KR101057017B1 - Anti-hair loss soap containing natural extract - Google Patents

Anti-hair loss soap containing natural extract Download PDF

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KR101057017B1
KR101057017B1 KR1020090040860A KR20090040860A KR101057017B1 KR 101057017 B1 KR101057017 B1 KR 101057017B1 KR 1020090040860 A KR1020090040860 A KR 1020090040860A KR 20090040860 A KR20090040860 A KR 20090040860A KR 101057017 B1 KR101057017 B1 KR 101057017B1
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우병하
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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00Compositions of detergents based essentially on soap
    • C11D9/04Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/22Organic compounds, e.g. vitamins
    • C11D9/38Products in which the composition is not well defined
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/10Washing or bathing preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/02Preparations for cleaning the hair
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q7/00Preparations for affecting hair growth
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D13/00Making of soap or soap solutions in general; Apparatus therefor
    • C11D13/10Mixing; Kneading
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D13/00Making of soap or soap solutions in general; Apparatus therefor
    • C11D13/14Shaping
    • C11D13/18Shaping by extrusion or pressing
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/70Biological properties of the composition as a whole

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Abstract

본 발명은 탈모방지 및 발모 성능을 가지고, 비듬방지 및 가려움증 개선 효과를 가진 비누 및 그 제조방법에 관한 것으로서, 구체적으로는 아연피리치온액, 덱스판테놀, 니코틴산아미드 및 비오틴으로 이루어진 제1 성분과 알로에추출물, 천궁추출물 및 당귀추출물로 이루어진 제2 성분을 함유하는 비누에 관한 것이다.The present invention relates to a soap having a hair loss prevention and hair growth performance, and to a dandruff prevention and itching improvement effect, specifically, a first component consisting of zinc pyrithione solution, dexpanthenol, nicotinic acid amide and biotin and aloe The present invention relates to a soap containing a second component consisting of an extract, a celestial extract and a Angelica extract.

비누, 탈모방지, 발모, 아연피리치온액, 알로에, 천궁 Soap, hair loss prevention, hair growth, zinc pyrithione solution, aloe, crossbow

Description

천연 추출물을 함유하는 탈모방지비누{Soap Comprising Herb Medicine Extracts for Preventing Loss of Hair}Soap Comprising Herb Medicine Extracts for Preventing Loss of Hair

본 발명은 탈모방지 및 발모 효능을 가진 비누 및 그 제조방법에 관한 것으로서, 구체적으로는 아연피리치온액, 덱스판테놀, 니코틴산아미드 및 비오틴으로 이루어진 제1 성분과 알로에추출물, 천궁추출물 및 당귀추출물로 이루어진 제2 성분을 함유하는 비누에 관한 것이다.The present invention relates to a soap having a hair loss prevention and hair regrowth effect, and a method for preparing the same, and specifically, comprising a first component consisting of zinc pyrithione solution, dexpanthenol, nicotinic acid amide and biotin, and aloe extract, celestial extract and Angelica extract. It relates to a soap containing the second component.

일반적으로 사람의 두발이 탈모되는 원인은 유전적인 요인, 노화의 진행, 약물 복용, 방사선 치료 및 중병 후 스트레스 등을 들 수 있다. 생화학적 및 생리학적 관전에서 탈모 현상은 과다 활동 두피 혈액순환의 문제 및 모발대사에 필수적인 영양소의 결핍 등의 원인에 의한 것이라고 일반적으로 알려져 있다. 상기 요인들은 단독으로 탈모를 유발할 수 있지만, 탈모요인들이 복합되어 탈모를 유발할 수도 있다.In general, the causes of human hair loss are genetic factors, aging progression, drug use, radiation therapy and post-stress stress. Hair loss in biochemical and physiological observations is generally known to be due to problems with hyperactive scalp blood circulation and lack of nutrients essential for hair metabolism. Although these factors alone can cause hair loss, hair loss factors may be combined to cause hair loss.

한편 생약성분의 추출물을 이용하여 두피에 바르거나 복용함으로써 발모를 촉진시키는 기술은 공개되어 있다. 한국등록특허 제157667호에서는 난초과 식물을 추출물을 이용하고 있고, 한국등록특허 제161338호에서는 웅지와 만형자를 이용하고 있고, 한국공개특허 제1996-40346호에서는 소나무추출물을 이용한 발모촉진제를 제안하고 있다.Meanwhile, techniques for promoting hair growth by applying or taking the scalp using extracts of herbal ingredients are disclosed. Korean Patent No. 157667 uses an extract of orchidaceae plants, Korean Patent No. 161338 uses a wormwood and mandrel, and Korean Patent Publication No. 1996-40346 proposes a hair growth promoter using pine extract. have.

