CN109394592A

CN109394592A - A kind of multiple-effect flesh bottom water of replenishing water and preserving moisture oil-control

Info

Publication number: CN109394592A
Application number: CN201811401146.1A
Authority: CN
Inventors: 喻敏; 罗曼琳
Original assignee: Medical Aesthetics Biotechnology (shanghai) Co Ltd
Current assignee: Medical Aesthetics Biotechnology (shanghai) Co Ltd
Priority date: 2018-11-22
Filing date: 2018-11-22
Publication date: 2019-03-01

Abstract

The invention discloses a kind of multiple-effect flesh bottom waters of replenishing water and preserving moisture oil-control, belong to cosmetic technical field, technical points include the component of following parts by weight: 50-90 parts of water, 3.4-50 parts of moisturizer, 0.1-5 parts of beta glucan, 0.02-2 parts of humic acid, 0.01-2 parts of mineral salt, and are releived 0.3-15 parts of agent.The present invention can not only reduce dry skin, peeling, or even play the generation of acne phenomenon by the replenishing water and preserving moisture and oil-control performance of raising facial skin；And the ability for resisting blue segment visible light and ultraviolet light to skin can also be improved.It is further advanced by and various mineral salt, humic acid, algae extract, hyaluronic acid is added, and the ingredients such as polypeptide, the skin conditions done in outer oil can be improved, various nutritional ingredients can be provided for skin surface cell, to help the reparation of barrier, prebiotics can also be provided for skin microbial simultaneously, the balance of skin biomembrane, the comprehensive maintenance action improved to facial skin are safeguarded with this.

Description

A kind of multiple-effect flesh bottom water of replenishing water and preserving moisture oil-control

Technical field

The invention belongs to cosmetic technical fields, more specifically, it relates to a kind of multiple-effect flesh bottom of replenishing water and preserving moisture oil-control Water.

Background technique

With the continuous promotion of economic fast development and living standards of the people, people increasingly focus on to human skin Maintenance.It shows according to statistics, most women any positions other always above body for the attention rate of face, face The classification that applies some make up includes that face cleaning product, facial mask, toner, essence, face cream, facial mask, BB frost, foundation cream and lip produce Product etc..

Female consumer can select after morning and evening progress skin cleaning, washed, it will usually think that facial skin is dry, Dry skin condition can further stimulate epidermis secretion grease and cause discomfort, or even mostly acne can be also crossed because of fat secretion The growth of acne, acne provides environment.

Most of women can spray some toners in face after completing to wash one's face at this time, excessively dry to alleviate face The case where occur, some alcohol components are only added in toner under normal circumstances, can be partly dissolved modification cutin planarization, The effect not protruded then for the oil-control maintenance etc. of skin；But the alcoholic content being added in some toners can also The phenomenon that stimulating skin, causing red swelling of the skin, or even play acne, therefore be also required to propose the new technical solution of one kind to solve State problem.

Summary of the invention

In view of the deficiencies of the prior art, the present invention intends to provide a kind of multiple-effect flesh bottom of replenishing water and preserving moisture oil-control Water can not only reduce dry skin, peeling, or even play acne by improving the replenishing water and preserving moisture and oil-control performance of facial skin The generation of phenomenon；And the ability for resisting blue segment visible light and ultraviolet light to skin can also be improved.

To achieve the above object, the present invention provides the following technical scheme that a kind of multiple-effect flesh bottom water of replenishing water and preserving moisture oil-control, Component including following parts by weight:

By using above-mentioned technical proposal, humic acid is the chief component of organic matter in natural water body, is mainly come Source is decomposition and low planktonic organism, the basic knot of humic acid of agron lower-molecular-weight component and water plant Structure is aromatic ring and alicyclic ring, and carboxyl, hydroxyl, carbonyl, quinonyl and methoxy functional group are connected on ring.Also just because of humic acid The influence of a variety of functional groups of complexity machine of molecular structure, just makes it with many physical and chemical properties, and make it have Good colloidality, dissolubility, ion exchangeable, adsorptivity, precipitability, complexing, oxidation-reduction quality and thermal stability Energy.Due to not containing halide in water used herein, the humic acid added at this time is able to ascend flesh bottom water sheet instead The good anti-oxidant and oil-control performance of body, while humic acid is in 280-400 nanometers of ultraviolet line segment and 400-450 nanometer There is obvious absorbability, so ultraviolet light and blue light can be stopped to a certain extent, thus effectively at blue light visible light section Improve the ability for resisting blue segment visible light and ultraviolet light of flesh bottom water.

And mineral salt is the mineralogical composition containing 70 various trace elements, such as selenium element, magnesium elements, Zn-ef ficiency, silicon member Element, calcium constituent and sodium element etc. can supplement various micro-element nutritions needed for facial skin cell, and enhancing cell is certainly Body vigor improves cell tolerance power, and can improve skin hydration power, is skin microbial to help to extend face's aging Prebiotics are provided, the balance of skin biomembrane is safeguarded with this.

