CN111494238A - Repairing and moistening mask containing carboxylated chitosan and preparation method thereof - Google Patents
Repairing and moistening mask containing carboxylated chitosan and preparation method thereof Download PDFInfo
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- CN111494238A CN111494238A CN202010426247.5A CN202010426247A CN111494238A CN 111494238 A CN111494238 A CN 111494238A CN 202010426247 A CN202010426247 A CN 202010426247A CN 111494238 A CN111494238 A CN 111494238A
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- facial mask
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- carboxylated chitosan
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- 229920001661 Chitosan Polymers 0.000 title claims abstract description 65
- 238000002360 preparation method Methods 0.000 title abstract description 15
- 230000001815 facial effect Effects 0.000 claims abstract description 81
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 45
- 229920002385 Sodium hyaluronate Polymers 0.000 claims abstract description 45
- 229940010747 sodium hyaluronate Drugs 0.000 claims abstract description 45
- YWIVKILSMZOHHF-QJZPQSOGSA-N sodium;(2s,3s,4s,5r,6r)-6-[(2s,3r,4r,5s,6r)-3-acetamido-2-[(2s,3s,4r,5r,6r)-6-[(2r,3r,4r,5s,6r)-3-acetamido-2,5-dihydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-2-carboxy-4,5-dihydroxyoxan-3-yl]oxy-5-hydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-3,4,5-trihydroxyoxane-2- Chemical compound [Na+].CC(=O)N[C@H]1[C@H](O)O[C@H](CO)[C@@H](O)[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@H](O[C@H]2[C@@H]([C@@H](O[C@H]3[C@@H]([C@@H](O)[C@H](O)[C@H](O3)C(O)=O)O)[C@H](O)[C@@H](CO)O2)NC(C)=O)[C@@H](C(O)=O)O1 YWIVKILSMZOHHF-QJZPQSOGSA-N 0.000 claims abstract description 45
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- IXPNQXFRVYWDDI-UHFFFAOYSA-N 1-methyl-2,4-dioxo-1,3-diazinane-5-carboximidamide Chemical compound CN1CC(C(N)=N)C(=O)NC1=O IXPNQXFRVYWDDI-UHFFFAOYSA-N 0.000 claims abstract description 18
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- CRJGESKKUOMBCT-VQTJNVASSA-N N-acetylsphinganine Chemical compound CCCCCCCCCCCCCCC[C@@H](O)[C@H](CO)NC(C)=O CRJGESKKUOMBCT-VQTJNVASSA-N 0.000 claims abstract description 17
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- VVGIYYKRAMHVLU-UHFFFAOYSA-N newbouldiamide Natural products CCCCCCCCCCCCCCCCCCCC(O)C(O)C(O)C(CO)NC(=O)CCCCCCCCCCCCCCCCC VVGIYYKRAMHVLU-UHFFFAOYSA-N 0.000 claims abstract description 17
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- ANZUDYZHSVGBRF-UHFFFAOYSA-N 3-ethylnonane-1,2,3-triol Chemical compound CCCCCCC(O)(CC)C(O)CO ANZUDYZHSVGBRF-UHFFFAOYSA-N 0.000 claims abstract description 15
- CDQSJQSWAWPGKG-UHFFFAOYSA-N butane-1,1-diol Chemical compound CCCC(O)O CDQSJQSWAWPGKG-UHFFFAOYSA-N 0.000 claims abstract description 15
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- NCZPCONIKBICGS-UHFFFAOYSA-N 3-(2-ethylhexoxy)propane-1,2-diol Chemical compound CCCCC(CC)COCC(O)CO NCZPCONIKBICGS-UHFFFAOYSA-N 0.000 description 1
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Classifications
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/733—Alginic acid; Salts thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0212—Face masks
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/494—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
- A61K8/4946—Imidazoles or their condensed derivatives, e.g. benzimidazoles
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/68—Sphingolipids, e.g. ceramides, cerebrosides, gangliosides
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- A—HUMAN NECESSITIES
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
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- A—HUMAN NECESSITIES
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/736—Chitin; Chitosan; Derivatives thereof
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- A—HUMAN NECESSITIES
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- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P17/00—Drugs for dermatological disorders
- A61P17/02—Drugs for dermatological disorders for treating wounds, ulcers, burns, scars, keloids, or the like
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
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- A—HUMAN NECESSITIES
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- Engineering & Computer Science (AREA)
- Bioinformatics & Cheminformatics (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Medicinal Chemistry (AREA)
- Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
- Organic Chemistry (AREA)