하지만 시중이 많이 유통되고 있는 탈모치료 및 발모제들은 효과가 미미하거나 탈모 방지 및 발모 효과가 없는 것이 대부분으로서 아직까지 효과적인 제품의 개발이 확인되지 않고 있다. 또한 종래에는 탈모치료용으로 주로 샴푸제제가 제안되고 있으나, 샴푸제제에 포함된 다른 화학성분으로 인하여 오히려 탈모방지 및 발모 효능이 저해되는 결과를 가져오는 것으로 보고되고 있다. However, commercially available hair loss treatments and hair regrowth agents are insignificant or have no hair loss prevention and regrowth effect, and thus, the development of effective products has not been confirmed. In addition, the shampoo formulation is mainly proposed for the treatment of hair loss in the past, but has been reported to result in the prevention of hair loss and hair retardation rather than due to other chemical components contained in the shampoo formulation.

본 발명자는 상기한 문제점들을 해결하기 위하여 탈모방지에 효과가 있는 유효성분과 천연 추출물을 일정한 비율로 혼합하여 탈모방지 및 발모에 효과가 있는 비누를 제조함으로써 본 발명을 완성하였다.The present inventors have completed the present invention by preparing a soap that is effective in preventing hair loss and hair growth by mixing an active ingredient and a natural extract in an effective ratio to prevent hair loss in order to solve the above problems.

본 발명은 효과적으로 탈모를 방지하고 발모를 촉진하고 안정성이 뛰어난 4가지 유효성분과 천연추출물을 함유하는 비누를 제공하는 것을 목적으로 한다.An object of the present invention is to provide a soap containing four effective ingredients and natural extracts that effectively prevent hair loss, promote hair growth, and have excellent stability.

상기한 과제를 해결하기 위하여, 본 발명의 적절한 실시 형태에 따르면, 아연피리치온액, 덱스판테놀, 니코틴산아미드 및 비오틴으로 이루어진 제1 성분 및 알로에추출물, 천궁추출물 및 당귀추출물로 이루어진 제2 성분을 함유하고, 상기 제1 성분과 제2 성분은 중량비로서 1:1 내지 1:3 인 것을 특징으로 하는 천연추출물 함유 비누를 제공한다.In order to solve the above problems, according to a preferred embodiment of the present invention, it contains a first component consisting of zinc pyrithione solution, dexpanthenol, nicotinic acid amide and biotin, and a second component consisting of aloe extract, astronomical extract and sugar extract And, the first component and the second component provides a natural extract-containing soap, characterized in that 1: 1 to 1: 3 by weight ratio.

본 발명의 다른 적절한 실시 형태에 따르면, 상기 제1 성분은 비누총중량 대비 아연피리치온액 1 내지 3중량%, 덱스판테놀 0.25 내지 1중량%, 니코틴산 아미드 0.1 내지 0.6중량%, 비오틴 0.01 내지 0.1중량%를 함유하는 것을 특징으로 하는 천연추출물 함유 비누를 제공한다.According to another suitable embodiment of the present invention, the first component is 1 to 3% by weight of zinc pyrithione solution, 0.25 to 1% by weight of dexpanthenol, 0.1 to 0.6% by weight of nicotinic acid amide, 0.01 to 0.1% by weight of biotin It provides a natural extract containing soap, characterized in that it contains.

본 발명의 또 다른 적절한 실시 형태에 따르면, 상기 제2 성분은 비누총중량 대비 알로에추출물 2 내지 4중량%, 천궁추출물 0.5 내지 2중량% 및 당귀추출물 0.5 내지 2중량%를 함유하는 것을 특징으로 하는 천연추출물 함유 비누를 제공한다.According to another suitable embodiment of the present invention, the second component contains 2 to 4% by weight of aloe extract, 0.5 to 2% by weight of the hormonal extract and 0.5 to 2% by weight of the Angelica extract, relative to the total weight of the soap. Provide extract-containing soap.

본 발명의 또 다른 적절한 실시 형태에 따르면, 상기 비누는 탈모방지 및 발모 성능을 가지는 것을 특징으로 하는 천연추출물 함유 비누를 제공한다.According to another suitable embodiment of the present invention, the soap provides a natural extract-containing soap, characterized in that it has a hair loss prevention and hair growth performance.