The moisturizer of addition is then a kind of hydrophilic Emollient materials, in oil-in-water (o/w) type matrix and water-soluble base In can effectively prevent moisture evaporation and scatter and keep substance used in moisture of skin.According to national Indoor Air Quality standards It is required that: winter indoor air humidity standard is 30%~60%, and the environment that humidity index (relative humidity) is 50%~60% is most Sense is comfortable, and room temperature is at 24 degree or less.The best relative humidity that human body is comfortable on indoors is 49%~51%.When upper Moisturizer is stated in lower humidity range (relative humidity is between 20%-40%) also with the ability of certain combination water, energy It is enough that skin is given to supplement moisture content, at the same they can also by humic acid, mineral salt and beta glucan in flesh bottom water etc. at (i.e. skin is aqueous for the equilibrium state that makes skin maintain higher than normal water content of exchanging of moisture content point between surrounding air Amount is in 50%- 60%), thus play the role of mitigating dry skin, it is a large amount of fuel-displaced thus to further improve facial skin Phenomenon, to play good oil-control and moisture-keeping function.And agent of releiving can reduce skin allergy, redness and acne etc. The generation of phenomenon can not only mention so that flesh bottom water is safer when in use, while when interacting with other compositions The high replenishing water and preserving moisture and oil-control performance of facial skin；And free radical can also be removed, thus effective delay skin aging, Increase skin elasticity.

In addition, beta glucan is primarily referred to as avenabeta glucosan, molecular formula is (C₆H₁₀O₅)_n, its basic structure is A kind of macromolecule β-D gluco-pyranose units being formed by connecting by D glucose with β-(1,4) and β-(1,3) glycosidic bond without point Branch linear glutinous polysaccharide, the ratio of both glycosidic bonds substantially 7:3.Wherein, the β-Portugal in avenabeta glucosan and other sources is poly- Sugar compares, and has the ability of preferably water-soluble and percutaneous permeability and stronger absorption small molecule, at this time oat β-Portugal After glycan can adsorb the substances such as moisturizer and the lot of trace mineral element of small-molecular-weight (i.e. low molecular weight), and it will borrow The Cutaneous permeation of avenabeta glucosan itself is helped to act on the moisturizer and lot of trace mine of small-molecular-weight (i.e. low molecular weight) The penetrations skin inner layer such as matter-element element carries out deep moisture-keeping function, reduces a large amount of secretions of facial skin grease, thus Improve the moisturizing and oil-control performance to skin.In addition, avenabeta glucosan also has the ability of stronger absorption small molecule, It can be competed with protein and polyphenol is combined by hydrogen bond, hydrophobic interaction etc., forming polysaccharide polyphenol complex is skin More longlasting oxidation resistance is provided.

Thus the flesh bottom water obtained after being mixed together moisturizer, beta glucan, humic acid, mineral salt, agent of releiving with water The replenishing water and preserving moisture and oil-control performance of facial skin can be effectively improved, reduces dry skin, peeling, or even play the hair of acne phenomenon It is raw；In addition the ability that facial skin resists blue segment visible light and ultraviolet light can also be improved, synthesis is improved to facial skin Maintenance action.

The present invention is further arranged to: the moisturizer includes at least following a kind of:

By using above-mentioned technical proposal, butanediol, glycerol, 1,2- pentanediol and 1,2- hexylene glycol is common More alcohol compounds can be partly dissolved and modify cutin, improve its planarization.Secondly, the performance of keeping humidity of D-sorbite is sweeter Oil mitigates, and can replace glycerol, and have the effects that good moisture absorption, water conservation；Simultaneously it can also chelating metal ion, and it is simultaneous Has certain antiseptic property.In addition, Anjidew NL50, also known as pyrrolidones hydroxy acid sodium, it is that one kind is naturally present in human skin Moisturizer, be the main component in keratoderma.The water absorbing capacity of Anjidew NL50 is very high, and moisture content can be absorbed from air, It is suitable with the hygroscopicity of hyaluronic acid and strong more than moisturizer such as glycerol, propylene glycol, sorbierites.Itself be clear, colorless without Smelly saltish liquid, it can make moisture content and cell combination, catch the moisture content for being several times as much as own wt, to improve flesh The good water suction of bottom water and moistening effect.

In addition, Sodium Hyaluronate is that a kind of glycosaminoglycan of fermentable sources is natural compared with the moisturizer that other are common Polymer, its hygroscopic capacity highest under low relative humidity (relative humidity 33%), and in high relative humidity (relative humidity 75%) hygroscopic capacity under is minimum, this unique property, and positive adaptation skin is such as dry under Various Seasonal, varying environment humidity Dry winter and moist summer, the requirement to cosmetics moisture-keeping function.Thus using Sodium Hyaluronate and other polyol classes It closes the moisturizing ingredients such as object, sorbierite and pyrrolidones hydroxy acid sodium to be used cooperatively, so that the moisturizing of flesh bottom water and damping effect are most It is good.