- Pharmacology & Pharmacy (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses a repairing and nourishing facial mask containing carboxylated chitosan and a preparation method thereof, the repairing and nourishing facial mask containing carboxylated chitosan consists of facial mask cloth and facial mask essence, and the facial mask essence consists of the following raw materials in parts by weight: 0.15-0.6 part of carboxylated chitosan, 0.1-0.3 part of sodium hyaluronate, 0.01-0.1 part of enzyme-digested oligomeric sodium hyaluronate, 0.1-0.6 part of sodium alginate, 0.1-0.5 part of ceramide, 1-4 parts of glycerol, 0.1-0.5 part of butanediol, 0.1-0.5 part of phenoxyethanol, 0.01-0.1 part of ethylhexyl glycerol, 0.05-0.3 part of chlorphenesin and 93-98 parts of purified water. The solution is homogenized and dispersed by a colloid mill during preparation, so that the production time and the cost are accelerated. According to the invention, the carboxylated chitosan and the sodium hyaluronate are combined, so that the self-repairing capability of the skin is improved, and the moisture is effectively preserved and supplemented.
Description
Technical Field
The invention belongs to the technical field of cosmetics, and particularly relates to a repairing moistening and nourishing facial mask containing carboxylated chitosan, and a preparation method of the repairing moistening and nourishing facial mask containing carboxylated chitosan.
Background
With the continuous improvement of living standard, the repairing and nourishing facial mask is widely used as a beauty and skin care product. The repairing and moisturizing facial mask essence is an important component of a facial mask, the effect of a product is directly influenced, but the existing facial mask essence mainly plays a role in repairing and moisturizing the epidermis, is poor in repairing and moisturizing effect, and can not meet the requirements of people.
The sodium hyaluronate is the main component of the existing repairing and moisturizing mask, and has the effects of moisturizing, nourishing, repairing and preventing skin injury, lubricating property, film forming property and thickening property. Sodium hyaluronate can promote the regeneration of skin at the injured part by promoting the proliferation and differentiation of epidermal cells and scavenging oxygen free radicals. In the prior art, the publication date is 2019, 08 and 23, and the publication number is CN110151653A, Chinese patent discloses a repair mask and a preparation method thereof, wherein the mask essence adopts the combination of sodium hyaluronate, a spiny pine algae extract, a kelp extract, a brown algae extract, a ditch carrageen and palmitoyl tetrapeptide-7, so that the repair effect is improved; through combining sodium alginate, promote the release of the repair composition in the facial mask cloth, improve the repair effect, but the repair composition is too complicated, and mostly is the plant extract, has sensitization risk to sensitive skin, is not ideal repair selection to the moisturizing effect of facial mask is relatively poor.
Research shows that the sodium hyaluronate and the chitosan are combined to accelerate the regeneration of epidermal cells, so that the skin is tender, smooth and elastic. When the skin suffers from mild burns and scalds, the preparation containing chitosan and sodium hyaluronate is smeared on the surface of the skin, so that the pain can be relieved, and the healing of the skin at the injured part can be accelerated. Because chitosan and sodium hyaluronate are difficult to dissolve, gel cosmetics are generally prepared.
At present, the facial masks in the market are various, particularly, facial masks with the functions of repairing and nourishing are mainly used in recent years, but most of the components contain repairing and nourishing components, the facial masks are not suitable for people with sensitive skin, anaphylactic reaction is easy to occur after long-term use, the preparation process is only mixing and stirring at different temperatures according to the characteristics of the components, the components are not well dispersed and homogenized, and the effects of the facial masks for repairing and nourishing cannot be effectively exerted.
Disclosure of Invention
In order to overcome the defects of the prior art, the invention provides the repairing and nourishing facial mask which has obvious repairing and nourishing effects, also has the functions of promoting wound healing, resisting bacteria and inflammation and contains carboxylated chitosan and can be used daily for a long time. The invention also aims to provide a preparation method of the repairing and nourishing facial mask containing the carboxylated chitosan, which has short production time and low production cost.
