CN108042388B - Moisturizing and skin-tendering mask and preparation method thereof - Google Patents
Moisturizing and skin-tendering mask and preparation method thereof Download PDFInfo
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
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- A61K8/65—Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
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Abstract
The invention discloses a moisturizing and skin-tendering mask and a preparation method thereof, and belongs to the technical field of masks. The invention comprises the following raw materials in percentage by weight: 3-10% of glycerin, 1.5-4.5% of butanediol, 1-4% of deep sea fish collagen peptide, 3-8% of trehalose, 0.05-2% of squalane, 0.15-2% of sodium hyaluronate, 1-5% of propylene glycol, 0.02-0.35% of xanthan gum, 0.02-0.45% of hydrogenated castor oil, 0.02-2% of polysorbate, 0.01-1% of phenoxyethanol, 0.01-0.4% of methyl paraben, 0.1-2% of beta-glucan, 0.01-0.5% of grape seed extract, 0.01-3% of aloe extract, 0.01-1% of dipotassium glycyrrhizinate and the balance of deionized water. The facial mask disclosed by the invention promotes the skin to absorb moisture, is beneficial to moisturizing the skin for a long time, has no stimulation, and has a good effect of moistening the skin.
Description
Technical Field
The invention belongs to the technical field of facial masks, and particularly relates to a moisturizing and skin-tendering facial mask and a preparation method thereof.
Background
Due to natural aging and external environmental factors, the skin gradually loses the protection function against external pollution and microorganisms, is more sensitive to surrounding harm, has increasingly poor environmental adaptation capability, can cause the skin to be dry due to lack of water due to solar irradiation, ionizing radiation and the like, and particularly can cause the skin to be sunburned due to long-term exposure in summer, so that the skin has the problems of dryness, looseness, allergy, dullness, lack of elasticity and the like. The skin of a human body is naturally aged from about 20 years old, and as the skin ages, sebum secretion is reduced, water retention capacity is reduced, the water barrier function of the skin gradually declines, and problems of dry skin, poor elasticity, increased wrinkles and the like begin to appear.
Cosmetics for alleviating or solving skin problems are various in types, and the mask is popular with consumers due to the characteristics of quick response, fashion and strong experience. In daily life, moisturizing is the most basic skin care means, and the skin is easy to increase the generation chance of wrinkles if the skin is lack of water, so most people select moisturizing facial masks to improve the moisture of the skin. The existing moisture mask has unsatisfactory moisture-preserving effect, and partial mask components contain chemical components, so that the mask cannot play a role in maintaining and sometimes causes the skin condition to be worse.
Disclosure of Invention
The invention aims to provide a moisturizing and skin-tendering mask and a preparation method thereof, and solves the problems that in the prior art, the moisturizing effect of a moisturizing mask is not ideal and the current situation of skin is easily endangered.
The invention relates to a moisturizing and skin-tendering mask which is mainly realized by the following technical scheme: comprises the following raw materials in percentage by weight: 3-10% of glycerin, 1.5-4.5% of butanediol, 1-4% of deep sea fish collagen peptide, 3-8% of trehalose, 0.05-2% of squalane, 0.15-2% of sodium hyaluronate, 1-5% of propylene glycol, 0.02-0.35% of xanthan gum, 0.02-0.45% of hydrogenated castor oil, 0.02-2% of polysorbate, 0.01-1% of phenoxyethanol, 0.01-0.4% of methyl paraben, 0.1-2% of beta-glucan, 0.01-0.5% of grape seed extract, 0.01-3% of aloe extract, 0.01-1% of dipotassium glycyrrhizinate and the balance of deionized water.
The mask prepared by matching the deep-sea fish collagen peptide with the grape seed extract, the beta-glucan and the hydrogenated castor oil has the advantages of low allergenicity, no pollution, no stimulation, no pathogeny of diseases of people and livestock, and the like, not only improves the economic value of corresponding fish, but also can reduce environmental pollution; under the auxiliary action of the trehalose, the aloe extract and the sodium hyaluronate, the moisture absorption of the skin is promoted, the long-time moisture retention of the skin is facilitated, and the moisture retention, skin moistening and aging delaying effects of the facial mask liquid are improved; the facial mask does not use ethanol, reduces the irritation of the facial mask liquid to the skin, is easy to be absorbed by a facial mask carrier, is convenient to use, and has the function of moistening the skin when being applied to the face.