The present invention is further arranged to: the agent of releiving, which includes at least, following one kind:

0.1-2 parts of dipotassium glycyrrhizinate；

0.1-2 parts of hydroxy phenylpropionyl amine benzoic acid.

By using above-mentioned technical proposal, dipotassium glycyrrhizinate has good anti-inflammatory, antiallergy, moisturizing and other effects, it can It to neutralize or reduce the noxious material of cosmetics, can also reduce, or even prevent certain cosmetics (such as concealing liquid, foundation cream The cosmetics such as liquid) allergic reaction.In addition, hydroxy phenylpropionyl amine benzoic acid is a kind of main component of Shu Min antipruritic, it has There is good anti-irritant, antipruritic, can effectively inhibit the phenomenon that red and swollen, oedema or itch occur for skin.Thus it uses Any one in above two ingredient can play the role of anti-inflammatory of releiving, and can protect human skin, reduce to skin Stimulation, so that skin is no longer sensitive fragile.

The present invention is further arranged to: at least further include having following one kind:

By using above-mentioned technical proposal, parahydroxyacet-ophenone also known as 4'- hydroxy acetophenone, inside cosmetics mainly It is used as antioxidant, simultaneously because parahydroxyacet-ophenone is a kind of natural plant extracts, is naturally present in compositae plant Stem, the leaf of artemisia scoparia, in the roots of plants such as Artemisia capillaris, Asclepiadaceae plant, kerr tylophora root, so it not only to improve flesh bottom water good Good antioxygenic property, and skin will not be stimulated, to application on human skin without any harm, use is safe.Secondly, carnosine scientific name β- Alanyl-L-histidin, it is a kind of dipeptides being made of two kinds of amino acid of Beta-alanine and L-Histidine, crystalline solid. Carnosine has very strong oxidation resistance, can remove during oxidative stress (under the light wave between 200nm-500nm range) The active oxygen radical (ROS) and alpha-beta unsaturated aldehyde for making the fatty acid excessive oxidation of cell membrane and being formed, help to improve Skin environment promotes the protective effect to skin；Flesh bottom water is for having the ultraviolet light of injury and blue segment visible skin simultaneously The blue light components of light have good absorption ability, it is possible thereby to illustrate that the flesh bottom water of the application can help to reduce light to skin The damage of skin improves anti-blue light and the effect of ultraviolet light of skin.

In addition, -1 copper of tripeptides, also known as copper tripeptides -1, Lan Tongsheng peptide GHK-Cu2⁺And copper peptide, consisting of glycine- Histidine-is from propylhomoserin-copper, and in aqueous solution, copper ion is not the yellow of copper metal and blue is presented.It can not only promote Make skin epidermis regeneration, restore that skin is young, reduce thickness wrinkle and scar, improves skin elasticity, make cells of superficial layer with Proliferation of fibroblast can more allow subcutaneous tissue to thicken, and keep skin no longer fragile sensitive, increase skin elasticity and toughness, The nutritional ingredient in flesh bottom water is allowed to be absorbed and utilized what can be maximized on the face.It also has strong organization protection simultaneously And antiinflammation, further wounded tissue can be protected from oxidative damage.According further to abosrption spectrogram it is found that from Light wave between 200nm- 500nm range, flesh bottom water have significant assimilation effect.Wherein, blue copper peptide can also stimulate glucose The formation of polyamine promotes epidermal cell proliferation (thickening), skin screen can also be further repaired under the action of maintaining skin elasticity Barrier, improves the protective action to blue segment visible light.

And contain the thick zymoprotein of seaweed SOD, alginic acid, calcium, iron, iodine, vitamin B complex, eicosapentaenoic in algae extract The compounding compound such as sour, amino acid and laminine (i.e. laminine), taurine and glycine betaine.Wherein, seaweed SOD is thick For zymoprotein as in algae extract pairs of one of effective component, it has the good anti-aging and anti-ultraviolet performance of raising, The opsonic action to skin can be further strengthened, reduces ultraviolet light to skin bring damaging action.

By using above-mentioned technical proposal, the present invention is further arranged to: at least further include having following one kind:

0.1-5 parts of trehalose；

0.1-1 parts of allantoin.