본 발명의 비누는 탈모를 방지하는 4가지의 유효성분과 발모를 촉진하는 3가지 천연물 추출성분을 일정비율로 함유하고 있기 때문에, 안정성이 뛰어나고 탈모방지 및 발모 효과를 가지고 있으며 비듬방지 및 가려움증개선 효과를 가지고 있다.Since the soap of the present invention contains four active ingredients to prevent hair loss and three natural product extract ingredients to promote hair growth at a certain ratio, it has excellent stability, hair loss prevention and hair growth effects, and has anti-dandruff and itching improvement effects. Have.

본 발명은 아연피리치온액, 덱스판테놀, 니코틴산아미드 및 비오틴으로 이루어진 제1 성분과 알로에추출물, 천궁추출물 및 당귀추출물로 이루어진 제2 성분을 일정한 비율로 혼합한 후 비누용기재에 첨가하여 비누를 제조함으로써, 탈모방지 및 발모 효과가 뛰어나고 안정성이 우수한 비누를 제조하였다The present invention is to prepare a soap by mixing a first component consisting of zinc pyrithione solution, dexpanthenol, nicotinic acid amide and biotin and a second component consisting of aloe extract, cheonung extract and sugar extract in a certain ratio and then added to a soap base By doing so, a soap having excellent hair loss prevention and hair regrowth effect and excellent stability was prepared.

본 발명에서 제1 성분은 아연피리치온액, 덱스판테놀, 니코틴산아미드 및 비오틴을 포함한다. In the present invention, the first component includes zinc pyrithione solution, dexpanthenol, nicotinic acid amide and biotin.

상기 제1 성분 중 아연피리치온액은 아연피리치온이 50중량%가 함유되어 있는 현탁액을 사용하는 것이 바람직하고, 전체비누중량 대비 1 내지 3중량%를 함유하는 것이 바람직하다. The zinc pyrithione liquid in the first component is preferably a suspension containing 50% by weight of zinc pyrithione, and preferably contains 1 to 3% by weight based on the total weight of the soap.

덱스판테놀은 전체비누중량대비 0.25 내지 1중량%, 니코틴산아미드는 0.1 내지 0.6중량%, 비오틴은 전체비누중량대비 0.01 내지 0.1 중량%를 함유하는 것이 바람직하다.Dexpanthenol is preferably 0.25 to 1% by weight based on the total weight of the soap, nicotinic acid amide is 0.1 to 0.6% by weight, biotin is preferably contained 0.01 to 0.1% by weight relative to the total soap.

제1 성분은 비누총중량에 대하여 총 함량이 3 내지 5중량%인 것이 바람직하다. 제1 성분이 3중량% 미만으로 함유되어 있는 경우 탈모방지효과가 낮아지고, 5중량% 이상 함유되어 있는 경우 유효성분의 두피 흡수율이 저해될 수 있다.The first component preferably has a total content of 3 to 5% by weight relative to the total weight of the soap. When the first component is contained in less than 3% by weight, the effect of preventing hair loss is lowered, and when contained in more than 5% by weight may inhibit the scalp absorption rate of the active ingredient.

본 발명의 비누는 제2 성분으로서 알로에추출물, 천궁추출물 및 당귀추출물로 이루어진 천연추출물을 함유하는데, 제 2성분은 전체비누중량대비 3 내지 8중량%인 것이 최적의 탈모 방지 및 발모효과를 나타낼 수 있다.Soap of the present invention contains a natural extract consisting of aloe extract, cheongung extract and Angelica extract as a second component, the second component is 3 to 8% by weight relative to the total weight of the soap can exhibit an optimal hair loss prevention and hair growth effect have.

알로에는 백합과의 늘푸른 여러해살이풀로서 상처치유 및 혈관행성촉진, 세포의 재생 및 증식유도, 피부와 신체의 노화방지에 효과가 있으며 두피에 사용하는 경우 두피의 혈행을 원활하게 하고 모근조직을 활성화하여 건강하게 하여 탈모예방에 도움이 되며 비듬이나 두피염증과 같은 피부질환에 특히 효과가 있는 것으로 알려져 있다.Aloe is an evergreen perennial herb that is effective in healing wounds and promoting blood vessels, inducing the regeneration and proliferation of cells, and preventing aging of skin and body. When used for scalp, it stimulates the blood circulation of the scalp and activates hair root tissue. It helps to prevent hair loss by being healthy, and is known to be particularly effective in skin diseases such as dandruff and scalp inflammation.

