CN107569432B - Herbal hand cream capable of nourishing, whitening, relieving and replenishing water and preparation method thereof - Google Patents
Herbal hand cream capable of nourishing, whitening, relieving and replenishing water and preparation method thereof Download PDFInfo
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Abstract
The invention provides herbal nourishing, whitening, relieving and moisturizing hand cream and a preparation method thereof, wherein the hand cream comprises the following raw materials: calendula oil, sesame oil, rapeseed oil, olive emulsifier, a universal self-emulsifying compound emulsifier AC-402, distilled water, sodium carboxymethylcellulose, carbomer 941, daylily extract, mangosteen bark extract, persimmon leaf extract, ginkgo leaf extract, cane shoot extract, mulberry extract, pea extract, rice extract, methyl silicone oil, glycerol, ethylparaben, 75% ethanol and essence. Compared with the prior art, the hand cream prepared by the invention has proper viscosity, is translucent, fine, smooth and refreshing, is fresh and elegant, can deeply nourish, lock water and whiten, makes hand skin comfortable and white, and can nourish healthy, white, tender and beautiful hands from inside to outside.
Description
Technical Field
The invention relates to a hand cream, and in particular relates to a herbal hand cream capable of nourishing, whitening, relieving and replenishing water and a preparation method thereof.
Background
The hand cream has the advantages that the hand cream is dry, dark yellow, sensitive to aging, easy to breed bacteria, easy to freeze, easy to be threatened by wounds and the like, and the hand cream is used for caring and protecting hands, so that the purposes of moisturizing and caring, maintaining and repairing are achieved.
The hand cream is used as a skin care product which can heal and smooth cracks and dryness of the skin and can effectively prevent and treat rough and dry hands in autumn and winter, and the hand cream can make the hand skin more tender and moist by frequent use in autumn and winter.
However, the hand cream on the market at present contains pigments and other stimulating components, for example, some hand creams can stimulate the skin, and particularly, if a wound exists on the skin, the skin cannot be healed easily; when there are problems such as barbs, peeling and cracking on the hand, irritating components such as pigments should be avoided.
Therefore, the novel green, safe and efficient hand cream can meet the desire of people to have two fine and smooth hands and enjoy high-quality life, and has wide application value and popularization prospect.
Disclosure of Invention
The invention aims to provide herbal hand cream for nourishing, whitening, relieving and moisturizing.
The invention also provides a preparation method of the herbal hand cream for nourishing, whitening, relieving and moisturizing.
The invention provides herbal hand cream capable of nourishing, whitening, relieving and replenishing water, which comprises the following raw materials in parts by weight:
the day lily extracting solution is prepared by the following method:
weighing appropriate amount of flos Hemerocallis, cutting into pieces, soaking for 0.5-0.8h, heating and reflux extracting for 3 times: adding 16-18 times of water for the first time, and extracting for 1.5-2.0 h; adding 12-14 times of water for the 2 nd time, and extracting for 1.0-1.5 hr; adding 8-10 times of water for 3 times, and extracting for 0.5-1.0 hr; filtering each time to obtain filtrate, mixing filtrates, and concentrating the volume of the filtrate to 3-8 times g/mL of the weight of flos Hemerocallis for use.
The mangosteen bark extract is prepared by the following method:
weighing appropriate amount of cortex Garciniae, cutting, soaking for 0.3-0.6 hr, heating and reflux extracting for 3 times: adding 18-22 times of water for the first time, and extracting for 1.0-2.5 hr; adding 14-18 times of water for the second time, and extracting for 1.0-2.0 hr; adding 10-14 times of water for 3 times, and extracting for 0.5-1.0 hr; filtering each time to obtain filtrate, mixing the filtrates, and concentrating the volume of the filtrate to 4-6 times g/mL of the weight of the mangosteen bark for later use.
The persimmon leaf extracting solution is prepared by the following method:
weighing appropriate amount of folium kaki, cutting, soaking in 75% ethanol for 0.4-1.0 hr, heating and reflux extracting for 3 times: adding 20-22 times of 75% ethanol for 1 time, and extracting for 1.0-2.0 hr; adding 16-18 times of 75% ethanol for 2 times, and extracting for 1.0-2.0 hr; adding 10-12 times of 75% ethanol for 3 times, and extracting for 0.5-1.0 hr; filtering each time to obtain filtrate, mixing filtrates, and concentrating the filtrate to volume of 2-6 times g/mL of folium kaki for use.
The ginkgo leaf extracting solution is prepared by the following method:
weighing appropriate amount of folium Ginkgo, cutting into pieces, soaking in 70% ethanol for 0.5-0.8 hr, heating and reflux extracting for 3 times: adding 20-25 times of 70% ethanol for 1 time, and extracting for 1.0-2.0 hr; adding 12-18 times of 70% ethanol for 2 times, and extracting for 1.0-2.0 hr; adding 70% ethanol 8-12 times the amount of the extract for the 3 rd time, and extracting for 1.0-2.0 hr; filtering each time to obtain filtrate, mixing filtrates, and concentrating the volume of the filtrate to 4-8 times g/mL of the weight of folium Ginkgo for use.
The wild rice stem extracting solution is prepared by the following method:
weighing appropriate amount of caulis Zizaniae Caduciflorae, cutting, soaking for 0.4-0.6h, heating and reflux extracting for 3 times: adding 22-26 times of water for the first time, and extracting for 1.5-2.0 h; adding 20-22 times of water for the second time, and extracting for 1.5-2.0 hr; adding 18-20 times of water for 3 times, and extracting for 1.0-2.0 hr; filtering each time to obtain filtrate, combining the filtrates, and concentrating the volume of the filtrate to 2-6 times g/mL of the weight of the cane shoots for later use.