By using above-mentioned technical proposal, it is by Liang Ge pyranoid ring Portugal that trehalose, which is a kind of double pools of stable irreducibility, What grape glycan molecule and 1,1- glycosidic bond linked.It is widely present in rudimentary plant such as algae, bacterium, fungi, insect with It is both a kind of Storage carbohydrate and the important products that stress be metabolized and in invertebrate.It also has excellent simultaneously Keep cell viability and the active characteristic of large biological molecule.Since Skin Cell is in high temperature, high and cold, dry, intensive ultraviolet radiation Under equal environment, easily loses moisture content and occur keratinization or even death falls off makes skin damage.In this case, trehalose One layer of special protective film can be formed in cell surface, the mucus being precipitated from film is not only moistened Skin Cell, also had The function that external heat is radiate, thus damage caused by protecting the skin from radioactivity.Meanwhile it is also able to maintain The original nutrition of skin and moisture content, avoid skin sunburn and melanin deposition, are effective against skin ageing phenomenon；It is precipitated from film Mucus can mildly moisturize the skin, make bright skin jade-like stone, gloss, tender.And allantoin is then a kind of amphoteric compound, it can be tied Close many kinds of substance formed double salt, have be protected from light, sterilization and anticorrosion, analgesic, antioxidation, so as to make skin keep moisture content, It moistens and soft.Thus protection skin can be improved using any one of the above substance, while facial skin being made to keep good Moisture content, moisten and pliability.

0.1-5 parts of fructose；

0.1-5 parts of maltose.

By using above-mentioned technical proposal, fructose and maltose are natural carbohydrates, they can play certain moisturizing Effect is especially had after being compounded using fructose and maltose with natural moisturizing factor (NMF ingredient) and other moisturizer good Good synergistic function.Understand according to test data and know: being intended for single use, 17% moisture content of skin is improved after 48 hours； After 72 hours, 10% moisture content of skin can be improved.

The present invention is further arranged to: the mineral salt includes selenium element, magnesium elements, Zn-ef ficiency, element silicon, calcium constituent, One of sodium element or lot of trace mineral element.

By using above-mentioned technical proposal, selenium element, magnesium elements, Zn-ef ficiency, element silicon, calcium constituent, sodium element is Common trace quantity mineral substance element can be improved containing for trace quantity mineral substance element in flesh bottom water by the way that above-mentioned trace quantity mineral substance element is added Amount, microelement needed for capable of giving facial skin when thus stating flesh bottom water in use further extend face's aging, are Skin microbial provides prebiotics, and the balance of skin biomembrane is safeguarded with this.

The present invention is further arranged to: further include following operating procedure:

The preparation of step 1, kettle raw material: water, humic acid and mineral salt are added in kettle；Stirring is opened, by glycerol, fourth two Pure and mild parahydroxyacet-ophenone sequentially adds main cooker, is heated to 80-85 DEG C, obtains kettle raw material；

Step 2 is pre-dissolved phase A, is pre-dissolved phase B, and being pre-dissolved the preparation of phase C:

<1>it is pre-dissolved the preparation of phase A: selecting the container of 15Kg cleaning that butanediol is added, Sodium Hyaluronate is then added to fourth two It is dispersed with stirring in alcohol uniformly；

<2>it is pre-dissolved the preparation of phase B: selecting the container of 5Kg cleaning that the mixed liquor of water, humic acid and mineral salt is added, it then will be sweet Oxalic acid dipotassium is added in the mixed liquor of water, humic acid and mineral salt, is dispersed with stirring uniformly；

<3>it is pre-dissolved the preparation of phase C: selecting the container of 5Kg cleaning that the mixed liquor of water, humic acid and mineral salt is added, then by flesh Peptide is added in the mixed liquor of water, humic acid and mineral salt, is dispersed with stirring uniformly；

Kettle raw material is pumped into main cooker by step 3, and addition is pre-dissolved phase A, is heated to 80-85 DEG C, opens stirring 200-300r/ Min stirs 30-40min, and stirring 150-200r/min is opened after being pre-dissolved phase A and sufficiently dissolving dispersion, starts to cool down；

60-65 DEG C is cooled to, water, glycerol, beta glucan, 1,2- hexylene glycol, 1,2- pentanediol, fructose, maltose, PCA is added Sodium, trehalose, allantoin, Sodium Hyaluronate, D-sorbite, algae extract, parahydroxyacet-ophenone, and it is pre-dissolved phase B, it stirs It is uniformly dispersed, continues to cool down；

Then cool to 40-45 DEG C, addition is pre-dissolved phase C, butanediol, 1,2- pentanediol, hydroxy phenylpropionyl amine benzoic acid, water, sweet - 1 copper of oil and tripeptides, stirs evenly, and continue to cool down；

Last main cooker is cooled to 30-40 DEG C, and sample detection is filtered discharge using 400 mesh filter clothes after detection is qualified and handles, with Flesh bottom water can be obtained after collecting packing in discharging afterwards.