The technical scheme for solving the technical problems is as follows:
the repairing and moistening facial mask containing the carboxylated chitosan consists of facial mask cloth and facial mask essence, wherein the facial mask essence consists of the following raw materials in parts by weight: 0.15-0.6 part of carboxylated chitosan, 0.1-0.3 part of sodium hyaluronate, 0.01-0.1 part of enzyme-digested oligomeric sodium hyaluronate, 0.1-0.6 part of sodium alginate, 0.1-0.5 part of ceramide, 1-4 parts of glycerol, 0.1-0.5 part of butanediol, 0.1-0.5 part of phenoxyethanol, 0.01-0.1 part of ethylhexyl glycerol, 0.05-0.3 part of chlorphenesin and 93-98 parts of purified water.
Further, the facial mask essence consists of the following raw materials in parts by weight: 0.3 part of carboxylated chitosan, 0.18 part of sodium hyaluronate, 0.02 part of enzyme-digested oligomeric sodium hyaluronate, 0.4 part of sodium alginate, 0.3 part of ceramide, 2 parts of glycerol, 0.3 part of butanediol, 0.3 part of phenoxyethanol, 0.03 part of ethylhexyl glycerol, 0.1 part of chlorphenesin and 96 parts of purified water.
Furthermore, 20-30 ml of the facial mask essence is adsorbed on each piece of facial mask cloth.
Furthermore, the mask membrane cloth is preferably a copper ammonia fiber membrane cloth, and any one of silk, non-woven fabric or cotton cloth can be selected.
Further, the facial mask essence also comprises allantoin in 0.1-0.4 parts by weight.
The invention also provides a preparation method of the repairing moistening and nourishing mask containing the carboxylated chitosan, which comprises the following steps:
(1) weighing the raw material components in parts by weight for later use;
(2) weighing 8-10 parts of purified water, heating to 70-75 ℃, adding the weighed chlorphenesin, and stirring for 2-5 minutes until the mixture is completely dissolved to obtain liquid A;
(3) cooling the liquid A to 55-60 ℃, adding sodium hyaluronate and enzyme-digested oligomeric sodium hyaluronate, stirring, and uniformly mixing to obtain liquid B;
(4) cooling the liquid B to 20-25 ℃, sequentially adding the carboxylated chitosan, the ceramide and the sodium alginate, stirring and uniformly mixing to obtain a liquid C;
(5) passing the liquid C through a colloid mill, and washing the colloid mill with 8-10 parts of purified water to obtain a liquid D;
(6) adding glycerol, butanediol, phenoxyethanol, ethylhexyl glycerol and the rest purified water into the liquid D, stirring while adding, mixing uniformly to obtain a liquid E, standing, and degassing;
(7) standing and degassing the liquid E, and filtering through a layer of filter cloth with 300 meshes to obtain mask essence;
(8) transferring the facial mask purifying solution to a charging barrel of a filling machine, adjusting the filling amount to be 20-30 ml, starting filling into facial mask bags with facial mask cloth, and packaging to obtain the product.
Further, the static degassing of the step (6) has a static time of 85-95 min.
Further, the allantoin is added in the step (4), namely after the liquid B is cooled to 20-25 ℃, the carboxylated chitosan, the ceramide, the sodium alginate and the allantoin are sequentially added, stirred and mixed uniformly to obtain a liquid C.
The colloid mill is made of a universal machinery manufacturing gallery model JMS-130.