As a preferred embodiment, the feed comprises the following raw materials in percentage by weight: 4-8% of glycerol, 2-4% of butanediol, 2-3.8% of deep sea fish collagen peptide, 5-7% of trehalose, 0.5-1.5% of squalane, 0.2-1.5% of sodium hyaluronate, 1.5-3% of propylene glycol, 0.05-0.25% of xanthan gum, 0.05-0.25% of hydrogenated castor oil, 0.05-0.15% of polysorbate, 0.05-0.9% of phenoxyethanol, 0.03-0.3% of methyl paraben, 0.1-2% of beta-glucan, 0.015-0.15% of grape seed extract, 0.05-2% of aloe extract, 0.01-0.5% of dipotassium glycyrrhizinate and the balance of deionized water. The deep sea fish collagen peptide selected by the invention has low molecular weight segment, balanced proportion and high skin transmittance, can enhance skin collagen regeneration through the skin surface layer, recovers skin elasticity, has high water solubility and contains a large amount of exposed hydrogen bond groups to promote compatibility with other medicines, and keeps a system stable; the trehalose has the advantages that the trehalose is long in moisturizing time on the basis of good moisturizing effect, has the effect of stabilizing a biological membrane and a protein structure, is formed by condensing two glucose molecules through hemiacetal hydroxyl, has strong hydrogen bonding capability, plays a thickening role on the basis of dissolution promotion, and enhances the system stability; squalane, a hydrocarbon composed of six isoprene double bonds, belongs to a terpenoid structure, strengthens and repairs the epidermis, effectively forms a natural protective film, helps the balance between the skin and the sebum, forms a stable system with cooperativity, effectiveness and compatibility with other components through hydrogen bonding groups, and stably exists in the system under the action of a mixed emulsifier; the trehalose has certain film forming property, and can form a protective film on the surface of skin to prevent water loss; squalane can inhibit peroxidation of skin lipid, can effectively permeate into skin, can promote proliferation of skin basal cells, and has certain effect of delaying skin aging; the deep sea fish collagen peptide can permeate surface skin to achieve deep moisture retention and provide nutrient substances for skin repair. The invention also uses functional components such as beta-glucan, grape seed extract, aloe extract and the like in a matching way to achieve the effects of moisturizing and tendering skin from inside to outside.
As a preferred embodiment, the feed comprises the following raw materials in percentage by weight: 5% of glycerin, 3.5% of butanediol, 3.5% of deep sea fish collagen peptide, 6% of trehalose, 0.75% of squalane, 0.45% of sodium hyaluronate, 2.5% of propylene glycol, 0.13% of xanthan gum, 0.15% of hydrogenated castor oil, 0.1% of polysorbate, 0.8% of phenoxyethanol, 0.2% of methylparaben, 0.1-2% of beta-glucan, 0.015-0.15% of grape seed extract, 0.1-1% of aloe extract, 0.01-0.2% of dipotassium glycyrrhizinate and the balance of deionized water. The functional components of the facial mask deep-sea fish collagen peptide, trehalose, squalane and the like in the formula can exert the maximum performance, so that the efficacy of the facial mask liquid is optimal, the components interact with each other, and the system is in the most stable state.
In a preferred embodiment, the aloe extract is a dry aloe polysaccharide content of greater than 800ppm and the grape seed extract has a proanthocyanidin content of greater than 90%. The aloe polysaccharide content in the dry powder aloe extract is more than 800ppm, and grape seeds contain a large amount of procyanidine and grape polyphenol, which are known as strong free radical scavengers and are one of high-efficiency antioxidants from plant sources; the grape seed extract has the effects of scavenging free radicals, repairing injured collagen and elastic fiber, improving various anaphylaxis, and astringing to make skin smooth, and can improve the effects of delaying aging and caring skin of facial mask liquid; the aloe extract has the effects of diminishing inflammation, resisting bacteria, enhancing skin elasticity, protecting skin mucosa, cleaning skin, resisting seborrhea, moistening skin, preventing aging and the like, and can be added to make the facial mask liquid be used for sensitive skin and enlarge the application range of the facial mask liquid.