It is not only simple to operate by using above-mentioned technical proposal, but also carry out being pre-dissolved phase A, pre- respectively in step 2 Molten phase B, and be pre-dissolved the preparation of phase C, Sodium Hyaluronate is soluble in butanediol at this time, at this time by being pre-dissolved the preparation process of phase A Dispersion degree of the Sodium Hyaluronate in entire flesh bottom water is can effectively improve；Secondly dipotassium glycyrrhizinate, carnosine are separately added into It is pre-mixed into the mixed liquor of water, humic acid and mineral salt, then by similar compatibility principle, improves glycyrrhizic acid two The dispersion degree of potassium, carnosine in entire flesh bottom water.Thus obtained skin base solution can not only improve the replenishing water and preserving moisture of facial skin And oil-control performance, dry skin, peeling are reduced, or even play the generation of acne phenomenon；But also has to improve and skin is resisted The ability of blue segment visible light.

In conclusion the invention has the following advantages:

1, the present invention can not only reduce dry skin, peeling by the replenishing water and preserving moisture and oil-control performance of raising facial skin, Even play the generation of acne phenomenon；And the ability for resisting blue segment visible light to skin can also be improved；

2, optimize, the ingredients such as various mineral salt, humic acid, algae extract, hyaluronic acid and polypeptide are added, can improve The skin conditions done in outer oil, can provide various nutritional ingredients for skin surface cell, form the cells of superficial layer of health, to help The reparation of barrier, while prebiotics can also be provided for skin microbial, the balance of skin biomembrane is safeguarded with this.

Detailed description of the invention

Fig. 1 is the ultraviolet-visible absorption spectroscopy figure of the flesh bottom water of the one of embodiment of the present invention；

Fig. 2 is that the skin moisture of the flesh bottom water of the one of embodiment of the present invention is lost blank testing results of comparison figure, wherein scheming In be divided into 3 groups, in each group, the light grey rectangular area on the left side is expressed as white space；And the Dark grey rectangle region on right side Domain representation is sample area；

Fig. 3 is the moisture loss TEWL comparative result figure that each sample is coated in skin surface；

Fig. 4 is that the skin moisture of the flesh bottom water of the one of embodiment of the present invention is lost test data figure；

Fig. 5 is the change of moisture content comparative result figure that each sample is coated in skin surface；

Fig. 6 is the histogram for the grease result of variations comparison that each sample is coated in skin surface；

Fig. 7 is that each sample is coated in the grease result of variations of skin surface and compares line chart, it is main it is to be tested be skin greasing people Group.

Specific embodiment

Invention is further described in detail with attached drawing with reference to embodiments.

Embodiment 1: a kind of multiple-effect flesh bottom water of replenishing water and preserving moisture oil-control, the component including parts by weight as shown in Table 1.

Its method made is added according to the component of the parts by weight of embodiment 1 in table 1, wherein parts by weight What component all referred in the description of the present application is the weight of specific ingredient, in grams, including following operating procedure:

The preparation of step 1, kettle raw material: water, humic acid and mineral salt are added in kettle；Stirring is opened, it then again will be sweet Oil, butanediol and parahydroxyacet-ophenone sequentially add main cooker, are heated to 80 DEG C, obtain kettle raw material.

<1>it is pre-dissolved the preparation of phase A: selecting the container of 15Kg cleaning that butanediol is added, be then added to Sodium Hyaluronate above-mentioned It is dispersed with stirring in butanediol uniformly；

<2>it is pre-dissolved the preparation of phase B: selecting the container of 5Kg cleaning that the mixed liquor of water, humic acid and mineral salt is added, it then will be sweet Oxalic acid dipotassium is added in the mixed liquor of above-mentioned water, humic acid and mineral salt, is dispersed with stirring uniformly；

<3>it is pre-dissolved the preparation of phase C: selecting the container of 5Kg cleaning that the mixed liquor of water, humic acid and mineral salt is added, then by flesh Peptide is added in the mixed liquor of above-mentioned water, humic acid and mineral salt, is dispersed with stirring uniformly；

Kettle raw material is pumped into main cooker by step 3, and addition is pre-dissolved phase A, is heated to 80 DEG C, opens stirring 200r/min, stirring 30min opens stirring 150r/min after being pre-dissolved phase A and sufficiently dissolving dispersion, starts to cool down；

Cool to 60 DEG C, be added water, glycerol, beta glucan, 1,2- hexylene glycol, 1,2- pentanediol, fructose, maltose, PCA sodium, Trehalose, allantoin, Sodium Hyaluronate, D-sorbite, algae extract, parahydroxyacet-ophenone, and it is pre-dissolved phase B, it is dispersed with stirring Uniformly, continue to cool down；

45 DEG C are then cooled to, is added and is pre-dissolved phase C, butanediol, 1,2- pentanediol, hydroxy phenylpropionyl amine benzoic acid, water, glycerol, And -1 copper of tripeptides, it stirs evenly, and continue to cool down；

Last main cooker is cooled to 35 DEG C or so, and sample detection is filtered discharge using 400 mesh filter clothes after detection is qualified and handles, And require that 2kg need to be more than or equal to from the withdrawal rate of material mouth, then flesh bottom water can be obtained after being packaged in discharging collection.