The mulberry extracting solution is prepared by the following method:
weighing a proper amount of mulberries, soaking for 0.6-0.8h, heating, refluxing and extracting for 3 times: adding 18-20 times of water for the first time, and extracting for 1.5-2.5 hr; adding 16-18 times of water for the 2 nd time, and extracting for 1.0-1.5 hr; adding 12-14 times of water for 3 times, and extracting for 1.0-1.5 hr; filtering each time to obtain filtrate, combining the filtrates, and concentrating the volume of the filtrate to 4-6 times g/mL of the weight of the mulberry for later use.
The pea extract is prepared by the following method:
weighing appropriate amount of pea coarse powder, soaking for 0.3-0.8h, heating and reflux extracting for 3 times: adding 16-20 times of water for the first time, and extracting for 1.5-2.0 h; adding 14-16 times of water for the 2 nd time, and extracting for 1.0-1.5 hr; adding 12-14 times of water for 3 times, and extracting for 0.5-1.0 hr; filtering each time to obtain filtrate, mixing filtrates, and concentrating the volume of the filtrate to 2-4 times g/mL of the weight of pea for use.
The rice extract is prepared by the following method:
weighing a proper amount of rice coarse powder, soaking for 0.2-0.6h, heating and refluxing for 3 times: adding 18-20 times of water for the first time, and extracting for 1.0-2.0 hr; adding 16-18 times of water for the 2 nd time, and extracting for 1.0-1.5 hr; adding 10-12 times of water for 3 times, and extracting for 0.5-1.0 hr; filtering each time to obtain filtrate, mixing filtrates, and concentrating the volume of the filtrate to 3-6 times g/mL of the weight of rice for use.
The essence is selected from one or more of sage essence, sensitive plant essence, jasmine essence, rose essence, cananga odorata essence, sandalwood essence or tangerine essence.
The invention provides a preparation method of herbal hand cream capable of nourishing, whitening, relieving and moisturizing, which comprises the following steps:
a) weighing 0.5-2.0g of sodium carboxymethylcellulose, adding into 50.0-100.0mL of distilled water, heating in water bath at 30-60 deg.C while stirring, and standing to make it fully swell to obtain sodium carboxymethylcellulose gel solution;
b) weighing 9410.5-2.0 g of carbomer, adding into 50.0-100.0mL of distilled water, heating in water bath at 60-80 deg.C under stirring, and standing to swell completely to obtain carbomer 941 gel solution;
c) weighing 0.5-0.8g of ethylparaben, adding into 1.0-2.0mL of 75% ethanol solution, and stirring to obtain antiseptic solution;
d) weighing 2.0-5.0g of sesame oil, 2.0-5.0g of calendula oil, 2.0-5.0g of rapeseed oil, 3.0-8.0g of olive emulsifier and 8.0g of universal self-emulsifying compound emulsifier AC-4023.0-8.0 g, uniformly mixing, heating in a water bath at 75-95 ℃, stirring while heating to uniformly mix to form an oil phase for later use;
e) weighing 20.0-45.0mL of distilled water, and heating in a water bath at 75-95 ℃ to serve as a water phase for later use;
f) when the water phase and the oil phase reach the same temperature, slowly pouring the water phase into the oil phase in a fine flow state, stirring in the same direction for 10-15min while adding until the water phase is a uniform yellowish milky matrix, stopping stirring, taking out from the water bath, and naturally cooling to room temperature;
g) adding 1.0-3.0mL of cane shoot extract, 1.0-3.0mL of day lily extract, 1.0-3.0mL of mangosteen bark extract, 1.0-3.0mL of persimmon leaf extract, 1.0-3.0mL of ginkgo leaf extract, 1.0-3.0mL of mulberry extract, 1.0-3.0mL of pea extract and 1.0-3.0mL of rice extract into an emulsion matrix, sequentially adding sodium carboxymethylcellulose solution, 941 carbomer gel solution, 2.0-5.0mL of methyl silicone oil, 2.0-5.0mL of glycerol and 0.2-0.35g of essence, finally adding a preservative solution, and uniformly stirring to obtain the fine and uniform herbal nourishing, moisturizing, whitening and soothing water replenishing cream.
The invention comprises the following components:
the calendula oil contains abundant linoleic acid and carotene, has the functions of calming and relaxing, and can condition sensitive skin, enhance the resistance of the skin and reduce the discomfort phenomenon of the sensitive skin. The xanthophyll contained in the calendula oil has antioxidant effect, can resist the damage of ultraviolet rays to the skin, and relieve the phenomena of skin redness, allergy and desquamation caused by excessive insolation.
The sesame oil is rich in vitamins, fatty acid and various trace elements, and can effectively form a protective film, thereby resisting ultraviolet radiation, isolating harmful substances and dust in the air and playing an excellent role in protecting the skin. Secondly, the sesame oil is rich in moisturizing factors, can prevent skin from drying and peeling, has a good moisturizing and water locking effect, and has a great effect on relieving the problems of skin itching, redness and swelling and the like caused by dryness. The sesame oil can effectively keep the elasticity of skin, delay skin aging, repair damaged cells in scars and restore smooth and fine skin after being used persistently.
The rapeseed oil is rich in glycerate, camellin, theasapogenol, vitamins and the like, and can promote the regeneration of inner cells, prevent water loss and nourish sebocytes. The rapeseed oil has the functions of maintaining beauty and keeping young, and can make the skin healthier and more moist. The rapeseed oil can prevent the damage of ultraviolet rays to the skin, avoid tanning, skin exposure and desquamation, and keep the skin fine, smooth, tender and glossy. The rapeseed oil can be used for moistening skin and preventing dryness, cracking and frostbite when being used for rubbing hands in winter. It has effects of eliminating fine lines, reducing mottle, protecting skin, keeping moisture, and preventing skin aging.