Compared with the prior art, the invention has obvious beneficial effects, and the technical scheme can show that:
according to the mask essence containing the carboxylated chitosan, the carboxylated chitosan is selected as the water-soluble chitosan, the self characteristics of the chitosan are utilized, the wound repairing capacity and the bacteria inhibiting and killing characteristics are realized, the repairing capacity of the sodium hyaluronate is synergistically enhanced by combining with the sodium hyaluronate, the remarkable repairing effect is achieved, the excellent repairing effect can be achieved by using a small amount of the chitosan, the chitosan can be used for a long time every day, meanwhile, the using amount of the expensive sodium hyaluronate is reduced, and the production cost is also reduced; the antibacterial and bactericidal property of the chitosan can also reduce the dosage of the preservative in the mask, and reduce the stimulation to the skin; the phenoxyethanol and the ethylhexyl glycerin are used as preservatives, and the carboxylated chitosan has the characteristics of synergistic effect in proportion, so that the antibacterial effect is enhanced; the mask essence containing the carboxylated chitosan has the advantages that the raw materials are mutually cooperated, the mask essence not only has remarkable repairing and nourishing effects, but also has the effects of promoting wound healing, resisting bacteria and diminishing inflammation, is used for the healing process of fine wounds, has the effect of active bacteriostasis, and has good repairing effect, quick response and no side effect. Tests show that the effect is reduced by the absence of any active ingredient, and the synergistic effect can be generated between the selected ingredients.
The preparation method provided by the invention scientifically maximizes the effect of each component by adding the components step by step, and after the carboxylated chitosan and the sodium hyaluronate are added, the mixed liquid is treated by using a colloid mill, so that the dissolution, dispersion and homogenization are accelerated, the stirring time and the production time are shortened, the production cost is reduced, the mask essence is filtered again by using filter cloth after the mixture is completely stood and degassed, and after the mask essence is soaked in mask cloth, the application effect is good, the effective components in the essence are fully released, and the repairing and nourishing effects are further improved.
Detailed Description
The present invention will be described in further detail with reference to the following examples and examples, but it should not be construed that the scope of the above subject matter of the present invention is limited to the following examples.
Example 1: the repairing and moistening facial mask containing the carboxylated chitosan consists of copper ammonia fiber membrane cloth and facial mask essence, wherein the facial mask essence consists of the following raw materials in parts by weight:
0.15 part of carboxylated chitosan, 0.1 part of sodium hyaluronate, 0.01 part of enzyme-digested oligomeric sodium hyaluronate, 0.1 part of sodium alginate, 0.1 part of ceramide, 1 part of glycerol, 0.1 part of butanediol, 0.1 part of phenoxyethanol, 0.01 part of ethylhexyl glycerol, 0.05 part of chlorphenesin and 93 parts of purified water.
The preparation method of the repairing moistening and nourishing mask containing the carboxylated chitosan comprises the following steps: (1) weighing the raw material components in parts by weight for later use; (2) weighing 8 parts of purified water, heating to 70 ℃, adding chlorphenesin, and stirring for 2 minutes until the purified water is completely dissolved to obtain a liquid A; (3) cooling the liquid A to 55 ℃, adding sodium hyaluronate and enzyme-digested oligomeric sodium hyaluronate, stirring, and uniformly mixing to obtain liquid B; (4) cooling the liquid B to 20 ℃, sequentially adding the carboxylated chitosan, the ceramide and the sodium alginate, stirring and uniformly mixing to obtain a liquid C; (5) passing the liquid C through a colloid mill, and washing the colloid mill with 8 parts of purified water to obtain a liquid D; (6) adding glycerol, butanediol, phenoxyethanol, ethylhexyl glycerol and the rest 77 parts of purified water into the liquid D, stirring while adding, mixing uniformly to obtain a liquid E, standing for 85min, and degassing; (7) standing and degassing the liquid E, and filtering through a layer of filter cloth with 300 meshes to obtain mask essence; (8) and transferring the facial mask purifying solution to a charging barrel of a filling machine, adjusting the filling amount to be 20ml, starting filling into facial mask bags with facial mask cloth, and packaging to obtain the product.
Example 2:
the repairing and moistening facial mask containing the carboxylated chitosan consists of copper ammonia fiber membrane cloth and facial mask essence, wherein the facial mask essence consists of the following raw materials in parts by weight: 0.3 part of carboxylated chitosan, 0.18 part of sodium hyaluronate, 0.02 part of enzyme-digested oligomeric sodium hyaluronate, 0.4 part of sodium alginate, 0.3 part of ceramide, 2 parts of glycerol, 0.3 part of butanediol, 0.3 part of phenoxyethanol, 0.03 part of ethylhexyl glycerol, 0.1 part of chlorphenesin and 96 parts of purified water.