천궁은 산형화과에 속하는 숙근성 초본으로 불규칙한 혹을 가진 근경을 약용으로 사용하는 경제성이 높은 약용 작물로써 기를 소통시키고 울체를 풀어주며 풍습을 제거하고 혈액순환을 촉진시킬뿐 아니라 진통작용이 있으며 자양강장작용이 있어 원기를 회복시키는 것으로 알려져 있어 두피에 사용하는 경우 두피의 혈액순환을 촉진시키는 효능이 있다. 특히 천궁 내의 페루릭산과 각종 알카로이드 성분이 피부영양공급에 중요한 영양소로 알려져 있다.Cheonggung is an medicinal herb that belongs to the cultivation family. It is an economical medicinal crop that uses roots with irregular lumps as a medicinal herb. It communicates, releases ulcers, removes customs, promotes blood circulation, and has analgesic effects. It has been known to restore energy, so when used on the scalp has the effect of promoting blood circulation of the scalp. In particular, peric acid and various alkaloids in the uterus are known as important nutrients for skin nutrition.

당귀는 미나리과에 속하는 두해 또는 여러해살이풀로서 특이한 냄새가 난다. 당귀는 뿌리를 약재로 사용하는데, 혈액순환을 원활히 하여 몸을 따뜻하게 해주며 피부에 탄력을 주어 맑고 깨끗하게 유지시켜 줄 뿐만 아니라 피부조직 및 모근을 건강하게 하는 기능이 있는 것으로 알려져 있다.Angelica is a perennial or perennial herb belonging to the Apiaceae, with a characteristic odor. Angelica is known to have roots as a medicinal herb, which is known to have a function of smoothing blood circulation and warming the body, giving elasticity to the skin to keep it clear and clean, as well as healthy skin tissue and hair roots.

상기 천연추출물은 통상적인 방법을 천연물로부터 추출할 수 있는데, 구체적으로는 천궁 및 당귀는 물과 혼합한 후 가열 및 추출하고 이를 여과 및 건조하여 추출물을 얻을 수 있다. 알로에는 알콜과 물의 혼합용매를 이용하여 추출하는 것이 바람직하다. 구체적으로는 알로에는 세절하여 건조하고, 알콜 또는 알콜과 물의 혼합용매로 추출하고 여과 및 건조시켜 얻을 수 있으며, 이때 알콜 또는 알콜과 물의 혼합용매는 5~100%의 에틸알콜이 바람직하다.The natural extract can be extracted from the natural method of the conventional method, specifically, the cheongung and Angelica can be mixed with water and then heated and extracted, filtered and dried to obtain the extract. Aloe is preferably extracted using a mixed solvent of alcohol and water. Specifically, the aloe is finely dried and can be obtained by extracting with alcohol or a mixed solvent of alcohol and water, filtering and drying, wherein the mixed solvent of alcohol or alcohol and water is preferably 5 to 100% ethyl alcohol.

제2 성분은 비누총중량대비 3 내지 8중량%인 것이 바람직한데, 구체적으로는 알로에추출물이 전체 비누중량 대비 2 내지 4중량%, 천궁추출물이 0.5 내지 2중량%, 당귀추출물이 0.5 내지 2중량%인 것이 바람직하다. 제2 성분인 천연물 추출물은 비누 제조시 미세한 분말로 사용하기 때문에 습윤제로서도 작용한다. The second component is preferably 3 to 8% by weight relative to the total weight of the soap, specifically 2 to 4% by weight of the total weight of the soap, 0.5 to 2% by weight of the archery extract, 0.5 to 2% by weight of the Angelica extract Is preferably. Natural product extract, which is the second component, acts as a humectant because it is used as a fine powder in soap production.

다음으로 제1 성분과 제 2성분을 공지의 비누용 기제와 함께 혼합한 후 바(bar)형태로 압출하여 제조한다. 제1 성분과 제2 성분은 입자크기가 100~500㎛정도로 분쇄하는 것이 바람직한데, 유효성분들의 입자크기가 미세하기 때문에 본 발명의 비누를 이용하여 모발을 세정하는 경우 탈모방지에 효과가 있는 제1 성분 및 제2 성분이 효과적으로 두피로 침투할 수 있게 된다.Next, the first component and the second component are mixed with a known base for soap and then extruded into a bar to prepare. It is preferable that the first component and the second component are pulverized to a particle size of about 100 ~ 500㎛, because the particle size of the active ingredient is fine, which is effective for preventing hair loss when washing hair using the soap of the present invention. The first component and the second component can effectively penetrate the scalp.