The daylily contains abundant carotene, and can effectively promote skin cell metabolism, prevent pachylosis and pigmentation, moisten skin, and delay aging. Frequent eating of the day lily can also moisten the skin, enhance the toughness and elasticity of the skin, and enable the skin to be tender, plump, smooth and soft, reduce wrinkles and eliminate color spots.
Mangosteen skin is rich in tannic acid. The tannic acid can help to treat acne and skin damage, accelerate tissue cell regeneration, increase natural luster of skin, protect skin from being influenced by oxidation of free radicals, help skin regeneration and repair, protect skin from being damaged, promote skin to emit youthful light, and make skin more clear and bright. In addition, the gamma-mangostin contained in the xanthone has good antioxidant property, and the xanthone contained in the xanthone has antibacterial activity on bacteria such as staphylococcus aureus.
Persimmon leaves have certain beauty-maintaining efficacy because they contain choline, rutin and tannin in addition to considerable amounts of proteins, amino acids and various vitamins. The contained tannic acid can kill various bacteria and fungi by permeating into water, and has good effects of cleaning and moistening skin.
Folium Ginkgo has effects in whitening skin and removing wrinkle. In the aspect of whitening, the flavone component in the ginkgo leaves can prevent the formation and deposition of pigment in the dermis, so as to achieve the effects of whitening the skin and preventing and treating pigment plaques. In addition, the trace elements such as zinc, manganese, molybdenum and the like contained in the black pigment can also clear oxygen free radicals and inhibit the growth of melanin. In the aspect of wrinkle removal, flavonoid glycoside and flavonol in the ginkgo leaves are both free radical scavenger, and can protect cells in the dermis, improve blood circulation, prevent the cells from being oxidized to generate wrinkles, and make the skin tender, white and elastic.
The glyceol contained in the cane shoots has good beautifying value. On one hand, the glycyl alcohol can eliminate active oxygen in the body and inhibit the activity of tyrosinase, thereby preventing the generation of melanin; on the other hand, the glyceol can soften the horny layer on the surface of the skin and make the skin smooth and fine.
Mulberry contains a large amount of nutrients necessary for human body, and can be used for caring skin. The mulberry contains abundant anthocyanin, is one of substances with strong oxidation resistance, can remove free radicals in vivo, and has the effects of maintaining beauty, keeping young and delaying senility. In addition, mulberry has the effects of improving skin blood supply, nourishing skin, whitening skin, and delaying skin aging.
Pea has good effect of moistening skin, and the pea has the efficacy of dispelling facial black speck and enabling the face to be glossy as recorded in compendium of materia medica. According to the invention, the pea extract is added, and since peas contain rich provitamin A, the provitamin A can be converted into vitamin A in vivo, and the pea extract has the effect of moistening skin. In addition, the pea is ground into powder and externally applied to an affected part, and can treat acne, carbuncle, swelling and other sore diseases; when the pea powder is used for bathing at ordinary times, the skin of people can be glossy and elastic.
The rice has strong whitening effect, and can supplement moisture of skin, so that the skin is smooth, fine and elastic. The nutrient components such as y-oryzanol, procyanidine and the like have particularly obvious skin care effect. The y-oryzanol is called as 'beauty essence', is a melanin inhibitor, can reduce capillary fragility and improve the function of peripheral vascular circulation of the skin while whitening and lightening spots, and further prevents skin chap, improves skin color and luster and makes the skin white and bright. The rice chaff sterol has the functions of locking water and replenishing water for skin, and can also promote skin metabolism, inhibit skin inflammation, prevent erythema solare and skin aging. The procyanidine can keep the skin with the proper elasticity and tension, avoid the skin from sagging and wrinkling, has the effects of resisting aging and eliminating wrinkles, enables the skin to be more elastic and active, and is full of youth wind.
The glycerin can form a layer of protective film on the surface of the skin to lock the moisture in the skin and isolate the external air from the skin, so that the loss of the moisture can be reduced, and the skin can be resisted from external invasion, thereby having the advantages of moistening and protecting the skin. In addition, the application of glycerol in winter can also prevent skin frost crack and chilblain.
The product selects various natural component extracts and vegetable oil, and all the components supplement each other, so that the product has multiple effects of nourishing, whitening, inhibiting bacteria, preventing sunburn, relieving and replenishing water, resisting skin aging and the like, can prevent skin from drying, peeling and water loss, and has excellent moisturizing and water locking effects.
Compared with the prior art, the hand cream prepared by the invention can effectively keep the elasticity of skin, prevent rough skin and pigmentation, moisten skin, enhance the toughness and elasticity of skin and enable skin to be tender, plump, smooth, soft, white, tender and comfortable.
Detailed Description
The following describes in detail specific embodiments of the present invention.
Example 1
A herbal hand cream for nourishing, whitening, relieving and moisturizing contains the following raw materials in parts by weight:
1.1 preparation of daylily extract
Weighing 40g of day lily, cutting into pieces, soaking in water for 0.5h, heating and reflux extracting for 3 times: adding 16 times of water for the first time, and extracting for 1.5 h; adding 12 times of water for the 2 nd time, and extracting for 1.0 h; adding 8 times of water for 3 times, and extracting for 0.5 h; filtering each time to obtain filtrate, mixing filtrates, and concentrating the volume of the filtrate to 3 times g/mL of the weight of flos Hemerocallis for use.