The preparation method of the repairing moistening and nourishing mask containing the carboxylated chitosan comprises the following steps: (1) weighing the raw material components in parts by weight for later use; (2) weighing 9 parts of purified water, heating to 73 ℃, adding chlorphenesin, and stirring for 3 minutes until the purified water is completely dissolved to obtain a liquid A; (3) cooling the liquid A to 58 ℃, adding sodium hyaluronate and enzyme-digested oligomeric sodium hyaluronate, stirring, and uniformly mixing to obtain liquid B; (4) cooling the liquid B to 23 ℃, sequentially adding the carboxylated chitosan, the ceramide and the sodium alginate, stirring and uniformly mixing to obtain a liquid C; (5) passing the liquid C through a colloid mill, and washing the colloid mill with 9 parts of purified water to obtain a liquid D; (6) adding glycerol, butanediol, phenoxyethanol, ethylhexyl glycerol and the rest 78 parts of purified water into the liquid D, stirring while adding, mixing uniformly to obtain a liquid E, standing for 90min, and degassing; (7) standing and degassing the liquid E, and filtering through a layer of filter cloth with 300 meshes to obtain mask essence; (8) and transferring the facial mask purifying solution to a charging barrel of a filling machine, adjusting the filling amount to 25ml, starting filling into facial mask bags with facial mask cloth, and packaging to obtain the product.
Example 3:
the repairing and moistening facial mask containing the carboxylated chitosan consists of copper ammonia fiber membrane cloth and facial mask essence, wherein the facial mask essence consists of the following raw materials in parts by weight: 0.6 part of carboxylated chitosan, 0.3 part of sodium hyaluronate, 0.1 part of enzyme-digested oligomeric sodium hyaluronate, 0.6 part of sodium alginate, 0.5 part of ceramide, 4 parts of glycerol, 0.5 part of butanediol, 0.5 part of phenoxyethanol, 0.1 part of ethylhexyl glycerol, 0.3 part of chlorphenesin and 98 parts of purified water.
The preparation method of the repairing moistening and nourishing mask containing the carboxylated chitosan comprises the following steps: (1) weighing the raw material components in parts by weight for later use; (2) weighing 10 parts of purified water, heating to 75 ℃, adding chlorphenesin, and stirring for 5 minutes until the water is completely dissolved to obtain liquid A; (3) cooling the liquid A to 60 ℃, adding sodium hyaluronate and enzyme-digested oligomeric sodium hyaluronate, stirring, and uniformly mixing to obtain liquid B; (4) cooling the liquid B to 25 ℃, sequentially adding the carboxylated chitosan, the ceramide and the sodium alginate, stirring and uniformly mixing to obtain a liquid C; (5) passing the liquid C through a colloid mill, and washing the colloid mill with 10 parts of purified water to obtain a liquid D; (6) adding glycerol, butanediol, phenoxyethanol, ethylhexyl glycerol and the rest 78 parts of purified water into the liquid D, stirring while adding, mixing uniformly to obtain a liquid E, standing for 95min, and degassing; (7) standing and degassing the liquid E, and filtering through a layer of filter cloth with 300 meshes to obtain mask essence; (8) and transferring the facial mask purifying solution to a charging barrel of a filling machine, adjusting the filling amount to be 30ml, starting filling into facial mask bags with facial mask cloth, and packaging to obtain the product.
Example 4:
the repairing and moistening facial mask containing the carboxylated chitosan consists of copper ammonia fiber membrane cloth and facial mask essence, wherein the facial mask essence consists of the following raw materials in parts by weight: 0.3 part of carboxylated chitosan, 0.18 part of sodium hyaluronate, 0.02 part of enzyme-digested oligomeric sodium hyaluronate, 0.4 part of sodium alginate, 0.3 part of ceramide, 2 parts of glycerol, 0.3 part of butanediol, 0.3 part of phenoxyethanol, 0.03 part of ethylhexyl glycerol, 0.1 part of chlorphenesin, 96 parts of purified water and 0.2 part of allantoin.