Embodiment 2-6: a kind of multiple-effect flesh bottom water of replenishing water and preserving moisture oil-control, difference from example 1 is that: such as table 1 Shown, the component of mass fraction is different.

A kind of table 1: the component of the parts by weight of embodiment 1-6 in the multiple-effect flesh bottom water of replenishing water and preserving moisture oil-control

Embodiment 7-12: a kind of multiple-effect flesh bottom water of replenishing water and preserving moisture oil-control, difference from example 1 is that: its mass parts Several components is different, as shown in table 2.

The component of the parts by weight of embodiment 7-12 in a kind of multiple-effect flesh bottom water of the replenishing water and preserving moisture oil-control of table 2

Comparative example 1: a kind of multiple-effect flesh bottom water of replenishing water and preserving moisture oil-control, using commercially available Co., Ltd, P&G SK- II facial treatment essence.

Comparative example 2: a kind of multiple-effect flesh bottom water of replenishing water and preserving moisture oil-control, using commercially available without print non-defective unit (Shanghai) business Co., Ltd without print non-defective unit toner.

Comparative example 3: a kind of multiple-effect flesh bottom water of replenishing water and preserving moisture oil-control, it is refined using commercially available Europe haod Lay The section Yan Shi pot marigold toner of (China) Co., Ltd.

Test one: ultraviolet and blue segment visible light spectrophotometric test

Subjects: it regard embodiment 9 as control sample 1.

Test process: by the sample 1 prepared in carrying out light splitting sweep test, 200nm- in 200-700nm wave-length coverage Primary every 5nm measurement between 700nm, will be zeroed after measurement calibration every time, and record data.

Test result: ultraviolet-visible absorption spectroscopy figure as shown in Figure 1.And from Fig. 1, it is apparent that from Light wave between 200nm-500nm range, flesh bottom water have significant assimilation effect.It wherein, is ultraviolet between 200-400nm The wave-length coverage of light.Wherein, the wave-length coverage of UVA is 320-400nm, and the wave-length coverage of UVB is 280-320nm.And blue light Wave-length coverage is 400-450nm, and famous American skin expert professor Kligman proposes famous " light aging is a kind of skin disease " judgement, systematically disclose injury of the ultraviolet light to skin earliest.Ultraviolet B radiation (UVB, 280-320nm) holds into skin Easily cause inflammatory reaction, lead to rubefaction, gradually melanism, also referred to as erythema ultraviolet light.Long wave ultraviolet (UVA, 320- The skin corium that can 400nm) reach skin is the principal element for causing skin retardance melanism and aging.Ultraviolet light can increase The production quantity of active oxygen radical (ROS) in skin histology causes free radical generation and a series of oxidative damage, causes Skin aging.

Thus it will be seen from figure 1 that flesh bottom water is for there is the blue light of the ultraviolet light of injury and blue segment visible light to skin There is good absorption ability in part, it may be said that the flesh bottom water of bright the application can help the damage for reducing light to skin.

Test two: skin moisture is lost test

Subjects: using embodiment 1-12 as test specimen 1-12.

Test method: 24 people of random selection carry out the use test of one-off, 6 hours improvement skin screens of test sample Hinder effect.

The test specimen prepared is coated in respectively in the dry skin by cleaning and drying, after absorbing completely, to this Locate skin and carry out primary moisture loss data test in real time every 15min, removes after a maximum value and a minimum value simultaneously Test its average value.

Evaluation requires: moisture loss is lower, indicates that skin barrier is better.Remarks: " ns " indicates p > 0.05, and " * " is indicated 0.01≤p < 0.05；" * * " indicates that 0.001≤p < 0.01, " * * * " indicate p < 0.001.

Test result: as shown in Fig. 2, using after test sample 1h and without using compared with any product, through epidermis moisture content Turnover rate conspicuousness reduces, and illustrates that product has effects that 1h conspicuousness water lock.

Using after test sample 3h and without using compared with any product, reduces, say through epidermis moisture loss rate conspicuousness Bright product has effects that 3h conspicuousness water lock.

Using after test sample 6h and without using compared with any product, there is no the change of conspicuousness through epidermis moisture loss rate Change.

Test three: the individual moisture loss test of each sample

Test is to sample: embodiment 9 is used as control sample 9, using comparative example 1-3 as control sample 1-3.

Test method: choosing the individual experimenter of dry skin, carries out the moisture loss contrast test of several samples, obtains Each sample data result it is as shown in Figure 3.

Test result: Fig. 3 can significantly find out that the overall moisture content bleed rate of control sample 2 and control sample 3 becomes Change trend is the trend of a rising, and test specimen 9 and control sample 1 are in a relatively steady range.And test sample Product 9 and control sample 1 compare, and 9 most of the time of test specimen compares 1 rate of control sample a relatively low position It sets, that is to say, that when most of, apply the skin at test specimen 9 and be lost speed than the skin moisture at control sample 1 Degree is slow.