1.2 preparation of the mangosteen bark extract
Weighing 50g of mangosteen skin, cutting into pieces, soaking for 0.3h, heating and refluxing for 3 times: adding 18 times of water for the first time, and extracting for 1.0 h; adding 14 times of water for the 2 nd time, and extracting for 1.0 h; adding 10 times of water for 3 times, and extracting for 0.5 h; filtering each time to obtain filtrate, combining the filtrates, and concentrating the volume of the filtrate to 4 times g/mL of the weight of the mangosteen bark for later use.
1.3 preparation of persimmon leaf extract
Weighing 40g of persimmon leaves, shearing, soaking in 75% ethanol for 0.4h, heating and reflux extracting for 3 times: adding 20 times of 75% ethanol for 1 time, and extracting for 1.0 hr; adding 16 times of 75% ethanol for 2 times, and extracting for 1.0 hr; adding 10 times of 75% ethanol for 3 times, and extracting for 0.5 hr; filtering each time to obtain filtrate, mixing filtrates, and concentrating the filtrate to 2 times g/mL of folium kaki weight for use.
1.4 preparation of Ginkgo biloba leaf extract
Weighing 50g of ginkgo leaves, cutting into pieces, soaking in 70% ethanol for 0.5h, heating and refluxing for 3 times: extracting with 20 times of 70% ethanol for 1.0 hr; adding 12 times of 70% ethanol for 2 times, and extracting for 1.0 hr; adding 8 times of 70% ethanol for 3 times, and extracting for 1.0 hr; filtering each time to obtain filtrate, combining the filtrates, and concentrating the volume of the filtrate to 4 times g/mL of the weight of the ginkgo leaves for later use.
1.5 preparation of Zizania latifolia extract
Weighing 30g of wild rice shoots, cutting, soaking for 0.4h, heating and refluxing for extraction for 3 times: adding 22 times of water for the first time, and extracting for 1.5 h; adding 20 times of water for 2 times, and extracting for 1.5 h; adding 18 times of water for 3 times, and extracting for 1.0 h; filtering each time to obtain filtrate, combining the filtrates, and concentrating the volume of the filtrate to 2 times g/mL of the weight of the cane shoots for later use.
1.6 preparation of Mulberry extract
Weighing 50g of mulberry, soaking for 0.6h, heating and refluxing for extraction for 3 times: adding 18 times of water for the first time, and extracting for 1.5 h; adding 16 times of water for the 2 nd time, and extracting for 1.0 h; adding 12 times of water for 3 times, and extracting for 1.0 h; filtering each time to obtain filtrate, combining the filtrates, and concentrating the volume of the filtrate to 4 g/mL times of the weight of the mulberry for later use.
1.7 preparation of pea extract
Weighing 30g of pea coarse powder, soaking for 0.3h, heating and refluxing for 3 times: adding 16 times of water for the first time, and extracting for 1.5 h; adding 14 times of water for the 2 nd time, and extracting for 1.0 h; adding 12 times of water for 3 times, and extracting for 0.5 h; filtering each time to obtain filtrate, combining the filtrates, and concentrating the volume of the filtrate to 2 times g/mL of the weight of the pea for later use.
1.8 preparation of Rice extract
Weighing 50g of rice coarse powder, soaking for 0.2h, heating and refluxing for 3 times: adding 18 times of water for the first time, and extracting for 1.0 h; adding 16 times of water for the 2 nd time, and extracting for 1.0 h; adding 10 times of water for 3 times, and extracting for 0.5 h; filtering each time to obtain filtrate, combining the filtrates, and concentrating the volume of the filtrate to 3 times g/mL of the weight of the rice for later use.
1.9 preparation of herbal hand cream for nourishing, whitening, relieving and moisturizing
a) Weighing 0.5g of sodium carboxymethylcellulose, adding into a beaker filled with 50.0mL of distilled water, heating in a water bath at 50 ℃, stirring while heating, and standing to fully swell to form sodium carboxymethylcellulose gel liquid for later use;
b) weighing 9410.5 g of carbomer, adding into a beaker filled with 50.0mL of distilled water, heating in a water bath at 60 ℃, stirring while heating, and standing to fully swell to form carbomer gel liquid for later use;
c) weighing 0.5g of ethylparaben, adding into a beaker containing 1.0mL of 75% ethanol solution, and uniformly stirring to form a preservative solution for later use;
d) weighing 2.0g of sesame oil, 2.0g of calendula oil, 3.0g of rapeseed oil, 3.0g of olive emulsifier and 3.0g of universal self-emulsifying compound emulsifier AC-4023.0 g, putting into a beaker 1, heating in a water bath at 75 ℃, stirring while heating to uniformly mix the components to form an oil phase for later use;
e) weighing 20.0mL of distilled water, pouring into a beaker 2, and heating in a water bath at 75 ℃ to be used as a water phase for later use;
f) when the water phase and the oil phase reach the same temperature, slowly pouring the water phase in the beaker 2 into the oil phase in the beaker 1 in a trickle shape, stirring for 10min in the same direction while adding until the water phase is a uniform light yellow milky matrix, stopping stirring, taking out from the water bath and naturally cooling to room temperature;
g) adding 1.0mL of wild rice stem extract, 1.0mL of day lily extract, 2.0mL of mangosteen bark extract, 1.0mL of persimmon leaf extract, 2.0mL of ginkgo leaf extract, 1.0mL of mulberry extract, 1.0mL of pea extract and 2.0mL of rice extract into an emulsion matrix, sequentially adding sodium carboxymethylcellulose gel liquid, carbomer 941 gel liquid, 2.0mL of methyl silicone oil, 2.0mL of glycerol and 0.2g of sage essence, finally adding a preservative solution, and uniformly stirring to obtain the fine and uniform herbal nourishing, whitening, soothing and moisturizing hand cream.