The preparation method of the repairing moistening and nourishing mask containing the carboxylated chitosan comprises the following steps: (1) weighing the raw material components in parts by weight for later use; (2) weighing 9 parts of purified water, heating to 73 ℃, adding chlorphenesin, and stirring for 3 minutes until the purified water is completely dissolved to obtain a liquid A; (3) cooling the liquid A to 58 ℃, adding sodium hyaluronate and enzyme-digested oligomeric sodium hyaluronate, stirring, and uniformly mixing to obtain liquid B; (4) cooling the liquid B to 23 ℃, sequentially adding carboxylated chitosan, ceramide, sodium alginate and allantoin, stirring, and uniformly mixing to obtain a liquid C; (5) passing the liquid C through a colloid mill, and washing the colloid mill with 9 parts of purified water to obtain a liquid D; (6) adding glycerol, butanediol, phenoxyethanol, ethylhexyl glycerol and the rest 78 parts of purified water into the liquid D, stirring while adding, mixing uniformly to obtain a liquid E, standing for 90min, and degassing; (7) standing and degassing the liquid E, and filtering through a layer of filter cloth with 300 meshes to obtain mask essence; (8) and transferring the facial mask purifying solution to a charging barrel of a filling machine, adjusting the filling amount to 25ml, starting filling into facial mask bags with facial mask cloth, and packaging to obtain the product.
Comparative example 1 differs from example 2 only in that it contains 0.01 parts of carboxylated chitosan.
Comparative example 2 differs from example 2 only in the absence of carboxylated chitosan.
Comparative example 3 differs from example 2 only in the absence of sodium hyaluronate.
Experimental example 1: moisture-keeping and nourishing effect of facial mask
The facial masks prepared in examples 1-4 and comparative examples 1-3 of the invention are taken, the tested population is 140 volunteers with the age of 28-45, the tested population is randomly distributed into 7 groups according to the parallel comparison principle, each group comprises 20 persons, the facial masks prepared in examples 1-4 and comparative examples 1-3 of the invention are respectively applied on the cleaned faces of 7 groups of tested persons for 15min, the moisture and elasticity conditions of the skin before and after the facial masks are applied are tested by a skin tester, and the test results are recorded as follows:
TABLE 1 moisturizing and nourishing effect of facial mask
From the above experimental results, it can be seen that the water content and skin elasticity of facial skin of volunteers are significantly increased after the repairing moistening mask containing carboxylated chitosan of the present invention is used, the effect is significantly better than that of comparative examples 1-3, example 2 is the best example, and the moisturizing effect is better in example 4 after allantoin is added. In addition, it can be seen from comparison with the comparative example that the volunteers used the facial mask solution prepared by the comparative example, the skin elasticity and water content were not as good as those of the group of example 4 of the present invention, and the carboxylated chitosan and sodium hyaluronate were contained, so that the better moisturizing and skin nourishing effects could be obtained, compared with the absence of either one, and the components of the repairing and nourishing facial mask containing carboxylated chitosan of the present invention had synergistic effect.
Experimental example 2: repairing effect of facial mask
The facial masks prepared in examples 1-4 and comparative examples 2-3 of the present invention were taken, and 130 volunteers with age of 28-45, reddened skin, sunburn, acne and water acupuncture were randomly assigned to 6 groups according to the parallel control principle, and 20 persons in each group were treated with the facial masks prepared in examples 1-4 and comparative examples 2-3 once a day for 15 days. The skin of the tester is observed respectively, the skin is compared before and after the mask is used, the repairing effect of the repairing mask is evaluated, and the comprehensive evaluation test result is as follows:
TABLE 2 skin repair Effect of the mask
Therefore, the repairing moistening and nourishing facial mask containing the carboxylated chitosan can achieve the obvious effect of repairing the skin, and repair the problems of facial redness and redness, acne muscle, and post-surgical repair with a water acupuncture, the facial mask of examples 1-4 can have calming, anti-inflammatory, and moisturizing effects on the skin, can repair damaged subcutaneous tissue, stimulate fibroblasts to generate collagen and elastin, promote skin metabolism, accelerate the healing of damaged skin caused by pox, greatly reduces acne marks, has no obvious needle eye marks after 3 to 5 days on average aiming at the healing wound convergence after the water laser acupuncture operation, the mask of comparative examples 2-3 had poor repairing effect, low healing speed of pox, no obvious change of pox mark during the test period, slow wound convergence for the repair after the laser acupuncture, and no obvious pinhole mark after 10-15 days. The carboxylated chitosan and the sodium hyaluronate in the mask essence of the repair mask are absent, and the carboxylated chitosan and the sodium hyaluronate are synergistic with each other, so that the skin repair effect can be improved.