비누제조과정에서 상기 제1 성분 및 제2 성분 이외에 착색제로서 산화티탄을 더 포함할 수 있으며, 착향제로서 라벤더오일, 페파민트오일, 티트리오일 등을 첨가하여 비누에서 천연추출물 냄새와 함께 라벤더나 페파민트 또는 티트리 향이 나도록 제조할 수 있다. In the soap manufacturing process, it may further include titanium oxide as a coloring agent in addition to the first component and the second component, and lavender or peppermint with the smell of natural extract from soap by adding lavender oil, peppermint oil, tea tree oil, etc. as a flavoring agent. Or it can be prepared to smell the tea tree.

본 발명의 비누는 상기 제1 성분과 제2 성분이 중량비로서 1:1 내지 1: 3 인 것이 바람직하고, 더욱 바람직하게는 1:1.69이다. 제1 성분과 제2 성분이 상기 비율로 혼합된 경우에 본 발명의 효과인 탈모방지효과가 뛰어나고, 발모효과도 기대 할 수 있으며, 유효성분이 두피에 효과적으로 침투할 수 있다.In the soap of the present invention, the first component and the second component are preferably 1: 1 to 1: 3 by weight, more preferably 1: 1.69. When the first component and the second component are mixed in the above ratio, it is excellent in hair loss prevention effect of the present invention, hair growth effect can be expected, and the active ingredient can effectively penetrate the scalp.

도 1은 본 발명의 비누의 제조공정을 나타낸 것이다.Figure 1 shows the manufacturing process of the soap of the present invention.

먼저 천연추출물을 제조한다(S11). 구체적으로는 알로에, 천궁 및 당귀로부터 알로에 추출물, 천궁 추출물 및 당귀 추출물을 제조한다. 알로에는 세절한 후 건조하고 이를 알콜 또는 알콜과 물의 혼합용매로 추출한다. 알콜 또는 알콜과 물의 혼합용매는 5~100%의 에틸알콜이 바람직하다. 천궁은 천궁 양의 2배 정도 되는 물과 혼합한 후 3 내지 5시간 동안 가열하여 천궁의 유효성분이 추출되게 한다. 가열된 혼합액을 여과수단이 구비된 압착기에 투입하여 압착 추출한 후 건조하여 분말형태의 천궁추출물을 제조한다. 당귀도 천궁과 동일한 방법으로 분말형태의 당귀 추출물을 제조한다.First, natural extracts are prepared (S11). Specifically, aloe extract, celestial extract and Angelica extract are prepared from aloe, celestial organ and Angelica. Aloe is chopped, dried and extracted with alcohol or a mixed solvent of alcohol and water. The alcohol or the mixed solvent of alcohol and water is preferably 5 to 100% ethyl alcohol. The uterus is mixed with water twice the amount of the uterus and heated for 3 to 5 hours to allow the active ingredient of the uterus to be extracted. The heated mixed solution is put into a compactor equipped with filtration means, compressed and extracted, and then dried to prepare a powdery cheonyeong extract. Angelica also produces powdered Angelica extract in the same manner as Cheongung.

다음으로 상기 알로에, 천궁 및 당귀로부터 추출한 천연 추출물로 이루어진 제2 성분과 상기 제1 성분을 혼합한 후 분쇄한다(S12). 상기 천연 추출물과 아연피리치온액, 덱스판테놀, 니코틴산아미드 및 비오틴으로 이루어진 제1 성분을 비드밀을 이용하여 입자크기가 100~500㎛가 되도록 분쇄한다. Next, a second component consisting of a natural extract extracted from the aloe, cheonggung and tangwi and the first component is mixed and ground (S12). The first component consisting of the natural extract and zinc pyrithione solution, dexpanthenol, nicotinic acid amide and biotin is ground to a particle size of 100 ~ 500㎛ using a bead mill.

다음으로 상기 분쇄물을 비누용기제에 첨가한 후 산화티탄과 착향제를 첨가하고 균일하게 혼합하여 비누화 공정을 진행한다(S13). 마지막으로 압출기에 비누화공정이 완료된 혼합물을 투입하고 압출하여 본 발명의 바 형태 비누를 제조한다(S14).Next, after the pulverized product is added to the soap container, the titanium oxide and the flavoring agent are added and uniformly mixed to proceed the saponification process (S13). Finally, the mixture is added to the extruded saponification process and extruded to prepare a bar soap of the present invention (S14).

상기와 같이 제조된 비누의 사용방법은 아래와 같다.How to use the soap prepared as described above is as follows.