Example 2
A herbal hand cream for nourishing, whitening, relieving and moisturizing contains the following raw materials in parts by weight:
2.1 preparation of daylily extract
Weighing 40g of day lily, cutting into pieces, soaking for 0.6h, heating and refluxing for extraction for 3 times: adding 16 times of water for the first time, and extracting for 1.5 h; adding 14 times of water for 2 times, and extracting for 1.5 h; adding 10 times of water for 3 times, and extracting for 1.0 h; filtering each time to obtain filtrate, mixing filtrates, and concentrating the volume of the filtrate to 5 times g/mL of the weight of flos Hemerocallis for use.
2.2 preparation of the mangosteen bark extract
Weighing 30g of mangosteen skin, cutting into pieces, soaking for 0.5h, heating and refluxing for extraction for 3 times: adding 20 times of water for the first time, and extracting for 2.0 h; adding 16 times of water for 2 times, and extracting for 1.5 h; adding 14 times of water for 3 times, and extracting for 1.0 h; filtering each time to obtain filtrate, combining the filtrates, and concentrating the volume of the filtrate to 5 g/mL of the mangosteen bark for later use.
2.3 preparation of persimmon leaf extract
Weighing 50g of persimmon leaves, shearing, soaking in 75% ethanol for 0.8h, and heating and reflux-extracting for 3 times: adding 22 times of 75% ethanol for the first time, and extracting for 1.5 hr; adding 18 times of 75% ethanol for 2 times, and extracting for 1.5 hr; adding 12 times of 75% ethanol for 3 times, and extracting for 1.0 hr; filtering each time to obtain filtrate, mixing filtrates, and concentrating the volume of the filtrate to 3 times g/mL of the weight of folium kaki for use.
2.4 preparation of Ginkgo biloba leaf extract
Weighing 40g of ginkgo leaves, cutting into pieces, soaking in 70% ethanol for 0.6h, heating and refluxing for 3 times: adding 22 times of 70% ethanol for 1 time, and extracting for 1.5 hr; adding 16 times of 70% ethanol for 2 times, and extracting for 1.5 hr; adding 10 times of 70% ethanol for 3 times, and extracting for 1.5 hr; filtering each time to obtain filtrate, combining the filtrates, and concentrating the volume of the filtrate to 6 times g/mL of the weight of the ginkgo leaves for later use.
2.5 preparation of Zizania latifolia extract
Weighing 50g of wild rice shoots, cutting, soaking for 0.5h, heating and refluxing for extraction for 3 times: adding 24 times of water for the first time, and extracting for 1.5 h; adding 20 times of water for 2 times, and extracting for 1.5 h; adding 18 times of water for 3 times, and extracting for 1.5 h; filtering each time to obtain filtrate, combining the filtrates, and concentrating the volume of the filtrate to 4 times g/mL of the weight of the cane shoots for later use.
2.6 preparation of Mulberry extract
Weighing 30g of mulberry, soaking for 0.6h, heating and refluxing for extraction for 3 times: adding 18 times of water for the first time, and extracting for 2.0 h; adding 16 times of water for the 2 nd time, and extracting for 1.0 h; adding 12 times of water for 3 times, and extracting for 1.0 h; filtering each time to obtain filtrate, combining the filtrates, and concentrating the volume of the filtrate to 5 g/mL times of the weight of the mulberry for later use.
2.7 preparation of pea extract
Weighing 50g of pea coarse powder, soaking for 0.6h, heating and refluxing for 3 times: adding 18 times of water for the first time, and extracting for 1.5 h; adding 15 times of water for 2 times, and extracting for 1.5 h; adding 12 times of water for 3 times, and extracting for 1.0 h; filtering each time to obtain filtrate, combining the filtrates, and concentrating the volume of the filtrate to 3 times g/mL of the weight of the pea for later use.
2.8 preparation of Rice extract
Weighing 40g of rice coarse powder, soaking for 0.5h, heating and refluxing for 3 times: adding 20 times of water for the first time, and extracting for 1.5 h; adding 18 times of water for 2 times, and extracting for 1.0 h; adding 12 times of water for 3 times, and extracting for 1.0 h; filtering each time to obtain filtrate, combining the filtrates, and concentrating the volume of the filtrate to 5 times g/mL of the weight of the rice for later use.
2.9 preparation of herbal hand cream for nourishing, whitening, relieving and moisturizing
a) Weighing 1.0g of sodium carboxymethylcellulose, adding into a beaker filled with 80.0mL of distilled water, heating in a water bath at 50 ℃, stirring while heating, and standing to fully swell to form sodium carboxymethylcellulose gel liquid for later use;
b) weighing 9411.0 g of carbomer, adding into a beaker filled with 90.0mL of distilled water, heating in a water bath at 70 ℃, stirring while heating, and standing to fully swell to form carbomer gel liquid for later use;
c) weighing 0.6g of ethylparaben, adding into a beaker containing 2.0mL of 75% ethanol solution, and uniformly stirring to form a preservative solution for later use;
d) weighing 3.0g of sesame oil, 2.0g of calendula oil, 4.0g of rapeseed oil, 4.0g of olive emulsifier and 4.0g of universal self-emulsifying compound emulsifier AC-4024.0 g, putting into a beaker 1, heating in a water bath at 90 ℃, stirring while heating to uniformly mix the components to form an oil phase for later use;
e) weighing 35.0mL of distilled water, pouring into a beaker 2, and heating in a water bath at 90 ℃ to serve as a water phase for later use;
f) when the water phase and the oil phase reach the same temperature, slowly pouring the water phase in the beaker 2 into the oil phase in the beaker 1 in a trickle shape, stirring for 12min in the same direction while adding until the water phase is a uniform light yellow milky matrix, stopping stirring, taking out from the water bath and naturally cooling to room temperature;
g) adding 2.0mL of wild rice stem extract, 2.0mL of day lily extract, 1.0mL of mangosteen bark extract, 2.0mL of persimmon leaf extract, 1.0mL of ginkgo leaf extract, 3.0mL of mulberry extract, 1.0mL of pea extract and 2.0mL of rice extract into an emulsion matrix, sequentially adding sodium carboxymethylcellulose gel solution, carbomer 941 gel solution, 4.0mL of methyl silicone oil, 3.0mL of glycerol and 0.3g of sensitive plant essence, finally adding a preservative solution, and uniformly stirring to obtain the fine and uniform nourishing, whitening, soothing and moisturizing hand cream.