As a preferred embodiment, the molecular weight of the deep-sea fish collagen peptide is 200-1500Da, and the yeast purity in the beta-glucan is 70-80%. The index of the hydrogenated castor oil in the invention conforms to ECOCERT certification; the beta-glucan is natural high-glycan, the macromolecular structure of the beta-glucan can fully lock water, water loss is prevented, and the beta-glucan has high-efficiency moisture retention performance, so that the skin is kept moist and smooth like silks, and the beta-glucan can promote the proliferation of fibroblasts (skin cells) and the synthesis of skin tissue matrixes (such as collagen, elastin, proteoglycan and other components), so that the skin elasticity is increased, and the skin is soft and tender, and the performance of the facial mask liquid is improved.
The invention relates to a preparation method of a moisturizing and skin-tendering mask, which is mainly realized by the following technical scheme: the method comprises the following steps: 1) adding glycerol, butanediol, propylene glycol and methyl hydroxybenzoate into water, heating to 80-85 deg.C, stirring to dissolve completely, and maintaining for 5-10min to obtain mixture 1; 2) stirring the mixture 1 obtained in the step 1) for 10-15min under a vacuum condition, and adding xanthan gum and trehalose to uniformly disperse the xanthan gum and the trehalose during stirring to obtain a mixture 2; 3) mixing hydrogenated castor oil, polysorbate and squalane, preheating to 80-85 ℃, adding into the mixture 2 obtained in the step 2) under vacuum, and stirring for 25-35min under vacuum at 80-85 ℃ to obtain a mixture 3; 4) cooling the mixture 3 obtained in the step 3) to 40-45 ℃, adding deep-sea fish collagen peptide, sodium hyaluronate, phenoxyethanol, beta-glucan, grape seed extract, aloe extract and dipotassium glycyrrhizinate, stirring in vacuum to completely dissolve the components, and filtering to obtain the product.
The preparation method of the facial mask is simple, short in process flow, low in operation temperature, mild in condition, high in production efficiency and easy to realize industrialization, and has no special requirements on equipment; in the preparation process, the effective components in the raw materials are thoroughly activated and fully retained, and the obtained facial mask promotes the absorption of skin on moisture, is beneficial to the long-time moisture retention of the skin, and improves the moisture retention, skin moistening and aging delaying effects of the facial mask liquid.
As a preferred embodiment, in the step 2), the stirring speed during the stirring process is 140-150 r/min. The raw materials are stirred in the emulsification process, the stirring speed is generally 140-150r/min, the stirring is mild and uniform, the phenomenon of nonuniform mixing due to local deposition of the raw materials is avoided, the active ingredients of the raw materials are not damaged, and the raw materials are fully and uniformly mixed according to the original ingredients of the raw materials.
As a preferred embodiment, the step 2) is carried out in an emulsifying pot under a vacuum degree of 0.12 to 0.15 MPa. Vacuum stirring can enable the mixing, dispersing, homogenizing and emulsifying effects to be better, meanwhile, bubbles are prevented from being generated in the stirring process, the high-speed shearing particle size is high in level and free of bubbles, and a facial mask liquid product with fine skin feeling can be obtained and is easier to absorb by the skin; in addition, the vacuum stirring can be used for vacuumizing and removing bubbles from the materials, and the influence on the product quality and the stability caused by the problem of bubbles in the later period can be effectively avoided.
As a preferred embodiment, in the step 3) and the step 4), the degree of vacuum stirring is 0.09 to 0.12 MPa. The vacuum stirring device can select different vacuum degrees according to product requirements, the vacuum stirring is used for ensuring that the effective components are not damaged, and the vacuum stirring is used for enabling the dispersion to be uniform and free of bubbles.
As a preferred embodiment, in the step 4), the mesh number of the filter screen during the filtration is 400-600 meshes. And filtering at a lower temperature, filtering and discharging by adopting a 400-mesh sieve, and detecting related indexes of the discharged material.