Test available conclusion from there through this, in two hours, moisture loss speed it is most slow be test specimen 9, followed by control sample 1, control sample 3, moisture loss it is fastest be control sample 2.It is faster to be lost speed, moisturizing Effect is poorer, thus moistening effect from by force to it is weak be successively test specimen 9, control sample 1, control sample 3, control sample 2.

Test four: the cuticula moisture content content measuring of flesh bottom water

Subjects: using embodiment 1-12 as control sample 1-12.

Test method: 24 people of random selection carry out the use test of one-off, 6 hours improvement skin screens of test sample Barrier and moisture-keeping functions.

The test specimen prepared is coated in respectively in the dry skin by cleaning and drying, after absorbing completely, to this Locate skin and carry out primary moisture loss data test in real time every 2 hours, 5 hours, removes a maximum value and a minimum value Afterwards and test its average value.

Evaluation requires: sample area cuticula moisture content increment is higher, indicates that product moistening effect is better.Remarks: " ns " is indicated P > 0.05, " * " indicate 0.01≤p < 0.05；" * * " indicates that 0.001≤p < 0.01, " * * * " indicate p < 0.001.

Test result: as shown in figure 4, using after test sample 1h and without using compared with any product, keratoderma Water content conspicuousness is promoted, and illustrates that product has 1h conspicuousness moisture-keeping efficacy.

Using compared with without using any product, keratoderma water content conspicuousness is promoted after test sample 3h, Illustrate that product has 3h conspicuousness moisture-keeping efficacy.

Using compared with without using any product, keratoderma water content conspicuousness is promoted after test sample 6h, Illustrate that product has 6h conspicuousness moisture-keeping efficacy.

Test the individual cuticula moisture content content measuring of five, each sample

Subjects: embodiment 9 is regard as control sample 1, using comparative example 1-3 as control sample 1-3.

Test method: choosing 15 individual experimenters of dry skin, and the cuticula moisture content content balance for carrying out 4 samples is surveyed Examination, the data result of 4 obtained samples are as shown in Figure 5.

Test result, the cuticula that Fig. 5 can significantly find out that several samples are smeared on the skin in two hours are aqueous Amount changes, and the water content of stratum corneum in figure has fluctuation.Wherein, the water content of stratum corneum energy of control sample 2 in two hours As soon as be enough maintained at it is more low-level numerically, but two hours are reduced to initial numerical value later.Namely It says, the moistening effect of control sample 2 can be only sustained within two hours.And control sample 3 and control sample 1 maintain always It is more than hour can to continue two for 70-75 numerical value or so, and moistening effect is substantially better than control sample 2.Moistening effect is best It is test specimen 1, its overall cuticula moisture content is able to maintain 85 or so, and relatively more steady within 150 minutes, far Better than other three samples.

From the point of view of moisture loss speed in conjunction with Fig. 3, the moisture loss speed of test specimen 1 is most slow, cuticula water content Highest, moistening effect are best.Followed by control sample 1 and control sample 3.Worst is control sample 2, moisture loss speed Degree is continuing to increase and water content of stratum corneum is in lasting reduction, and the time that moistening effect maintains is short.

Test six: skin oil and fat variation test

Subjects: using embodiment 1-12 as control sample 1-12.

Test method: 30 people of random selection carry out the use test of one-off, 2 hours improvement skin screens of test sample Barrier and moisture-keeping functions.The flesh bottom water prepared is coated in dry skin, a real time data test is carried out every 15min, goes Except after a maximum value and a minimum value and testing its average value.

Evaluation requires: skin oil and fat content is lower, indicates that oil-control effect is better.Remarks: " ns " indicates p > 0.05, " * " table Show 0.01≤p < 0.05；" * * " indicates that 0.001≤p < 0.01, " * * * " indicate p < 0.001.

Test result: as shown in fig. 6, using after test sample 2h and without using compared with any product, forehead skin oil Rouge content conspicuousness reduces, and illustrates that product has conspicuousness 2h oil-control effect.

Test seven: the individual's skin grease of each sample changes test

Subjects: embodiment 12 is regard as test specimen 1, using comparative example 1-3 as control sample 1-3.

Test method: choosing 30 individual experimenters of skin greasing, and the cuticula moisture content content balance for carrying out 4 samples is surveyed Examination.

Test result: Fig. 7 can be seen that control sample 2 and control sample 3 was coated in Oily within two hours Grease change curve is in rising trend, that is to say, that does not have oil-control effect.And the oil-control effect of test specimen 1 and control sample 1 Fruit is clearly.In Fig. 7, the oil-control effect of control sample 1 is best, the grease control of skin can be existed within two hours Within 40, and it is able to maintain.The oil-control effect of test specimen 1 is taken second place, and can control within 50, slightly above control sample 1, but It is the low numerical value that grease is also able to maintain within two hours.