Example 3
A herbal hand cream for nourishing, whitening, relieving and moisturizing contains the following raw materials in parts by weight:
3.1 preparation of daylily extract
Weighing 40g of day lily, cutting into pieces, soaking for 0.8h, heating and refluxing for extraction for 3 times: adding 18 times of water for the first time, and extracting for 2.0 h; adding 14 times of water for 2 times, and extracting for 1.5 h; adding 10 times of water for 3 times, and extracting for 1.0 h; filtering each time to obtain filtrate, mixing filtrates, and concentrating the volume of the filtrate to 8 times g/mL of the weight of flos Hemerocallis for use.
3.2 preparation of the mangosteen bark extract
Weighing 60g of mangosteen skin, cutting into pieces, soaking for 0.6h, heating and refluxing for extraction for 3 times: adding 22 times of water for the first time, and extracting for 2.5 h; adding 18 times of water for 2 times, and extracting for 2.0 h; adding 14 times of water for 3 times, and extracting for 1.0 h; filtering each time to obtain filtrate, combining the filtrates, and concentrating the volume of the filtrate to 6 times g/mL of the weight of the mangosteen bark for later use.
3.3 preparation of persimmon leaf extract
Weighing 50g of persimmon leaves, shearing, soaking in 75% ethanol for 1.0h, heating and reflux extracting for 3 times: adding 22 times of 75% ethanol for the first time, and extracting for 2.0 hr; adding 18 times of 75% ethanol for 2 times, and extracting for 2.0 hr; adding 12 times of 75% ethanol for 3 times, and extracting for 1.0 hr; filtering each time to obtain filtrate, mixing filtrates, and concentrating the volume of the filtrate to 6 times g/mL of the weight of folium kaki for use.
3.4 preparation of Ginkgo biloba leaf extract
Weighing 50g of ginkgo leaves, cutting into pieces, soaking in 70% ethanol for 0.8h, heating and refluxing for 3 times: adding 25 times of 70% ethanol at 1 time, and extracting for 2.0 hr; extracting with 18 times of 70% ethanol for 2 times for 2.0 hr; adding 12 times of 70% ethanol for 3 times, and extracting for 2.0 hr; filtering each time to obtain filtrate, combining the filtrates, and concentrating the volume of the filtrate to 8 times g/mL of the weight of the ginkgo leaves for later use.
3.5 preparation of Zizania latifolia extract
Weighing 30g of wild rice shoots, cutting, soaking for 0.6h, heating and refluxing for extraction for 3 times: adding 26 times of water for the first time, and extracting for 2.0 h; adding 22 times of water for the 2 nd time, and extracting for 2.0 h; adding 20 times of water for 3 times, and extracting for 1.0 h; filtering each time to obtain filtrate, combining the filtrates, and concentrating the volume of the filtrate to 6 times g/mL of the weight of the cane shoots for later use.
3.6 preparation of Mulberry extract
Weighing 50g of mulberry, soaking for 0.8h, heating and refluxing for extraction for 3 times: adding 20 times of water for the first time, and extracting for 2.5 h; adding 18 times of water for 2 times, and extracting for 1.5 h; adding 14 times of water for 3 times, and extracting for 1.5 h; filtering each time to obtain filtrate, combining the filtrates, and concentrating the volume of the filtrate to 6 g/mL times of the weight of the mulberry for later use.
3.7 preparation of pea extract
Weighing 40g of pea coarse powder, soaking for 0.8h, heating and refluxing for 3 times: adding 20 times of water for the first time, and extracting for 2.0 h; adding 16 times of water for 2 times, and extracting for 1.5 h; adding 14 times of water for 3 times, and extracting for 1.0 h; filtering each time to obtain filtrate, combining the filtrates, and concentrating the volume of the filtrate to 4 times g/mL of the weight of the pea for later use.
3.8 preparation of Rice extract
Weighing 30g of rice coarse powder, soaking for 0.6h, heating and refluxing for 3 times: adding 20 times of water for the first time, and extracting for 2.0 h; adding 18 times of water for 2 times, and extracting for 1.5 h; adding 12 times of water for 3 times, and extracting for 1.0 h; filtering each time to obtain filtrate, combining the filtrates, and concentrating the volume of the filtrate to 6 times g/mL of the weight of the rice for later use.