하루에 1회 정도 비누로 머리를 샴푸하거나 비누거품이 발생된 채로 5 내지 10분 정도 방치하여 제1 성분의 유효성분과 제2 성분인 천연물의 약리성분이 두피에 흡수되게 할 수 있다. 이때 제1 성분의 유효성분과 제2 성분의 약리 성분이 두피조직에 흡수되면 두피의 혈액순환이 원활하게 되어 두피조직과 모근 및 모공의 세포활성이 왕성하게 될 뿐만 아니라 모근을 건강하게 하고 모발의 생장을 촉진하고 탈모를 방지하게 된다. 또한 일반적으로 시판되는 샴푸와 달리 비누 형태로 제조되었기 때문에 샴푸에 포함된 다량의 계면활성제에 의한 부작용도 방지할 수 있다.Shampoo the hair with soap once a day or leave the soap bubbles for about 5 to 10 minutes to allow the active ingredient of the first component and the pharmacological component of the natural product of the second component to be absorbed into the scalp. At this time, when the active ingredient of the first ingredient and the pharmacological ingredient of the second ingredient are absorbed into the scalp tissue, blood circulation of the scalp is smoothed, and the cellular activities of the scalp tissue, the hair root and the pores are not only active, but also the hair roots are healthy and the hair growth is performed. Promotes and prevents hair loss. In addition, since it is manufactured in the form of soap unlike commercially available shampoos, it is possible to prevent side effects caused by the large amount of surfactants included in the shampoo.

상기 샴푸 과정에서 비누거품발생과 함께 머리의 두피를 가볍게 지압해 주면 유효성분이 두피 속으로 더 잘 흡수되게 한다. 비누의 사용은 하루에 1회 사용으로 한정되는 것은 아니며, 하루에 2회를 사용하거나 이틀에 1회를 사용하는 경우에도 효과를 기대할 수 있다.When the pressure of the scalp of the head lightly with soap bubbles in the shampoo process, the active ingredient is better absorbed into the scalp. The use of soap is not limited to one use per day, and the effect can be expected even when used twice a day or once every two days.

이하에서 실시예를 들어서 본 발명을 상세하게 설명하지만, 제시된 실시예는 예시적인 것으로 이 분야에서 통상의 지식을 가진 자는 본 발명의 기술적 사상을 벗어나지 아니하고 제시된 실시예에 대한 다양한 변형 또는 수정 발명을 할 수 있다. 본 발명은 이와 같은 변형 또는 수정발명에 의하여 제한되지 아니하고 다만 아래에 첨부된 청구범위에 의해서만 제한된다.Hereinafter, the present invention will be described in detail with reference to the following examples, but the embodiments presented are exemplary, and a person of ordinary skill in the art may make various modifications or modifications to the present embodiments without departing from the technical spirit of the present invention. Can be. The invention is not limited by these modifications or variations, but only by the claims appended hereto.

실시예 1Example 1

아연피리치온액 2.10g(아연피리치온 1.05g), 덱스판테놀 0.50g, 니코틴산아미드 0.30g, 비오틴 0.06g을 비누용 기재 90.94g와 혼합한 후, 알로에추출물 3.0g, 천궁추출물 1.0g, 당귀추출물 1.0g을 첨가하였다. 착색제로서 산화티탄과 라벤다향 HF-6900을 전체중량 100g이 되도록 첨가하여 혼합물을 제조한다. 상기 혼합물을 비드밀을 이용하여 입자크기가 100㎛ 내지 500㎛가 될 때까지 분쇄한 후 균일하게 혼합한 후 바(bar) 형태로 압출하여 제조하였다. 2.10 g of zinc pyrithione solution (1.05 g of zinc pyrithione), 0.50 g of dexpanthenol, 0.30 g of nicotinic acid amide, and 0.06 g of biotin were mixed with 90.94 g of a base material for soap, followed by 3.0 g of aloe extract, 1.0 g of celery extract, and Angelica gigas. 1.0 g of extract was added. As a colorant, a mixture was prepared by adding titanium oxide and lavender-flavored HF-6900 to a total weight of 100 g. The mixture was pulverized until the particle size was 100 μm to 500 μm using a bead mill, and then uniformly mixed and extruded to form a bar.