Compared with the prior art, the invention has the beneficial effects that: the mask prepared by matching the deep-sea fish collagen peptide with the grape seed extract, the beta-glucan and the hydrogenated castor oil has the advantages of low allergenicity, no pollution, no stimulation, no pathogeny of diseases of people and livestock, and the like, not only improves the economic value of corresponding fish, but also can reduce environmental pollution; under the auxiliary action of the trehalose, the aloe extract and the sodium hyaluronate, the moisture absorption of the skin is promoted, the long-time moisture retention of the skin is facilitated, and the moisture retention, skin moistening and aging delaying effects of the facial mask liquid are improved; the facial mask does not use ethanol, reduces the irritation of the facial mask liquid to the skin, is easy to be absorbed by a facial mask carrier, is convenient to use, and has the function of moistening the skin when being applied to the face; the preparation method of the invention has the advantages of simplicity, short process flow, low operation temperature, mild conditions, no special requirements on equipment, thorough activation and full reservation of effective components in the raw materials, high production efficiency and easy realization of industrialization.
Detailed Description
The technical solutions of the present invention will be described clearly and completely with reference to specific embodiments of the present invention, and it should be understood that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
The moisturizing and skin tendering mask comprises the following raw materials in percentage by weight: 3-10% of glycerin, 1.5-4.5% of butanediol, 1-4% of deep sea fish collagen peptide, 3-8% of trehalose, 0.05-2% of squalane, 0.15-2% of sodium hyaluronate, 1-5% of propylene glycol, 0.02-0.35% of xanthan gum, 0.02-0.45% of hydrogenated castor oil, 0.02-2% of polysorbate, 0.01-1% of phenoxyethanol, 0.01-0.4% of methyl paraben, 0.1-2% of beta-glucan, 0.01-0.5% of grape seed extract, 0.01-3% of aloe extract, 0.01-1% of dipotassium glycyrrhizinate and the balance of deionized water.
Preferably, the feed comprises the following raw materials in percentage by weight: 4-8% of glycerol, 2-4% of butanediol, 2-3.8% of deep sea fish collagen peptide, 5-7% of trehalose, 0.5-1.5% of squalane, 0.2-1.5% of sodium hyaluronate, 1.5-3% of propylene glycol, 0.05-0.25% of xanthan gum, 0.05-0.25% of hydrogenated castor oil, 0.05-0.15% of polysorbate, 0.05-0.9% of phenoxyethanol, 0.03-0.3% of methyl paraben, 0.1-2% of beta-glucan, 0.015-0.15% of grape seed extract, 0.05-2% of aloe extract, 0.01-0.5% of dipotassium glycyrrhizinate and the balance of deionized water.
Further preferably, the feed comprises the following raw materials in percentage by weight: 5% of glycerin, 3.5% of butanediol, 3.5% of deep sea fish collagen peptide, 6% of trehalose, 0.75% of squalane, 0.45% of sodium hyaluronate, 2.5% of propylene glycol, 0.13% of xanthan gum, 0.15% of hydrogenated castor oil, 0.1% of polysorbate, 0.8% of phenoxyethanol, 0.2% of methylparaben, 0.1-2% of beta-glucan, 0.015-0.15% of grape seed extract, 0.1-1% of aloe extract, 0.01-0.2% of dipotassium glycyrrhizinate and the balance of deionized water.
Specifically, the aloe extract is dry aloe polysaccharide content of more than 800ppm, and the grape seed extract contains procyanidin content of more than 90%.
Further, the molecular weight of the deep-sea fish collagen peptide is 200-1500Da, and the yeast purity in the beta-glucan is 70-80%.
A preparation method of the moisturizing and skin-tendering mask comprises the following steps: 1) adding glycerol, butanediol, propylene glycol and methyl hydroxybenzoate into water, heating to 80-85 deg.C, stirring to dissolve completely, and maintaining for 5-10min to obtain mixture 1; 2) stirring the mixture 1 obtained in the step 1) for 10-15min under a vacuum condition, and adding xanthan gum and trehalose to uniformly disperse the xanthan gum and the trehalose during stirring to obtain a mixture 2; 3) mixing hydrogenated castor oil, polysorbate and squalane, preheating to 80-85 ℃, adding into the mixture 2 obtained in the step 2) under vacuum, and stirring for 25-35min under vacuum at 80-85 ℃ to obtain a mixture 3; 4) cooling the mixture 3 obtained in the step 3) to 40-45 ℃, adding deep-sea fish collagen peptide, sodium hyaluronate, phenoxyethanol, beta-glucan, grape seed extract, aloe extract and dipotassium glycyrrhizinate, stirring in vacuum to completely dissolve the components, and filtering to obtain the product.