The above description is only a preferred embodiment of the present invention, and is not intended to limit the present invention in any way, and any simple modification, equivalent change and modification made to the above embodiment according to the technical spirit of the present invention are within the scope of the present invention without departing from the technical spirit of the present invention.
Claims (8)
1. The repairing and moistening facial mask containing the carboxylated chitosan consists of facial mask cloth and facial mask essence, and is characterized in that: the facial mask essence is prepared from the following raw materials in parts by weight: 0.15-0.6 part of carboxylated chitosan, 0.1-0.3 part of sodium hyaluronate, 0.01-0.1 part of enzyme-digested oligomeric sodium hyaluronate, 0.1-0.6 part of sodium alginate, 0.1-0.5 part of ceramide, 1-4 parts of glycerol, 0.1-0.5 part of butanediol, 0.1-0.5 part of phenoxyethanol, 0.01-0.1 part of ethylhexyl glycerol, 0.05-0.3 part of chlorphenesin and 93-98 parts of purified water.
2. The repairing moistening mask containing carboxylated chitosan according to claim 1, wherein: the facial mask essence is prepared from the following raw materials in parts by weight: 0.3 part of carboxylated chitosan, 0.18 part of sodium hyaluronate, 0.02 part of enzyme-digested oligomeric sodium hyaluronate, 0.4 part of sodium alginate, 0.3 part of ceramide, 2 parts of glycerol, 0.3 part of butanediol, 0.3 part of phenoxyethanol, 0.03 part of ethylhexyl glycerol, 0.1 part of chlorphenesin and 96 parts of purified water.
3. The repairing moistening mask containing carboxylated chitosan according to claim 1, wherein: 20-30 ml of the facial mask essence is adsorbed on each piece of facial mask cloth.
4. The repairing moistening mask containing carboxylated chitosan according to claim 1, wherein: the facial mask membrane cloth is a copper ammonia fiber membrane cloth.
5. The repairing moistening mask containing carboxylated chitosan according to claim 1, wherein: the facial mask essence also comprises allantoin in 0.1-0.4 parts by weight.
6. A method for preparing a repairing and nourishing facial mask containing carboxylated chitosan according to any one of claims 1 to 5, which is characterized in that: comprises the following steps
(1) Weighing the raw material components in parts by weight for later use;
(2) weighing 8-10 parts of purified water, heating to 70-75 ℃, adding the weighed chlorphenesin, and stirring for 2-5 minutes until the mixture is completely dissolved to obtain liquid A;
(3) cooling the liquid A to 55-60 ℃, adding sodium hyaluronate and enzyme-digested oligomeric sodium hyaluronate, stirring, and uniformly mixing to obtain liquid B;
(4) cooling the liquid B to 20-25 ℃, sequentially adding the carboxylated chitosan, the ceramide and the sodium alginate, stirring and uniformly mixing to obtain a liquid C;
(5) passing the liquid C through a colloid mill, and washing the colloid mill with 8-10 parts of purified water to obtain a liquid D;
(6) adding glycerol, butanediol, phenoxyethanol, ethylhexyl glycerol and the rest purified water into the liquid D, stirring while adding, mixing uniformly to obtain a liquid E, standing, and degassing;
(7) standing and degassing the liquid E, and filtering through a layer of filter cloth with 300 meshes to obtain mask essence;
(8) transferring the facial mask purifying solution to a charging barrel of a filling machine, adjusting the filling amount to be 20-30 ml, starting filling into facial mask bags with facial mask cloth, and packaging to obtain the product.
7. The method for preparing the repairing moistening mask containing the carboxylated chitosan according to claim 6, wherein the steps of: the static degassing of the step (6) has a static time of 85-95 min.
8. The method for preparing the repairing moistening mask containing the carboxylated chitosan according to claim 6, wherein the steps of: and (3) adding the allantoin in the step (4), namely adding the carboxylated chitosan, the ceramide, the sodium alginate and the allantoin in sequence when the liquid B is cooled to 20-25 ℃, stirring and uniformly mixing to obtain a liquid C.
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