상기의 방법으로 제조된 본 발명의 비누를 탈모현상이 있는 성인남성 20명에게 매일 1회 사용하게 하였다. 샴푸방법은 비누를 이용하여 충분히 거품을 발생시켜서 모발 및 두피에 마사지 하면서 도포한 다음 5분 정도 경과한 후 거품을 깨끗하게 세정하였다. 비누 사용 후 10일 경과후부터 20명 중 10명이 탈모증상이 경감하였고, 15일 내지 20일 경과한 시점에서 20명 중 18명은 탈모증상이 줄어들기 시작하였고, 1개월 경과 시점에서는 80~90%까지 탈모 현상이 경감하는 현상이 관찰되었다. 또한 1개월 경과 후부터는 솜털과 같은 초기발모현상이 관찰되기 시작하였고, 2개월이 경과하면서 발모된 머리카락이 점점 굵어지는 것이 관찰되었다.Soap of the present invention prepared by the above method was used once daily to 20 adult men with hair loss. In the shampoo method, the foam was sufficiently generated by using soap and then applied to the hair and the scalp while being massaged, and after 5 minutes, the foam was washed cleanly. After 10 days of use, 10 out of 20 alleviated alopecia, and after 15 to 20 days, 18 out of 20 began to reduce alopecia, up to 80-90% after one month. The phenomenon of alleviating the hair loss phenomenon was observed. In addition, after one month, the initial hair growth phenomenon such as down was started to be observed, and the hair was gradually thickened after two months.

본 발명에 의해 제조된 비누에 대한 안정성 시험 결과를 아래 표 1에 나타내었다. 안정성 시험은 장기보전시험 조건(온도 25± 2℃/상대습도 60± 5%)에서 24개월간 안정성 시험을 하였는데, 함량시험 및 질량(용량) 편차시험을 통하여 유효 성분인 아연피리치온, 덱스판테놀, 니코틴산아미드 및 비오틴의 안정성을 확인하였다. The stability test results for the soaps prepared by the present invention are shown in Table 1 below. The stability test was performed for 24 months under long-term preservation test conditions (temperature 25 ± 2 ℃ / relative humidity 60 ± 5%), and the content of zinc pyrithione and dexpanthenol were tested through the content test and mass (dose) deviation test. , The stability of nicotinic acid amide and biotin was confirmed.

함량시험은 아연피리치온의 경우 본 발명의 비누 약 800mg 및 표준품 약 9mg을 가지고 식약성고시 “대한약전외의약품등기준” 아연피리치오현탁액 정량법에 따라 시험하였다. 덱스판테놀은 본 발명의 비누 약 1.0g 및 표준품 약 5mg을 가지고 이하 식약청고시“대한약전외의약품등기준” 덱스판테놀·디메칠설폭시드·헤파린나트륨겔 정량법에 따라 시험하였다. 니코틴산아미드는 본 발명의 비누 약 100mg 및 표준품 약 30mg을 희석액에 넣어 녹여 정확하게 50ml로 한 액 5ml를 가지고 이하 식약청고시 “대한약전외의약품등기준” 일반시험법 비타민시험법 니코틴산아미드 정량법에 따라 시험하였다. 비오틴은 본 발명의 비누 약 800mg 및 표준품 약 25mg을 물에 넣고 정확하게 100ml로 한 약 2ml를 가지고 물로 전처리하여 이하 식약청고시 “대한약전외의약품등기준” 일반시험법 비타민시험법 비오틴 정량법에 따라 시험하였다.In the content test of zinc pyrithione, about 800 mg of soap of the present invention and about 9 mg of standard product were tested according to the quantitative analysis method of zinc pyridio suspension of the Korean Food Standard. Dexpanthenol was tested according to the following method of determination of dexantenol, dimethyl sulfoxide, heparin sodium gel with the following about 1.0 g of the soap of the present invention and about 5 mg of standard product. Niacinamide was dissolved by diluting about 100mg of the soap of the present invention and about 30mg of the standard product in a diluted solution to make exactly 50ml. The following test was conducted according to the General Test Method Vitamin Test Method Nicotinic Acid Amide Assay Method when notified by the Korea Food and Drug Administration. . Biotin was prepared according to the general test method vitamin test method biotin quantitative method of the following "Prescribed by Korean Pharmaceutical Standards" when notified by KFDA after about 800mg of the soap of the present invention and about 25mg of a standard product in water and precisely 2ml of 100ml. .

질량편차시험은 본 발명의 비누를 가지고 식약청 고지 “의약품등의 질량(용량)편차기준및시험방법”에 따라 시험한다.The mass deviation test is carried out according to the KFDA notification of "mass (dose) standard and test method of drugs, etc." with the soap of the present invention.

안정성 시험결과를 아래 표 1이 나타냈다.Table 1 below shows the stability test results.