Preferably, in the step 2), the stirring speed during the stirring process is 140-150 r/min.
Further preferably, the step 2) is carried out in an emulsifying pot, and the vacuum degree under the vacuum condition is 0.12-0.15 MPa.
Specifically, in the step 3) and the step 4), the vacuum degree of vacuum stirring is 0.09-0.12 MPa.
Further, in the step 4), the mesh number of the filter screen during filtering is 400-600 meshes.
Example one
A preparation method of the moisturizing and skin-tendering mask comprises the following steps:
1) the following raw materials were weighed out in the proportions indicated in the third column of data in table 1:
glycerin, butylene glycol, deep sea fish collagen peptide, trehalose, squalane, sodium hyaluronate, propylene glycol, xanthan gum, hydrogenated castor oil, polysorbate, phenoxyethanol, methylparaben, beta-glucan, grape seed extract, aloe extract, dipotassium glycyrrhizinate and deionized water;
2) adding glycerol, butanediol, propylene glycol and methyl hydroxybenzoate into water, heating to 80 deg.C, stirring to dissolve completely, and maintaining for 10min to obtain mixture 1;
3) stirring the mixture 1 obtained in the step 2) for 10min under a vacuum condition, and adding xanthan gum and trehalose to uniformly disperse the xanthan gum and the trehalose during stirring to obtain a mixture 2;
4) mixing hydrogenated castor oil, polysorbate and squalane, preheating to 80 ℃, adding into the mixture 2 obtained in the step 3) under a vacuum condition, stirring for 25min under a vacuum condition, and stirring at 80 ℃ to obtain a mixture 3;
5) cooling the mixture 3 obtained in the step 4) to 40 ℃, adding deep-sea fish collagen peptide, sodium hyaluronate, phenoxyethanol, beta-glucan, grape seed extract, aloe extract and dipotassium glycyrrhizinate, stirring in vacuum to completely dissolve the mixture, and filtering to obtain the product.
Example two
A preparation method of the moisturizing and skin-tendering mask comprises the following steps:
1) the following raw materials were weighed according to the ratios indicated in the fourth column of data in table 1:
glycerin, butylene glycol, deep sea fish collagen peptide, trehalose, squalane, sodium hyaluronate, propylene glycol, xanthan gum, hydrogenated castor oil, polysorbate, phenoxyethanol, methylparaben, beta-glucan, grape seed extract, aloe extract, dipotassium glycyrrhizinate and deionized water;
2) adding glycerol, butanediol, propylene glycol and methyl hydroxybenzoate into water, heating to 85 deg.C, stirring to dissolve completely, and maintaining for 5min to obtain mixture 1;
3) stirring the mixture 1 obtained in the step 2) for 15min under a vacuum condition, and adding xanthan gum and trehalose to uniformly disperse the xanthan gum and the trehalose during stirring to obtain a mixture 2;
4) mixing hydrogenated castor oil, polysorbate and squalane, preheating to 85 ℃, adding into the mixture 2 obtained in the step 3) under a vacuum condition, and stirring for 35min under a vacuum condition at 85 ℃ to obtain a mixture 3;
5) cooling the mixture 3 obtained in the step 4) to 45 ℃, adding deep-sea fish collagen peptide, sodium hyaluronate, phenoxyethanol, beta-glucan, grape seed extract, aloe extract and dipotassium glycyrrhizinate, stirring in vacuum to completely dissolve the mixture, and filtering to obtain the product.
EXAMPLE III
A preparation method of the moisturizing and skin-tendering mask comprises the following steps:
1) weighing the following raw materials according to the proportion shown in the fifth column of data in table 1:
glycerin, butylene glycol, deep sea fish collagen peptide, trehalose, squalane, sodium hyaluronate, propylene glycol, xanthan gum, hydrogenated castor oil, polysorbate, phenoxyethanol, methylparaben, beta-glucan, grape seed extract, aloe extract, dipotassium glycyrrhizinate and deionized water;
2) adding glycerol, butanediol, propylene glycol and methyl hydroxybenzoate into water, heating to 81 deg.C, stirring to dissolve completely, and maintaining for 9min to obtain mixture 1;
3) stirring the mixture 1 obtained in the step 2) for 14min under a vacuum condition, and adding xanthan gum and trehalose to uniformly disperse the xanthan gum and the trehalose during stirring to obtain a mixture 2;
4) mixing hydrogenated castor oil, polysorbate and squalane, preheating to 84 ℃, adding into the mixture 2 obtained in the step 3) under a vacuum condition, stirring for 32min under a vacuum condition, and stirring at 83 ℃ to obtain a mixture 3;
5) cooling the mixture 3 obtained in the step 4) to 41 ℃, adding deep-sea fish collagen peptide, sodium hyaluronate, phenoxyethanol, beta-glucan, grape seed extract, aloe extract and dipotassium glycyrrhizinate, stirring in vacuum to completely dissolve the mixture, and filtering to obtain the product.