3.9 preparation of herbal hand cream for nourishing, whitening, relieving and moisturizing
a) Weighing 2.0g of sodium carboxymethylcellulose, adding into a beaker filled with 100.0mL of distilled water, heating in a water bath at 60 ℃, stirring while heating, and standing to fully swell to form sodium carboxymethylcellulose gel liquid for later use;
b) weighing 9412.0 g of carbomer, adding into a beaker filled with 100.0mL of distilled water, heating in a water bath at 80 ℃, stirring while heating, and standing to fully swell to form carbomer gel liquid for later use;
c) weighing 0.8g of ethylparaben, adding into a beaker containing 2.0mL of 75% ethanol solution, and uniformly stirring to form a preservative solution for later use;
d) weighing 5.0g of sesame oil, 4.0g of calendula oil, 5.0g of rapeseed oil, 6.0g of olive emulsifier and 6.78 g of universal self-emulsifying compound emulsifier AC-4024.0 g, putting into a beaker 1, heating in a water bath at 95 ℃, stirring while heating to uniformly mix the components to form an oil phase for later use;
e) weighing 25.0mL of distilled water, pouring into a beaker 2, and heating in a water bath at 95 ℃ to serve as a water phase for later use;
f) when the water phase and the oil phase reach the same temperature, slowly pouring the water phase in the beaker 2 into the oil phase in the beaker 1 in a trickle shape, stirring for 15min in the same direction while adding until the water phase is a uniform light yellow milky matrix, stopping stirring, taking out from the water bath and naturally cooling to room temperature;
g) adding 3.0mL of cane shoot extract, 3.0mL of day lily extract, 2.0mL of mangosteen bark extract, 2.0mL of persimmon leaf extract, 1.0mL of ginkgo leaf extract, 3.0mL of mulberry extract, 3.0mL of pea extract and 2.0mL of rice extract into an emulsion matrix, sequentially adding sodium carboxymethylcellulose gel liquid, carbomer 941 gel liquid, 3.0mL of methyl silicone oil, 5.0mL of glycerol and 0.25g of rose essence, finally adding a preservative solution, and uniformly stirring to obtain the fine and uniform herbal nourishing whitening and soothing moisturizing cream.
Example 4
The physical and chemical indexes of the examples 1, 2 and 3 are as follows:
4.1 Properties
The hand cream prepared by the invention is light red, has proper consistency, is dense, translucent, fine and uniform, has good spreadability and fragrant smell.
4.2 pH check
The pH value of the hand cream prepared by the invention is measured by a pH meter and is measured to be 6.5-7.0.
4.3 Cold-Heat test
The hand cream prepared by the invention is packaged in a cream bottle and refrigerated in a refrigerator at 4 ℃ for one month to observe no layering phenomenon. The hand cream has no phenomena of layering, emulsification and odor change and the like in a constant temperature box at 55 ℃ for 24 hours.
4.4 centrifugal test
The hand cream prepared by the invention is packaged in a test tube with a plug, and is centrifuged at 3000r/min for 20min without layering.
4.5 Room temperature standing experiment
The hand creams prepared in examples 1, 2 and 3 were placed in the cream, respectively, and left to stand at room temperature for 6 months, without any delamination, any change in feeling after use, and any change in odor.
4.6 irritation test and allergy test
The back of the white mouse was cut off, and a suitable amount of the hand cream prepared in examples 1, 2 and 3 was applied to the cut-off portion, and compared with the non-applied portion, no irritation or allergic reaction was observed.
Appropriate amounts of the hand creams prepared in examples 1, 2 and 3 were applied to different positions on the hand surface of volunteers (15-65 years old and 120 persons), and no redness, rash or blister appeared after 30 minutes.
Example 5
Trial effect experiment:
the efficacy of the hand creams manufactured in examples 1, 2, and 3 was evaluated by the trial feeling as follows. 120 women of 20-45 years old are selected as trial objects by adopting a civil survey scoring method, are randomly equally divided into three groups, and are respectively smeared on hands by the hand cream prepared in the embodiment 1, the embodiment 2 and the embodiment 3. The product is used twice daily for two months. The using effects of the ingredients are divided into 5 points: the fifth is the highest score, which means better and very satisfactory; 4, the classification is very good; 3 is acceptable; a score of less than 3 is not acceptable. The average scores are given below and the results are given in the table below:
table 1 comprehensive effect investigation
In conclusion, the hand cream prepared by the invention has good moisture retention, nourishing, whitening, bacteriostasis, sun protection and anti-aging effects, and after the hand cream is used, the skin elasticity is good, and the skin is tender, bright, white and moist.
Claims (1)
1. The herbal hand cream capable of nourishing, whitening, relieving and moisturizing is characterized by comprising the following raw materials in parts by weight:
the day lily extracting solution is prepared by the following method:
weighing appropriate amount of flos Hemerocallis, cutting into pieces, soaking for 0.5-0.8h, heating and reflux extracting for 3 times: adding 16-18 times of water for the first time, and extracting for 1.5-2.0 h; adding 12-14 times of water for the 2 nd time, and extracting for 1.0-1.5 hr; adding 8-10 times of water for 3 times, and extracting for 0.5-1.0 hr; filtering each time to obtain filtrate, mixing filtrates, and concentrating the volume of the filtrate to 3-8 times g/mL of the weight of flos Hemerocallis for use;
the mangosteen bark extract is prepared by the following method:
weighing appropriate amount of cortex Garciniae, cutting, soaking for 0.3-0.6 hr, heating and reflux extracting for 3 times: adding 18-22 times of water for the first time, and extracting for 1.0-2.5 hr; adding 14-18 times of water for the second time, and extracting for 1.0-2.0 hr; adding 10-14 times of water for 3 times, and extracting for 0.5-1.0 hr; filtering each time to obtain filtrate, mixing the filtrates, and concentrating the volume of the filtrate to 4-6 times g/mL of the weight of the mangosteen bark for later use;
the persimmon leaf extracting solution is prepared by the following method:
weighing appropriate amount of folium kaki, cutting, soaking in 75% ethanol for 0.4-1.0 hr, heating and reflux extracting for 3 times: adding 20-22 times of 75% ethanol for 1 time, and extracting for 1.0-2.0 hr; adding 16-18 times of 75% ethanol for 2 times, and extracting for 1.0-2.0 hr; adding 10-12 times of 75% ethanol for 3 times, and extracting for 0.5-1.0 hr; filtering each time to obtain filtrate, mixing filtrates, and concentrating the filtrate to volume of 2-6 times g/mL of folium kaki for use;
the ginkgo leaf extracting solution is prepared by the following method:
weighing appropriate amount of folium Ginkgo, cutting into pieces, soaking in 70% ethanol for 0.5-0.8 hr, heating and reflux extracting for 3 times: adding 20-25 times of 70% ethanol for 1 time, and extracting for 1.0-2.0 hr; adding 12-18 times of 70% ethanol for 2 times, and extracting for 1.0-2.0 hr; adding 70% ethanol 8-12 times the amount of the extract for the 3 rd time, and extracting for 1.0-2.0 hr; filtering each time to obtain filtrate, mixing filtrates, and concentrating the volume of the filtrate to 4-8 times g/mL of the weight of folium Ginkgo;
the wild rice stem extracting solution is prepared by the following method:
weighing appropriate amount of caulis Zizaniae Caduciflorae, cutting, soaking for 0.4-0.6h, heating and reflux extracting for 3 times: adding 22-26 times of water for the first time, and extracting for 1.5-2.0 h; adding 20-22 times of water for the second time, and extracting for 1.5-2.0 hr; adding 18-20 times of water for 3 times, and extracting for 1.0-2.0 hr; filtering each time to obtain filtrate, mixing the filtrates, and concentrating the volume of the filtrate to 2-6 times g/mL of the weight of Zizania latifolia for later use;
the mulberry extracting solution is prepared by the following method:
weighing a proper amount of mulberries, soaking for 0.6-0.8h, heating, refluxing and extracting for 3 times: adding 18-20 times of water for the first time, and extracting for 1.5-2.5 hr; adding 16-18 times of water for the 2 nd time, and extracting for 1.0-1.5 hr; adding 12-14 times of water for 3 times, and extracting for 1.0-1.5 hr; filtering each time to obtain filtrate, combining the filtrates, and concentrating the volume of the filtrate to 4-6 times g/mL of the weight of the mulberry for later use;
the pea extract is prepared by the following method:
weighing appropriate amount of pea coarse powder, soaking for 0.3-0.8h, heating and reflux extracting for 3 times: adding 16-20 times of water for the first time, and extracting for 1.5-2.0 h; adding 14-16 times of water for the 2 nd time, and extracting for 1.0-1.5 hr; adding 12-14 times of water for 3 times, and extracting for 0.5-1.0 hr; filtering each time to obtain filtrate, mixing filtrates, and concentrating the volume of the filtrate to 2-4 times g/mL of the weight of pea for use;
the rice extract is prepared by the following method:
weighing a proper amount of rice coarse powder, soaking for 0.2-0.6h, heating and refluxing for 3 times: adding 18-20 times of water for the first time, and extracting for 1.0-2.0 hr; adding 16-18 times of water for the 2 nd time, and extracting for 1.0-1.5 hr; adding 10-12 times of water for 3 times, and extracting for 0.5-1.0 hr; filtering each time to obtain filtrate, mixing filtrates, and concentrating the volume of the filtrate to 3-6 times g/mL of the weight of rice for use;
the preparation method of the herbal hand cream with the effects of nourishing, whitening, relieving and moisturizing comprises the following steps:
a) weighing 0.5-2.0g of sodium carboxymethylcellulose, adding into 50.0-100.0mL of distilled water, heating in water bath at 30-60 deg.C while stirring, and standing to make it fully swell to obtain sodium carboxymethylcellulose gel solution;
b) weighing 9410.5-2.0 g of carbomer, adding into 50.0-100.0mL of distilled water, heating in water bath at 60-80 deg.C under stirring, and standing to swell completely to obtain carbomer 941 gel solution;
c) weighing 0.5-0.8g of ethylparaben, adding into 1.0-2.0mL of 75% ethanol solution, and stirring to obtain antiseptic solution;
d) weighing 2.0-5.0g of sesame oil, 2.0-5.0g of calendula oil, 2.0-5.0g of rapeseed oil, 3.0-8.0g of olive emulsifier and 8.0g of universal self-emulsifying compound emulsifier AC-4023.0-8.0 g, uniformly mixing, heating in a water bath at 75-95 ℃, stirring while heating to uniformly mix to form an oil phase for later use;
e) weighing 20.0-45.0mL of distilled water, and heating in a water bath at 75-95 ℃ to serve as a water phase for later use;
f) when the water phase and the oil phase reach the same temperature, slowly pouring the water phase into the oil phase in a fine flow state, stirring in the same direction for 10-15min while adding until the water phase is a uniform yellowish milky matrix, stopping stirring, taking out from the water bath, and naturally cooling to room temperature;
g) adding 1.0-3.0mL of cane shoot extract, 1.0-3.0mL of day lily extract, 1.0-3.0mL of mangosteen bark extract, 1.0-3.0mL of persimmon leaf extract, 1.0-3.0mL of ginkgo leaf extract, 1.0-3.0mL of mulberry extract, 1.0-3.0mL of pea extract and 1.0-3.0mL of rice extract into an emulsion matrix, sequentially adding sodium carboxymethylcellulose solution, 941 carbomer gel solution, 2.0-5.0mL of methyl silicone oil, 2.0-5.0mL of glycerol and 0.2-0.35g of essence, finally adding a preservative solution, and uniformly stirring to obtain the fine and uniform herbal nourishing, moisturizing, whitening and soothing water replenishing cream.
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