시험항목Test Items 시험기준Test standard 시험결과Test result 최초first 3개월3 months 6개월6 months 9개월9 months 12개월12 months 18개월18 months 24개월24 months 함량시험(%)Content test (%) 아연피리치온Zinc pyrithione 90.0% 이상90.0% or more 101.4101.4 101.7101.7 101.5101.5 100.0100.0 99.799.7 98.098.0 97.397.3 덱스판테놀Dexpanthenol 90.0% 이상90.0% or more 115.0115.0 115.6115.6 113.3113.3 114.3114.3 112.8112.8 112.6112.6 110.1110.1 니코틴산아미드Nicotinic acid amide 90.0% 이상90.0% or more 113.8113.8 114.0114.0 112.8112.8 110.5110.5 109.7109.7 110.5110.5 109.6109.6 비오틴Biotin 90.0% 이상90.0% or more 118.4118.4 116.4116.4 114.4114.4 113.8113.8 113.6113.6 113.7113.7 113.4113.4 질량(용량)
편차시험
Mass (capacity)
Deviation test
1)비누10개내용물의 평균질량은 표시량 이상
2)개개의 내용물의 질량은 표시량의 95% 이상
1) The average mass of the contents of 10 soaps
2) The mass of each content is more than 95% of the indicated quantity
적합fitness -- -- -- -- -- --

표 1에 나타난 바와 같이 본 발명의 비누는 장기보전시험 조건(온도 25± 2℃/상대습도 60± 5%)에서 24개월간 안정성 시험을 실시한 결과, 성상, 확인시험, 함량시험, 질량(용량)편차시험 등의 시험항목에서 유의적인 변화가 발견되지 않았으며, 24개월간 안정하였다.As shown in Table 1, the soap of the present invention was subjected to a stability test for 24 months under long-term preservation test conditions (temperature 25 ± 2 ° C./relative humidity 60 ± 5%). No significant change was found in the test items such as the deviation test, and it was stable for 24 months.

도 1은 본 발명에 따른 비누의 제조공정이다.1 is a manufacturing process of the soap according to the present invention.

Claims (4)

비누총중량 대비 아연피리치온액 1 내지 3중량%, 덱스판테놀 0.25 내지 1중량%, 니코틴산아미드 0.1 내지 0.6중량% 및 비오틴 0.01 내지 0.1 중량%를 비누용 기제와 혼합한 후, 알로에추출물 2 내지 4중량%, 천궁추출물 0.5 내지 2중량%, 당귀추출물 0.5 내지 2중량% 및 착색제 1 내지 2중량%를 첨가하여 비누조성물을 제조하고, 1 to 3% by weight of zinc pyrithione solution, 0.25 to 1% by weight of dexpanthenol, 0.1 to 0.6% by weight of nicotinic acid amide and 0.01 to 0.1% by weight of biotin are mixed with the base for soap, and then 2 to 4% by weight of soap. %, 0.5 to 2% by weight of cheongung extract, 0.5 to 2% by weight of Angelica extract and 1 to 2% by weight of a colorant to prepare a soap composition, 상기 비누조성물은 입자크기가 100~500㎛가 되도록 분쇄한 후 비누 형태로 제조하는 것을 특징으로 하는 천연 추출물 함유 비누.The soap composition is a natural extract-containing soap, characterized in that in the form of a soap after milling the particle size to 100 ~ 500㎛. 삭제delete 삭제delete 제 1항에 있어서, 상기 비누는 탈모방지 및 발모 성능을 가지는 것을 특징으로 하는 천연추출물 함유 비누.The soap according to claim 1, wherein the soap has hair loss prevention and hair growth performance.
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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR102033372B1 (en) 2018-12-20 2019-11-29 김광남 Functional soap composition with seaweed ear extract and process for preparing the same
KR20210088068A (en) 2020-01-06 2021-07-14 차순례 the depilation prevention functionality soap and the manufacturing method thereof in which the natural oil component is contained

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* Cited by examiner, † Cited by third party
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KR100818175B1 (en) 2007-12-12 2008-04-02 주식회사 태웅이엘에스 Hair treatment compositions

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR100818175B1 (en) 2007-12-12 2008-04-02 주식회사 태웅이엘에스 Hair treatment compositions

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR102033372B1 (en) 2018-12-20 2019-11-29 김광남 Functional soap composition with seaweed ear extract and process for preparing the same
KR20210088068A (en) 2020-01-06 2021-07-14 차순례 the depilation prevention functionality soap and the manufacturing method thereof in which the natural oil component is contained

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