Example four
A preparation method of the moisturizing and skin-tendering mask comprises the following steps:
1) the following raw materials were weighed according to the ratio indicated by the sixth column of data in table 1:
glycerin, butylene glycol, deep sea fish collagen peptide, trehalose, squalane, sodium hyaluronate, propylene glycol, xanthan gum, hydrogenated castor oil, polysorbate, phenoxyethanol, methylparaben, beta-glucan, grape seed extract, aloe extract, dipotassium glycyrrhizinate and deionized water;
2) adding glycerol, butanediol, propylene glycol and methyl hydroxybenzoate into water, heating to 84 deg.C, stirring to dissolve completely, and maintaining for 6min to obtain mixture 1;
3) stirring the mixture 1 obtained in the step 2) for 11min under a vacuum condition, and adding xanthan gum and trehalose to uniformly disperse the xanthan gum and the trehalose during stirring to obtain a mixture 2;
4) mixing hydrogenated castor oil, polysorbate and squalane, preheating to 81 ℃, adding into the mixture 2 obtained in the step 3) under a vacuum condition, stirring for 28min under a vacuum condition, and stirring at 82 ℃ to obtain a mixture 3;
5) cooling the mixture 3 obtained in the step 4) to 44 ℃, adding deep-sea fish collagen peptide, sodium hyaluronate, phenoxyethanol, beta-glucan, grape seed extract, aloe extract and dipotassium glycyrrhizinate, stirring in vacuum to completely dissolve the mixture, and filtering to obtain the product.
EXAMPLE five
Weighing the raw materials according to the proportion shown in the seventh column of data in the table 1, and preparing the moisturizing and skin-tendering mask according to the method in the first embodiment.
EXAMPLE six
Weighing the raw materials according to the proportion shown in the eighth column of data in the table 1, and preparing the moisturizing and skin-tendering mask according to the method of the second embodiment.
EXAMPLE seven
Weighing the raw materials according to the proportion shown in the ninth column of data in the table 1, and preparing the moisturizing and skin-tendering mask according to the method in the third embodiment.
The facial masks prepared by the methods of the first to seventh embodiments of the present invention and two existing commercially available facial masks each containing a polypeptide are respectively subjected to performance test experiments, including a moisturizing performance measurement experiment, a DPPH effect elimination experiment and a superoxide anion elimination experiment, and the related experiments are performed by referring to a test method in the daily chemical industry 2011, vol. 3, vol. 41, which is published by the research and development of a pollock skin collagen polypeptide composition water-washing facial mask compiled by yan mingbu yan et al (i.e., the daily chemical industry 2011,41(3): 194-.
As can be seen from table 2, the facial mask of the present invention shows significant advantages at 12h of the experiment, and the moisture retention rate thereof is significantly greater than that of the existing commercially available facial masks containing polypeptides, i.e., the first control sample and the second control sample, and when the experiment time is gradually increased from 12h to 72h, the moisture retention rate of the facial mask of the present invention is gradually decreased, and meanwhile, the moisture retention rates of the existing commercially available facial masks containing polypeptides, i.e., the first control sample and the second control sample, are also gradually decreased; however, the moisture retention rate of the mask of the present invention was higher than that of the conventional commercial mask containing the polypeptide, i.e., the control sample i and the control sample ii, in the same experimental time. Therefore, the mask disclosed by the invention has obvious water replenishing and moisturizing advantages.
