall breaking and extracting method for Chinese herbal medicine and formulation |
| JP2006022050A (en) * | 2004-07-08 | 2006-01-26 | Kanebo Cosmetics Inc | Cosmetic |
| CN104758207A (en) * | 2015-03-16 | 2015-07-08 | 湖州品创孵化器有限公司 | Eye essence liquid improving dark eye circles |
| CN105640868A (en) * | 2016-01-30 | 2016-06-08 | 海南京润珍珠生物技术股份有限公司 | Pearl amino acid stayup brightening and moistening mask and preparation method thereof |
| CN105853339A (en) * | 2016-06-17 | 2016-08-17 | 麻本莲 | Whitening anti-wrinkle mask |
| CN105687055B (en) * | 2016-03-23 | 2017-07-18 | 广东芭薇生物科技股份有限公司 | A kind of eye maintenance Essence and preparation method thereof |
| CN107157850A (en) * | 2017-06-22 | 2017-09-15 | 西林县大银子铁皮石斛种销农民专业合作社 | A kind of dendrobium candidum eye skin care item and preparation method thereof |
| CN107281088A (en) * | 2017-07-13 | 2017-10-24 | 成都新柯力化工科技有限公司 | A kind of Rice oil face cream and preparation method thereof |
-
2018
- 2018-02-13 CN CN201810150002.7A patent/CN108186519B/en active Active
Patent Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1364468A (en) * | 2001-01-19 | 2002-08-21 | 赵国林 | Wall breaking and extracting method for Chinese herbal medicine and formulation |
| JP2006022050A (en) * | 2004-07-08 | 2006-01-26 | Kanebo Cosmetics Inc | Cosmetic |
| CN104758207A (en) * | 2015-03-16 | 2015-07-08 | 湖州品创孵化器有限公司 | Eye essence liquid improving dark eye circles |
| CN105640868A (en) * | 2016-01-30 | 2016-06-08 | 海南京润珍珠生物技术股份有限公司 | Pearl amino acid stayup brightening and moistening mask and preparation method thereof |
| CN105687055B (en) * | 2016-03-23 | 2017-07-18 | 广东芭薇生物科技股份有限公司 | A kind of eye maintenance Essence and preparation method thereof |
| CN105853339A (en) * | 2016-06-17 | 2016-08-17 | 麻本莲 | Whitening anti-wrinkle mask |
| CN107157850A (en) * | 2017-06-22 | 2017-09-15 | 西林县大银子铁皮石斛种销农民专业合作社 | A kind of dendrobium candidum eye skin care item and preparation method thereof |
| CN107281088A (en) * | 2017-07-13 | 2017-10-24 | 成都新柯力化工科技有限公司 | A kind of Rice oil face cream and preparation method thereof |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN117547498A (en) * | 2024-01-11 | 2024-02-13 | 珠海远大美业生物科技有限公司 | Distilled grain skin beautifying liquid and preparation method and application thereof |
| CN117547498B (en) * | 2024-01-11 | 2024-04-26 | 贵州科益创生物科技有限公司 | Distilled grain skin beautifying liquid and preparation method and application thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN108186519B (en) | 2021-01-05 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN104490678B (en) | A kind of rosemary hydrosol toner and preparation method thereof | |
| CN108991301A (en) | A kind of compound drink and preparation method thereof with beauty sleep-aid function | |
| CN106539048B (en) | Edible selenium-rich areca-nut brine and method for preparing areca-nuts by using edible selenium-rich areca-nut brine | |
| CN104013564A (en) | Oil-tea camellia honey moisturizer | |
| KR20120133799A (en) | Functional soap and manufacturing method of it | |
| CN101259095A (en) | Skin care products for neck and preparation technique thereof | |
| CN101869542B (en) | Toner comprising pawpaw extract and lotus leaf extract and preparation method thereof | |
| CN107349167A (en) | Cosmetic composition and its preparation method and application | |
| CN102058513B (en) | Chinese herbal medicine crude solution and cosmetic containing same | |
| CN108186519A (en) | cassia seed eye essence and preparation method thereof | |
| KR101606381B1 (en) | Manufacture method of complex beauty Salt using solar salt processing environmentally friendly | |
| CN112370378A (en) | Cosmetic containing guayule troponin stock solution and preparation method thereof | |
| CN104138002A (en) | Health food with weight reducing function and preparing method of health food | |
| CN105640836B (en) | A kind of surfactant and preparation method thereof containing lotus active constituent | |
| CN108450962A (en) | A kind of solid beverage and preparation method thereof for Woman health | |
| CN107308068A (en) | A kind of face cream of the extract containing Spirullina | |
| CN112156048A (en) | Natural whitening face cleaning powder and preparation method thereof | |
| CN106821932A (en) | A kind of cosmetics containing west safflower extract solution | |
| CN107279865A (en) | A kind of maca oyster dietary product and preparation method thereof | |
| CN101991037B (en) | Angelica-aronia melanocarpa pill and manufacturing method thereof | |
| KR101057017B1 (en) | Anti-hair loss soap containing natural extract | |
| CN105010657A (en) | Health care tea capable of maintaining beauty for females | |
| CN109700690A (en) | A kind of Poria cocos moisturizing emulsion and preparation method thereof | |
| CN107802556A (en) | A kind of moisture-keeping composition and contain said composition cosmetics | |
| CN108783006A (en) | A kind of broiler chicken feed additive and the preparation method and application thereof, broiler fodder |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |