CN112807268B

CN112807268B - Non-greasy make-up and food-homologous aloe gel derived from raw juice and preparation method thereof

Info

Publication number: CN112807268B
Application number: CN202110059318.7A
Authority: CN
Inventors: 郑宇强; 陆伟; 熊菲菲; 李�杰; 郁新弟; 王鹏泽; 王彩霞; 马云龙; 贾福怀
Original assignee: Ningbo Yufangtang Biotechnology Co ltd
Current assignee: Ningbo Yufangtang Biotechnology Co ltd
Priority date: 2021-01-18
Filing date: 2021-01-18
Publication date: 2022-06-03
Anticipated expiration: 2041-01-18
Also published as: CN112807268A

Abstract

The invention discloses a non-sticky greasy make-up and edible homologous aloe gel derived from raw juice, which is characterized by comprising the following components: the skin care cream comprises polydecamaric acid/tetradecanedioic acid polyglycerol ester, diglycerol sesquicaprylate, inulin, potassium glycyrrhetate, epsilon-polylysine, citric acid, menthol, konjac gum powder, 1 wt% nano retinal dispersion, recombinant collagen wrinkle-removing peptide, erythritol and desensitized aloe gel juice. The invention also discloses a preparation method of the non-greasy make-up and edible aloe gel. Compared with the prior art, the non-greasy make-up and edible aloe gel disclosed by the invention has the effects of moisturizing, diminishing inflammation, resisting allergy, dispelling itch and the like, and can eliminate greasy skin feeling of the aloe gel.

Description

Non-greasy make-up and food-homologous aloe gel derived from raw juice and preparation method thereof

Technical Field

The invention relates to the technical field of daily chemical maintenance, in particular to a non-sticky greasy make-up and edible homologous aloe gel derived from raw juice and a preparation method thereof.

Background

The pure natural aloe gel is gel obtained by cleaning, disinfecting and peeling fresh leaves of aloe for more than two years and then taking out juice, and is pursued with the upgrade of skin care ideas of people in recent years, mainly because the natural aloe gel has the following effects and effects:

(1) the aloe gel has the functions of inhibiting the reproduction of acne bacillus, diminishing inflammation and sterilizing, regulating the secretion of sebum, moistening skin, promoting local metabolism, preventing skin keratinization, inhibiting inflammation on the acne, draining secretion, reducing or avoiding scars, astringing wounds, promoting cell regeneration and lightening scars;

(2) promoting wound healing-Aloe gel has effects of calming, diminishing inflammation, sterilizing, and stopping bleeding, such as skin accidental abrasion, laceration, puncture, cut, contusion, crush injury, sprain, scald and burn etc., and can be applied with a layer of Aloe gel after cleaning skin gently for sterilizing, diminishing inflammation, relieving pain, and healing wound;

(3) itching-dry air in autumn and winter, the skin is prone to dehydration, and skin itching can be caused by the moisture content in the epidermis being lower than the necessary content. The aloe gel has excellent moisturizing effect, can be mixed with cells to deeply moisturize and repair the damage caused by dry skin, and has obvious relieving effect on the symptoms of dry pruritus;

(4) the aloe gel has the effects of inhibiting bacteria and diminishing inflammation, can neutralize cytotoxin causing inflammation, kill pathogenic bacteria such as staphylococcus and beta hemolytic streptococcus, and has good anti-inflammatory effect on pustule sore, folliculitis, paronychia, stomatitis, lip ulcer, toothache and the like;

(5) the aloe gel is rich in nutrients for astringing skin and activating cell activity, so that the skin moistening and whitening effects are satisfactory. For example, aloin, anthraquinone and cinnamate contained in Aloe have effect in absorbing ultraviolet, and can be used for preventing sunburn. Amino acids and organic acids contained in Aloe vera gel can inhibit tyrosinase activity and inhibit melanin formation;

(6) detoxification-the detoxification effect of aloe vera gel an ancient formulation was used. Aloe has strong basicity, and can neutralize acidic toxin produced by pathogenic bacteria, and relieve inflammation and remove toxic substances;

(7) hair care-aloe vera gel has a nursing effect on human hair and reduces dandruff, which has been already confirmed by people in the southern Fujian region;

(8) promoting cell regeneration-Aloe gel has strong repair ability of new cell accumulation from bottom to top on damaged part of tissue;

(9) the prickly heat-prickly heat treatment is caused by inflammation of tissues around sweat pores due to high ambient temperature and humidity and unsmooth sweat excretion, and the aloe gel has good antibacterial and anti-inflammatory effects and is useful for treating the prickly heat;

(10) relieving solar dermatitis-solar dermatitis occurs in the area exposed to sunlight. Mild erythema in mild cases, edematous erythema in moderate cases, clear borders, local pain and discomfort, and blisters and bullae in severe cases. The aloe gel has good bactericidal effect, anti-inflammatory effect and analgesic effect, and can effectively relieve solar dermatitis.

(11) The itching-relieving and inflammation-diminishing effects of mosquito bites and insect bites are caused by the fact that insects force bacteria or viruses to invade the skin to infect the skin, and aloe has the outstanding effects of sterilizing, diminishing inflammation and neutralizing cytotoxin, can effectively kill pathogenic bacteria, relieve pain and promote wound healing, so that the effect on the diseases is obvious.

Because of the numerous medical cosmetic and health-care functions of natural aloe vera gel, it is creditably entitled "all-purpose gel".

The artificial blending type aloe gel with the appearance extremely similar to that of the natural aloe gel is successfully developed in the industry by the inspiration of the pleasant appearance of the natural aloe gel and the overcoming of the defects of stability and the like, and certain core functions can be artificially adjusted and occupy a considerable market share. The aloe gel takes natural aloe vera dry powder as a base material, synthesizes high polymer thickening, enhances the anticorrosion by chemical preservatives, takes a plurality of herb extracts as concepts, integrates the latest achievements (such as whitening wrinkle-removing peptide, plant sheep placenta, nano gold and the like) of modern bioengineering into universal aloe gel, has thousands of varieties, and wins the joy of vast young consumers.

However, the world graduation has no universal property, and the aloe gel of Yaya 'universal glue' is no exception. The natural aloe raw juice gel which is not processed at all has allergy risk, a part of efficacies of the aloe juice which is processed by impurity removal and desensitization are greatly reduced, and certain aloe raw material powder loses most efficacies due to the limitation of a drying process and the content of active ingredients is not ideal, so that the aloe gel prepared only can rely on a large amount of synthetic additives to enhance the effects. In fact, the universal natural aloe gel which can be commercialized and covers all the effects is poor in market.

Moreover, both the pure natural aloe juice gel and the artificially prepared aloe gel can generate unpleasant sticky feeling when being applied to the skin surface of a human body and rubbed to be quick-drying, and the technical field has been for many years, but the viscosity reduction effect cannot be satisfied by consumers. The following may be attributed to the following:

(1) the natural aloe juice gel has the inherent property. The obtained product of natural aloe leaf can be divided into two parts, one part is yellow juice exuded from the cut of the leaf, and the other part is gel left after the yellow juice is completely exuded. The former mainly contains anthraquinone and its glycoside, naphthalenone, resin and organic acid; anthraquinones are the main components in the exudate of aloe leaves, and account for about 9% to 30% of the dried material of the exudate. The substances have a plurality of types, have extremely high viscosity when being dried quickly, and are easy to be oxidized to increase the sticky feeling; the latter mainly contains saccharides (monosaccharide, polysaccharide and polymer), protein, calcium oxalate, fiber and the like, and has stronger stickiness when being half-dried;

(2) the problem of artificial compounding aloe gel. Because the desensitized aloe powder is used as a raw material and contains more saccharides (monosaccharides, polysaccharides and polymers) with strong viscosity, proteins and the like, in addition, a considerable amount of synthetic high molecular polymers are added for increasing the consistency, and the superposition results cause extremely uncomfortable sticky feeling when being half-dry and even stick to skin;

(3) compatibility problem. The whole face pursues the efficacy of the aloe gel, namely the all-purpose gel, adds natural functional components, and deliberately shows the transparent and beautiful appearance similar to the natural aloe gel, so that the finished product has poor durability and storage property (suspected of unexpected phenomena such as oxidation, hydrolysis, Maillard reaction, polycondensation and the like), and most of the metamorphic products are sticky substances.

Disclosure of Invention

The first technical problem to be solved by the invention is to provide a greasiness-free make-up and edible homologous aloe gel derived from raw juice aiming at the current situation of the prior art, which has the effects of moisturizing, diminishing inflammation, resisting allergy, dispelling itch and the like, and can eliminate the greasy skin feel of the aloe gel.

The second technical problem to be solved by the invention is to provide the preparation method of the non-greasy make-up edible homologous aloe gel, which is convenient to operate, free of complex equipment and environment-friendly.

The technical scheme adopted by the invention for solving the first technical problem is as follows: the greasy-free make-up and edible homologous aloe gel derived from the raw juice is characterized by comprising the following components in parts by mass:

the above components are selected from food grade materials which can be used in cosmetics, and the components themselves or each group of the components are derived from natural materials and can be decomposed into natural products.

Wherein the diglycerol eicosanedioate/tetradecanedioate is a main material for eliminating sticky skin feel, preferably a product of Japan Kogyo, INCI is polyglycerol-10 eicosadipate/tetradecanedioate, and trade name is Neosol-aqua;

the dimeric glyceryl sesquicaprylate is food-grade odorless, preferably a product of Yinmei United technology limited company, model UN-154, of Foshan;

the epsilon-polylysine is cationic polymerization polypeptide which is used as a food preservative and consists of 25-30 lysine residues, the polymerization degree is higher than decapeptide, the molecular weight is 3600-4300, and the epsilon-polylysine is preferably a product of Zhengzhou Benafer bioengineering GmbH.

The inulin is edible chicory root extract, is colorless and transparent after being dissolved in water, is preferably a product of Xianting company of France, and is named as NATULIN NC 100;

the potassium glycyrrhetate is an edible licorice extract, the content of the potassium glycyrrhetate is more than 98 percent, and the aqueous solution is colorless and transparent;

the 1 wt% nano retinal dispersion is: the medical phospholipid inclusion body with food-grade retinene is a nano-grade dispersion liquid, consists of retinene, food-grade ascorbic acid, caprylic/capric glyceride (GTCC, food grade), edible phospholipid, edible glycerol and water, is dispersed in the water to be in a yellowish transparent state, and is preferably selected from a product of Purui biological medicine technology Limited company under the name of Nanoactive RAL;

the recombinant COLLAGEN wrinkle-removing peptide is a compound consisting of SOLUBLE COLLAGEN (SOLUBLE COLLAGEN) from fermentation sources, FIBRONECTIN (FIBRONECTIN), ELASTIN (ELASTIN), sodium Hyaluronate (HA), sodium polyglutamate (r-PGA), ACETYL HEXAPEPTIDE (ACETYL HEXAPEPTIDE-8), glycerol and water, and is preferably a liquid product (without 1, 2-hexanediol and needing refrigeration) with a specific specification from the research center of recombinant human COLLAGEN engineering in Jiangsu province (Richcrystal COLLAGEN wrinkle-removing peptide (GAF1500) of Jiangsu mountain Confucius, Jiangsu province);

the erythritol, the citric acid and the menthol are more than 99% of food-grade or pharmaceutical-grade products;

the konjac gum powder series cosmetic and food-grade white powder has the viscosity of more than or equal to 36000mPa.s (NDJ-1 type rotational viscometer, No. 4 rotor, 12r/min and 30 ℃), and is preferably a Hubei uniform konjac biotech product manufactured by the company Limited;

the desensitized aloe gel juice is a gel obtained by peeling aloe vera and taking out juice, and is a pure natural raw juice obtained by a high tech desensitization process, is colorless and transparent, needs refrigeration, and is preferably a product of Yunnan Wanlv biological products GmbH.

The pH value of the non-sticky cosmetic and edible homologous aloe gel is 6.0-6.5.

The technical scheme adopted by the invention for solving the second technical problem is as follows: the preparation method of the non-greasy make-up and edible aloe gel is characterized by comprising the following steps:

(1) the pre-batching process comprises the following steps:

under the condition of stirring, putting potassium glycyrrhetate into the desensitized aloe gel juice which accounts for 1/8 of the total mass of the desensitized aloe gel juice, heating to 50-60 ℃, and dissolving for 0.5-1 hour until the system is completely transparent to obtain a material A;

under the condition of stirring, adding citric acid into the desensitized aloe gel juice which accounts for 1/8 of the total mass of the desensitized aloe gel juice, heating to 50-60 ℃, and dissolving for 0.5-1 hour until the system is completely transparent to obtain a material B;

under the condition of stirring, adding epsilon-polylysine into an aloe juice which accounts for 1/8 of the total mass of the desensitized aloe gel juice, heating to 70-80 ℃, dissolving for 0.5-1 hour until the system is completely transparent, and cooling to 40-45 ℃ to obtain a material C;

under the condition of stirring, controlling the temperature to be 45 ℃, adding the material B into the material A in batches within 0.5-1 hour, then supplementing and stirring for ten-fifteen minutes, completely mixing the mixture, adding the material C into the mixture in batches within 0.5-1 hour, controlling the temperature to be 55-60 ℃, supplementing and stirring for 1 hour until the system is completely transparent, cooling to 45 ℃ and preparing the solution D for later use;

under the condition of stirring, controlling the temperature to be 50-60 ℃, scattering the inulin and the konjac glucomannan powder material into the aloe juice which accounts for 1/2 of the total mass of the desensitized aloe gel juice in batches within 0.5-1 hour, heating to 50-60 ℃, and dissolving for 2-3 hours until the system is completely transparent to obtain a material E;

under the stirring condition, controlling the temperature to be 50-60 ℃, putting erythritol, didecanedioic acid/tetradecanedioic acid polyglycerol ester and diglyceride sesquicaprylate into an aloe juice accounting for 1/8 of the total mass of the desensitized aloe gel juice, heating to 50-60 ℃, dissolving for 0.5-1 hour until the system is completely transparent, then cooling to 40-45 ℃, adding menthol to dissolve for 0.5-1 hour until the system is completely homogeneous, and obtaining a material F;

(2) blending process:

under the stirring condition, controlling the temperature to be 55-60 ℃, slowly adding the material D into the material E in batches within 0.5-1 hour, supplementing and stirring for 1-2 hours until the system is in a light-transmitting homogeneous state, then cooling to 45 ℃, adding the material F within 0.5-1 hour, supplementing and stirring for 1 hour until the system is in the light-transmitting homogeneous state, the consistency is high, and the gelation phenomenon appears;

(3) the synergy process comprises the following steps:

and (3) under the stirring condition, controlling the temperature to be 45-48 ℃, adding 1 wt% of nano retinal dispersion and recombinant collagen wrinkle-removing peptide into the material obtained in the process (2), supplementing and stirring for 0.5-1 hour until the system is in a light-transmitting homogeneous high-viscosity state, and aging for 20-30 hours at room temperature to obtain the required greasiness-free make-up and edible homologous aloe gel.

Compared with the prior art, the invention has the advantages that:

(1) the invention finds a docosane diacid/tetradecanedioic acid polyglycerol ester/inulin/epsilon-polylysine smoothing system, creatively solves the long-standing problem that the aloe which puzzles the industry for a long time generates unpleasant sticky feeling when being smeared on the surface of the skin of a human body and rubbed to be quick-drying, and creatively improves the refreshing skin feeling of aloe gel series products; the reason is that the optimal gold proportion of the three components is explored, and the new application of the raw materials is discovered, and the detailed description is as follows:

the didecanedioic acid/tetradecanedioic acid polyglycerol esters represented by didecanedioic acid/tetradecanedioic acid polyglycerol-10 esters, also called water-soluble ester oil, are originally used as additives for increasing the surface conductivity of skin, and because the higher the conductivity of the skin is, the better the moisture retention of stratum corneum is, the substances accepted in the industry belong to stratum corneum long-acting moisturizing agents; the inventor finds that the substances can not only reduce the sticky feeling of cream, but also eliminate the aversive sticky and sticky skin feeling of aqueous gel consisting of a large amount of high-molecular polymers when the aqueous gel is semi-dry, and can also obviously improve the uncomfortable experience of adhesion of polyhydric alcohol substances such as glycerin and the like to skin, and when the pH value of a system reaches 6-6.5, the skin becomes smooth and quick like silicone oil; the ester formed by the diglyceride and the polyglycerol with abundant cyclic structures is of a staggered and complex cage structure, and after the ester is spread on skin, a great amount of water-locking polyester layers which increase electric conductivity, weaken static electricity and are super-smooth are covered on the outermost layer, so that the viscous effect of glue substances is obviously weakened, and the refreshing property of the aloe glue during semi-drying is greatly improved;

inulin, which is originally used in health food, has the effects of reducing blood sugar, relieving diabetes symptoms, enhancing digestion and defecation functions, promoting metabolism, removing eczema, improving vascular disorder, losing weight and the like; the inulin is a chicory root extract screened from a plurality of varieties, belongs to a non-ionic fructose polymer, but surprisingly finds that certain polymeric fragments of the inulin can be intercepted, can be used in resident hair conditioner to replace silicone oil to be used as a smoothing agent, and has the functions of resisting static electricity and resisting the stickiness of water gel;

the epsilon-polylysine with the molecular weight of 3600-4300 is already common knowledge as a new cosmetic and food homologous preservative, but the cationic polymerized polypeptide consisting of 25-30 lysine residues is a new discovery of the inventor when being used as a slip synergist in aqueous polymer gel, which is mainly caused by the fact that the added epsilon-polylysine has excellent antistatic and friction reducing effects and enhances the cationic electrical property of the polyglyceryl eicosanedioate/tetradecanedioate;

in a word, the synergic drag reduction and slip enhancement system of the eicosanedioic acid/the tetradecanedioic acid polyglycerol ester/the inulin/the polylysine can be concluded that hydrophilic components which are easy to cause sticky skin feeling in a polyglycerol cage-shaped structure with polyester characteristics are filled with water-soluble inulin with a smooth silicone oil-like function, and under the coordination of a cationic electric substance epsilon-polylysine charge-imparting agent, the negative charge sticky effect on the surface of the skin is greatly weakened, the wear resistance of the slip oil is enhanced, and the skin is separated by a slip cage-shaped polyester layer during smearing, so that the adhesiveness of a synthetic high molecular polymer and certain natural colloids is greatly weakened;

(2) the invention originally finds that the strong and brisk cosmetic and food homologous thickener-konjac gum can be thickened in a weak cation (polylysine) system, so that the compatibility of various active components is obviously improved, and the final system is characterized by transparent microemulsion;

(3) according to the invention, potassium glycyrrhetate as an anti-inflammatory and bacteriostatic main material with anions and polylysine as an antiseptic and smoothing agent with cations are combined in the same system (without flocculation precipitation) in a skillful frying manner, namely, the negative charge of glycyrrhetate is shielded by creating an environment with a pH value of 6.0-6.5, and the transparency of an aloe gel final product is good by means of solubilization and dispersion of polyglycerol ester and the suspension action of konjac gum;

(4) the invention finds a novel cosmetic and food homologous preservative epsilon-polylysine/diglycerol sesquicaprylate composition, skillfully uses the preservative synergistic property of caprylate, and easily solves the long-term storage preservative problem of the natural aloe gel containing various easily-deteriorated high-nutrition components (such as protein peptide, vitamin, amino acid, phospholipid and the like);

(5) by applying the high-tech achievement of foreward defense, the nano retinal dispersion liquid and the recombinant collagen wrinkle-removing peptide are blended, and the refreshing agent menthol (erythritol solubilization and synergism) is combined, so that the edible aloe gel disclosed by the invention has the effects of whitening, skin tendering, acne removal, speckle reduction, inflammation diminishing, relieving, itching relieving, swelling subsiding, moisture retention and the like, and can be similar to the effect of a 'universal gel' of natural aloe;

the innovative technical scheme creates unexpected effects for products, namely, creatively finds a synergic drag-reduction and slip-increase system of the eicosanedioic acid/the tetradecanedioic acid polyglycerol ester/the inulin/the polylysine, greatly weakens the adhesive property of the synthetic high molecular polymer and certain natural colloids, successfully solves the long-standing problem that the aloe which puzzles the industry for a long time generates unpleasant adhesive feeling when being applied to the surface of the skin of a human body and rubbed to be quick-drying, and simultaneously integrates the high-tech achievements of forever to create multifunctional effects, so that the aloe gel really becomes the 'all-purpose adhesive'.

Detailed Description

The present invention will be described in further detail with reference to examples.

Example 1:

(1) the pre-batching process comprises the following steps:

in a 200-liter high-quality stainless steel batching pot, under the stirring condition, the rotating speed is controlled to be 100rpm, 5 kg of potassium glycyrrhetate is put into 55.03 kg of aloe juice, the temperature is raised to 55 ℃, and the potassium glycyrrhetate is dissolved for 0.6 hour until the system is completely transparent, so that material A is obtained;

in a 100-liter high-quality stainless steel batching pot, under the stirring condition, the rotating speed is controlled to be 100rpm, 4 kg of citric acid is put into 55.03 kg of aloe juice, the temperature is raised to 52 ℃, and the citric acid is dissolved for 0.5 hour until the system is completely transparent, thus obtaining material B;

in a 100-liter high-quality stainless steel batching pot, under the stirring condition, the rotating speed is controlled to be 100rpm, 5 kg of epsilon-polylysine is put into 55.03 kg of aloe juice, the temperature is raised to 72 ℃, the dissolution is carried out for 0.5 hour until the system is completely transparent, and the temperature is cooled to 45 ℃ to obtain a material C;

under the stirring condition, controlling the temperature to be 45 ℃, adding the material B into the material A in batches within half an hour, then supplementing and stirring for fifteen minutes until the mixture is completely transparent, adding the material C into the mixture in batches within half an hour, controlling the temperature to be 60 ℃, supplementing and stirring for 1 hour until the system is completely transparent, cooling to be 45 ℃, and calling liquid D for later use;

in a 500-liter high-quality stainless steel batching pot, under the stirring condition, the rotating speed is controlled to be 80rpm, the temperature is controlled to be 58 ℃, 20 kg of inulin and 6 kg of konjac glucomannan powder are scattered into 220.15 kg of aloe juice in batches within 1 hour, the temperature is increased to 55 ℃, and the inulin and the konjac glucomannan powder are dissolved for 2.5 hours until the system is completely transparent, so that material E is obtained;

in a 100-cubic-liter high-quality stainless steel mixing pot, under the stirring condition, the rotating speed is controlled to be 100rpm, the temperature is controlled to be 56 ℃, 15 kg of erythritol, 15 kg of polyglycerol-10 eicosadidate/tetradecadidate and 10 kg of diglycerol sesquicaprylate are put into 55.03 kg of aloe juice, the temperature is raised to 60 ℃, the mixture is dissolved for 1 hour until the system is completely transparent, then the temperature is lowered to 42 ℃, 0.75 kg of menthol is added for dissolving for 1 hour until the system is completely homogeneous, and a material F is obtained;

(2) blending process

Under the condition of stirring, controlling the rotating speed at 100rpm, controlling the temperature at 58 ℃, slowly adding the material D into the material E in batches within 1 hour, supplementing and stirring for 2 hours until the system is in a light-transmitting homogeneous state, then cooling to 45 ℃, adding the material F within half an hour, supplementing and stirring for 1 hour until the system is in the light-transmitting homogeneous state, the consistency is high, and the gelation phenomenon appears;

(3) synergistic process

And (3) under the stirring condition, controlling the temperature to be 45 ℃, adding 9 kg of 1 wt% of nano retinal dispersion and 10 kg of recombinant collagen wrinkle-removing peptide into the material obtained in the process (2), supplementing and stirring for 1 hour until the system is in a light-transmitting homogeneous high-viscosity state, aging for 24 hours at room temperature, and measuring the pH value to be 6.5 to obtain the required non-sticky greasy make-up edible homologous aloe gel.

Example 2:

(1) the pre-batching process comprises the following steps:

in a 200-liter high-quality stainless steel batching pot, under the stirring condition, the rotating speed is controlled to be 100rpm, 1 kg of potassium glycyrrhetate is put into 55.2 kg of aloe juice, the temperature is raised to 55 ℃, and the potassium glycyrrhetate is dissolved for 0.5 hour until the system is completely transparent, so that material A is obtained;

in a 100-liter high-quality stainless steel batching pot, under the stirring condition, the rotating speed is controlled to be 100rpm, 3 kg of citric acid is put into 55.2 kg of aloe juice, the temperature is raised to 52 ℃, and the citric acid is dissolved for 0.8 hour until the system is completely transparent, thus obtaining material B;

in a 100-liter high-quality stainless steel batching pot, under the stirring condition, the rotating speed is controlled to be 100rpm, 2 kg of epsilon-polylysine is put into 55.2 kg of aloe juice, the temperature is raised to 72 ℃, the dissolution is carried out for 0.6 hour until the system is completely transparent, and the temperature is cooled to 45 ℃ to obtain a material C;

under the condition of stirring, controlling the temperature to be 45 ℃, adding the material B into the material A in batches within half an hour, then supplementing and stirring for fifteen minutes until the mixture is completely transparent, adding the material C into the mixture in batches within 0.8 hour, controlling the temperature to be 60 ℃, supplementing and stirring for 1 hour until the system is completely transparent, cooling to be 45 ℃, and calling as liquid D for later use;

in a 500-liter high-quality stainless steel batching pot, under the stirring condition, the rotating speed is controlled to be 80rpm, the temperature is controlled to be 58 ℃, 10 kg of inulin and 5 kg of konjac glucomannan powder are scattered into 220.75 kg of aloe juice in batches within 0.8 hour, the temperature is raised to 60 ℃, and the inulin and the konjac glucomannan powder are dissolved for 3 hours until the system is completely transparent, so that material E is obtained;

in a 100-cubic-liter high-quality stainless steel mixing pot, under the stirring condition, the rotating speed is controlled to be 100rpm, the temperature is controlled to be 56 ℃, 10 kg of erythritol, 5 kg of polyglycerol-10 eicosadidate/tetradecadidate and 5 kg of diglycerol sesquicaprylate are put into 55.2 aloe juice, the temperature is raised to 60 ℃, the dissolution is carried out for 1 hour until the system is completely transparent, then the temperature is reduced to 42 ℃, 0.5 kg of menthol is added for dissolution for 0.8 hour until the system is completely homogeneous, and a material F is obtained;

(2) blending process

Under the condition of stirring, controlling the rotating speed at 100rpm, controlling the temperature at 58 ℃, slowly adding the material D into the material E in batches within 0.8 hour, supplementing and stirring for 2 hours until the system is in a light-transmitting homogeneous state, then cooling to 45 ℃, adding the material F within half an hour, supplementing and stirring for 1.8 hours until the system is in the light-transmitting homogeneous state, the consistency is high, and the gelation phenomenon appears;

(3) synergistic process

And (3) under the stirring condition, controlling the temperature to be 45 ℃, adding 5 kg of 1 wt% of nano retinal dispersion and 12 kg of recombinant collagen wrinkle-removing peptide into the material obtained in the process (2), supplementing and stirring for 1 hour until the system is in a light-transmitting homogeneous high-viscosity state, aging for 24 hours at room temperature, and measuring the pH value to be 6.5 to obtain the required non-sticky greasy make-up edible homologous aloe gel.

Example 3:

(1) the pre-batching process comprises the following steps:

in a 200-liter high-quality stainless steel batching pot, under the stirring condition, the rotating speed is controlled to be 100rpm, 2 kg of potassium glycyrrhetate is put into 49.8 kg of aloe juice, the temperature is raised to 50 ℃, and the potassium glycyrrhetate is dissolved for 0.8 hour until the system is completely transparent, thus obtaining material A;

in a 100-liter high-quality stainless steel batching pot, under the stirring condition, the rotating speed is controlled to be 100rpm, 5 kg of citric acid is put into 49.8 kg of aloe juice, the temperature is raised to 55 ℃, and the citric acid is dissolved for 0.8 hour until the system is completely transparent, thus obtaining material B;

in a 100-liter high-quality stainless steel batching pot, under the stirring condition, the rotating speed is controlled to be 100rpm, 4 kg of epsilon-polylysine is put into 49.8 kg of aloe juice, the temperature is raised to 78 ℃, the dissolution is carried out for 0.8 hour until the system is completely transparent, and the temperature is cooled to 42 ℃ to obtain a material C;

under the condition of stirring, controlling the temperature to be 45 ℃, adding the material B into the material A in batches within 0.8 hour, then supplementing and stirring for twelve minutes, enabling the mixture to be completely transparent, adding the material C into the mixture in batches within 0.6 hour, controlling the temperature to be 55 ℃, supplementing and stirring for 1 hour until the system is completely transparent, cooling to be 45 ℃, and calling as liquid D for later use;

in a 500-liter high-quality stainless steel batching pot, under the stirring condition, the rotating speed is controlled to be 80rpm, the temperature is controlled to be 60 ℃, 25 kg of inulin and 8 kg of konjac glucomannan powder are sprinkled into 199.2 kg of aloe juice in batches within 0.8 hour, the temperature is raised to 59 ℃, and the inulin and 8 kg of konjac glucomannan powder are dissolved for 3 hours until the system is completely transparent, so that material E is obtained;

in a 100-cubic-liter high-quality stainless steel mixing pot, under the stirring condition, the rotating speed is controlled to be 100rpm, the temperature is controlled to be 54 ℃, 12 kg of erythritol, 12 kg of polyglycerol-10 eicosadidate/tetradecadidate and 8 kg of diglycerol sesquicaprylate are put into 49.8 kg of aloe juice, the temperature is raised to 55 ℃, the mixture is dissolved for 0.6 hour until the system is completely transparent, then the temperature is lowered to 43 ℃, 0.6 kg of menthol is added, the mixture is dissolved for 0.8 hour until the system is completely homogeneous, and a material F is obtained;

(2) blending process

Under the condition of stirring, controlling the rotating speed at 100rpm, controlling the temperature at 57 ℃, slowly adding the material D into the material E in batches within 0.8 hour, supplementing and stirring for 1 hour until the system is in a light-transmitting homogeneous state, then cooling to 45 ℃, adding the material F within 1 hour, supplementing and stirring for 1 hour until the system is in the light-transmitting homogeneous state, the consistency is high, and the gelation phenomenon appears;

(3) synergistic process

And (3) under the stirring condition, controlling the temperature to be 46 ℃, adding 10 kg of 1 wt% of nano retinal dispersion and 15 kg of recombinant collagen wrinkle-removing peptide into the material obtained in the process (2), supplementing and stirring for 0.5 hour until the system is in a light-transmitting homogeneous high-viscosity state, aging for 28 hours at room temperature, and measuring the pH value to be 6.5 to obtain the required non-sticky greasy make-up edible homologous aloe gel.

The cosmetic and edible aloe vera gel prepared in example 1 was subjected to performance testing (the test data for examples 2 and 3 are similar to example 1) using the following specific test items:

skin elasticity improvement/wrinkle resistance/pore shrinkage/moisture retention indexes of the cosmetic and edible aloe gel prepared in example 1 were measured using a measuring instrument (VISIA-CR Corneometer CM825 current meter MPA585 Primos), and are detailed in table 1.

Table 1:

as can be seen from table 1:

(1) this experimenter crowd (24 people), after 30 minutes of single use above-mentioned cosmetic and edible homology aloe glue, promote elasticity immediately, the test result shows: compared with the cosmetic and edible aloe gel sample before use after being used for 30 minutes once, the elasticity of the skin in a test area is obviously increased (P <0.001), which indicates that the test sample has the effect of instantly improving the elasticity;

(2) the test results of the test subject population (24 persons) after using the cosmetic and edible homologous aloe gel for 2 weeks show that: after the test sample is used for 2 weeks, compared with the test sample before the test sample is used, the number, the volume, the area and the length of the fishtail lines in the test area are obviously reduced (P <0.001, P-0.001, P <0.001, P <0.001), and the test sample has 2-week fishtail line reducing effect;

compared with the skin stratum corneum water content in a test area before use after the cosmetic and edible homologous aloe gel is used for testing a sample for 2 weeks, the moisture content of the skin stratum corneum in the test area is remarkably increased (P is less than 0.001), and the test sample has the moisturizing effect for 2 weeks;

compared with the skin elasticity in the area before use after the cosmetic and edible homologous aloe gel is used for testing the sample for 2 weeks, the elasticity of the skin in the tested area is obviously increased (P <0.001), which indicates that the tested sample has the elasticity improving effect for 2 weeks;

(3) the test results of the test subject population (24 persons) after using the cosmetic-edible homologous aloe gel for 4 weeks show that: after the test sample is used for 4 weeks, compared with the test sample before the test sample is used, the number, the volume, the area and the length of the fishtail lines in the test area are obviously reduced (P <0.001, P <0.001, P <0.001, P <0.001), and the test sample has 4-week fishtail line relieving effect;

compared with the skin stratum corneum water content in the test area before use after 4 weeks by using the cosmetic and edible homologous aloe gel test sample, the water content of the skin stratum corneum in the test area is remarkably increased (P is less than 0.001), and the test sample has a moisturizing effect for 4 weeks;

compared with the cosmetic and edible homologous aloe gel before use after the test sample is used for 4 weeks, the elasticity of the skin in the test area is obviously increased (P <0.001), which indicates that the test sample has the effect of improving the elasticity for 4 weeks;

after 4 weeks of using the cosmetic and edible aloe gel test sample, compared with the cosmetic and edible aloe gel test sample before use, the pore area ratio in the test area is obviously reduced (P is 0.031), and the test sample has the 4-week pore refining effect.

The basic skin care properties of the cosmetic and edible aloe gel prepared in example 1 were determined in comparison to a commercially available typical aloe gel, as detailed in table 2.

Table 2:

as can be seen from table 2: the cosmetic and edible homologous aloe gel disclosed by the invention is more excellent in skin care core indexes such as pH value, skin feel comfort, moisturizing effect and the like than the typical aloe gel on the market.

With reference to GBZ/T240.2-2011 chemical toxicology evaluation program and relevant steps of part 2 acute oral toxicity test of test method, the acute oral toxicity LD50 of the aloe gel prepared in example 1 on white rats is measured to be larger than 10700mg/kg, and the product series of the aloe gel is proved to be in an actual non-toxic level range, so that the aloe gel is indirectly proved to be accidentally mistaken for human bodies and is also proved to be harmless to health because the aloe gel is in the middle of human metabolism and the final product is in the non-toxic level range.

The mechanical data related to the combing property of the greasiness-free make-up edible homologous aloe gel prepared in the embodiment 1 of the invention and the commercial classical aloe gel after soaking and drying hair are tested by a tensile tester method, and the greasiness is indirectly estimated:

(1) overview

The tension tester is a tester specially used for hair combing performance evaluation, and simulates the action of combing hair by a person through a standard comb, a bundle of hair is combed and recorded by a terminal. When the comb passes through the hair fibers, it shows the force (unit: gf) loaded within a specified displacement (unit: mm) when it is pulled against the resistance of the hair. The stickiness of the aloe gel is indirectly estimated by detecting the index of the change of combing force of the hair tresses before and after soaking the sample.

(2) Materials and methods

(2.1) Main instruments and materials

A tension meter;

a constant temperature and humidity incubator;

a plurality of hair strands: length 50cm, weight about 16 g;

aloe vera gel: the non-greasy make-up edible homologous aloe gel of the invention and the commercial classical aloe gel are diluted by 10 times by water.

(2.2) Hair Strand Pre-treatment

Several tresses of the same length (50cm) and weight (about 16g) were prepared. Firstly, washing twice by using tap water of 40-C; then placing the hair bundle in a beaker filled with 5g of sodium dodecyl sulfate and 1000ml of water, heating to 80 ℃ and soaking; then placing the beaker in a constant temperature and humidity box at 45 ℃ for two hours; finally, the mixture is washed by tap water until no foam exists, and is naturally dried.

Treating an aloe gel sample: weighing 4g of aloe vera gel sample diluted 10 times with water, rubbing the aloe vera gel sample onto the treated tresses of hair to a uniform state, standing for 5 minutes, rinsing the tresses of hair with tap water, and blowing the tresses of hair with a natural wind blower for thirty minutes to be nearly dry.

(2.3) combing Property test

The dry combing property of the hair strands after the aloe gel infiltration treatment diluted 10 times with water was measured on a tensile tester.

Firstly, connecting a host power supply, turning on a computer, and preheating an instrument for more than half an hour;

collecting all the samples forming the test sample together, and marking each sample; opening software, creating a new sample, selecting a test method, and naming the new sample;

combing hair with a plastic comb, fixing a hair sample to be tested with a proper clamp, and naturally placing a hair bundle in the middle of the comb;

and fourthly, after the calibration and zero setting of the instrument are completed, starting to test the hair bundle, stretching the hair bundle at the speed of 300mm/min, displacing by 200ram, and taking the load value of displacement between 100 mm and 200 mm. In order to reduce the measurement error due to the different strands, the same strand was tested 5 times in duplicate and the average was taken (the program automatically recorded the data and calculated the average).

(3) Results and discussion

The test was conducted to examine the degree of influence of the non-greasy make-up homologous aloe gel prepared in example 1 of the present invention and the commercially available classical aloe gel on the combing property of hair, and the average load (gf) of the hair tresses treated with two types of aloe gel diluted 10 times with water was measured and recorded by a tensile tester to compare the combing force of dry hair, and the data results are detailed in table 3.

Table 3:

name of sample	Average load (gf)
		The invention relates to a non-greasy make-up and edible aloe gel	28.27335
Commercially available classic aloe vera gel	94.26578

As can be seen from table 3: after being soaked, the average load (gf) of the cosmetic food homologous aloe gel without greasy feeling on hair drying comb is obviously smaller than that of the commercial classical aloe gel, which indirectly shows that the product of the invention has less greasy feeling when being semi-dried.

Claims

1. The greasy-free make-up and edible homologous aloe gel derived from the raw juice is characterized by comprising the following components in parts by mass:

the epsilon-polylysine is cation polymerization polypeptide which is used as a food preservative and consists of 25-30 lysine residues, the polymerization degree is higher than that of decapeptide, and the molecular weight is 3600-4300.

2. The non-greasy cosmetic syngenic aloe vera gel according to claim 1, wherein: the polyglyceryl eicosanedioate/tetradecanedioate is manufactured by Nippon Kogyo, INCI is polyglyceryl-10 eicosadipate/tetradecanedioate, and Neosolve-AquaS is a trade name.

3. The non-slimy cosmetic syngenic aloe vera gel according to claim 1 wherein the inulin is a food chicory root extract.

4. The non-greasy cosmetic syngenic aloe vera gel according to claim 1, wherein: the potassium glycyrrhizinate is an edible licorice extract.

5. The non-greasy cosmetic syngenic aloe vera gel according to claim 1, wherein: the konjac powder is white powder which is a cosmetic and food grade, and the viscosity is more than or equal to 36000 mPa.s.

6. The non-greasy cosmetic syngenic aloe vera gel according to claim 1, wherein: the 1 wt% nano retinene dispersion is a medical food-grade retinene-compatible phospholipid inclusion body and is a nano dispersion.

7. The non-greasy cosmetic homologous aloe vera gel according to claim 1, wherein: the desensitized aloe gel juice is pure natural juice obtained by removing skin of aloe vera and taking out juice and performing desensitization process.

8. The non-greasy cosmetic syngenic aloe vera gel according to claim 1, wherein: the pH value of the non-greasy make-up and edible aloe gel is 6.0-6.5.

9. A method of preparing a non-greasy cosmetic syngenic aloe gel according to any of claims 1 to 8, characterized in that it comprises the following steps:

(1) the pre-batching process comprises the following steps:

under the condition of stirring, putting potassium glycyrrhetate into the desensitized aloe gel juice with the total mass of 1/8, heating to 50-60 ℃, and dissolving for 0.5-1 hour until the system is completely transparent to obtain a material A;

under the stirring condition, controlling the temperature to be 45 ℃, adding the material B into the material A in batches within 0.5-1 hour, then supplementing and stirring for ten-fifteen minutes, enabling the mixture to be completely transparent, adding the material C into the mixture in batches within 0.5-1 hour, controlling the temperature to be 55-60 ℃, supplementing and stirring for 1 hour until the system is completely transparent, cooling to be 45 ℃, and calling the solution D for later use;

under the condition of stirring, controlling the temperature to be 50-60 ℃, scattering inulin and konjac glucomannan powder into the aloe juice accounting for 1/2 of the total mass of the desensitized aloe gel juice in batches within 0.5-1 hour, heating to 50-60 ℃, and dissolving for 2-3 hours until the system is completely transparent to obtain a material E;

(2) blending process:

(3) the synergy process comprises the following steps:

and (3) under the stirring condition, controlling the temperature to be 45-48 ℃, adding 1 wt% of nano retinal dispersion and recombinant collagen wrinkle-removing peptide into the material obtained in the step (2), performing supplementary stirring for 0.5-1 hour until the system is in a light-transmitting homogeneous high-viscosity state, and aging for 20-30 hours at room temperature to obtain the required non-greasy make-up edible homologous aloe vera gel.