Table 2 comparison table of different mask moisture retention performance test results
TABLE 3 comparison of the results of different mask DPPH removal and Performance tests
As can be seen from Table 3, the mask of the invention has a DPPH removal rate of 83.23% in DPPH removal effect experiments, and all the masks have DPPH removal rates higher than that of the existing commercial mask containing polypeptides, namely a control sample I and a control sample II; therefore, the mask of the present invention showed better DPPH-removing effect than the control one and the control two. The facial mask liquid contains components such as small molecular weight collagen peptide, grape seed extract, aloe extract and the like, has high-efficiency antioxidant effect, and explains experimental results of high DPPH and superoxide anion clearance rate in principle. In addition, when the facial mask disclosed by the invention is used for removing superoxide anions, the removal rate of the facial mask to the superoxide anions is 15.03-16.90%, which is far greater than 9.90% and 6.30%, namely the removal rate of the facial mask to the superoxide anions is obviously higher than that of the existing commercial facial masks containing the polypeptide, namely the control sample I and the control sample II; therefore, the mask of the present invention showed better superoxide anion scavenging effect compared to the control one and the control two.
Compared with the prior art, the invention has the beneficial effects that: the mask prepared by matching the deep-sea fish collagen peptide with the grape seed extract, the beta-glucan and the hydrogenated castor oil has the advantages of low allergenicity, no pollution, no stimulation, no pathogeny of diseases of people and livestock, and the like, not only improves the economic value of corresponding fish, but also can reduce environmental pollution; under the auxiliary action of the trehalose, the aloe extract and the sodium hyaluronate, the moisture absorption of the skin is promoted, the long-time moisture retention of the skin is facilitated, and the moisture retention, skin moistening and aging delaying effects of the facial mask liquid are improved; the facial mask does not use ethanol, reduces the irritation of the facial mask liquid to the skin, is easy to be absorbed by a facial mask carrier, is convenient to use, and has the function of moistening the skin when being applied to the face; the preparation method of the invention has the advantages of simplicity, short process flow, low operation temperature, mild conditions, no special requirements on equipment, thorough activation and full reservation of effective components in the raw materials, high production efficiency and easy realization of industrialization.
The above description is only for the purpose of illustrating the preferred embodiments of the present invention and is not to be construed as limiting the invention, and any modifications, equivalents, improvements and the like that fall within the spirit and principle of the present invention are intended to be included therein.
Claims (9)
1. The moisturizing and skin tendering mask is characterized in that: the water-replenishing and skin-tendering mask comprises the following raw materials in percentage by weight:
3-10% of glycerin, 1.5-4.5% of butanediol, 1-4% of deep sea fish collagen peptide, 3-8% of trehalose, 0.05-2% of squalane, 0.15-2% of sodium hyaluronate, 1-5% of propylene glycol, 0.02-0.35% of xanthan gum, 0.02-0.45% of hydrogenated castor oil, 0.02-2% of polysorbate, 0.01-1% of phenoxyethanol, 0.01-0.4% of methyl paraben, 0.1-2% of beta-glucan, 0.01-0.5% of grape seed extract, 0.01-3% of aloe extract, 0.01-1% of dipotassium glycyrrhizinate and the balance of deionized water;
the preparation method of the moisturizing and skin-tendering mask comprises the following steps:
1) adding glycerol, butanediol, propylene glycol and methyl hydroxybenzoate into deionized water, heating to 80-85 deg.C, stirring to dissolve completely, and maintaining for 5-10min to obtain mixture 1;
2) stirring the mixture 1 obtained in the step 1) for 10-15min under a vacuum condition, and adding xanthan gum and trehalose to uniformly disperse the xanthan gum and the trehalose during stirring to obtain a mixture 2;
3) mixing hydrogenated castor oil, polysorbate and squalane, preheating to 80-85 ℃, adding into the mixture 2 obtained in the step 2) under vacuum, and stirring for 25-35min under vacuum at 80-85 ℃ to obtain a mixture 3;
4) cooling the mixture 3 obtained in the step 3) to 40-45 ℃, adding deep-sea fish collagen peptide, sodium hyaluronate, phenoxyethanol, beta-glucan, grape seed extract, aloe extract and dipotassium glycyrrhizinate, stirring in vacuum to completely dissolve the components, and filtering to obtain the product.