Test eight, skin brightness variation test

Subjects: embodiment 8 is regard as test specimen 1, using comparative example 1-3 as control sample 1-3.

Test method: the flesh bottom water (specimen sample 1) prepared is coated in dry skin according to embodiment 8, is being smeared A real time data test is carried out before 4 kinds of samples and after a hour respectively.

Testing standard: in skin brightness test, L value is higher, and it is whiter to represent skin；A value is higher, and it is redder to represent skin； B value is higher, and it is more yellow to represent skin；T value is higher, and it is brighter to represent skin.

Test result: from table 3 it is observed that test specimen 1 and control sample 1, after smearing a hour, skin is aobvious Work bleaches.Control sample 3 does not bleach not only, instead the several points of blackening.From a value, skin after four kinds of samples are smeared Redden phenomenon, but the general red degree of test specimen 1 is minimum, 2 highest of control sample.From b value, control sample 2 is short The effect of yellowing is improved in phase well, the only b value of control sample 1 slightly increases.

Generally speaking, control sample 2 allows heat flush phenomenon most serious.The whiteness of control sample 3 reduces most；And it is right Product 1 increase skin yellowing in the same old way, also have promotion to whitening skin degree.Although wherein 1 appearance of test specimen is brownish black, But it can increase the L value of skin, white luminance instead.

3 each sample of table is coated in the brightness change Comparative result of skin surface

	L	a	b
				Test specimen 1	2.235	0.76	-0.23
Control sample 1	2.28	0.77	0.345
				Control sample 2	0.175	1.845	-3.34
Control sample 3	-3.06	0.86	-0.155

Specific embodiment is only explanation of the invention, is not limitation of the present invention, and those skilled in the art are readding It can according to need the modification that not creative contribution is made to the present embodiment after running through this specification, but as long as in the present invention Scope of the claims in all by the protection of Patent Law.

Claims

1. a kind of multiple-effect flesh bottom water of replenishing water and preserving moisture oil-control, which is characterized in that the component including following parts by weight:

50-90 parts of water；

3.4-50 parts of moisturizer；

0.1-5 parts of beta glucan；

0.02-2 parts of humic acid；

0.01-2 parts of mineral salt；

It releives 0.3-15 parts of agent.

2. a kind of multiple-effect flesh bottom water of replenishing water and preserving moisture oil-control according to claim 1, which is characterized in that the moisturizer is extremely Few includes following a kind of:

1-10 parts of butanediol；

1-10 parts of glycerol；

1-10 parts of 1,2- pentanediol；

0.1-5 parts of 1,2- hexylene glycol；

0.1-2 parts of Sodium Hyaluronate；

0.1-5 parts of D-sorbite；

0.1-5 parts of Anjidew NL50.

3. a kind of multiple-effect flesh bottom water of replenishing water and preserving moisture oil-control according to claim 1, which is characterized in that described to releive agent extremely Less include following one kind:

0.1-2 parts of dipotassium glycyrrhizinate；

0.1-2 parts of hydroxy phenylpropionyl amine benzoic acid.

4. a kind of multiple-effect flesh bottom water of replenishing water and preserving moisture oil-control according to claim 1, which is characterized in that at least further include having It is following a kind of:

0.1-1 parts of parahydroxyacet-ophenone；

0.1-2 parts of carnosine；

0.1-2 parts of -1 copper of tripeptides；

0.1-5 parts of algae extract.

5. a kind of multiple-effect flesh bottom water of replenishing water and preserving moisture oil-control according to claim 1, which is characterized in that at least further include having It is following a kind of:

0.1-5 parts of trehalose；

0.1-1 parts of allantoin.

6. a kind of multiple-effect flesh bottom water of replenishing water and preserving moisture oil-control according to claim 1, which is characterized in that at least further include having It is following a kind of:

0.1-5 parts of fructose；

0.1-5 parts of maltose.

7. a kind of multiple-effect flesh bottom water of replenishing water and preserving moisture oil-control according to claim 1, which is characterized in that the mineral salt packet Include selenium element, magnesium elements, Zn-ef ficiency, element silicon, calcium constituent, one of sodium element or lot of trace mineral element.

8. a kind of multiple-effect flesh bottom water of replenishing water and preserving moisture oil-control according to claim 1, which is characterized in that preparation method packet Include following operating procedure:

60-65 DEG C is cooled to, water, glycerol, beta glucan, 1,2- hexylene glycol, 1,2- pentanediol, fructose, maltose, PCA is added Sodium, trehalose, allantoin, Sodium Hyaluronate, D-sorbite, algae extract, parahydroxyacet-ophenone, and it is pre-dissolved phase B, stirring point It dissipates uniformly, continues to cool down；