2. The hydrating rejuvenating mask as defined in claim 1, wherein: comprises the following raw materials in percentage by weight:
4-8% of glycerol, 2-4% of butanediol, 2-3.8% of deep sea fish collagen peptide, 5-7% of trehalose, 0.5-1.5% of squalane, 0.2-1.5% of sodium hyaluronate, 1.5-3% of propylene glycol, 0.05-0.25% of xanthan gum, 0.05-0.25% of hydrogenated castor oil, 0.05-0.15% of polysorbate, 0.05-0.9% of phenoxyethanol, 0.03-0.3% of methyl paraben, 0.1-2% of beta-glucan, 0.015-0.15% of grape seed extract, 0.05-2% of aloe extract, 0.01-0.5% of dipotassium glycyrrhizinate and the balance of deionized water.
3. The hydrating rejuvenating mask as set forth in claim 2, wherein: comprises the following raw materials in percentage by weight:
5% of glycerin, 3.5% of butanediol, 3.5% of deep sea fish collagen peptide, 6% of trehalose, 0.75% of squalane, 0.45% of sodium hyaluronate, 2.5% of propylene glycol, 0.13% of xanthan gum, 0.15% of hydrogenated castor oil, 0.1% of polysorbate, 0.8% of phenoxyethanol, 0.2% of methylparaben, 0.1-2% of beta-glucan, 0.015-0.15% of grape seed extract, 0.1-1% of aloe extract, 0.01-0.2% of dipotassium glycyrrhizinate and the balance of deionized water.
4. The hydrating rejuvenating mask as set forth in any one of claims 1 to 3, wherein:
the aloe extract has a dry aloe polysaccharide content of greater than 800ppm, and the grape seed extract has a procyanidin content of greater than 90%.
5. The hydrating rejuvenating mask as set forth in any one of claims 1 to 3, wherein:
the molecular weight of the deep-sea fish collagen peptide is 200-1500 Da.
6. The hydrating rejuvenating mask as defined in claim 1, wherein:
in the step 2), the stirring speed in the stirring process is 140-150 r/min.
7. The hydrating rejuvenating mask as defined in claim 1, wherein:
the step 2) is carried out in an emulsifying pot, and the vacuum degree under the vacuum condition is 0.12-0.15 MPa.
8. The hydrating rejuvenating mask as defined in claim 1, wherein:
in the step 3) and the step 4), the vacuum degree of vacuum stirring is 0.09-0.12 MPa.
9. The hydrating rejuvenating mask as defined in claim 1, wherein:
in the step 4), the mesh number of the screen during filtering is 400-600 meshes.
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| CN108815018A (en) * | 2018-05-28 | 2018-11-16 | 黑龙江力海鑫生物科技股份有限公司 | A kind of castor rat-tail muscle extracts the facial mask liquid and preparation method thereof of collagen peptide |
| CN108420757B (en) * | 2018-06-02 | 2021-02-12 | 杭州兰茜化妆品有限公司 | Moisturizing lotion and preparation process thereof |
| CN110559240A (en) * | 2018-06-05 | 2019-12-13 | 冯松平 | whitening and anti-aging mask and preparation method thereof |
| CN109044946A (en) * | 2018-09-27 | 2018-12-21 | 张言聚 | A kind of whitening and moisturizing facial mask liquid and its preparation process |
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| CN109394592A (en) * | 2018-11-22 | 2019-03-01 | 医美生物科技(上海)有限公司 | A kind of multiple-effect flesh bottom water of replenishing water and preserving moisture oil-control |
| CN109568151A (en) * | 2019-01-14 | 2019-04-05 | 恒天量子（厦门）科技有限公司 | A kind of Essence skin care moisture saver mask and preparation method thereof containing small-molecular peptides |
| CN112336668A (en) * | 2019-08-06 | 2021-02-09 | 中国科学院烟台海岸带研究所 | Deep sea fish collagen peptide seaweed rejuvenating facial mask and preparation method thereof |
| CN111773170A (en) * | 2020-08-03 | 2020-10-16 | 广州虹美生物科技有限公司 | Facial mask patch added with grease and preparation method |
| CN113230183A (en) * | 2021-05-13 | 2021-08-10 | 广州市万千粉丝化妆品有限公司 | Preparation with skin cell repairing active protein peptide and preparation method thereof |
| CN114010572A (en) * | 2021-11-17 | 2022-02-08 | 广东画景医药生物科技有限公司 | Marine collagen firming sleeping mask and preparation method thereof |
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